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Examen Elim

This document presents calculations for a distillation column. Key parameters include: - Feed flow rate of 5862.05 kg/h with composition of 0.0888 kg A/kg LS. - Distillate rate of 7.8948 m3/h with composition of 0.4878 kmol A/kmol G2 and 0.3278 volume fraction of A. - Bottom rate of 4.7265 kmol/h with composition of 4.397 kg/hm2 and 32.78% volume of A. The distillation column has a diameter of 0.5818 m and height of 3.8 m.

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Dulce Mariel
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0% found this document useful (0 votes)
40 views13 pages

Examen Elim

This document presents calculations for a distillation column. Key parameters include: - Feed flow rate of 5862.05 kg/h with composition of 0.0888 kg A/kg LS. - Distillate rate of 7.8948 m3/h with composition of 0.4878 kmol A/kmol G2 and 0.3278 volume fraction of A. - Bottom rate of 4.7265 kmol/h with composition of 4.397 kg/hm2 and 32.78% volume of A. The distillation column has a diameter of 0.5818 m and height of 3.8 m.

Uploaded by

Dulce Mariel
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PPTX, PDF, TXT or read online on Scribd
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𝑉 𝐿 2=¿

𝑉 𝐿𝑖 ∗ 𝑓 .𝑖=𝑉 𝐿 2

( 𝑘 𝑦 . 𝑎 )𝑚
𝑓 .𝑖=60 −70 %

𝐾𝑚𝑜 𝑙 𝐴
𝑌 𝐴 2=
𝑘𝑚𝑜𝑙 𝐺𝑆

𝑚3
𝐺 𝑉 2=
h

𝑉 𝐺2
Componentes -AGOTAMIENTO-
A=
LS 𝐿
GS= 𝐿𝑉 2=131.58
𝑚𝑖𝑛

𝑘 𝑔𝐴
2 𝑥 𝐴 2=0.023
𝑘 𝑔 𝐿2

Componentes
PMA= 58 T= 110° C 𝑇 𝐴=0.96 ∗ 𝐿 𝐴 2
PM219 𝐺 𝑆 =1.7 𝐺 𝑆𝑚𝑖𝑛 P= 2.2 atm
𝑘𝑔
PMGS= 18 𝜌 𝐿=760 3
𝑚
𝑌 𝐴 ∗=9.3 ∗ 𝑋 𝐴
𝑚
𝑉 𝐿𝑖 =0.75 𝑓 .𝑖=0.66
𝑚𝑖𝑛
1

𝑘𝑚𝑜 𝑙 𝐴 𝐿 𝐴 1=0.04 ∗ 𝐿 𝐴 2
𝑦 𝐴 1=0.005
𝑘𝑚𝑜 𝑙 𝐺 1
𝑟 𝐿 =0.55 ∗ 𝑅 𝑇
𝑘𝑚𝑜𝑙
( 𝑘 𝑦 . 𝑎 )𝑚 =65.2 3 𝑟 𝐺 =0.45 ∗ 𝑅𝑇
h 𝑚 (∆ 𝑦 )
𝑥 𝐴2 0.023 𝑘𝑔 𝐴
𝑋 𝐴 2= = =0.02354
1 − 𝑥 𝐴 2 1 −0.023 𝑘 𝑔 𝐺𝑆

𝑘 𝑔 𝐿𝑆
219
𝑃 𝑀 𝐿𝑆 𝑘𝑔 𝐴 𝑘𝑚𝑜 𝑙 𝐿𝑆 𝑘𝑚𝑜 𝑙 𝐴
𝑋 𝐴 2= 𝑋 𝐴 2 ∗ =0.02354 ∗ =0.0888
𝑃𝑀𝐴 𝑘 𝑔𝐿 𝑆 𝑘 𝑔𝐴 𝑘𝑚𝑜 𝑙 𝐿𝑆
58
𝑘𝑚𝑜 𝑙 𝐴

𝑋 𝐴 1=0.04 ∗ 𝑋 𝐴 2
𝑘𝑚𝑜 𝑙 𝐴 −3 𝑘𝑚𝑜 𝑙 𝐴
𝑋 𝐴 1=0.04 ∗ 𝑋 𝐴 2 =0.04 ∗ 0.0888 =3.552 𝑥 10
𝑘𝑚𝑜 𝑙 𝐿𝑆 𝑘𝑚𝑜 𝑙 𝐿𝑆

