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Introduction To Basic Lab Instruments and Their Uses

The document provides an introduction to basic laboratory instruments used in physics experiments, detailing their usage, least count, and methods for error analysis and graph plotting. It emphasizes the importance of understanding physical principles, accurate measurements, and the significance of significant figures in reporting experimental results. Additionally, it outlines procedures for preparing experiments, using various instruments like Vernier callipers and screw gauges, and methods for plotting graphs and performing least squares fitting.

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Prince Bharati
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0% found this document useful (0 votes)
37 views9 pages

Introduction To Basic Lab Instruments and Their Uses

The document provides an introduction to basic laboratory instruments used in physics experiments, detailing their usage, least count, and methods for error analysis and graph plotting. It emphasizes the importance of understanding physical principles, accurate measurements, and the significance of significant figures in reporting experimental results. Additionally, it outlines procedures for preparing experiments, using various instruments like Vernier callipers and screw gauges, and methods for plotting graphs and performing least squares fitting.

Uploaded by

Prince Bharati
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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INTRODUCTION TO BASIC LAB INSTRUMENTS: THEIR USAGE,

LEAST COUNT, ERROR ANALYSIS AND GRAPH PLOTTING

“It doesn't matter how beautiful your theory is, it doesn't matter how smart you
are. If it doesn't agree with experiment, it's wrong.”
Richard P. Feynman
Introduction: Conducting experimental work involves far more than just recording a set
of observations. An experimenter must first possess a deep understanding of the physical
principles that form the foundation of the experiment. It is essential to clearly grasp the
aim or objective of the experiment and the methods by which it should be executed.
Furthermore, a solid theoretical background regarding the entity or parameter being
investigated is crucial. Without this knowledge, the experimenter's efforts may yield little
meaningful insight. Therefore, a comprehensive understanding of the underlying physical
principles is the foremost prerequisite for any successful experimental endeavor.

First Step to Physics Laboratory: Physics governs every event around us, making it
essential for students to keenly observe and understand the cause-and-effect
relationships that manifest as phenomena. Each phenomenon in physics is governed by
specific laws, which are verified through experiments. These experiments, using precise
instruments, form the foundation of physics. The success of any experiment depends on
the accuracy and reliability of measurements.

In physics practicals, experiments are designed to achieve specific quantitative results:


determining physical constants like gravity (g), measuring quantities such as the focal
length of a lens, comparing values like the EMFs of two cells, and verifying laws like Ohm’s
law and Newton’s law of cooling.

While these laws and constants have already been accurately established, the purpose of
student laboratory work is to familiarize them with the instruments they study in theory
and to develop the habit of taking careful readings, aiming to achieve results that closely
match standard values with minimal error.

Getting Ready For an Experiment:

1. Study the Theory: Read the experiment's theory multiple times until you fully
understand the procedure and purpose.
2. Visualize Measurements: Clearly picture the measurements and observations,
focusing on those that require extra precision.
3. Gather Apparatus: List and collect all necessary equipment before starting.
4. Prepare Observation Tables: Create a table to record observations in sequence
to avoid missing data.
5. Check Instruments: Verify the accuracy and constants of tools like screw gauges,
callipers, and spherometers.
6. Test Time Devices: Ensure stopwatches or clocks are accurate and thermometers
are unbroken.
7. Inspect Optical Instruments: Confirm telescopes and microscopes have clear
cross-wires and are properly focused.
8. Examine Electrical Instruments: Ensure batteries are charged, and
galvanometers, ammeters, and voltmeters are correctly calibrated.
9. Check Electrical Connections: Ensure wires are tightly stretched, clean, and
properly soldered.
10. Sketch Circuit Diagrams: Draw and get circuit diagrams checked by a teacher
before making connections.
11. Draw Graphs: Use large graphs with suitable scales, and express results in proper
units with justified significant figures.
12. Use Accurate Methods: Prefer methods that balance two effects for greater
accuracy.
13. Comprehensive Observations: Make observations over a wide range, and
extrapolate graphs with broken lines if needed.

• BASIC INSTRUMENTS AND THEIR USES, LEAST COUNT.


In our physics laboratory we use some basic instruments to measure
fundamentals quantities like length, mass, time, temperature etc. It is very much
important to us to know up to what accuracy the instruments can measure a
quantity. The minimum value that an instrument can measure is known as the
least count of the instrument.
In our laboratory we use instruments like meter scale, Vernier Callipers, Screw
Gauge, Spherometer, Thermometer, Ammeter and Voltmeter etc.

In order to measure radius, thickness and curvature very accurately , we use


Vernier calliper, screw gauge and spherometer respectively.

