SARVAJANIK UNIVERSITY

Sarvajanik College of Engineering and Technology

Bachelor of Technology

B. Tech. Semester III

Subject Code: BTCH13303
Subject Name: Chemical Engineering Process Technology I

Type of course: Professional Core Course

Prerequisite: Xth Standard Biology course, Physical Chemistry
Rationale: The course offers fundamental principles of chemical engineering Unit processes
and Manufacturing technology. This course offers important contribution to understand
chemical reactions present in different production routes for various chemicals. Many
complex chemical reactions and complex transport processes occur for Industrial mfg.
Teaching and Examination Scheme:

TEACHING Theory Marks Practical Marks Total

SCHEME
L T P C TEE CA1 CA2 TEP CA3
2 0 2 2 60 25 15 30 20 150

CA1: Continuous Assessment (assignments/projects/open book tests/closed book tests CA2:

Sincerity in attending classes/class tests/ timely submissions of assignments/self-learning
attitude/solving advanced problems TEE: Term End Examination TEP: Term End Practical Exam
(Performance and viva on practical skills learned in course) CA3: Regular submission of Lab
work/Quality of work submitted/Active participation in lab sessions/viva on practical skills learned
in course

Content:
Sr. Teaching Module
Topics
No. Hrs. Weightage
1 Introduction
Definition and importance of unit processes in chemical
engineering, Concept of unit operation and unit processes and
their role in systematizing the cognitive structure of chemical 3
industries, Classification of unit processes, Chemical process
kinetics and Factors affecting, Symbols used in Chem. 10 %
Engineering, Process flow diagram, Introduction to thermo-
chemistry along with appropriate case studies.

For the A.Y. 2022-23

 SARVAJANIK UNIVERSITY
Sarvajanik College of Engineering and Technology
Bachelor of Technology

2. Halogenation Process
Definition and scope of halogenation reactions,
Thermodynamics and kinetics of halogenation reactions
Halogenating agents, Industrial halogenation with types of 10%
3
equipment,
Production of
Chlorobenzene, Benzene hexa chloride and vinyl chloride
from Ethylene and Acetylene.
3. Chlor-Alkali Industry Process
Electrolysis of brine, technology involved and corrosion issues
related to it.
Manufacturing of
Manufacture of soda ash by solvay and modified solvay 3 10%
process, Electrolytic process for caustic soda, different types
of cell, manufacturing of chlorine and hydrogen, hydrochloric
acid, common salt by vacuum evaporation process

4. Esterification and Hydrolysis

Process
Definition and scope of Esterification, Esterification by
organic acids and by carboxylic acid derivatives, Esters by
addition to unsaturated systems and inorganic acids,
Definition and scope of hydrolysis, Hydrolyzing agents, 3 10%
Materials susceptible to hydrolysis, Kinetics,
thermodynamics, and mechanism of hydrolysis, Equipment
for hydrolysis with technical operations.
Manufacturing of
Mfg. of starch, dextrose and sucrose
5. Hydrogenation Process
Definition and scope of hydrogenation, Hydrogen: production
and properties, Gas catalytic hydrogenation and hydrogenation,
Kinetics and thermodynamics of hydrogenation reactions,
General principles concerning hydrogenation catalysts, 7%
2
Industrial hydrogenation of fat & oil, Production of methanol
from CO2 & H2. Hydrogen production technologies

Manufacturing of
Hydrogenated Veg. Oil and margarine.

For the A.Y. 2022-23

 SARVAJANIK UNIVERSITY
Sarvajanik College of Engineering and Technology
Bachelor of Technology

