NEW Course Structure: B. Tech.

(Chemical Engineering)
SEMESTER-I
S. No. Course Code Subject L T P Cr
1 PH-11101 Physics-I 3 1 0 4
2 HS-11101/ English Language and Composition/ 2 1 0 3
CS-11101 Computer Programming
3 CY-11101/AM- Chemistry/Engineering Mechanics 3 1 0 4
11101
4 MA-11101 Mathematics-I 3 1 0 4
5 ME- Engineering Graphics/Workshop 1 0 3 3
11101/11102
6 HS-11102/PH- Communication Skill Workshop 0 0 3 2
11201 Physics (Lab)
7 CY-11201/AM- Chemistry (Lab)/Engineering 0 0 3 2
11201 Mechanics (Lab)
8 HS-11201/CS- Language Lab/Computer 0 0 3 2
11201 Programming (Lab)
Total Credit 24
SEMESTER-II
S. No. Course Code Subject L T P Cr
1 PH-12102 Physics-II 3 1 0 4
2 HS-12101/CS- English Language and Composition/ 2 1 0 3
12101 Computer Programming
3 CY-12101/AM- Chemistry/Engineering Mechanics 3 1 0 4
12101
4 MA-12101 Mathematics-II 3 1 0 4
5 ME- Engineering Graphics/Workshop 1 0 3 3
12101/12102
6 CE-12101 Environment & Ecology 2 0 0 2
7 HS-12102/PH- Communication Skill 0 0 3 2
12201 Workshop/Physics (Lab)
8 CY-12201/AM- Chemistry (Lab)/Engineering 0 0 3 2
12201 Mechanics (Lab)
9 HS-12201/CS- Language Lab/Computer 0 0 3 2
12201 Programming (Lab)
Total Credit - - - 26
SEMESTER-III
S. No. Course Code Subject L T P Cr
1 CH-13101 Chemical Process Principles 3 1 4
2 CH-13102 Process Instrumentation 3 3
3 AM-13103 Material Science and Engineering 3 3
4 EE-13111 Basic Electrical and Electronics 3 3
5 MA-13104 Numerical Methods and Statistical 2 1 3
Techniques
6 AM-13107 Fluid Flow Operations and Hydraulic 3 1 4
Machines
7 ME- 13201 Computational Lab 3 2
8 AM-13203 Material Science Lab 3 2
9 AM-13207 Fluid Flow Operations Lab 3 2
Total Credit 26
SEMESTER-IV
S. No. Course Code Subject L T P Cr
1 CH-14101 Fluid Particle Mechanics and 3 1 4
Mechanical Operations
2 CH-14102 Heat Transfer Operations 3 1 4
3 CH-14103 Mass Transfer-I 3 1 4
4 CH-14104 Chemical Engineering 3 1 4
Thermodynamics-I
5 CY-14101 Organic and Physical Chemistry 2 1 3
 6 CH-14251 Heat Transfer Lab 3 2
7 CH-14252 Fluid Particle Mechanics and 3 2
Mechanical Operations Lab
8 CY-14251 Organic and Physical Chemistry Lab 3 2
Total Credit 25
SEMESTER-V
S. No. Course Code Subject L T P Cr
1 CH-15101 Chemical Reaction Engineering-I 3 1 4
2 CH-15102 Mass Transfer-II 3 1 4
3 CH-15103 Process Dynamics and Control 3 1 4
4 CH-15104 Chemical Engineering 3 1 4
Thermodynamics-II
5 HS-15101 Principles of Management 3 3
6 CH-15251 Mass Transfer Lab 3 2
7 CH-15252 Process Dynamics and Control Lab 3 2
8 CH-15253 Process Simulation Lab 3 2
Total Credit 25
SEMESTER-VI
S. No. Course Code Subject L T P Cr
1 CH-16101 Chemical Reaction Engineering-II 3 1 4
2 CH-16102 Transport Phenomena 3 1 4
3 CH-16103 Environmental Pollution, Monitoring 3 1 4
and Control
4 CH-16104 Process Equipment Design 3 1 4
5 CH-16105 Chemical Technology 3 1 4
6 HS-16101 Communication Skills Workshop 2 0
7 CH-16251 Chemical Technology Lab 3 2
8 CH-16252 Chemical Reaction Engineering Lab 3 2
9 CH-16253 Environmental Engineering Lab 3 2
Total Credit 26
SEMESTER-VII
S. No. Course Code Subject L T P Cr
1 CH-17101 Petroleum Refining and 3 1 4
Petrochemicals
2 CH-17102 Optimization of Chemical Processes 3 1 4
3 OE-17501 Open Elective-I 3 3
4 CH-17331-CH- Professional Elective – I 3 1 4
17340
5 CH-17341-CH- Professional Elective – II 3 1 4
17350
6 CH-17691 Major Project – I 12 6
Total Credit 25
SEMESTER-VIII
S. No. Course Code Subject L T P Cr
1 CH-18101 Hazards and Safety in Chemical 3 1 4
Industries
2 CH-18102 Plant Design and Economics 3 1 4
3 OE-18501 Open Elective-II 3 3
4 CH-18331-CH- Professional Elective – III 3 1 4
18340
5 CH-18341-CH- Professional Elective – IV 3 1 4
18350
6 CH-18691 Major Project – II 12 6
Total Credit 25

Total Credits = 24 (I) + 26 (II) + 26 (III) + 25 (IV) + 25 (V) + 26 (VI) + 25 (VII) + 25 (VIII) = 202
 LIST OF PROFESSIONAL ELECTIVES FOR UG COURSE
STRUCTURE

