AS 2331.

0—2006
AS 2331.0—2006

Australian Standard®
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Methods of test for metallic and related

coatings

Part 0: Method selection guide

 This Australian Standard® was prepared by Committee MT-009, Metal Finishing. It was
approved on behalf of the Council of Standards Australia on 19 July 2006.
This Standard was published on 14 August 2006.

The following are represented on Committee MT-009:

• Australasia Institute of Metal Finishing

• Australian Chamber of Commerce and Industry
• Australian Industry Group
• Department of Defence
• Galvanizers Association of Australia
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• Institute of Materials Engineering Australia

• The Royal Australian Chemical Institute
• Society of Automotive Engineers-Australia

This Standard was issued in draft form for comment as DR 06289.

Standards Australia wishes to acknowledge the participation of the expert individuals that
contributed to the development of this Standard through their representation on the
Committee and through public comment period.

Keeping Standards up-

up-to-
to- date
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using a current Standard, which should include any amendments that may have been
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Standards Australia welcomes suggestions for improvements, and encourages readers to

notify us immediately of any apparent inaccuracies or ambiguities. Contact us via email at
[email protected],
[email protected] or write to Standards Australia, GPO Box 476, Sydney, NSW 2001.
 AS 2331.0—2006

Australian Standard®
This is a free 7 page sample. Access the full version at http://infostore.saiglobal.com.

Methods of test for metallic and related

coatings

Part 0: Method selection guide

Originated as AS 2331.0—2001.
Second edition 2006.

COPYRIGHT
© Standards Australia
All rights are reserved. No part of this work may be reproduced or copied in any form or by
any means, electronic or mechanical, including photocopying, without the written
permission of the publisher.
Published by Standards Australia GPO Box 476, Sydney, NSW 2001, Australia
ISBN 0 7337 7682 5
 AS 2331.0—2006 2

PREFACE
This Standard was prepared by the Australian members of the Joint Standards
Australia/Standards New Zealand Committee MT-009, Metal Finishing, to supersede
AS 2331.0—2001, Methods of test for metallic and related coatings, Part 0: Introduction
and list of methods.
After consulting with stakeholders in both countries, Standards Australia and Standards
New Zealand decided to develop this Standard as an Australian Standard rather than an
Australian/New Zealand Standard.
The objective of this edition is to revise the guide by describing the scope and application
of each Standard in the series and to include four new Standards.
All Standards in the AS 2331 series apply to metallic and related coatings. However, it
should be noted that test methods for paint and related coatings are specifically covered in
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the AS/NZS 1580, Paints and related materials—Methods of test, series of Standards.
This Standard is Part 0 of a series of Standards covering the methods of tests for metallic
and related coatings.
The series comprises the following Parts:
AS
2331 Methods of test for metallic and related coatings
2331.0 Method 0: Method selection guide (this Standard)
2331.1.1 Method 1.1:
Local thickness tests—Micrographic examination of cross-sections
2331.1.2 Method 1.2:
Local thickness tests—Coulometric method
2331.1.3 Method 1.3:
Local thickness tests—Magnetic method
2331.1.4 Method 1.4:
Local thickness tests—Magnetic induction and eddy current
methods
2331.1.5 Method 1.5: Local thickness tests—Beta-backscatter method
2331.1.6 Method 1.6: Local thickness tests—Taper section method
2331.1.7 Method 1.7: Local thickness tests—Measurement of dry film thickness of thin
coating systems particularly by coil coated products by destructive
means using a boring device
2331.2.1 Method 2.1: Tests for average coating mass per unit area or for thickness—
Dissolution methods―Strip and weigh, and analytical
2331.2.3 Method 2.3: Tests for average coating mass per unit area or for thickness—
Hydrogen evolution method for zinc coatings
2331.3.1 Method 3.1: Corrosion and related property tests—Neutral salt spray test (NSS
test)
2331.3.2 Method 3.2: Corrosion and related property tests—Acetic acid salt spray test
(ASS test)
2331.3.3 Method 3.3: Corrosion and related property tests—Copper accelerated acetic
salt spray test (CASS test)
2331.3.4 Method 3.4: Corrosion and related property tests—Thioacetamide anti-tarnish
and porosity test
2331.3.5 Method 3.5: Corrosion and related property tests—Sulfur dioxide/hydrogen
sulfide porosity tests
2331.3.6 Method 3.6: Corrosion and related property tests—Electrographic porosity test
2331.3.7 Method 3.7: Corrosion and related property tests—Corrodkote (Corr) test
2331.3.8 Method 3.8: Corrosion and related property tests—Humidity test―24 h cycle,
damp heat
2331.3.9 Method 3.9: Corrosion and related property tests—Porosity test―Ferroxyl test
 3 AS 2331.0—2006