1. VERNIER CALLIPERS:
To measure length, breadth, thickness, inner or outer radius we can use Vernier
callipers.

The main scale is divided into millimetres. The Vernier scale has 10 divisions on it
which together are equal to 9 scale divisions i.e. to 9 mm. The difference between
one scale division and one Vernier division is called the Vernier constant of the
instrument.
Now, 10 vernier division (V.D) = 9 main scale division (S.D)
𝟗 𝟗
∴ 𝟏 𝐕. 𝐃 = S.D = 𝟏𝟎 𝒎𝒎 = 𝟎. 𝟗 𝒎𝒎
𝟏𝟎
𝑆𝑜, 𝑣𝑒𝑟𝑛𝑖𝑒𝑟𝑐𝑜𝑛𝑠𝑡𝑎𝑛𝑡 𝑜𝑟 𝑙𝑒𝑎𝑠𝑡𝑐𝑜𝑢𝑛𝑡 = (1𝑆. 𝐷 − 1𝑉. 𝐷) = (1 - 0.9) 𝑚𝑚 =
0.1 𝑚𝑚 = 0.01 𝑐𝑚
So, the least count or Vernier constant of the Vernier Callipers is 0.01 cm.

This can also be alternatively calculated as :


𝑽𝒂𝒍𝒖𝒆 𝒐𝒇 𝟏 𝒎𝒂𝒊𝒏 𝒔𝒄𝒂𝒍𝒆 𝒅𝒊𝒗𝒊𝒔𝒊𝒐𝒏 𝟏 𝒎𝒎
Least Count (LC) = = = 𝟎. 𝟏 𝒎𝒎 = 𝟎. 𝟎𝟏 𝒄𝒎
𝑻𝒐𝒕𝒂𝒍 𝒏𝒖𝒎𝒃𝒆𝒓 𝒐𝒇 𝒅𝒊𝒗𝒊𝒔𝒊𝒐𝒏𝒔 𝒐𝒏 𝒗𝒆𝒓𝒏𝒊𝒆𝒓 𝒔𝒄𝒂𝒍𝒆 𝟏𝟎

How to read Vernier:

The main scale reading in a Vernier callipers: The first division of Vernier will
cross certain value in main scale. Then the value in the main scale shows the main
scale reading.
Vernier scale Reading: The div in the Vernier scale which exactly coincides with
one of the main scale division is the Vernier scale reading.
Total Reading: If the main scale reading in slide calliper is M and Vernier scale
reading (V.S.R) is X, then your total reading is T= M+(V.S.R)*LC (write in cm).

Below are some examples:

2. SCREW GAUGE:
It is a device for measuring with considerable accuracy, the diameters of wires. It
consists essentially of a screw, with a uniform pitch, which moves in a nut. The
wire is held between the jaws A and B which should then be pressed just tight. The
screw gauge is provided with two scales a linear scale called as pitch scale usually
graduated in millimetres and a circular scale

divided into 100 equal parts. When the s––crew is given one complete rotation, it
advances or recedes by one millimetre. This distance is called the pitch of the
screw.

𝒑𝒊𝒕𝒄𝒉 𝟏 𝒎𝒎
∴ Least Count of the screw gauge = = = 𝟎. 𝟎𝟏 𝒎𝒎.
𝑻𝒐𝒕𝒂𝒍 𝒏𝒖𝒎𝒃𝒆𝒓 𝒐𝒇 𝒅𝒊𝒗𝒊𝒔𝒊𝒐𝒏𝒔 𝒐𝒏 𝒄𝒊𝒓𝒄𝒖𝒍𝒂𝒓 𝒔𝒄𝒂𝒍𝒆 𝟏𝟎𝟎

It means that the instrument can measure up to 0.01 mm. The accuracy of a screw
gauge is more than that of a Vernier callipers.

Note: The crew must always be turned either forwards only (or backwards only) to
avoid the back-lash error, which is produced by the slipping of the screw in the nut.

3. SPHEROMETER:

It is a device for measuring the thicknesses of thin plates and the radii of curvature
of spherical surfaces. In our lab we various types of spherometers with which we
can measure the bending of a beam in Young’s modulus experiment or we can also
measure the elongation of a wire in case of Searle’s Apparatus. It carries a small
vertical scale usually divided into millimetres. A screw, whose pitch is usually one
mm and which carries a circular disc (having a circular scale divided into 100
equal parts, engraved on it) at its top.

The least count of this instrument can be calculated in same ways as that of a screw
gauge.