A) Professional Electives- I & II

S. No. Subject Proposed Subject Name

Code Course Code

1. CH-1731 CH-17331 INTRODUCTION TO BIOCHEMICAL ENGINEERING

2. CH-1732 CH-17332 ALTERNATE ENERGY SOURCES
3. CH -1733 CH -17333 POLYMER SCIENCE AND TECHNOLOGY
4. CH -1734 CH -17334 FOOD TECHNOLOGY AND ENGINEERING
5. CH -1735 CH -17335 FERTILIZER TECHNOLOGY
6. CH -1736 CH -17336 TWO PHASE FLOW AND HEAT TRANSFER
7. CH -1737 CH -1737 ADVANCED PROCESS CONTROL
8. CH -1738 CH -17338 MATHEMATICAL METHODS IN CHEMICAL ENGINEERING
9. CH -1739 CH -17339 INTERFACIAL SCIENCE AND ENGINEERING
10. CH -1740 CH -17340 BIOENERGY ENGINEERING
11. CH -1741 CH -17341 ELECTROCHEMICAL ENGINEERING
12. CH -1742 CH -17342 INDUSTRIAL CATALYSIS

B) Professional Electives- III & IV

S. No. Subject Proposed Subject Name

Code Course Code
1. CH -1831 CH -18331 INTRODUCTION TO NANOTECHNOLOGY
2. CH -1832 CH -18332 INTRODUCTION TO PROCESS INTENSIFICATION
3. CH -1833 CH -18333 ADVANCED SEPARATION PROCESSES
4. CH -1834 CH -18334 PROCESS MODELING AND SIMULATION
5. CH -1835 CH -18335 INTRODUCTION TO MULTIPHASE FLOW
6. CH -1836 CH -18336 ENERGY ENGINEERING
7. CH -1837 CH -18337 SCALE-UP IN PROCESS INDUSTRIES
8. CH -1838 CH -18338 SOLID WASTE MANAGEMENT
9. CH -1839 CH -18339 INDUSTRIAL CORROSION AND SURFACE COATING
10. CH -1840 CH -18340 INDUSTRIAL ENZYME ENGINEERING AND
FERMENTATION TECHNIQUES
11. CH -1841 CH -18341 ADVANCES IN FLUIDIZATION ENGINEERING
12. CH -1842 CH -18342 UPSTREAM HYDROCARBON ENGINEERING

Note:
VII Semester VIII Semester
 Section - 1
DETAILED SYLLABUS OF
COURSES
 3rd Semester Syllabus
CH-13101: CHEMICAL PROCESS PRINCIPLES

L: T: P: Cr = 3:1:0:4

Objectives: To impart fundamental knowledge about various unit systems for chemical
process calculations and to give insight of material and energy balances in
various unit operations and processes.

LESSON PLAN
UNIT 1 [7L]
Introduction to various system of units and dimensions, basic quantities and units, derived
quantities and units, stoichiometric principles, composition relations, density and specific
gravity.
UNIT 2 [7L]
Behaviors of Ideal gases, kinetic theory of gases, application of ideal gas law, gaseous
mixtures, volume changes with change in composition, vapor pressure, effect of
temperature on vapor pressure, vapor pressure plots, vapor pressure of immiscible liquids
solutions.
UNIT 3 [8L]
Humidity, saturation, vaporization, condensation, wet and dry bulb thermometry, solubility,
crystallization and dissolution, solubility of gases.
UNIT 4 [9L]
Material Balance in unit operations, material balance without chemical reaction, material
balance involving chemical reaction, combustion of solids, liquids, and gaseous fuels,
recycling operations, bypassing operations, purging operations.
UNIT 5 [9L]
Thermophysics, components of energy balance equations, heat capacity of gases, liquids,
and solids, estimation of heat of fusion, heat of vaporization, thermo chemistry, Hess's law
of constant heat summation, heat of reaction, effect of temperature on standard heat of
reaction, calculation of theoretical flame temperature and actual flame temperature.
Text Books and References: 1. O.A.Hougen, K.M. Watson, R.A. Ragatz, "Chemical Process
Principles", Vol. I, CBS Publishers and Distributors, 1995.
2. K.V. Narayanan, B. Lakshmikutty, “Stoichiometry and Process
Calculations”, PHI Learning Pvt. Ltd., 2006.
3. D.M. Himmelblau, J.B. Riggs, '"Basic Principles and
Calculations in Chemical Engineering", PHI Learning Pvt.
Ltd., 2014.
4. B.I. Bhatt, S.M.Vora, "Stoichiometry", Tata McGraw Hill
Publishers Ltd., 1996.
5. V.Venkataramani, N.Anantharaman, "Process Calculations",
PHI Learning Pvt. Ltd., 2011.
 CH-13102: PROCESS INSTRUMENTATION

L: T: P: Cr = 3:0:0:3

Objectives: To impart knowledge of basic process instrumentations used in the chemical

industries along with performance characteristics of measuring instruments
andanalysis of experimental data.

LESSON PLAN

UNIT 1 Introduction to Instruments and Their Representation: [4 L]

Application of instrument systems, functional elements of a measurement system,

classification of instruments, standards and calibration.

UNIT 2 Temperature Measurements: [4 L]

Temperature Scales, temperature measuring instruments: liquid in glass thermometer,

bimetallic thermometer, resistance temperature detectors (RTD), thermocouples,
pyrometry.

UNIT 3 Pressure Measurements: [4 L]

Measurement of moderate pressure, high pressure and low pressure (vacuum), calibration
and standardization.

UNIT 4 Flow Measurements: [5 L]

Positive displacement meters, variable head meters, variable area meters (rotameters),
weirs and notches, pitot tube, electromagnetic flow meter, hot wire anemometer, ultrasonic
flow meters, laser Doppler anemometer.