6. Oils, Fats, Soaps & Detergents Process

Vegetable oil Extraction method using Mechanical and Solvent
extraction process , hydrogenation of oil, cleaning mechanism
of soaps and detergents, 3 10%
Manufacturing of.
Manufacturing of soaps and glycerine, manufacturing of
detergents.
7. Hydrolysis Process
Definition and types of hydrolysis, Hydrolyzing agents,
Kinetics, thermodynamics, and mechanism of hydrolysis, 7%
2
Industrial Hydrolysis of fat, hydrolysis of carbohydrates,
starch to dextrose, Manufacturing of ethanol from ethylene
(shell process) Mfg. of phenol from benzene sulfonic.
8. Sugar, Paints, Pigments Manufacturing Process
Manufacturing of Sugar, Paints, different types of
pigments such as white, blue, red, yellow, green, brown, 2 7%
etc , Varnishes, Industrial Coatings, printing inks,
Polishes etc
9. Cement & Glass Manufacturing
Lime stone beneficiation and Manufacturing of cement, types 2 7%
of cement, manufacturing of glass, types of glass.
10. Amination by ammonolysis Tehcnology
Definition & types of reactions, Aminating agents, Physical
and Chemical factors affecting it. Catalyst used in
ammonolysis, Kinetics and Thermodynamics of ammonolysis 2 7%
Manufacturing Process
Mfg. of Aniline from chlorobenzene and Nitroaniline from
Dichloro Nitro Aniline
11 Sulfonation and sulfation Technology
Definition and scope of sulfonation and sulfation, Chemical
and physical factors in sulfonation and sulfation, The
desulfonation reaction, Use of SO3, SO2, H2SO4 as sulfonating 7%
2
and sulfating agents and their applications,
Manufacturing Process
Mfg. of Benzene sulfonates, Sulfation of Dimethyl
Ether and Lauryl Alcohol.
12 Dyes and Intermediates:
Classification of dyes according to constitution and application,
various dyes such as Azo dyes, Anthroquione dyes, Triamyl 7%
2
dyes, dispersed dyes, Misc. Dyes such as azine, oxazines,
thiazines, thiazoles, nitro dyes etc. Various dye intermediates
based on unit processes ,Manufacturing Processes of

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 SARVAJANIK UNIVERSITY
Sarvajanik College of Engineering and Technology
Bachelor of Technology

Suggested Specification table with Marks (Theory/Practical):

% Distribution of Marks
R Level U Level A Level N Level E Level C Level
30 30 15 15 05 05
Legends: R: Remembrance, U: Understanding; A: Application, N: Analyze, E: Evaluate C: Create
and above Levels (Revised Bloom’s Taxonomy)
Note: This specification table shall be treated as a general guideline for students and teachers. The
actual distribution of marks in the question paper may vary slightly from above table.
Reference Text Books:

Sr. Title of book Author(s) Publisher and Year of Publication

No. /article details like ISBN publication Edition

1 Shreve’s Chemical George F. McGraw Hill 5th

Process Industries Austin International
2 Dryden’s Outlines M. Gopala Rao East West Press Pvt. 2nd
of Chemical & Marshall Ltd., Ne
Technology, Sitting,

Course Outcome:
Sr. No. CO Statement Marks %
After learning this subject, students will be able to weightage
CO-1 To make students aware about all the Process technology for mfg of 30
different chemicals long with case studies.
CO-2 To understand the principles behind reaction mechanism for different 20
chemicals.
CO-3 To make student understand the global scenario of chemical sectors 20

CO-4 To utilize the renewable energy in problem solving where conventional 10

energy are not fruitful and require replacement.
CO-5 To understand the design and applications of power generating devices 10
using renewable energy sources as per industrial requirement

CO-6 Resolve all technological and economical problems arise in the chemical 10
manufacturing plants.

Mapping with POs:

For the A.Y. 2022-23

 SARVAJANIK UNIVERSITY
Sarvajanik College of Engineering and Technology
Bachelor of Technology

PO1 PO2 PO3 PO4 PO5 PO6 PO7 PO8 PO9 PO10 PO11 PO1 PS PSO PSO
2 O1 2 3

CO-1 2 2 2
3 3 2 1 1 3 3 3 2 2 2 3

CO-2 2 2 1
3 3 2 1 1 3 3 3 2 2 2 3

CO-3 1 1 1
3 3 2 1 1 3 3 3 2 2 2 3

CO-4 2 2 3
3 3 2 1 1 3 3 3 2 2 2 2

CO-5 2 2 3
3 3 2 1 1 3 3 3 2 2 2 2

CO-6 2 2 2
3 3 2 1 1 3 3 3 2 2 2 3

Rationale*

Rationale*: Engineering students should learn the principles of biochemistry, genetics, molecular
biology, and cell biology. Many complex chemical reactions and complex transport processes occur
due to biomaterials can be studied by the students.
LIST OF PRACTICALS:

Crystallization of Sugar
To determine chiral chemical concentration using polarimeter
To prepare Aspirin from Salicylic acid
Soap & Detergent manufacture
Determine acid number of oil sample
To determine the percentage of nitrogen content of given NH4Clsample by Formaline method.
To determine nitrogen content of given (NH4) 2SO4 sample by Formaline method.
Major Equipment: Polari meter

List of Open Source/learning website:

For the A.Y. 2022-23
 SARVAJANIK UNIVERSITY
Sarvajanik College of Engineering and Technology
Bachelor of Technology

https://nptel.ac.in/courses/103/106/103106108/

List of Open Source Software:

https://www.openmodelica.org/

https://dwsim.inforside.com.br/new/

For the A.Y. 2022-23