Casting Procedures 97
Casting Procedures 97
Casting Procedures 97
Introduction Steps in casting Spruing Investing patterns Burn out procedure Casting machines Casting techniques
Casting procedure
Principles of casting Casting defects Casting of ceramics Casting of titanium Casting procedure in RPD conclusion
Introduction
Structural faults in dental castings can result from any combination of problems related to spruing, investing, wax elimination, alloy melting, casting & solidification of the casting. The ability to produce smooth and well fitting castings require strict adherence to certain fundamentals.....
SPRUING
Spruing is an art which is not well understood.. Off all the procedures involving casting work, the spruing technique has a paramount importance in producing a complete & dense casting.
Definitions (GPT-8)
Sprue : the channel or hole through which plastic or metal is poured or cast into a gate or reservoir and then into a mould Sprue former : a wax, plastic, or a metal pattern used to form the channel or channels allowing molten metal to flow into a mold to make a casting Sprue button : the material remaining in the reservoir of the mold after a dental casting
Basic Requirements
To form a mount for the wax pattern To create a channel for elimination of wax during burn out To form a channel for entry of molten alloy during casting
Provides a reservoir of molten metal which compensates for alloy shrinkage during solidification
Taggart (1907), introduced the lost wax technique Asgar & Peyton (1959), stated that flaring should occur at the sprue/wax pattern junction Strickland et al (1959), stated the importance of the type, shape location & direction other than the size of the sprue Bruce (1964), tested the different methods of spruing patterns Rousseau (1964), described a casting method with a constricted sprue
Sprue Formers
Wax
Plastic/Resin
Metal sprues
Factors to be considered
Size Length Shape Number Attachment Location Angulation
Size
Usually large-diameter sprue is recommended The diameter of sprue should be equal to the thickest portion the wax pattern.
There are various gauges of sprue former gauge 6, 8, 10, 12, 14, 16, 18 (0.4cm - 0.1cm)
Usually for molar and metal ceramic restoration 10-gauge (2.5mm) Premolars and partial coverage restoration 12-gauge (2.0mm)
Length
The sprue should be long enough to place pattern 6 mm from the trailing end of casting ring usually it should be in the range of 2.5 mm.
Very short sprue porosity in casting at the junction of sprue and pattern. Very long sprue sprue solidifies first leading to casting shrinkage and incomplete casting.
Shape
The sprue former should be straight to reduce chances of creating turbulence in molten metal entering the mold. High turbulence of alloy cause porosity.
Number
Usually a single sprue is used for small castings. When two thick sections of a pattern are connected by thin part of wax, two separate sprues should be attached to each thick portion
Attachment
Attachment of sprue former and wax pattern: 1. The connection is generally flared - high density gold 2. It is restricted for low density alloys
Types Of Spruing
There are 2 types of spruing 1. Direct spruing 2. Indirect spruing Fig:1
Fig:2
Direct spruing
The sprue former provides a direct connection between the pattern area and the sprue base/ crucible former.
When two thick portions of wax are separated by thin wax, then 2 separate sprues should be attached using direct spruing.
Factors to be considered:
1. Location of attachment
2. Angulation of sprue 3. Attachment morphology
Location of attachment
Pin ledge restoration sprue is located towards the incisal aspect of lingual surface and angled suitably. Full veneer crown sprue is attached to Maxillary buccal and mandibular lingual cusp. Partial veneer crown sprue is attached to cusp that encompasses the preparation.
Angle of attachment
The sprue should be attached to pattern such that it makes 45 degrees to the walls of mold, which decreases the turbulence of molten alloy. If the sprue is placed perpendicular to the mold wall, it induces high turbulence in molten alloy, leading to creation of a hot spot on mold wall. This results in localized shrinkage porosity.
It should be placed away from thin / delicate parts of pattern to prevent fracture of investment.
Attachment morphology
The transition should be smooth Irregularities produces tags of investment which is vulnerable for fracture by molten alloy Usually it is flared for high density gold alloys but restricted for low density alloys. Flaring acts as reservoir and facilitates the entry of molted alloy into the mold area.