UNIT 5 Miscellaneous Measurements: [8 L]

Liquid level, pH, viscosity, conductivity, humidity, gas composition, and nuclear radiation.
Static and Dynamic characteristics of measuring instruments, Analysis of experimental data

Text Books and References: 1. D. P. Eckman, “Industrial Instrumentation” CBS New Delhi,
2004.
2. J.P. Holman, “Experimental methods for Engineers” 7th ed.
Tata McGraw Hill, New Delhi, 2007.
3. B.C. Nakra, K.K.Chaudhry, “Instrumentation, Measurement
and Analysis” 2nded., Tata McGraw Hill, New Delhi, 2004.
4. Patranabis, D., “Principles of Industrial Instrumentation” Tata
McGraw Hill, New Delhi, 1999.
5. Doebelin, E., “Measurement Systems: Applications and
Design” 4thed., McGrawHill, 1990.

1.
 AM-13103: MATERIAL SCIENCE AND ENGINEERING

L: T: P: Cr = 3:1:0:4

Objectives: At the end of the course the student will have an understanding of science and
engineering aspect of materials. The major focus shall be on the structure,
properties, processing, and application of common as well as advanced
engineering materials.
Prerequisite: The prerequisite for the course includes a sound knowledge in atomic structure,
atomic bonding in solids, crystal structures, crystalline and noncrystalline
materials, polymers, and some common properties of materials. (A quiz may be
conducted by course co-coordinator (class teacher) within 15 days to check
prerequisite knowledge acquired by students.)

LESSON PLAN

UNIT 1: Introduction 3L

Historical perspective of Materials Science, Structure and properties relationship of

Engineering Materials, Classification of materials, Advanced Materials.
UNIT 2: Structure of Solids and Characterization of Materials 6L

Introduction to crystal structures and systems, Metallic structures, Ceramic crystal

structures, Carbon nano-structures, Crystallographic directions and planes, Miller
indices, Density computations, Crystallography, Diffraction methods, Electron
microscopy, Metallography, Thermal characterization techniques.
UNIT 3: Imperfections in Solids 4L

Point defects, Dislocations, Interfacial Defects, Bulk defects.

UNIT 4: Diffusion 4L

Diffusion mechanisms, steady and non-steady state diffusion, Factors that influence
diffusion, Law’s of diffusion, Applications of Diffusion.

UNIT 5: Mechanical Behaviour of Materials 6L

Elastic and plastic properties, Creep, Fatigue, Fracture, Heat treatment of steels.
UNIT 6: Phase Diagrams and Phase Transformations 6L

Unary, Binary, Equilibrium phase diagrams, Eutectic, Eutectoid, Peritectic and

peritectoidreactions,Transformation rate effects and TTT diagrams.Microstructure and
property changes in iron-carbon system, Iron-Carbon (Fe-C or Fe-Fe3C) Diagram.
UNIT 7: Ceramic Materials 2L

Ceramic types, Properties, ProcessingApplication, Advanced ceramics.

UNIT 8: Composites 2L

Introduction, Applications, Particle reinforced composites; Fiber reinforced composites,

Structural composites.
UNIT 9: Thermal, Electrical, Magnetic, Optical Properties 5L

Heat capacity, Thermal expansion, Thermal conductivity, Thermal stresses, Electrical

conduction, Semi conductivity, Super conductivity, Electrical conduction in ionic ceramics
and in polymers, Dielectric behavior, Ferroelectricity, Piezoelectricity, Diamagnetism and
paramagnetism, Ferromagnetism, Antiferromagnetism and ferrimagnetism, Influence of
temperature on magnetic behavior, Domains and hysteresis, Optical properties of metals,
Optical properties of nonmetals, Application of optical phenomena.
UNIT 10: Economic, Environmental and Social Issues of Material Usage 2L

Economic considerations, Environmental and societal considerations, Recycling issues, Life

cycle analysis and its use in design.

Text Books and References: 1. Callister W. D. Jr., Materials Science and Engineering An
Introduction.
2. Van Vlack, Material Science.
3. Raghavan V, Material Science.
4. K. M. Gupta, Material Science and Engineering
 EE-1305: BASIC ELECTRICAL AND ELECTRONICS

L: T: P: Cr = 3:0:0:3

LESSON PLAN

UNIT 1: INTRODUCTION TO ELECTRICAL ENERGY

Generation: Types of power Plant, Functional Block diagram of generating stations
(Hydel& Thermal Stations); Transmission,DistributionandUtilization,Domestic
Wiring: Materials, accessories & ratings of the wiring materials, types of wiring,
earthing and electricity rules.
Electric Circuits:
Basic Circuit Elements, Ohm’s law, KCL & KVL, Node & Loop Analysis,
Superposition, Thevenin’s Theorem & Norton’s Theorem, Maximum Power
Transfer Theorem.
Steady-state analysis of AC circuits:
Sinusoidal and phasor representation of Voltage & current, single phase ac circuit
behavior of R, L and C. Combination of R, L and C in series and parallel,
Resonance. Three-phase circuits.
Transformer& Rotating Machines: Principle of operation and construction of
single-phase transformer, efficiency and voltage regulation. Principle of
electromagnetic energy conversion, Starting and speed control of DC and AC motors

UNIT 2: ELECTRONICS ENGINEERING

Semiconductor Devices: Junction Diode, Bipolar -junction Transistor, JFET and

MOSFET, Linear IC and its applications

Digital circuits: Number systems, conversion of bases, Boolean Algebra, logic

gates, Concept of universal gate, Flip-Flops and counter.

UNIT 3: MEASUREMENT AND MECHATRONICS INSTRUMENTATION

Measuring Instruments: Types of instruments, working principles of Ammeter,

Voltmeter, Wattmeter & Energy meter, Digital instruments, Oscilloscopes.

