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    Acid and Base Standarization

    Uploaded by

    Septiani Rasidah
    This document outlines a laboratory experiment on acid-base titration and standardization. The objectives are to demonstrate the titration technique and calculate molarity. The theory discusses properties of common acids and bases used (HCl and NaOH) and titration principles. The methodology explains how HCl and NaOH solutions were standardized against borax and oxalic acid, respectively. The results give the volumes of acid and base used over three trials and the calculated molarities. Key points are identifying the endpoint, equivalence point, and using appropriate pH indicators for each titration.

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    © All Rights Reserved
    Download as PPTX, PDF, TXT or read online from Scribd

    Acid and Base Standarization

    Uploaded by

    Septiani Rasidah
    76 views15 pages
    This document outlines a laboratory experiment on acid-base titration and standardization. The objectives are to demonstrate the titration technique and calculate molarity. The theory discusses properties of common acids and bases used (HCl and NaOH) and titration principles. The methodology explains how HCl and NaOH solutions were standardized against borax and oxalic acid, respectively. The results give the volumes of acid and base used over three trials and the calculated molarities. Key points are identifying the endpoint, equivalence point, and using appropriate pH indicators for each titration.

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    This document outlines a laboratory experiment on acid-base titration and standardization. The objectives are to demonstrate the titration technique and calculate molarity. The theory discusses properties of common acids and bases used (HCl and NaOH) and titration principles. The methodology explains how HCl and NaOH solutions were standardized against borax and oxalic acid, respectively. The results give the volumes of acid and base used over three trials and the calculated molarities. Key points are identifying the endpoint, equivalence point, and using appropriate pH indicators for each titration.

    Copyright:

    © All Rights Reserved
    Download as PPTX, PDF, TXT or read online from Scribd
    Download as pptx, pdf, or txt
    76 views15 pages

    Acid and Base Standarization

    Uploaded by

    Septiani Rasidah
    This document outlines a laboratory experiment on acid-base titration and standardization. The objectives are to demonstrate the titration technique and calculate molarity. The theory discusses properties of common acids and bases used (HCl and NaOH) and titration principles. The methodology explains how HCl and NaOH solutions were standardized against borax and oxalic acid, respectively. The results give the volumes of acid and base used over three trials and the calculated molarities. Key points are identifying the endpoint, equivalence point, and using appropriate pH indicators for each titration.

    Copyright:

    © All Rights Reserved
    Download as PPTX, PDF, TXT or read online from Scribd
    Download as pptx, pdf, or txt
    of 15

    Acid and Base Standarization

    reated by

    sri Aminah 151411003

    eptiani Rasidah 1514110

    A Chemical Engineering

    Objective

    Result
    &
    Discussion

    Methodology

    Theory
    Equilibriu
    m

    Tools
    &
    Ingredient

    Outline Of
    Presentation

    Objective

    To demonstrate the
    basic laboratory
    technique of titration

    To learn to calculate
    molarity based on
    titrations

    Theory

    High purity
    Stability (low reactivity)
    Low hygroscopicity (to minimize
    weight changes due to humidity)
    High equivalent weight (to
    minimize weighing errors)[3]
    Non-toxicity
    Ready and cheap availability

    secondary standard is
    usually standardized
    against a primary
    standard.

    Theory
    Hidrokloride
    acid

    Hydrochloric
    acid is a clear,
    colorless,
    highly
    pungent solution
    of
    hydrogen chloride
    (HCl) in water
    HCl can use for

    Sodium
    Hidrokside

    Sodium hydroxide
    (NaOH) is an a
    white. NaOH is
    available in pellets,
    flakes, granules,
    and as prepared
    solutions at a
    number of different

    Theory
    Titration is a method used in measuring the
    amount of an analytical reagent necessary to react
    quantitatively with the sample.
    Acid-base titrations are important for counting
    concentrations of acids and bases.
    The point at which the equivalence point has been
    reached is called the theoretical end point.
    In titration used indicator to detected by some
    physical change, such as colour change, to
    indicate the endpoint.

    Tools & Ingredients


    1. Tools

    Beaker

    Spatula

    Volumetric Flask

    Erlenmeyer flask Pipet Filler

    Pipet

    Funnel

    analytical balance

    Stirrer stick

    Buret, Klem & Statif

    2. Ingredients

    Aquadest
    NaOH 1 N
    HCl 1 N
    Indicator PP
    Indicator MM
    Indicator MO

    Methodology
    1. Strandarization Acid
    25
    ml Aquadest
    1 gram
    Boraks

    Solution 1

    Aquadest
    Solution 1

    Solution 2

    5 ml Solution
    2
    Indicator
    MM 3 drop

    Solution 3

    sodium hidroxide

    2. Strandarization Base
    25 ml
    Aquadest
    0,63
    Oxalic
    acid

    Aquadest1
    Solution

    Aquadest
    50drop
    ml2
    10
    ml Solution
    Indicator
    PP

    Solution 1

    Solution 2

    Solution 3

    Result and Discussion


    Standarizasion of HCl
    Trial 1

    Trial 2

    Trial 3

    Volume of Boraks
    used

    5 mL

    5 mL

    5 mL

    Molarity of
    Boraks used

    0,1 N

    0,1 N

    0,1 N

    6,00 mL

    5,55 mL

    5,61 mL

    Volume of HCl
    used
    Averange of
    volume HCl
    Molarity of NaOH
    sol'n

    5,72 mL
    0,09 N

    Result and Discussion


    Standarizasion of NaOH
    Trial 1

    Trial 2

    Trial 3

    Volume of Oxalic
    acid used

    10 mL

    10 mL

    10 mL

    Molarity of
    Oxalic acid used

    0,1 N

    0,1 N

    0,1 N

    Volume of NaOH
    used

    11,85 mL

    11,95 mL

    12,00 mL

    Averange of
    volume NaOH
    Molarity of NaOH
    sol'n

    11,93 mL
    0,08 N

    Result and Discussion


    The end point of an acid-base titration is the point where
    the indicator changes colour
    Equivalence point is the point where there are equal
    amounts (in moles) of acid and base
    The indicator that we used in standarizasion of HCl is the
    methyil red, where the ph range is around 4,8 to 6,0
    The indicator that we used in standarizasion of NaOH is the
    phenolphthalein, where the ph range is around 8.2 to 10.0
    In order to make sure that sample dissolved completely,
    we have to shake the flask thoroughly.

    Result and Discussion


    The titration curve

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