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PL Experiment ?

The document discusses the preparation and analysis of photoluminescence (PL) in doped and non-doped zinc sulfide (ZnS) materials. It outlines the experimental setup, including the chemicals and equipment required, as well as the procedures for preparing the samples and obtaining PL spectra. The results indicate variations in optical properties due to doping, with specific focus on Raman scattering and peak identification.

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bikramorigaon
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5 views5 pages

PL Experiment ?

The document discusses the preparation and analysis of photoluminescence (PL) in doped and non-doped zinc sulfide (ZnS) materials. It outlines the experimental setup, including the chemicals and equipment required, as well as the procedures for preparing the samples and obtaining PL spectra. The results indicate variations in optical properties due to doping, with specific focus on Raman scattering and peak identification.

Uploaded by

bikramorigaon
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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cheniLal toopceuipotatiou

nanoseyitals by chemiaf
metlkad Kecoyd photoluwuwscence ped ra
amd analy2e your result.
backqrowMd: Photolumineswnu (pL) in tue
ni aion tom a moteria
pron igat
Bone
foms
TO1Y (umin Scene poum au che mili
-sLenu, lectrotuminseu, mihaualu mvesenu,
ete. PL
in venionduto involve eion loom tue
exutation
vam ow eery level trom it atey t
hith pwoto albove tue band ap eeY
e PL iM cni condu ocur due to the
tramiton ot harge anTiers om the onduetion
bamd to tue valame uond
invglving de te cts tevels.
iN wsed to
Aspe tomter is ULoTd tw PL spetra
t owtsts tue follouing main pavts : 0
woochomater sam ple hom oe omd )

de tecto. Te PL ewiion toom the matrial n


wlleeted im a pen pen dicular rect or to the
inidet loeawn n or dey to avoid lutrr ferenu

t the woring d a spe chro tluYO meter


supey
frutaton
MOochmmatoy
- chromaty

ittuxtatina te wor king Detetor

Data prrusoY

in
Doping
their chamqt
mcon duton io Wnon to lead to
invano PD perttes such on
letial nd optial Zns is a gooye 11
KVT sicone
-üWe teTm lead to theçT
change
The preAt ex perimentoad work jo to am0 Popertie
mdoped 2s and Nn-do pe Zns by a prce pat
umil
ad om paru PL prv perfin.
chmials and Equigmut
Eaui Qmutt tequirced
Zinc acette. sodiu msulphi u,
man g9ue
7an funnel, destilled weter.
Fper , Uv-viible spetr pleoto metpr spetto
tun meter.
Prouduu
for wdoped 2n
To prapace a IM Sol"
di iles water
presparatioml
zinc
aeate n Lo
dirtilleA wateY

sol dd 0 m dis tled wter in it


n diitilled for hat aan
keop Hhe mixtute sol" m

use qlam Au nnel and tlter papem to eparate


pteipaten toom the soluton wah te
pruupitates sevecal timen ing the distted
water.
for Mm -dopped KnS preeparcation
To prceparce
2Àne atate wate,

di ti lled wate.
E frceparte o.o2M(0.0u l0.06 HMuue in 0 me ditled
Mix the 2ine atate ol" MuU, lou
addittom o te Na,s tol"
keey tue mixtuee -sol" mdistur bed or halt
Wou.
Aunl and lte pepert to Jepareate
reipitates tom tue
pot ertae times wtng det astlled watoY
Calurtation

|000

0.96 M2lne ace tete

tor

(060
2
4. 803 m

oride
wslerr man Mangamr lond 161.8?9m/wul
0.0u(61.89 x,
Dlsuri

inLomng
tit trom th tolva Ramam scatering

length nd tor Kaman pealk in aloag


a cowtt. As a rcut peak teesultiy tom
Aaman siatrring tat spetaliy whn hamging
fu exutatiom uoavele -ngth olih can be wd
to
idutit the haman peak at 49 Mm

360

For s). Mu do pped 2Zns, t Pead i0 olb Ved

- - 0.00I D6 nm1
360

tt, nteut w7t to olhuot equal to Kamay


tt o water Tucotote we co obied comde
ut
thant peaks olb served at
are
be caus
aUse Ramam scatlering 4 watr.

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