Transducers and Sensors: for measurement of displacement, velocity, acceleration,

force, torque, liquid level, flow, temperature etc.

Signal Conditioning: Operational Amplifiers and Circuits, Instrumentation

amplifiers, Voltage to Current converters and Current boosters, Logarithmic
amplifiers filters.

Timing Circuits: VCO, Waveform Generator, 555 timer circuits

Converters: Analog to Digital and Digital to Analog Conversion, Sample and Hold
circuits, Analog, multiplexers, de-multiplexers
 Power Control: SCRs, Triacs and other solid state devices various power converters
and power control

Actuators and Motors: Actuators, BrushedDC servo motors, Brushless PM motors

and controllers, The AC induction motor as a servo drive, stepper motor.

Controllers for automation: Introduction to microprocessors, Automation of

systems using microcontrollers.

Text books and References:

1. V. Del Toro: Principle of Electrical Engineering, PHI

2. W. H. Hayt&Kemmerley, Engineering Circuit Analysis, McGraw Hill.
3. Millman&Halkias, Integrated Electronics, TMH
4. Boylstad&Nashishky, Electronic Devices & circuits, PHI
5. Mavino& Leach, Digital Principles and applications.
6. W.D. Cooper Electronic Instrumentation & Measurement Techniques,
PHI
7. D.V.S. Murthy, Transducer and Instrumentation,
8. Richard M. Crowder, Electric Drives and their Controls
9. Douglas V. Hall, Microprocessors and interfacing programming and
Hardware
10. Scot Mackenzie ,The 8051 Microcontrollers
 MA-1304: NUMERICAL METHODS AND STATISTICAL TECHNIQUES

L: T: P: Cr = 2:1:0:3

Objectives: Objective of this course is to make students proficient in some numerical and
statistical methods to solve certain types of problems and also to determine the
maximum possible error in the numerical solution.
Prerequisites: This course is one of the basic courses of mathematics for engineering students.
There are many problems in science and engineering which cannot be solved exactly.
Even when a method exists to solve a problem, it may be too complicated to use the
method or in most cases, we may have to add an infinite number of terms. In such
situations, we use numerical methods. Many non-linear and complex physical
problems can be solved through numerical methods.

LESSON PLAN
UNIT-1 Errors in numerical computation, Algebraic and Transcendental Equations: 8L

Errors in numerical computation and their analysis, Bisection method, Iteration method,
Newton-Raphson Method, Method of False Position, rate of convergence, Method for
complex root, Muller’s Method, Quotient Difference method,.

UNIT-2Interpolation: 9L

Introduction, Errors in Polynomial interpolation, Finite differences, Decision of errors,

Newton’s formula for interpolation, Gauss, Sterling, Bessel’s, Everett’s Formula, Interpolation
by unevenly spaced points, Lagrange interpolation formula, Divided Difference, Newton’s
General interpolation Formula.

UNIT-3 Curve Fitting, Cubic Spline & Approximation: 7L

Introduction, Method of Least Square curve fitting procedures, Fitting a straight line, Curve
fitting by sum of exponential, Data fitting with cubic splines, Approximation of functions.

UNIT-4 Numerical Integration and Differentiation: 5L

Introduction, Numerical differentiation, Picard Iteration Method of Solution, Numerical

integration, Trapezoidal rule, Simpson 1/3 rule, Simpson 3/8 rule, Booles&Weddles rule,
Euler- Maclariaun formula, Gaussian Formula, Numerical evaluation of singular integrals.

UNIT-5 Numerical Linear Algebra: 6L

Numerical techniques for finding solution of system of linear equations and eigen values:
Gauss Jordan, Gauss Seidel methods, Power method for estimating eigen values: LU and LL *
factorization of matrices.

UNIT –6 Statistical Computations: 7L

Discrete and continuous distribution, of function, Poisson and Normal Distribution, Mean
&Variance, Moment Generation Function, linear statistical model, theory of least squares and
analysis of variance, least squares estimates, and their precision. Test of significance and
interval estimates based on least squares theory in one way, two way and three way classified
data, Regression Analysis, Least Square fit, Polynomial fit, Linear and Nonlinear Regression,
 orthogonal polynomials, discriminate analysis.

Text Books and References: 1. C.F.Gerald and P.O.Wheatley, Applied Numerical Analysis,
Pearson Education

2. M.K.Jain, S.R.K.Iyenger and R.K.Jain, Numerical Methods for

Scientific andEngineering Computation, Wiley Eastern Ltd.

3. S.S Sastry, Introductory Methods of Numerical Analysis, Prentice

Hall

4. S.Rajasekharan, Numerical Methods for Science and Engineering,

S.Chand.

5. James I. Buchman and Peter R.Turner, Numerical Methods and

Analysis, McGraw-Hills Inc

2.
 AM-13107: FLUID FLOW OPERATIONS AND HYDRAULIC MACHINES

L: T: P: Cr = 3:1:0:4

LESSON PLAN

UNIT-1: Introduction to Fluid Mechanics- Statics and Kinematics 8 L

Fluid and continuum, Physical properties of fluids, Types of fluid flows, Rheology
of fluids.
Manometers, pressure transducers, pressure on plane and curved surfaces, centre of
pressure, fluid masses subjected to linear acceleration and uniform rotation about an
axis. Kinematics of Fluid flow: steadiness, uniformity, rotational and irrotational
flows, streamline, streakline, pathline, continuity equation, stream function and
velocity potential, applications of potential flow.

