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180nm Fabrication Process Flow

The document outlines the 180 nm CMOS fabrication process flow, detailing each step from silicon substrate preparation to silicide formation. It includes methods, materials, and metrology for various stages such as shallow trench isolation, gate formation, and source/drain formation. Each section emphasizes the importance of quality checks and the consequences of contamination or flawed processes on overall yield.
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0% found this document useful (0 votes)
163 views58 pages

180nm Fabrication Process Flow

The document outlines the 180 nm CMOS fabrication process flow, detailing each step from silicon substrate preparation to silicide formation. It includes methods, materials, and metrology for various stages such as shallow trench isolation, gate formation, and source/drain formation. Each section emphasizes the importance of quality checks and the consequences of contamination or flawed processes on overall yield.
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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180 nm CMOS Fabrication Process Flow

Big picture of fabrication process flow 2


1. Si substrate preparation

2. Shallow Trench Isolation (STI) Formation


Wire
3. Well Formation
Contact
Gate Side wall
4. Gate Formation N-type P-type
Source/Drain Source/Drain
5. Lightly Doped Drain (LDD) Formation Shallow trench
isolation (STI)

6. Side wall formation Si substrate


P-type Well N-type Well
N-type
Light Doped Drain

P-type
7. Source/Drain Formation Light Doped Drain Si Poly-Si High N-Dopant
(≃1020 cm-3)
SiO2 Silicide
High P-Dopant
8. Silicide Formation Si3N4 TiN/Ti (≃1020 cm-3)
Tungsten Low-k Low P-Dopant
(≃1016 cm-3)
9. Contact Formation Cu
Low N-Dopant
(≃1016 cm-3)
10. Wire Formation
Si Substrate Preparation – Quality Check 3
Explanation
Check the quality of the substrates received from the supplier.

Why important ?
If the substrate preparation is flawed, the entire downstream
process may be wasted. Therefore, it is essential to carefully verify

What, Why, How do we do in this process?

What Why How


Dopant concentration Affect built-in potential ・Sheet Resistance
check of PN junction, leading ・SIMS
Si to fluctuate Vth
Crystallographic Affect carrier mobility ・XRD
Orientation defect check ・Photoluminescence
Bow and Wrap Focus misalignment ・Stylus profiler
during exposure, leading
CD variation
Si Substrate Preparation - Cleaning 4
Explanation
Native, oxide, organic contaminants, and metal impurities are
removed prior to starting the fabrication process

Why important ?
If there is contamination on the silicon substrate, it may become
trapped beneath the gate, leading to defects. It can also alter
etching and deposition characteristics, ultimately affecting yield.

Si
Shallow Trench Isolation – Thermal Oxidation 5

Purpose : Sacrificial layer for ion implantation


protecting product area against CMP

Method : Thermal Oxidation

Deposited material : Silicon Dioxide

Thickness : 10 nm
Si
SiO2 Metrology : Spectroscopy Ellipsometry
Shallow Trench Isolation – Stopping layer deposition 6

Purpose : Stopping layer against CMP

Method : Low Pressure CVD

Deposited material : Silicon Nitride

Thickness : 20~50 nm?

Si Metrology : Spectroscopy Ellipsometry


SiO2
Si3N4
Shallow Trench Isolation – STI Patterning 7

Purpose : Form pattern on wafer

Method : Coating, Exposure, Development

Deposited material : Photoresist

Thickness : 300~800 nm

Si Metrology : Spectroscopy Interferometry


SiO2
Si3N4
Resist
Shallow Trench Isolation – RIE Etching 8

Purpose : Form Shallow Trench

Method : RIE

Etched material : SiN/SiO2/Si

Thickness : 700 nm~2 µm

Si Metrology : Stylus Profiler


SiO2
Si3N4
Resist
Shallow Trench Isolation – Resist Stripping 9

Purpose : Strip resist

Method : O2 ashing

Etched material : Photoresist

Thickness : 300 ~ 800 nm

Si Metrology : Surface Particle Inspection System


SiO2
Si3N4
Resist
Shallow Trench Isolation – SiO2 Deposition 10

Purpose : Overfill Trench

Method : TEOS CVD (TEOS is good coverage)

Deposited material : Silicon Dioxide

Thickness : 1.5 ~ 2.5 µm

Si Metrology : Spectroscopic Interferometry


SiO2
Si3N4
Resist
Shallow Trench Isolation – Planarization 11

Purpose : Planarize surface for embedding Silicon


dioxide into STI

Method : Chemical Mechanical Polishing(CMP)


(Colloidal silica, Alumina slurry)

