AS 1038.10.

3—1998

Australian Standard™
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Coal and coke—Analysis and

testing

Part 10.3: Determination of trace

elements—Coal and coke—
Determination of boron content—
ICP-AES method
 This Australian Standard was prepared by Committee MN/1, Coal and Coke. It was
approved on behalf of the Council of Standards Australia on 27 February 1998 and
published on 5 June 1998.

The following interests are represented on Committee MN/1:

ACIRL
Australasian Institute of Mining and Metallurgy
Australian Coal Association
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Australian Coal Preparation Society

Australian Institute of Energy
Bureau of Steel Manufacturers of Australia
Coalfield Geology Council of New South Wales
CSIRO, Division of Coal and Energy Technology
Department of Mines and Energy, Queensland
Electricity Supply Association of Australia
Institution of Engineers, Australia
Minerals Council of Australia
Royal Australian Chemical Institute
University of New South Wales
University of Newcastle
University of Queensland

Review of Australian Standards. To keep abreast of progress in industry, Australian Standards are subject
to periodic review and are kept up to date by the issue of amendments or new editions as necessary. It is
important therefore that Standards users ensure that they are in possession of the latest edition, and any
amendments thereto.
Full details of all Australian Standards and related publications will be found in the Standards Australia
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This Standard was issued in draft form for comment as DR 96494.

 AS 1038.10.3—1998
This is a free 5 page sample. Access the full version at http://infostore.saiglobal.com.

Australian Standard™

Coal and coke—Analysis and

testing

Part 10.3: Determination of trace

elements—Coal and coke—
Determination of boron content—
ICP-AES method

Originated as AS 1038.10.3 — 1988.

Second edition 1998.

Published by Standards Australia

(Standards Association of Australia)
1 The Crescent, Homebush, NSW 2140
ISBN 0 7337 1925 2
 AS 1038.10.3 — 1998 2

PREFACE

This Standard was prepared by the Standards Australia Committee MN/1, Coal and Coke
to supersede AS 1038.10.3 — 1988, Coal and coke — Analysis and testing,
Part 10.3: Determination of trace elements — Coal, coke and fly-ash — Determination of
boron content — Spectrophotometric methods. It was prepared as one of a series of
methods for the determination of trace elements in coal and coke.
The determination of the trace elements in coal and coke is becoming more important due
to the considerable emphasis being placed on the effect of these elements on the
environment. International buyers are becoming increasingly aware of the need for more
detailed knowledge of the coals that they are purchasing and may request trace element
analysis. In order to have accurate and precise results for this analysis it is imperative that
standard methods be available.
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The objective of this Standard is to provide a method for determining the boron content of
coal and coke. The objective of the revision is to replace the spectrophotometric method
with an inductively coupled plasma atomic emission spectrometric method.

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 3 AS 1038.10.3 — 1998

CONTENTS
Page
1 SCOPE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
2 REFERENCED DOCUMENTS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
3 DEFINITIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
4 PRINCIPLE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
5 SAFETY . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
6 REAGENTS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
7 APPARATUS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
8 SAMPLE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
9 PROCEDURE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
10 CALCULATION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
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11 REPORTING OF RESULTS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
12 PRECISION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
13 TEST REPORT . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
 This is a free preview. Purchase the entire publication at the link below:

AS 1038.10.3-1998, Coal and coke - Analysis and

testing Determination of trace elements - Coal and
coke - Determination of boron content - ICP-AES
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method

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