UNIT-2: Dynamics of Fluid Flow and Dimensional Analysis 8 L

Euler’s Equation of motion along a streamline and its integration, Bernoulli’s

equation and its applications, momentum equation and its application to pipe bends.
Flow measurement by Pitot tube, orifice, Venturi, nozzle, and bend meter, rotameter.
Dimensional Analysis, Buckingham’s Pi theorem, important dimensionless numbers
and their physical significance, geometric, kinematic and dynamic similarity, model
studies, Hydraulic similitude.

UNIT-3: Laminar and Turbulent Flows 8 L

Equation of motion for laminar flow through pipes, Stokes law, transition from
laminar to turbulent flow, types of turbulent flow, isotropic and homogenous
turbulence, scale and intensity of turbulence, eddy viscosity, Prandtl’s mixing length
theory, velocity distribution in turbulent flow over smooth and rough surfaces,
resistance to flow, minor losses, pipe in series and parallel, power transmission
through a pipe, three reservoir problems and pipe network.

UNIT-4: Hydrodynamic Boundary Layer 8 L

Introduction with a historical background, boundary layer, displacement and

momentum thickness, boundary layer over a flat plate, Prandtl boundary layer
equation, laminar boundary layer, application of momentum equation, turbulent
boundary layer, laminar sub-layer, separation and its control, drag and lift, drag on a
sphere, 2D cylinder and airfoil, Magnus effect.

UNIT-5: Introduction to Compressible Flow 3 L

Thermodynamic processes, continuity equation, work done in an isothermal process

and adiabatic process, sonic velocity, Mach number, Mach line, Mach angle and
Mach cone, properties a stagnation point, flow through a convergent-divergent
nozzle and De Laval nozzle, Normal and oblique shocks, Rayleigh and Fanno flows.
UNIT-6: Introduction to Pumps & Compressors 5 L

Pumps: Classifications & applications, losses and efficiencies, work and power
input, cavitations and maximum suction lift, specific ad minimum speed,
comparison between centrifugal and reciprocating pumps, multistage pumps, pumps
in series and parallel. Compressors: Introduction to Hydroelectric power station and
its components, Classification of turbines and pumps, similarity laws and specific
speed, efficiency, cavitations.

Text Books and References:

1. Fox, R.W., McDonald, A.T., Introduction to Fluid Mechanics, 7th edition, Wiley India.
2. Ojha, C.S.P., Berndtsson, R., Chandramouli, P.N., Fluid Mechanics and Machinery,
OxfordUniversity Press, New Delhi.
3. Majumdar, B., Fluid Mechanics with Laboratory Manual, PHI Learning, New Delhi.
4. Som, S.K. and Biswas G, Introduction of Fluid Mechanics & Fluid Machines, TMH,
New Delhi.
5. Mohanty, A.K., Fluid Mechanics, PHI Learning, New Delhi.
6. Shames, I.H., Mechanics of Fluids, McGraw Hill, International Students Edition.
7. Agarwal, S.K., Fluid Mechanics and Machinery, TMH, New Delhi.
8. Rathakrishnan E., Instrumentation, Measurements and Experiments in Fluids, CRC
Press, New York.
9. Garde, R.J., Fluid Mechanics through Problems, New Age International Pvt. Ltd, New
Delhi.
10. Lal, J., Hydraulic Machines, Metropolitan Book Co. Pvt. Ltd., Delhi.
11. Yahya, S.M., Fans, Blowers & Compressors, New Age International Pvt. Ltd., New
Delhi.
 ME-1351 COMPUTATIONAL LAB

L: T: P: Cr = 0:0:3:2
List of Experiment

1. Make a program to evaluate a given polynomial f (x ) for a given value of x using

Horner’s Rule.
2. Make a program to find the derivative of a given polynomial f (x ) for a given value of x
.
3. Make a program to find the roots of a given polynomial f (x ) using following methods:
(i) Bisection method.
(ii) Method of False Position.
(iii) Iteration method.
(iv) Newton-Raphson method.
(v) Secant method.
(vi) Muller’s method.
(vii) Lin-Bairstow’s method.
(viii) Quotient-Difference method.
4. Make a program to solve the given set of equations using Gauss-Seidel Iterative method.
5. Make a program to determine the following difference tables for given data points:
(i) Forward Difference table.
(ii) Backward Difference table.
(iii) Central Difference table.
(iv) Divided Difference table.
6. Make a program to find the interpolation polynomial / interpolation value of f (x ) at a
specified value for evenly spaced data points using the following methods:
(i) Newton’s Forward and Backward Difference methods.
(ii) Gauss, Stirling, Bessel’s and Everett’s methods.
7. Make a program to find the interpolation polynomial / interpolation value of f (x ) at a
specified value for unevenly spaced data points using the following methods:
(i) Lagrange Interpolation method
(ii) Newton’s General Interpolation method.
8. Make a program to fit a given polynomial to the given set of data points and to evaluate it
at a specified value of x .
9. Make a program to find the nth (n = 1, 2 and 3) derivative of f (x ) at a specified value of
x for the given set of data points.
10. make a program to find the numerical integration of f (x ) at a specified value of x for the
given set of data points using the following rules:
(i) Trapezoidal rule.
(ii) Simpson 1/3 & Simpson 3/8 rules.
(iii) Boole’s and Weddle’s rules.
(iv) Gaussian formula.
 AM-13203: MATERIAL SCIENCE LABORATORY

L: T: P: Cr = 0:0:3:2
List of Experiment

1. Study of various dislocation models, drawing burgers circuit and finding Burgers vector.

2. Study of various unit cells and crystals for,

a) Their geometry and symmetry,

b) Total number of atoms and their arrangement,
c) Effective number of atoms per unit cell,
d) Co-ordination number,
e) Atomic packing efficiency,
f) Determining density,
g) Concept of Miller indices and Inter-planer spacing.