Polished material : Silicon Dioxide

Si Thickness : 500 ~ 700 nm


SiO2
Si3N4
Metrology : In-situ end point detection
Resist
(Reflectivity, Torque)
Shallow Trench Isolation – Remove Stopping layer 12

Purpose : To remove Stopping layer

Method : Wet Etching (Hot Phosphorous acid)

Etched material : Silicon Nitride

Thickness : 20 ~ 50 nm

Si Metrology : Surface analysis (FT-IR, XPS)


SiO2
Si3N4
Resist
Well Channel Formation – N-MOS Well Patterning 13

Purpose : Being able to protect from Ion


implantation

Method : Coating, Exposure, Development

Deposited material : Photoresist

Thickness : 300 ~ 800 nm


Si
SiO2 Metrology : Spectroscopy Interferometry
Si3N4
Resist
Well Channel Formation – N-MOS Well Ion Implantation 14

Purpose : Implant Dopant for forming N-MOS Well

Method : Ion Implantation

Implanted material : Boron

Concentration : 1016 ~ 1017 cm-3

Thickness : Few hundred nm ~ µm


Si
SiO2
Metrology : Secondary Ion Mass Spectroscopy
Si3N4
Resist
(SIMS)
P-Dopant
Well Channel Formation – N-MOS Well Pattern Stripping 15

Purpose : Strip resist

Method : O2 ashing

Etched material : Photoresist

Thickness : 300 ~ 800 nm

Si Metrology : Surface Particle Inspection System


SiO2
Si3N4
Resist

P-Dopant
Well Channel Formation – P-MOS Well Patterning 16

Purpose : Being able to protect from Ion


implantation

Method : Coating, Exposure, Development

Deposited material : Photoresist

Thickness : 300 ~ 800 nm


Si
SiO2 Metrology : Spectroscopy Interferometry
Si3N4
Resist

P-Dopant
Well Channel Formation – P-MOS Well Ion Implantation 17

Purpose : Implant Dopant for forming P-MOS Well

Method : Ion Implantation

Implanted material : Phosphorous

Concentration : 1016 ~ 1017 cm-3

Thickness : Few hundred nm ~ µm


Si
SiO2
Metrology : Secondary Ion Mass Spectroscopy
Si3N4
Resist
(SIMS)
P-Dopant

N-Dopant
Well Channel Formation – P-MOS Well Resist Stripping 18

Purpose : Strip resist

Method : O2 ashing

Etched material : Photoresist

Thickness : 300 ~ 800 nm

Si Metrology : Surface Particle Inspection System


SiO2
Si3N4
Resist

P-Dopant

N-Dopant
Well Channel Formation – Remove Sacrificial layer 19

Purpose : To Remove the sacrificial layer


(Because damaged by ion implantation)

Method : Wet Etching (BHF)

Etched material : Silicon dioxide

Thickness : 10 nm
Si
SiO2 Metrology : Surface analysis (FT-IR, XPS)
Si3N4
Resist

P-Dopant

N-Dopant
Gate Formation – Gate oxidation 20

Purpose : To form Gate oxidation

Method : Thermal oxidation

Deposited material : Silicon dioxide

Thickness : few nm

Si Metrology : Spectroscopic Ellipsometry(On line)


SiO2 X-ray Refractometry (Off line)
Si3N4
Resist

P-Dopant

N-Dopant
Gate Formation – Gate deposition 21

Purpose : To form poly silicon

Method : LP-CVD

Deposited material : Poly-Si, a-Si

Thickness : 5 ~ 30 nm

Si Poly-Si Metrology : Spectroscopic Ellipsometry


SiO2
Si3N4
Resist

P-Dopant

N-Dopant
Gate Formation – Gate patterning 22

Purpose : Gate patterning

Method : Coating, Exposure, Development

Deposited material : Photoresist

Thickness : Few hundred nm

Si Poly-Si Metrology : Spectroscopy Interferometry


SiO2 (Thickness)
Si3N4
CD-SEM (Dimension)
Resist

P-Dopant

N-Dopant
Gate Formation – Gate Etching 23

Purpose : Gate Etching (Isotropic etching )

Method : RIE (Cl base gas)

Etched material : Poly-Si, a-Si

Thickness : Few hundred nm

Si Poly-Si Metrology : Spectroscopy Interferometry


SiO2 (Thickness)
Si3N4
CD-SEM (Dimension)
Resist

P-Dopant

N-Dopant
Gate Formation – Stripping resist 24

Purpose : Strip resist

Method : O2 ashing

Etched material : Photoresist

Thickness : 300 ~ 800 nm

Si Poly-Si Metrology : Surface Particle Inspection System


SiO2
Si3N4
Resist

P-Dopant

N-Dopant
Gate Formation – Re-oxidation 25

Purpose : To reform the sacrificial layer for LDD


implantation.
Because Gate oxide(SiO2) is physically
etched due to isotropic RIE.