2331.3.10 Method 3.10: Corrosion and related property tests—Cracks and pores in
chromium
2331.3.11 Method 3.11: Corrosion and related property tests—Chemical residue tests
2331.3.12 Method 3.12: Corrosion and related property tests—Cyclic salt fog/UV exposure
of organically coated metal
2331.3.13 Method 3.13: Corrosion and related property tests—Wet (salt fog)/dry/humidity
2331.4.1 Method 4.1: Physical tests—Qualitative adhesion tests
2331.4.2 Method 4.2: Physical tests—Ductility
2331.4.4 Method 4.4: Physical tests—Assessment of intensity of shot-peening
2331.4.5 Method 4.5: Physical tests—Electroplated plastics―Thermal cycling tests
2331.4.7 Method 4.7: Physical tests—Resistance to scratching
The term ‘informative’ has been used in this Standard to define the application of the
appendix to which it applies. An ‘informative’ appendix is only for information and
guidance.
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 AS 2331.0—2006 4

CONTENTS

Page

SECTION 1 SCOPE AND GENERAL

1.1 SCOPE ........................................................................................................................ 5
1.2 REFERENCED DOCUMENTS .................................................................................. 5
1.3 DEFINITIONS ............................................................................................................ 6

SECTION 2 METHOD SECTION GUIDE— LOCAL THICKNESS TESTS

2.1 METHOD 1.1: MICROGRAPHIC EXAMINATION OF CROSS-SECTIONS.......... 7
2.2 METHOD 1.2: COULOMETRIC METHOD ............................................................. 7
2.3 METHOD 1.3: MAGNETIC METHOD ..................................................................... 7
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2.4 METHOD 1.4: MAGNETIC INDUCTION AND EDDY CURRENT METHODS .... 8
2.5 METHOD 1.5: BETA-BACKSCATTER METHOD .................................................. 8
2.6 METHOD 1.6: TAPER SECTION METHOD............................................................ 9
2.7 METHOD 1.7: MEASUREMENT OF DRY FILM THICKNESS OF THIN
COATING SYSTEMS PARTICULARLY BY COIL COATED PRODUCTS BY
DESTRUCTIVE MEANS USING A BORING DEVICE............................................ 9

SECTION 3 METHOD SELECTION GUIDE—TESTS FOR AVERAGE COATING MASS

PER UNIT OR FOR THICKNESS
3.1 METHOD 2.1: DISSOLUTION METHODS―STRIP AND WEIGH, AND
ANALYTICAL.......................................................................................................... 10
3.2 METHOD 2.3: HYDROGEN EVOLUTION METHOD FOR ZINC COATINGS ... 10