3. To study the effect of a surface treatment (Etching) on the strength of glass.

4. Heat treatment processes (Annealing, Normalizing, Quenching) and comparison of

hardness before & after heat treatment.
5. To predict creep characteristic of materials by plotting strain vs. time curves for
different loadings.

6. Comparative study of microstructures of different given specimens (mild steel, grey C.I.,
brass, and copper).

7. Specimen preparation for micro structural examination by cutting, grinding, polishing

and etching of aluminium specimen.

8. Fabrication of composite by hand-lay up technique.

9. Mechanical testing of composite made by hand-lay up technique in experiment no. 8.

10. To study the fatigue behavior of a given sample.

 AM-13207: FLUID FLOW OPERATIONS LABORATORY

L: T: P: Cr = 0:0:3:2

Pre-requisite: Fluid Mechanics/ Fluid Flow Operations

List of Experiment

1. To verify the momentum equation using the experimental set-up on diffusion of

submerged air jet.

2. To study the boundary layer velocity profile over a flat plate and to determine the
boundary layer thickness.

3. To study the transition from laminar to turbulent flow and to determine the lower
critical Reynolds number.

4. To study the variation of friction factor ‘f ’ for turbulent flow in commercial pipes.

5. To calibrate an orifice meter, venturimeter, and bend meter and study the variation of
the co-efficient of discharge with the Reynolds number.

6. To study the impact of jets in a flat plate.

7. To study performance of two Centrifugal pumps connected in series and parallel.

8. To study performance of a Reciprocating pump.

Text Books and References:

1. Singh, S. Experiments in Fluid Mechanics, PHI Learning, New Delhi.
2. Prakash, M.N.S., Experiments in Hydraulics and Hydraulic Machines: Theory and
Procedures, PHI Learning, New Delhi.
3. Majumdar, B., Fluid Mechanics with Laboratory Manual, PHI Learning, New Delhi.
 4th Semester Syllabus

CH-14101: FLUID PARTICLE MECHANICS AND MECHANICAL OPERATIONS

L: T: P: Cr = 3:1:0:4

Objectives: To impart necessary basic knowledge in order to understand, analyse and solve
problems related to electrochemical processes.

Prerequisites: Students will learn and have the knowledge on electrical double layer,
Electrocatalysis and different types of electrochemical techniques. The students
will have a practical ability to analyse electrochemical design models, thermal
behaviour of reactors and electrochemical reactors.

LESSON PLAN

UNIT-1: PROPERTIES OF PARTICULATE SOLID 6L

Introduction to unit operations and their role in Chemical Engineering industries. Types
of mechanical operations, Characteristics of solid particles: shape &size, Differential
and cumulative screen analysis, specific surface area, particle population, different
mean diameters for a mixture of particles.

UNIT-2: HANDLING OF PARTICULATE SOLID 7L

Conveying: Types of conveyors, Mechanical - belt, chain, screw conveyors, elevators
& pneumatic conveyors. Storage of solids in bulk protected and unprotected piles,
bines, silos, hoppers, feeders, mass flow and funnel flow bins. Weighing of bulk solids
and weighing techniques.

UNIT-3: MECHANICAL SEPARATION 8L

Classification of separation methods for mixtures of solid-solid, solid-gas and solid-
liquid. Screening, Classifiers, Magnetic separation, Electrostatic separation. Gravity
settling, sedimentation, jigging, floatation and elutriation. Continuous thickeners,
decantation, Phase separation: centrifugal separation, electrostatic precipitators. Gas-
solid separation: gravity settling, impingement separators, cyclone separators,
Scrubbers.
UNIT -4: SIZE REDUCTIONAND ENLARGEMENT 8L
Principles of size reduction: Specific properties of solids for size reduction. Energy
required for size reduction. Crushing and grinding efficiency. Laws of crushing,
pulverization and ultrafine grinding. Classification of crushing and grinding equipment.
Size enlargement: Scope and applications, size enlargement techniques, principle of
granulation, briquetting, pelletisation, and flocculation.

UNIT-5: FILTRATION 6L
 Theory of filtration, Principles of cake filtration, Batch and continuous filters, Flow
through filter cake and filter media, Filter aids, compressible and incompressible filter
cakes, Filtration equipments - selection, classification and working operations.

UNIT-6: MIXING OF SOLIDS & PASTES 4L

Mixing and agitation - Mixing of liquids (with or without solids), Mixing of
powders, Selection of suitable mixers, Mixing equipments.

Text Books and 1. Coulson and Richardson, Chemical Engineering, Vol.2 Butterworth
References: Heinemann Pub
2. Perry R.H. & Chilton C.H., “Chemical Engineers Hand Book”, McGraw hill.
3. Foust A. S. & Associates, “Principles of Unit Operations” John Wiley and
Sons.
4. McCabe Smith, “Unit Operation in Chemical Engineering” 5th ed. McGraw
Hill.
 CH-14102: HEAT TRANSFER OPERATIONS

L: T: P: Cr = 3:1:0:4

Objectives: To understand the principles and applications heat transfer.

Prerequisites: To learn heat transfer by conduction, convection and radiation and design heat
transfer equipments like evaporator and heat exchanger

LESSON PLAN

UNIT-1: Introduction to Heat Transfer: 4L

Concept of the mechanism of heat flow: conduction, convection and radiation; effect of
temperature on thermal conductivity of materials; introduction to combined heat transfer
mechanism.

UNIT-2: Conduction: 10 L
One-dimensional general differential heat conduction equation in rectangular, cylindrical
and spherical coordinate system; initial and boundary conditions. Steady state one
dimensional heat conduction: Composite system in rectangular, cylindrical and spherical
coordinates without energy generation; thermal resistance concept; analogy between heat
and electrical flow; thermal contact resistance; critical thickness of insulation. Fins of
uniform cross sectional area; error of measurement of temperature in thermometer wells,
volumetric internal energy generation, solution of 2D steady state problems using
relaxation method. Transient Conduction: Transient heat conduction with known
temperature distribution within the system; lumped heat analysis of transient heat
conduction problem, time constant of thermocouples.