Indirect spruing
Indirect spruing uses the same basic principles of spruing. But the only difference lies in attachment of 3 running horizontal bars. The whole indirect sprue complex consist of 3 parts:
Manifold sprue. Horizontal running bar. Feeder sprue.
Once spruing is done the wax pattern and sprue former assembly is carefully removed from the die. During removal of pattern no pressure should be applied to prevent its distortion.
Then it is positioned into the crucible former to adjust the distance between the wax pattern and casting ring for INVESTING..
INVESTING
GPT8 Terminology..
Investing : The process of covering, enveloping, wholly (or) in part an object such as denture tooth, wax form, crown, etc with a suitable material before processing, soldering, casting.
Dental casting Investment: Material consisting principally of an allotrope of silica and a bonding agent. The bonding substance may be gypsum (for use in lower casting temperature) (or) phosphates and silica (for use in higher casting temperatures).
Refractory : Difficult to fuse/corrode, capable of enduring high temperatures Refractory investment : An investment that can withstand high temperature using a soldering/casting.
Essentials..
It should produce mould expansion to compensate for casting shrinkage. Should have sufficient strength at room & high temperature. Inner surface of the mold should not break at a high temperature. Should exhibit sufficient strength, to withstand the force of molten alloy entering the mold. Inner surface of mold should be smooth.
Its history can be traced back around 3000 B.C. But origin of lost wax technique, when viewed makes its presence in the writings of theophilus (11th Century).
11th Century Theophilus Described lost wax technique, which was a common practice prevailed in 11th century. 1558 Benvenuto Cellini claimed to have attempted, use of wax and clay for preparation of castings.
Basic composition..
Refractory Materials : The most commonly used refractory material is silicon dioxide in form quartz, crystoballite. Binder : commonly used binders are - calcium sulfate hemihydrate Others are Sodium silicate, ethyl silicate, ammonium sulfate, sodium phosphate. Other chemical modifiers Reducing agents Ex : Charcoal Sodium chloride, boric acid to shrinkage, during dehydration of calcium sulfate dihydrate. Potassium sulfate (accelerator) Copper powder(reducing agent)/magnesium oxide
Expansion..
This property of investment is needed for compensation of casting shrinkage of alloy. The expansion occurs because of:1. Normal setting expansion 2. Hygroscopic setting expansion 3. Thermal expansion.
Crucible former
Helps to hold & place the sprue in the center of the casting ring Helps to contour the investment surface They may be preformed or contoured with wax
A ring liner is placed on the inner surface of the casting ring Should be placed a few mm short of the ring It can be either
1. asbestos liners (used earlier)
2. non-asbestos liners a) Cellulose (paper), b) Aluminium silicate ceramic
Casting ring
Choice of the ring:
The diameter and the length of the ring should be selected rightly.
Produces consistent, accurate & predictable castings Facilitates controlled thermal expansion
Brush technique
Hand spatulate the mix to incorporate the powder quickly Coat the wax pattern with the investment Carefully coat the internal surface & the margin of the pattern Fill the ring slowly, starting from the bottom
Vacuum technique
Parts of vacc-u-spat lid with bowl: Pedal, spindle drive nut vacuum outlet hole with ring Parts of vacc-u-vester: Drive chuck Vibratory knob Vacuum outlet & vacuum guage
Method
First hand spatulate the mix Attach the vacuum hose & mix accordingly to the manufacturers recommendations Invert the bowl & fill the ring under vibration Remove the vacuum hose before setting of the mixer Immediately clean the bowl & mixing blade under running water
Setting of investment
It can be: In open air hygroscopic technique controlled water added technique
In open air
Usually when high heat TE technique is used. The investment is allowed to set in open air for 1 hour. The setting time is 1 hour for both GBI & PBI.