Method : Thermal oxidation

Deposited material : Silicon dioxide

Si Poly-Si Thickness : 10 nm
SiO2
Si3N4
Metrology : Spectroscopy Ellipsometry
Resist

P-Dopant

N-Dopant
Lightly Doped Drain (LDD) Formation – NMOS Patterning 26

Purpose : Being able to protect from Ion


implantation

Method : Coating, Exposure, Development

Deposited material : Photoresist

Thickness : 300 ~ 800 nm


Si Poly-Si
SiO2 Metrology : Spectroscopy Interferometry
Si3N4
Resist

P-Dopant

N-Dopant
Lightly Doped Drain (LDD) Formation – LDD implantation 27

Purpose : To form LDD for preventing from hot


carrier effect.

Method : Ion implantation

Implanted material : Phosphorous, Boron

Concentration : 1016 ~ 1017 cm-3


Si Poly-Si
SiO2 Metrology : Secondary Ion Mass Spectroscopy
Si3N4
(SIMS)
Resist

P-Dopant

N-Dopant
※P-MOS LDD is omitted
Lightly Doped Drain (LDD) Formation – Resist strip 28

Purpose : Strip resist

Method : O2 ashing

Etched material : Photoresist

Thickness : 300 ~ 800 nm

Si Poly-Si Metrology : Surface Particle Inspection System


SiO2
Si3N4
Resist

P-Dopant

N-Dopant
Lightly Doped Drain (LDD) Formation – Remove sacrificial layer 29

Purpose : To Remove the sacrificial layer


(Because damaged by ion implantation)

Method : Wet Etching (BHF)

Etched material : Silicon dioxide

Thickness : 10 nm
Si Poly-Si
SiO2 Metrology : Surface analysis (FT-IR, XPS)
Si3N4
Resist

P-Dopant

N-Dopant
Lightly Doped Drain (LDD) Formation –Form sacrificial layer 30

Purpose : To reform the sacrificial layer for LDD


implantation.
Because Gate oxide(SiO2) is physically
etched due to isotropic RIE.

Method : Thermal oxidation

Deposited material : Silicon dioxide

Si Poly-Si Thickness : 10 nm
SiO2
Si3N4
Metrology : Spectroscopy Ellipsometry
Resist

P-Dopant

N-Dopant
Side wall formation– SiN Deposition 31

Purpose : To form sidewall film for determining


the channel length

Method : TEOS CVD ( is better )

Deposited material : Silicon Nitride

Thickness : Few hundred nm

Si Poly-Si Metrology : Spectroscopy interferometry


SiO2
Si3N4
Resist

P-Dopant

N-Dopant
Side wall formation– Anisotropic etching

Purpose : To form sidewall film for determining


the channel length

Method : RIE ( as anisotropic as possible)

Etched material : Silicon Nitride

Thickness : Few hundred nm

Si Poly-Si Metrology : Spectroscopy interferometry


SiO2
Si3N4
Resist

P-Dopant

N-Dopant
Source/ Drain Formation– Patterning 33

Purpose : Being able to protect from Ion


implantation

Method : Coating, Exposure, Development

Deposited material : Photoresist

Thickness : 300 ~ 800 nm


Si Poly-Si
SiO2 Metrology : Spectroscopy Interferometry
Si3N4
Resist

P-Dopant

N-Dopant
Source/ Drain Formation– Ion implantation 34

Purpose : To form LDD for preventing from hot


carrier effect.

Method : Ion implantation

Implanted material : Arsenic, Boron difluoride

Concentration : 1020 cm-3


Si Poly-Si
SiO2 Metrology : Secondary Ion Mass Spectroscopy
Si3N4
(SIMS)
Resist

P-Dopant

N-Dopant
※P-MOS LDD is omitted
Source/ Drain Formation– Resist Strip 35

Purpose : Strip resist

Method : O2 ashing

Etched material : Photoresist

Thickness : 300 ~ 800 nm

Si Poly-Si Metrology : Surface Particle Inspection System


SiO2
Si3N4
Resist

P-Dopant

N-Dopant
Source/ Drain Formation– Annealing 36

Purpose : To recover damage caused by


implantation
To combine dopant and substrate

Method : Furnace annealing


(Vertical furnace annealing)

Temperature : Over 1000℃


Si Poly-Si
SiO2
Si3N4
Resist

P-Dopant

N-Dopant
Source/ Drain Formation– Remove sacrificial layer 37

Purpose : Removal of the sacrificial layer is


required to facilitate the formation of silicide on
the surface

Method : Wet Etching (BHF)

Etched material : Silicon dioxide

Si Poly-Si Thickness : 10 nm
SiO2
Si3N4
Metrology : Surface analysis (FT-IR, XPS)
Resist

P-Dopant

N-Dopant
Silicide Formation – Deposit Silicide Material 38

Purpose : Silicide materials are deposited by


sputtering to react with silicon and form low-
resistance metal silicide contacts during
annealing.