UNIT-3: Convective Heat Transfer: 10 L

Newton’s Law of Cooling, Types of convective heat transfer, Laminar and Turbulent
flows, Hydrodynamic and thermal boundary layers, Navier-Stokes Equation, Non-
dimensional numbers, Buckingham Pi Theorem. Forced Convection: Basic concept;
hydrodynamic boundary layer; thermal boundary layer; flow over a flat plate; flow across
a single cylinder and a sphere; flow inside tubes; empirical heat transfer relations; relation
between fluid friction and heat transfer; liquid metal heat transfer. Natural Convection:
Physical mechanism of natural convection; buoyant force; empirical heat transfer
relations natural convection over vertical planes and a cylinder, horizontal planes and
cylinders, and a sphere.

UNIT-4: Thermal Radiation: 6L

Basic radiation concept; radiation properties of surfaces; black body radiation laws;
Kirchhoff’s Law, Plank Law and Wien’s Displacement Law, view factor concept; black
body radiation exchange; radiation exchange between diffuse non black bodies in an
enclosure; radiation shields; solar radiations.

UNIT-5: Heat Exchangers: 4L

Type of heat exchangers; fouling factor; overall heat transfer coefficient; logarithmic
mean temperature difference (LMTD) method; effectiveness-NTU method; compact heat
 exchangers.

UNIT-6: Condensation and Boiling: 6L

Introduction to condensation phenomena; heat transfer relations for laminar film
condensation over vertical surfaces and a horizontal tube; pool boiling.

Text Books and References: 1 Heat Transfer: A Practical Approach, McGraw Hill, 2nd
Edition.
2. Heat Transfer by J.P.Holman, McGraw Hill Book Company.
3. Principles of Heat Transfer by F. Kreith, and S.B. Marks,
A.B.Pvt. Ltd.
4. Fundamentals of Heat Transfer by F.P Incorpera and
P.D.Dewitt, John Wiley and Sons, Fifth Edition.
 CH-14103: MASS TRANSFER – I

L: T: P: Cr = 3:1:0:4

Objectives: To impart knowledge on fundamentals of mass transfer phenomena on molecular

level and apply on the Chemical Engineering unit operations concerned with the
problem of changing the composition of solution.

LESSON PLAN

UNIT 1: Diffusion: 6L
,
Fick s Law of diffusion, Molecular and Eddy diffusion, Pseudo steady state diffusion,
Measurement and calculation of diffusivities, Diffusion in gaseous mixture, liquid
mixtures and solids, Unsteady state diffusion.

UNIT 2: Inter-phase mass transfer: 6L

Mass transfer coefficients and their correlations, theories of mass transfer: film theory,
two film theory, penetration and surface removal models, mass, momentum and heat
transfer analogies, Mass transfer equipments: batch and continuous stage wise contactors,
differential contactors.

UNIT 3: Absorption: 8L
Principle of gas absorption, solubility theory, choice of solvent and packing, gas-Liquid
equilibria, tray column: graphical and analytical method, design of packed towers:
contacts between gas and liquid, pressure drop and limiting flow rates, HTU, NTU, HETP
concepts for calculation of height of packed column, diameter of packed column,
absorption with chemical reaction.

UNIT 4: Adsorption: 8L
Principle and types of adsorption, nature of adsorbents, adsorption isotherms, stage wise
and continuous contact operations, unsteady state: Fixed-bed adsorption, adsorption
equipments, ion exchange.

UNIT 5: Humidification: 7L
Definitions related with humidity, wet bulb theory, enthalpy of pure substances, adiabatic
gas-liquid contact operation, methods of humidification and dehumidification, design of
cooling towers.

UNIT 6: Drying: 5L
Theory and mechanism of drying, drying characteristics, drying rate curve, classification
of dryers, different modes of drying operations, design of batch and continuous dryers.

Text Books and References: 1. R.E.Treybal, "Mass Transfer Operations",McGraw Hill Book
Co., New York.
2. W.L. McCabe, J.C. Smith, P. Harriot, "Unit Operations of
Chemical Engineering",McGraw Hill Book Co., New York.
3. J.M. Coulson, J.F. Richardson, "Chemical Engineering", Vol.
I, II, III, Pergamon Press, Newyork.
 CH-14104: CHEMICAL ENGINEERING THERMODYNAMICS - I

L: T: P: Cr = 3:1:0:4

LESSON PLAN
UNIT-1: 9L
Introduction to thermodynamics. System, surroundings, boundaries, classification of
systems. Unit and dimensions, conversion factors. Properties of systems, equilibrium,
processes, heat and work interaction. The work interaction. Thermodynamic definition of
work .characteristics of the work interaction. Evaluation of work. Adiabatic systems and
processes.

UNIT-2: 8L
Diathermic boundary, Zeroth law. Isothermal states. Empirical temperature. Principles of
thermometry. Scales of temperature. Gas thermometer. The ideal gas. Ideal gas
temperature scale. The first law. Basic form. Energy of a system. The heat interaction.
Sign convention. First law for open systems. Steady-flow energy equation and its
applications.
UNIT-3: 10 L
Equations of state. Properties of gases. Properties of steam. Introduction to steam tables.
Other equations of state. Vander Waals gas. Critical state. Reduced equation of state. The
second law. Kelvin-Planck and Clausius statements. Equivalence of statements. Carnot
theorem. Thermodynamic temperature. Kelvin scale. Carnot engine, refrigerator and heat
pump.