Hygroscopic technique
Once the casting ring is poured it is immersed into a water bath at 38 degrees temperature immediately This can be altered by: W:P ratio W:P HSE Time of immersion the delay HSE temp. of water HSE
After 1 hr
In a study by Nakai A, Ogura H when Mg(OH)2 or Ca(OH)2 was added at more than 4.0 mass% to the investment, it was useful in preventing the blackening of the as-cast surfaces of an Ag-Pd-Cu-Au alloy. As for differences in the effects between Mg(OH)2 and Ca(OH)2, they were not found
In a study by Bandyopadhyay-Ghosh et al both gypsum and phosphate bonded investments could be successfully used for the lost-wax casting of fluorcanasite glasses.
In a study conducted by Lyon HW et al it was found that vaccum investing eliminated 95% of nodules as compared to 17% of nodule free casting produced from hand mixing. Guilin Y et al the type of investment affects the microstructure and microhardness of the alpha-case layer of titanium castings. Based on the thickness of the surface reaction layer and the surface microhardness of titanium castings, MgO-based investment materials may be the best choice for casting these materials.
Trouble shooting
Improper mixing Errors in heating the investment Errors due to altered W:P ratio
Casting (GPT8)
something that has been cast in a mold; an object formed by the solidification of a fluid that has been poured or injected into a mold
1301 B.C
Gold casting
Crucible
Carbon crucibles Clay crucibles Quartz /zirconia - alumina
Gold melted with a blowpipe was then forced into the plaster mold by means of casting machine, which utilized compressed air
Inlay Mold
CASTING MACHINES
Casting machines provide the means for transferring the molten alloy from the crucible to the mold.
1.Pneumatic force (or) Air pressure type. 2.Centrifugal force type
PNEUMATIC FORCES
1.Steam pressure
2. THE PRESSURE / VACUUM 3. THE VACUUM / PRESSURE
Steam pressure
v A very old method
The molten alloy is pushed and sucked simultaneously into the mould.
These machines first evacuate the chamber to reduce oxidation and then apply air pressure to push the metal uniformly.
Melting chamber
Flask chamber
When the melting process has been completed, the casting tilts down and the molten titanium flows into the refractory mold.
CENTRIFUGAL FORCES
spring driven
Motor driven
Spring driven
Motor driven
Classification based on How metal melts on the 1. Torch melting centrifugal casting machine 2. casting machines Electrical resistance heated casting machine
3. Induction melting machines 4. Direct current arc melting machines
CASTING MACHINE
The alloy is melted electrically by a resistance heating , then cast into the mold centrifugally by motor (or) spring action
Resistance heating
Resistance heat develops when flow of current was opposed by a opposite power
e
e e p
p
p
Ceramics ,high-palladium alloys, palladiumsilver alloy, nickel chromium alloys or cobalt chromium alloy
The DICOR casting machine used for castable ceramics features a platinum electric resistance-type muffle mounted on a motor driven straight centrifugal casting arm.
The alloy is melted by an induction field that develops within a crucible surrounded by water-cooled metal tubing.
The electric induction furnace is a transformer in which an alternating current flows through the primary winding coil and generates a variable magnetic field in the location of the alloy to be melted in a crucible
It is more commonly used for melting base metal alloys not been used for noble alloy casting as much as other machines
Arc is produced between two electrodes: The alloy and the water-cooled tungsten electrode generates heat.
D
-----------------------------------------
cathode
B
C
----------------------------------------anode
The temperature within the arc exceeds 4000oC and the alloy melts very quickly. This method has a high risk for over heating the alloy.
The alloy is vacuum arc melted and cast by pressure in an organ atmosphere.
5 Metal receiver
6 Mold
Casting techniques
Burnout furnaces
Place the ring with the sprue facing down or on a raised object in the furnace.
Burnout techniques
Mold heating
Casting techniques
Pneumatic force
spring loaded
Casting procedure
The casting machine is given three (or) four clock wise turns and locked in position with the pin
The cradle and counter balance weights are checked for the appropriate size of the casting ring to minimize turbulence for the flow of metal.