SECTION 4 METHOD SELECTION GUIDE—CORROSION AND RELATED

PROPERTY TESTS
4.1 METHOD 3.1: NEUTRAL SALT SPRAY TEST (NSS TEST)................................ 11
4.2 METHOD 3.2: ACETIC ACID SALT SPRAY TEST (ASS TEST) ......................... 11
4.3 METHOD 3.3: COPPER ACCELERATED ACETIC ACID SALT SPRAY TEST
(CASS TEST) ............................................................................................................ 11
4.4 METHOD 3.4: THIOACETAMIDE ANTI-TARNISH AND POROSITY TEST ..... 11
4.5 METHOD 3.5: SULFUR DIOXIDE/HYDROGEN SULFIDE POROSITY TESTS. 12
4.6 METHOD 3.6: ELECTROGRAPHIC POROSITY TEST ........................................ 12
4.7 METHOD 3.7: CORRODKOTE (CORR) TEST ...................................................... 12
4.8 METHOD 3.8: HUMIDITY TEST―24 h CYCLE, DAMP HEAT .......................... 12
4.9 METHOD 3.9: POROSITY TESTS―FERROXYL TEST ....................................... 13
4.10 METHOD 3.10: CRACKS AND PORES IN CHROMIUM ..................................... 13
4.11 METHOD 3.11: CHEMICAL RESIDUE TESTS ..................................................... 13
4.12 METHOD 3.12: CYCLIC SALT FOG/UV EXPOSURE OF ORGANICALLY
COATED METAL .................................................................................................... 13
4.13 METHOD 3.13: WET (SALT FOG)/DRY/HUMIDITY........................................... 14

SECTION 5 METHOD SELECTION GUIDE—PHYSICAL TESTS

5.1 METHOD 4.1: QUALITATIVE ADHESION TESTS.............................................. 15
5.2 METHOD 4.2: DUCTILITY .................................................................................... 15
5.3 METHOD 4.4: ASSESSMENT OF INTENSITY OF SHOT-PEENING .................. 15
5.4 METHOD 4.5: ELECTROPLATED PLASTICS―THERMAL CYCLING TESTS. 15
5.5 METHOD 4.7: RESISTANCE TO SCRATCHING.................................................. 16

APPENDIX A ALIGNMENT WITH ISO AND OTHER NATIONAL STANDARDS...... 17

 5 AS 2331.0—2006

STANDARDS AUSTRALIA
Australian Standard
Methods of test for metallic and related coatings

Part 0: Method selection guide

SECT ION 1 SCOPE AND GENERA L

1.1 SCOPE
This Standard gives guidance on the selection of the appropriate methods for the testing of
metallic and related coatings. In the following Clauses the scope and principle of each
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Standard in the series are specified.

This series of Standards are arranged in four categories:
Part 1: Local thickness tests
Part 2: Tests for average coating mass per unit area or for thickness
Part 3: Corrosion and related property tests
Part 4: Physical tests
NOTES:
1 Since the last edition of this Standard two Standards in this series have been withdrawn, viz.
AS 2331.2.2—1980 on the time of gassing method and AS 2331.4.6—1990 on solderability.
2 Since the last edition of this Standard four Standards have been included in the series, viz.
AS 2331.1.7 (see Clause 2.7), AS 2331.3.12 (see Clause 4.12), AS 2331.3.13 (see Clause
4.13) and AS 2331.4.7 (see Clause 5.5).

1.2 REFERENCED DOCUMENTS

The following documents are referred to in this Standard:
AS
1247 Metallic coatings—Rating of test specimens and manufactured articles subject
to corrosion tests
4108 Metal finishing—Glossary of terms in electroplating and related processes
ISO
1463 Metallic and oxide coatings—Measuring of coating thickness—Microscopical
method
2177 Metallic coatings—Measurement of coating thickness—Coulometric method by
anodic dissolution
2178 Non-magnetic coatings on magnetic substrates—Measurement of coating
thickness—Magnetic method
2819 Metallic coatings on metallic substrates—Electrodeposited and chemically
deposited coatings—Review of methods available for testing adhesion
3543 Metallic and non-metallic coatings―Measurement of thickness―Beta
backscatter method

www.standards.org.au  Standards Australia

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AS 2331.0-2006, Methods of test for metallic and

related coatings Method selection guide
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