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    Coal Analysis Parameter

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    Yuliyanti Yuliyanti
    Parameter analysis involves testing various properties of coal samples including: 1) Moisture content, proximate analysis (ash, volatile matter, fixed carbon), and ultimate analysis (carbon, hydrogen, nitrogen, sulfur, oxygen). 2) Heating value including gross calorific value and net calorific value. 3) Additional tests such as ash fusion temperatures, Hardgrove grindability index, and size distribution analysis.

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    Coal Analysis Parameter

    Uploaded by

    Yuliyanti Yuliyanti
    227 views21 pages
    Parameter analysis involves testing various properties of coal samples including: 1) Moisture content, proximate analysis (ash, volatile matter, fixed carbon), and ultimate analysis (carbon, hydrogen, nitrogen, sulfur, oxygen). 2) Heating value including gross calorific value and net calorific value. 3) Additional tests such as ash fusion temperatures, Hardgrove grindability index, and size distribution analysis.

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    Coal Analysis Parameter

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    Parameter analysis involves testing various properties of coal samples including: 1) Moisture content, proximate analysis (ash, volatile matter, fixed carbon), and ultimate analysis (carbon, hydrogen, nitrogen, sulfur, oxygen). 2) Heating value including gross calorific value and net calorific value. 3) Additional tests such as ash fusion temperatures, Hardgrove grindability index, and size distribution analysis.

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    © All Rights Reserved
    Download as PPT, PDF, TXT or read online from Scribd
    Download as ppt, pdf, or txt
    227 views21 pages

    Coal Analysis Parameter

    Uploaded by

    Yuliyanti Yuliyanti
    Parameter analysis involves testing various properties of coal samples including: 1) Moisture content, proximate analysis (ash, volatile matter, fixed carbon), and ultimate analysis (carbon, hydrogen, nitrogen, sulfur, oxygen). 2) Heating value including gross calorific value and net calorific value. 3) Additional tests such as ash fusion temperatures, Hardgrove grindability index, and size distribution analysis.

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    Parameter Analisa

    SUCOFINDO
    Definisi dari Parameter Analisa :
    Total Moisture
    Proxymate Analysis
    Gross Calorific Value
    Ultimate Analysis
    Ash Analysis
    Ash Fusion Temperatures
    Hardgrove Grindability Index
    Size Distribution
    Analisa Lainnya
    Kaltim Prima Coal
    Date
    Analisa Batubara
    Total Moisture
     Proximate Analisis

     Ultimate Analisis

     Calorific Value

     Crusible Swelling umber

     Ash Analisis

     Ash Fusion Temperature

     Hard Grove Grindability Index


     dll
    Total Moisture

     Direct method ( Oven 105 °C )


     Bertahap.

    a) % Free Moisture / Air Dry Loss


    - Suhu Kamar ( 24 h )
    - Oven 40°C ( 3 h )
    b) % Residual Moisture (Oven 105°C
    under nitrogen)
    Proximate Analisis
     Moisture in the Analysis Sample
     Ash Content

     Volatile Matter

     Fixed Carbon
    Moisture In the Analysis Sample
     1,0000 g sample at 0, 212 mm
     Oven 107 °C

     Minimum Free Space Oven

    Oven 107°C

    Weight Weight
    Coal Coal
    before after
    heating heating
    Ash Content
     1,0000 g sample, 0, 212 mm
     Furnace 750 °C or 815 °C

    Muffel 750°C
    or 815°C
    Weight Weight
    COAL Residu
    before after
    heating heating
    Volatile Matter
     1,0000 g sample, 0, 212 mm
     Muffel/furnace 900 °C or 950 °C (7 min)

    Muffel 900°C
    or 950°C

    Weight Weight
    Coal Coal
    before after
    heating heating
    Fixed Carbon
     Karbon Padat
     Kalkulasi FC = ( 100 - M - Ash - VM )

    M
    FC Ash
    VM
    Ultimate Analysis
     Total
    Sulphur
     Nitrogen

     Carbon

     Hydrogen

     O xygen
    Total Sulphur
     M= ( ESCHA , High Temp. Furnace, LECO)
    a) ESCHA ( Grafimetri ) 2 x 24 jam
    b) High Temp. Furnace. (Titrimetri) 30 mnt
    c) LECO ( Infra Red ) 2 mnt
     Form Sulphur :
    a) Pyritic Sulphur
    b) Sulfat Sulphur
    c) Organik Sulphur
    Nitrogen
     M= ( Mikro & Makro Kjeldal )
    Tj. % Nitrogen in Coal
    Efek terhdap Pencemaran Udara
    ( NO2 , NOx , NO )
    Carbon & Hydrogen
     Total Carbon & Hidrogen in Coal
    ( High Temp. Furnace & LECO )

    High Temp
    1350°C or
    LECO
    Weight Coal Weight
    & Weight Absorben
    Absorben CO2 & H2O
    before after
    heating heating
    N M
    O Ash
    Oxigen C H

    Besarnya kebutuhan oxigen pada


    pembakaran dan untuk memprediksi gas
    buangan yang dihasilkan setelah
    pembakaran batubara.

    Oxigen = Dari hasil kalkulasi


    = 100 - ( M+Ash+TS+N+C+H )
    Calorific Value
     KCal/kg , Cal/gr , BTU/lb , MJ
     Gross CV & Net CV
     Gross CV

    BOMB CALORIMETER Calculation


    ( Delta t = °C ) Gross CV

    Weight Coal

     NET CV
    ASTM Net CV(ar) Cal/gr = GCV (ar) - 5,72 ( 9 x H (ar))
    BS/ISO Net CV(ar) J/gr = GCV J/gr(ar) - (212x H (ar))-
    (0,8 x O (ar)) - ( 2,45 x TM)
    Crusible Swelling Number
    (C S N)

    FURNACE Bandingkan
    dengan Standart
    (0-9)
    COAL
    Ash Analisis
    Ash Composition
    SiO2
    Al2O3
    Fe2O3
    TiO2
    Furnace CaO
    AAS, SPECTRO MgO
    Ash K2O
    Coal Na2O
    Mn3O4
    P2O5
    SO3
    Ash Analysis
    Ash Composition
     Slagging Factor = (Base/Acid) x % TS (db)

     Fouling Factor = ( Base / Acid ) x % Na2O


    Ash Fusion Temperature
    ( AFT )

    Pengamatan
    AFT Furnace a. Initial Def temp.
    Reduksi b. Spherical
    Oxidasi c. Hemispherical
    Ash Coal d. Flow
    Hard Grove Grindability Index
    ( HGI )

    HGI Calculation
    Machine based on
    Coal standard
    sample
    Size Analysis

    + 100 mm a %
    + 50 mm b%
    + 32,5 mm c %
    + 22,5 mm d%
    + 11,2 mm e%
    + 6,3 mm f %
    + 4,75 mm g %
    + 2,00 mm h%
    + 1,00 mm I%
    + 0,5 mm j%
    - 0,5 mm k%
    Terima kasih

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