A clay\carbon crucible for the gold alloy being cast is placed in the machine. The torch is lit and adjusted
Reducing zone
Preheating crucible
This preheating avoids formation during casting excessive slag
The alloy is heated in the reducing part of the flame until it is ready to cast A reducing flux is used in melting the alloy (50% boric acid powder and 50% fused borax ) it increases fluidity and reduces potential for oxidation.
When reducing zone is in contact-the surface of the gold is bright and mirror like. Oxidizing zone in contact-dull film or dross development. When gold alloy is ready to cast it will be white hot, forming smooth pool.
The casting machine arm is then released to make the casting. Providing enough force to cause the liquid alloy to flow into the mold.
The machine is allowed to spin until it has slowed enough that it can be stopped by hand, and the ring is removed with casting tongs
Quenching
After the casting has solidifies, the ring is removed and quenched in water as soon as the button exhibits a dull-red glow.
weights
Casting pressure
The pressure should be applied for at least 4 sec. the mold is filled and the alloy is solidified in 1sec. or less but it is quite soft during the early stages.
Base metal alloys are bench-cooled to room temperature before the casting is removed from the investment
1.
Process of melting and casting takes place in an evacuated two chamber system with a continuous flow of argon gas Titanium ingot is heated in a copper crucible Prevents overheating & reaction
2.
Laws of casting
Ingersoll & Walding (1986) formulated an expanded set of 17 separate recommendations for spruing, investing, burnout, melting & casting procedures. Collectively these guidelines are referred to as the laws of casting.
2 nd Law Of Casting
Orient wax patterns so all the restoration margins will face the trailing edge when the ring is positioned in the casting machine: Add a wax dot to the crucible so that, it will guide us in placing the ring in casting machine Penalty: cold shuts and short margins
Defects in casting
Defects in casting can be eliminated or minimised by strict adherence to prescribed procedures. Defects in casting can generally be divided into:
Distortion Poor surface finish
fins / spines nodules veins and ridges rough surface
Distortion
In most cases distortion of the casting can be attributed to distortion of the wax pattern The wax pattern distortion can be minimised by careful and proper manipulation of the wax and handling of the pattern. In addition, some of distortion of the wax pattern can be caused by hardening of the investment around it, whereby setting and hygroscopic expansion could lead to uneven deformation of the walls of the wax pattern. This depends, on the other hand, on the type of wax, thickness and configuration of the pattern
Porosity
Main causes of the porosity of alloy castings are: 1) Solidification defects
Localized shrinkage porosity Micro porosity Pin hole porosity Gas inclusion Sub surface porosity
2) Trapped gases
3) Residual air
Solidification Defects
Solidification defects cold lead to two different manifestations of porosity: Localised shrinkage porosity Microporosity.
If the sprue is not properly designed and implemented then it may solidify before the feeding is complete thus preventing a continuous supply of molten alloy This type of defect usually occurs close to the spruecasting junction
Suck-back porosity
If hot spot is created on in the mould near to the sprue this causes the local region to freeze last and cause porosity Generally occurs at occlusocervical line angle that is not well rounded
This can be eliminated by flaring the point of sprue attachment and by lowering casting temperature by 30C
Microporosity
It is also caused by solidification shrinkage, but generally happens in fine grain alloys when the solidification is too rapid for the microvoids to segregate. This in turn is caused the mould or casting temperature being too low.
Sub-Surface Porosity
Caused by simultaneous nucleation of solid grains and gas bubbles It can be dimnished by controlling the rate at which molten metal enters the mold
In case of low castin/mold temperature it can occur on the outer surface Factors to be considered:
1. 2. 3. 4. Dense investments Tendency for mold to clog Venting Proper burn out
Incomplete Casting
If the molten alloy is prevented from fully or partially filling the mould, insufficient venting of the mould and high viscosity of the metal If the air in the mould could not be vented quickly once the molten allow is poured into the mould, its back pressure will prevent compete filling of the mould by the molten alloy If the elimination of the wax patter was not fully complete, the pores of the investment might become filled with the combustion products thus preventing venting of the air which can cause similar issue to the above
Castable Ceramics
Mold conditioning
Two stage technique1.The invested pattern is placed in a cold furnace, the temperature is raised to 249C, and maintained for 30 min (heat soak). 2.The temperature is raised to 899C, and maintained for 2 hrs (heat soak).