Method : Sputtering

Deposited material : Ti, Co or Ni etc.

Si Poly-Si Thickness : 30 ~ 80 nm
SiO2
Si3N4
Resist
Metrology : Ellipsometry, XRR, XRF
P-Dopant

N-Dopant
Silicide (Before annealing)
Silicide Formation – 1st Annealing 39

Purpose : Initiate the reaction between the


deposited metal and the underlying silicon to form
a preliminary silicide phase
(C49 phase which is high resistivity).

Method : Furnace annealing

Deposited material : Si + Silicide material


(Ti, Co, Ni)
Si Poly-Si
SiO2
Temperature : 600 ~ 700℃
Si3N4
Resist

P-Dopant

N-Dopant
Silicide (Before annealing)
Silicide Formation – Wet Etching 40

Purpose : To eliminate only the non-silicide area

Method : Wet etching (HF + H2O2)

Etched material : Silicide material

Si Poly-Si
SiO2 Silicide
Si3N4
Resist

P-Dopant

N-Dopant
Silicide Formation – 2nd Annealing 41

Purpose : To convert the high-resistance C49


phase into the low-resistance C54 phase.

Method : Furnace annealing

Deposited material : Silicide material

Temperature : 700 ~ 900℃

Si Poly-Si Note: Why this flow?


SiO2 Silicide (1st anneal → Wet etching → 2nd anneal)
Si3N4
Resist
This sequence helps prevent unintended silicide
P-Dopant
formation and reduces the risk of electrical failure.
N-Dopant
Contact Formation – Deposit Inter level dielectric 42

Purpose : Stopping layer for the Contact etching.


Because Source/Drain is different height.

Method :LPCVD, SOG

Deposited material : Silicon Nitride / Silicon Dioxide

Thickness : Few hundred nm


Si Poly-Si
SiO2 Silicide
Si3N4
Resist

P-Dopant

N-Dopant
Contact Formation – Planarization 43

Purpose : Before contact patterning, the surface


must be flat to avoid fluctuations in focus during
lithography.

Method : CMP

Polished material : Silicon Dioxide

Thickness : Few hundred nm


Si Poly-Si
SiO2 Silicide Metrology : Spectroscopy Interferometry
Si3N4
Resist

P-Dopant

N-Dopant
Contact Formation – Adjust the thickness of ILD 44

Purpose : Due to the possibility that the CMP


endpoint detection may not function effectively with
this film configuration, an additional film thickness
will be deposited at this point.

Method : LP CVD

Polished material : Silicon Dioxide

Si Poly-Si Thickness : Few hundred nm


SiO2 Silicide (Depending on the measured data)
Si3N4
Resist

P-Dopant
Metrology : Spectroscopy Interferometry
N-Dopant
Contact Formation – Contact Patterning 45

Purpose : Being able to protect from Ion


implantation

Method : Coating, Exposure, Development

Deposited material : Photoresist

Thickness : Few µm
Si Poly-Si
SiO2 Silicide Metrology : Spectroscopy Interferometry
Si3N4
Resist

P-Dopant

N-Dopant
Contact Formation – Contact Etching 1 46

Purpose : Since there is a step between the


source/drain and the gate, contact etching is
performed down to the SiN stop layer.

Method : RIE (CHF3 Gas)

Etched material : Silicon dioxide

Thickness : Few hundred nm


Si Poly-Si
SiO2 Silicide
Si3N4
Metrology : Stylus profiler
Resist

P-Dopant

N-Dopant
Contact Formation – Contact Etching 2 47

Purpose : Etching until reaching the silicide layer


to complete contact etching

Method : RIE

Etched material : Silicon nitride

Thickness : Few hundred nm

Si Poly-Si
Metrology : Stylus profiler
SiO2 Silicide
Si3N4
Resist

P-Dopant

N-Dopant
Contact Formation – Photoresist Stripping 48

Purpose : Strip resist

Method : O2 ashing

Etched material : Photoresist

Thickness : 300 ~ 800 nm

Si Poly-Si Metrology : Surface Particle Inspection System


SiO2 Silicide
Si3N4
Resist

P-Dopant

N-Dopant
Wire Formation – Barrier layer deposition 49

Purpose : Prevent Tungsten from diffuse with


Silicon. Deposit Barrier layer

Method : CVD ( is better because good coverage)