∴ Least Count of the spherometer:


𝑝𝑖𝑡𝑐ℎ
= 𝑇𝑜𝑡𝑎𝑙 𝑛𝑢𝑚𝑏𝑒𝑟 𝑜𝑓 𝑑𝑖𝑣𝑖𝑠𝑖𝑜𝑛𝑠 𝑜𝑛 𝑐𝑖𝑟𝑐𝑢𝑙𝑎𝑟 𝑠𝑐𝑎𝑙𝑒
1 𝑚𝑚
=
100
= 0.01 𝑚𝑚.
Below are the different types of spherometers

Fig. 2: Spherometer used in Searle’s Apparatus

Fig. 3 Spherometer attached to a travelling microscope


4. STOP WATCH
In our lab we use stop watch, which can measure time in steps of 0.01 seconds. So, the
least count of the stop watch is 0.01 sec.

Stop watch 1: reading is 1 min 15.21 (60+15.21) 𝑠 = 75.21 𝑠.


While in stop watch 2: the reading is 14.31= (14+31× 0.01) 𝑠 = 14.31 s

❖ Apart from these we use thermometer, Ammeter, Voltmeter whose least count is easily
found by looking at the instrument. Just see the smallest div in the scale of the
instruments.

Introduction to error analysis:


2.1. INTRODUCTION

When students report their final results, there's often a misconception that these results
must perfectly match the standard value. This can sometimes lead to unhealthy practices
aimed at achieving artificially accurate results. However, it's crucial for students to
understand that exact matches with standard values are often a matter of chance.
Deviations from the standard value should not be discouraging. The key is to conduct the
experiment with care, sincerity, and honesty in collecting data.

The result should be (i) presented with the correct numerical figures and units, and (ii)
reflect the reliability of the findings. The accuracy of the result is conveyed through
'Significant Figures,' while the reliability is indicated by accounting for 'Experimental
Errors.' Finally, we will explore the use of different types of graph papers, such as linear,
semi-log, and log-log, and their specific applications.

2.2. SIGNIFICANT FIGURES

The number of significant figures in the final result of an experiment depends on the
precision of the measurements made during the experiment.

2.3. PERCENTAGE ERROR IN EXPERIMENTS

In experiments, we measure physical quantities using tools like vernier callipers, screw
gauges, spherometers, stopwatches, thermometers, and balances. The errors in these
measurements, denoted by ΔL, Δr, ΔT, ΔQ, etc., are typically taken as the least count of the
instrument used. Examples include:

1. Length Measurement: When measuring length with a meter rod, the error ΔL is
1 mm (0.1 cm), which is the smallest graduation on the scale.
2. Diameter/Length with Callipers: The error ΔL is 0.1 mm (0.01 cm), the least
count of the callipers.
3. Diameter/Thickness with Screw Gauge: The error ΔL is 0.01 mm (0.001 cm),
corresponding to the least count of the screw gauge.
4. Mass Measurement: Using a good balance, the error Δm in mass is typically 5 mg
or 10 mg (0.005 g or 0.01 g), depending on the balance's accuracy. For larger
masses, like in Searle's apparatus or a sonometer, the error Δm can be around 10
grams or more.
5. Time Measurement: With a stopwatch (that can measure milli-second)
graduated to 0.001 seconds, the error Δt is 0.001 seconds, respectively. For a stop
clock graduated in seconds, where each second is divided into three ticks, the
error Δt is approximately 0.33 seconds.
6. Temperature Measurement: Using thermometers graduated in half or one-tenth
degrees, the error Δθ is 0.5°C or 0.1°C, respectively, reflecting the smallest
graduation on the thermometer.

Example of percentage calculation:

❖ Note on Plotting Graphs

Plotting a graph involves several key steps:

1. Define the Function: Determine the mathematical function or data you want to
plot.
2. Choose the Range: Decide the range of values for the x-axis and y-axis.
3. Set Up the Plot: Create a coordinate system, plot the points or function, and
label the axes.
4. Customize the Plot: Add titles, legends, and adjust styles to make the graph
clear and informative.

Example: Plotting a Simple Function

The independent variables should be plotted along X-axis and the dependent
variable should be plotted along Y-axis.

Note on Least Squares Fitting

Least Squares Fitting is a statistical method used to find the best-fitting curve or line
through a set of data points. The goal is to minimize the sum of the squared differences
(errors) between the observed values and the values predicted by the model.

Steps for Least Squares Fitting:

1. Define the Model: Choose the type of model (e.g., linear, quadratic) that you
believe fits the data.
2. Formulate the Objective Function: The objective is to minimize the sum of the
squared residuals (errors):
3. Solve for Parameters: Use optimization techniques to find the model parameters
that minimize the objective function.
4. Plot the Data and Fit: Visualize the data points and the fitted curve or line to
evaluate the fitting.
Let's fit a linear model 𝑦 = 𝑚𝑥 + 𝑐 (equation of straight line) to a set of data points using
least squares fitting. Below is an

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