Casting
A 4 gm ceramic ingot is loaded in the ceramic crucible. The amount of ceramic material required to make a good casting can be determined when multiplied by a conversion factor of 2.6, the weight of the wax pattern, sprues and button should not exceed 4gm .
Casting technique
The casting ring is removed form the machine and allowed to cool for 45 min before divesting.
On the surface of the workingcast wax pattern is made from prefabricated wax elements
deflasking
Literature review
In a study by baltag et al, the lowest porosity in titanium circumferential clasp arms was obtained with sprues attached perpendicularly to the minor connectors, regardless of sprue diameter Conventional sprue directions produced significantly higher porosity in clasp lingual arms, the amount of porosity increasing with sprue diameter.
Principles of casting
Casting defects Casting of ceramics Casting of titanium Casting procedure in RPD conclusion
Spruing
Investing patterns Burn out procedure Casting machines Casting techniques Casting procedure
critical appraisal.....
.....will help to assure the supreme quality of this form of invigorating care.....
References
1. K. J. Anusavice, Phillips Science of Dental Materials, 11th edition, W. B. Saunders co 2003, pg: 295-350 2. Introduction to metal ceramic technology, W.P. Naylor, Quintessence publishing co, inc ,1992, pg: 65-82 3. J.F.MaCabe, applide dental materials, 8th edition, blackwell science publication, pg:69-71 4. M.Gladwin, Clinical Aspects of Dental Materials, Lippincott Williams & Willikins publishing, 1999, pg:115-126 5. Craig R.G, Restorative Dental Materials;10th edition; St.Louis: Mosby, 1997, pg:457-480
6.
Baltag I et al: Internal porosity of cast titanium removable partial dentures: influence of sprue direction and diameter on porosity in simplified circumferential clasps. Dent Mater. 2005 Jun;21(6):530-7 7. Mohammed H et al: Button versus buttonless castings for removable partial denture frameworks, J Prosthet Dent. 1994 Oct;72(4):433-44 8. Peregrina AM, Rieger MR: Evaluating six sprue designs used in making high-palladium alloy castings, J Prosthet Dent. 1986 Aug;56(2):192-6 9. Ballard GT et al: Permeability and porosity of dental casting investments, J Prosthet Dent. 1975 Aug;34(2):170-8 10. Muller H.J et al, Surfactant containing phosphate investment, dent mater, 2: 42-44: 1986
11.
Nakai A et al: Development of casting investment preventing blackening of noble metal alloys. Part 4: effect of Mg(OH)2 and Ca(OH)2 as additives, Dent Mater J. 2007 Nov;26(6):870-4
12. Bandyopadhyay-Ghosh et al: The effect of investment materials on the surface of cast fluorcanasite glasses and glass-ceramics, J Mater Sci Mater Med. 2007 Aug 1 13. Guilin Y et al: The effects of different types of investments on the alpha-case layer of titanium castings, J Prosthet Dent. 2007 Mar;97(3):157-64 14. Creating a buttonless casting by using preformed wax sprues, W. J. Padilla et al, J Prosthet Dent, 76, 3, Sep 1996, Pg: 327-329 15. Lyon HW et al: effectiveness of vacuum investing in the elimination of surface defects of gold castings, J Am Dent Assoc 46:197, 1953
Thank you
Casting Defects
Discontinuities in castings
that exhibit a size, shape, orientation, or location that makes them detrimental to the useful service life of the casting
Porosity is pockets of gas inside the metal caused by microshrinkage, e.g. dendritic shrinkage during solidification.