Deposited material : TiN/Ti

Thickness : Few ten nm


Si Poly-Si
SiO2 Silicide Metrology :
Si3N4 TiN/Ti
Thickness → Spectroscopy Ellipsometry, XRR,XRF
Resist

P-Dopant
Coverage → FIB, SEM, TEM
N-Dopant
Wire Formation – Tungsten layer Deposition 50

Purpose : Deposit Wiring layer

Method : CVD ( is better because good coverage)

Deposited material : Tungsten

Thickness : Few hundred nm ~ few µm

Metrology :
Si Poly-Si Thickness → Spectroscopy Ellipsometry, XRR,XRF
SiO2 Silicide Coverage → FIB, SEM, TEM
Si3N4 TiN/Ti
Resist Tungsten

P-Dopant

N-Dopant
Wire Formation – Planarization 51

Purpose : To embed tungsten into contact hole

Method : CMP (Al2O3, H2O2 slurry)

Planarized material : Tungsten

Thickness : Few hundred nm ~ few µm

Metrology :
Si Poly-Si Thickness → Spectroscopy Ellipsometry, XRR,XRF
SiO2 Silicide Coverage → FIB, SEM, TEM
Si3N4 TiN/Ti
Resist Tungsten

P-Dopant

N-Dopant
Wire Formation – ILD deposition 52

Purpose : To provide insulation between metal


layers

Method : PE-CVD

Planarized material : FSG, SIOC, p-SIOC

Thickness : Few hundred nm ~ few µm

Si Poly-Si Metrology :
SiO2 Silicide Thickness → Spectroscopy Ellipsometry, XRR,XRF
Si3N4 TiN/Ti Density → Spectroscopy Ellipsometry
Resist Tungsten

P-Dopant Low-k
N-Dopant
Wire Formation – ILD patterning 53

Purpose : Being able to protect from Ion


implantation

Method : Coating, Exposure, Development

Deposited material : Photoresist

Thickness : Few µm
Si Poly-Si
SiO2 Silicide Metrology : Spectroscopy Interferometry
Si3N4 TiN/Ti
Resist Tungsten

P-Dopant Low-k
N-Dopant
Wire Formation – Electrode Formation Etching 54

Purpose : To ensure that the semiconductor


operates properly by allowing electrical signals
and power to flow between components.

Method : RIE

Deposited material : FSG, SIOC, p-SIOC

Thickness : Few hundred nm ~ few µm


Si Poly-Si
SiO2 Silicide Metrology : Sylus profiler
Si3N4 TiN/Ti
Resist Tungsten

P-Dopant Low-k
N-Dopant
Wire Formation – Stripping 55

Purpose : Strip resist

Method : O2 ashing

Etched material : Photoresist

Thickness : 300 ~ 800 nm

Si Poly-Si Metrology : Surface Particle Inspection System


SiO2 Silicide
Si3N4 TiN/Ti
Resist Tungsten

P-Dopant Low-k
N-Dopant
Wire Formation – Deposit barrier layer for Via 56

Purpose : Prevent copper from diffuse, erosion.

Method : Sputtering

Deposited material : TiN/Ti/Cu


TiN→ Barrier metal
Ti →Adhesion layer
Cu→ Copper underlayer

Thickness : Few ten nm


Si Poly-Si
SiO2 Silicide Metrology :
Si3N4 TiN/Ti
Resist Tungsten
Coverage → FIB, SEM, TEM
P-Dopant Low-k
N-Dopant Cu
Wire Formation – Copper Electroplating 57

Purpose : Filling copper to form wire

Method : Electroplating (Copper sulfate plating)

Deposited material : Cu

Thickness : Few µm

Metrology :
Si Poly-Si
Thickness → XRF
SiO2 Silicide
Si3N4 TiN/Ti
Resist Tungsten

P-Dopant Low-k
N-Dopant Cu
Wire Formation – Copper Planarization 58

Purpose : To embed copper into contact wire

Method : CMP (Colloidal Silica, H2O2 slurry)

Planarized material : Copper

Thickness : Few µm

Metrology :
Si Poly-Si Thickness → XRF
SiO2 Silicide Coverage → FIB, SEM, TEM
Si3N4 TiN/Ti
Resist Tungsten

P-Dopant Low-k
N-Dopant Cu

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