𝑌 𝐴1 𝑌𝐴2
= 𝑋 𝐴1 ∗ = 𝑋 𝐴2∗
9.3 9.3

𝑦 𝐴1 0.005 − 3 𝑘𝑚𝑜 𝑙 𝐴
𝑌 𝐴 1= = =5.025 𝑥 10
1− 𝑦 𝐴 1 1 −0.005 𝑘𝑚𝑜 𝑙 𝐺𝑆

𝑇 𝐴= 𝐿𝑆 ∗ ( 𝑋 𝐴 2 − 𝑋 𝐴 1 )= 𝐺𝑆 ∗ ( 𝑌 𝐴 2 −𝑌 𝐴 1 ) =𝐺 𝑠𝑚𝑖𝑛 ∗(𝑌 𝐴 2 𝑚𝑎𝑥 −𝑌 𝐴 1 )

1.7 ∗ 𝐺𝑆𝑚𝑖𝑛 ∗ ( 𝑌 𝐴 2 −𝑌 𝐴 1 ) =𝐺 𝑠𝑚𝑖𝑛 ∗(𝑌 𝐴 2 𝑚𝑎𝑥 −𝑌 𝐴 1 )

( 𝑌 𝐴 2𝑚𝑎𝑥 −𝑌 𝐴 1)
𝑌 𝐴 2= +𝑌 𝐴 1
1.7
𝑘𝑚𝑜 𝑙 𝐴
𝑌 𝐴 2 ∗=9.3 ∗ 𝑋 𝐴 2=9.3 ∗ 0.0888=0.8258 =𝑌 𝐴 2 max
𝑘𝑚𝑜 𝑙 𝐺𝑆

( 𝑌 𝐴 2𝑚𝑎𝑥 −𝑌 𝐴 1) 0.8258 −5.025 𝑥 10 −3 −3 kmol A


𝑌 𝐴 2= +𝑌 𝐴 1= +5.025 𝑥 10 =0.4878
1.7 1.7 kmol GS

𝑌 𝐴 1 5.025 𝑥 10− 3 0.4878 𝑘𝑚𝑜 𝑙 𝐴


−4 kmol A 𝑦 𝐴 2= =0.3278
𝑋 𝐴 1 ∗= = =5.403 x 10 1+ 0.4878 𝑘𝑚𝑜 𝑙𝐺 2
9.3 9.3 kmol LS

𝑌 𝐴 2 0.4878 𝑘𝑚𝑜 𝑙 𝐴
𝑋 𝐴2∗= = =0.0524
9.3 9.3 𝑘𝑚𝑜 𝑙 𝐿𝑆

𝑘𝑚𝑜 𝑙 𝐴
𝑌 𝐴 1 ∗=9.3 ∗ 𝑋 𝐴 1 =9.3 ∗ 3.552 𝑥 10 −3 =0.033
𝑘𝑚𝑜 𝑙 𝐺𝑆

𝑘𝑚𝑜𝑙 𝐴
𝑦 𝐴1 ∗=0.0319
𝑘𝑚𝑜𝑙 𝐿1
𝐿 1 𝑚3 60 𝑚𝑖𝑛 𝑚3
𝐿𝑉 2=131.58 ∗ ∗ =7.8948
𝑚𝑖𝑛 1000 𝐿 1h h

𝑘𝑔
𝐿2 h 𝑚
3
𝐿𝑉 2= = =
𝜌 𝐿 𝑘𝑔 h
3
𝑚

𝑚3 𝑘𝑔 𝑘𝑔
𝐿 2=𝐿 𝑉 2 ∗ 𝜌 𝐿 =7.8948 ∗760 3 =6000.048
h 𝑚 h

𝐿2 6000.048 𝑘𝑔
𝐿 2= 𝐿 𝑆 ∗ ( 1+ 𝑋 𝐴 2 ) ∴ 𝐿 𝑆 = = =5862.05
( 1+ 𝑋 𝐴 2 ) 1+0.02354 h

𝐿𝑆 5862.05 𝑘𝑚𝑜𝑙
𝐿𝑆 = = =26.7673
𝑃 𝑀 𝐿𝑆 219 h
𝑘𝑚𝑜𝑙 𝑟 𝐺 =0.45 ∗ 𝑅𝑇
( 𝑘 𝑦 . 𝑎 )𝑚 =65.2
h 𝑚 3 (∆ 𝑦 )

𝑘𝑚𝑜 𝑙 𝐴
( 𝐾 𝑦 . 𝑎 )𝑚 =0.45 ∗ ( 𝑘𝑦 . 𝑎 )=0.45 ∗65.2=29.34 3
h𝑚 (∆ 𝑦)
262.059 −100.352 𝑘𝑚𝑜𝑙
( 𝐾 𝑋 . 𝑎 )𝑚= 262.059
¿=168.46 3
𝐿𝑛( ) h 𝑚 (∆ 𝑋 )
100.352
𝑚
𝑉 𝐿𝑖 =0.75 𝑓 .𝑖=0.66
𝑚𝑖𝑛
𝑚3
𝑚 𝑚 60 𝑚𝑖𝑛 𝑚 𝐿𝑉 2 h
𝑉 𝐿 2=𝑉 𝐿𝑖 ∗ 𝑓 . 𝑖=0.75 ∗ 0.66=0.495 ∗ =29.7 𝑉 𝐿 2= = 2
𝑚𝑖𝑛 𝑚𝑖𝑛 1h h 𝑆 𝑚
𝑚3
7.8948
𝐿𝑉 2 h 2
𝑆= = =0.2658 𝑚
𝑉 𝐿2 𝑚
29.7
h

√ √
𝑆 0.2658
𝐷= =¿ =¿ 0.5818 𝑚 ¿ ¿
𝜋 0.785
4

𝑘𝑚𝑜𝑙
𝐿𝑆 𝑋 𝐴2− 𝑋 𝐴1 26.7673 −3
h 0.0888 −3.552 𝑥 10
𝑍= ∗ = ∗
𝑆 ∗ ( 𝐾 𝑋 .𝑎 )𝑚 ( 𝑋 𝐴 2 − 𝑋 𝐴 2 ∗ ) − ( 𝑋 𝐴 1 − 𝑋 𝐴 1 ∗ ) 0.2658 ∗ 168.46 𝑘𝑚𝑜𝑙 ( 0.0888 − 0.0524 ) − (3.552 𝑥 10− 3 − 5.403 x 10− 4 )
¿
h 𝑚3 ( ∆ 𝑋 )
( )
𝑋 𝐴2 − 𝑋 𝐴2 ∗ 𝐿𝑛¿ ¿
𝐿𝑛
𝑋 𝐴1 − 𝑋 𝐴1∗

𝑍 =0.5977 𝑚 ∗ 6.3628=3.8 𝑚
𝐺2 =𝐺 𝑆 ∗(1+𝑌 𝐴 2)

𝑘𝑚𝑜𝑙 −3
𝐿𝑆 ∗( 𝑋 𝐴 2 − 𝑋 𝐴 1) 26.7673 ∗( 0.0888 −3.552 𝑥 10 )
h 𝑘𝑚𝑜𝑙
𝐺 𝑆= = −3
= 4.7265
(𝑌 𝐴 2 −𝑌 𝐴 1 ) 0.4878 −5.025 𝑥 10 h

𝑘𝑚𝑜𝑙
𝐺2 =𝐺 𝑆 ∗ ( 1+𝑌 𝐴 2 ) =4.7265 ∗ ( 1+0.4878 )=7.03209
h

𝐺2 =𝐺 𝐴2+𝐺𝑆=𝐺𝑆 ∗𝑌 𝐴2 +𝐺 𝑆=𝐺 𝑆 ∗(1+𝑌 𝐴2)


𝑘𝑔
𝑃 𝑀 𝐺 2 =𝑦 𝐴 2 ∗ 𝑃 𝑀 𝐴 + ( 1 − 𝑦 𝐴 2 ) ∗ 𝑃 𝑀 𝐺𝑆=0.3278 ∗58+ (1 − 0.3278 ) ∗219=166.2242
𝑘𝑚𝑜𝑙

𝐺2 7.03209∗ 166.2242 𝒌𝒈
= =𝟒𝟑𝟗𝟕 .𝟔𝟖𝟎𝟕
𝑆 0.2658 𝒉𝒎𝟐
% 𝑣𝑜𝑙𝑢𝑚𝑒𝑛=𝑦 𝐴 2 ∗ 100=0.3278 ∗100=32.78 %

𝑃 ∗ 𝐺𝑉 2=𝐺2 ∗ 𝑅 ∗𝑇

𝐺2 ∗ 𝑅 ∗ 𝑇 7.03209 ∗ 0.08205 ∗(25+273.15) 𝑚


3
𝐺𝑉 2= = =172.027
𝑃 1 h

𝐺2 ∗ 𝑅 ∗ 𝑇 7.03209 ∗ 0.08205 ∗(110 +273.15) 𝑚3


𝐺𝑉 2= = =100.487
𝑃 2.2 h
- A G O T A M I E N T O-

GAS LÍQUIDO

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