UNIT-4: 7L
Clausius in equality. Definition of entropy. Combined first and second law, Evaluation of
entropy. Principle of increase of entropy. Irreversibility and energy. Lost work.

UNIT-5: 5L
Introduction to cycles. Classifications of cycles. Gas power cycles- Otto, Diesel, Brayton,
Vapour power cycle- Rankine cycle, vapour- compression refrigeration cycle.

Text Books and References: 1. Engineering thermodynamics by P K Nag, Tata McGraw Hill.
2. Thermodynamics: An engineering approach by Cengel&
Boles, McGraw Hill.
3. Engineering and Chemical Thermodynamics by Milo D
Koretsky, Wiley Publications.
 CY-1401: ORGANIC AND PHYSICAL CHEMISTRY

L: T: P: Cr = 2:1:0:3

LESSON PLAN

REACTIONS AND REAGENTS:

Basic ideas relating to addition, substitutions, elimination, oxidation and reduction reactions -
Electrophilic and Nucleophilic. Organometallic compounds- Grignard reagent - Synthesis of
different types of compounds like alcohol, aldehyde, acid, amine and organometallic.
Acetoacetic ester - tautomerism- Base hydrolysis - Acid hydrolysis - Malonic ester - cyano
acetic esters- synthesis of dicarboxylic acids and Unsaturated acids.

CARBOHYDRATES:
Carbohydrates - Classification - Reactions of Glucose and fructose- Inter conversion -
Ascending and descending of series. Structure of glucose and fructose.Industrial uses of
cellulose and starch.

ALICYCYCLIC COMPOUNDS, AROMATIC COMPOUNDS, FATS AND OILS:

Alicyclic Compounds- Nomenclature - synthesis of alicyclic compounds using carbon -
acroyloin condensation - Diels Alder reaction Freunds's synthesis - Bayer's strain theory
postulates, drawbacks- theory of strainless rings- conformations of cyclohexane. Coal tar
distillation, separation of benzene, toluene, phenol and naphthalene- Aromaticity exhibited by
these compounds. Fats and oils - Saponification- hydrogenation of oils.

AMINO ACIDS, PROTEINS AND DYES:

Amino acids and proteins- classification -synthesis of amino acids - reactions of carboxyl group
and amino group -peptide linkage-endgroup analysis-colour reaction of proteins- denaturation.
Dyes-colors and constitution -chromophores and auxochromes- quinine theory and electron
theory of dyes- preparation colour and application of azodyes-acidic. basic, mordant, direct
azodyes-Triphenylmethane dyes - malachite green, crystal violet, Rosaniline, prosaniline
mordant dyes- application. Vat dyes-indigo-synthesis and application.

HETEROCYCLIC COMPOUNDS AND NATURAL PRODUCTS:

Heterocyclic compounds-synthesis and reaction of pyrrole ,furan ,thiophene, pyridine, quinine,
isoquinoline and anisole. Alkaloids-Isolation from natural products-colour reaction-structural
elucidation of nicotine.Terpenoids- Isolation - Isoprene rule-structural elucidation of citral.

REACTION KINETICS:
Law of Mass action. Rate order and molecularity of chemical reactions.Methods for their
evaluation.Calculation of rate constants. Consecutive – Parallel and opposing reactions. Chain
reactions.Energy of activation - Theories on reaction rates. Heterogeneous reactions - zero
order reactions - Catalysis - Theory and applications - Inhibitors - Promotors - enzyme
catalysis.

PHASE EQUILIBRIA:
Phase rule: Application - to one components system (water, sulphur and carbon dioxide), Two
component systems (Eutetic, Intermediate compound formation and solid solutions) and simple
three component systems. Solutions: Ideal and non ideal solutions solubility of gases in liquids.
Henry's law. Completely miscible liquids - Rauolt's law - vapour pressure and boiling point
diagrams. Partially miscible liquids – Critical solution temperature -completely immiscible
 liquids - Nerns: distribution law – Dilute solution and their colligative properties. Molecular
weight determination using these properties.

ELECTRICAL CONDUCTANCE:
Electrolytes - strong electrolytes and weak electrolytes - Arrhenius theory of electrolytic
dissociation. Debye - Huckell Onsager theory; Ostwald's dilution law - solubility of electrolytes
and solubility product - common ion action - acids, bases - definitions) based on proton
transference, dissociation constant, amphoteric electrolyte - pH -Buffer solutions. Salts - water
of crystallisation, double salts, complex ions and salts, introduction to co-ordination theory -
hydrolysis.

ELECTRODE POTENTIAL: Electrode potential-Hydrogen electrode, reference electrodes,

electrochemical series, Faraday's laws of electrolysis. Decomposition potential, over voltage,
definitions of current density, current concentration, current efficiency, energy consumption;
electrical conductance, oxidation - reduction redox couple; e.m.f. and energy relations.
Conductometry, Potentiometry - Their applications.

Text Books and References:

1. K. J. Laidler, "Chemical Kinetics", 3rd Edn., Harper & Row Publishers,1987.I.L. Finar,
"Organic Chemistry", (Vol. I & II) 5th Edn., ELBS, London.
2. Morrison and Boyd, “A Text Book of Organic Chemistry", 5th and 6th Edn., Prentice Hall of
India.
3. B. R. Puri and SL. R. Sharma, "Principles of Physical Chemistry", ShobanLalNagin Chand &
Co.
4. P.L. Soni, "Text Book of Physical Chemistry", S. Chand & Co., New Delhi.
 CH-14251: HEAT TRANSFER LAB

L: T: P: Cr = 0:0:3:2
List of Experiment

1. To determine the thermal conductivity of metal bar.

2. To determine Heat transfer through composite wall.
3. To determine the thermal conductivity of insulating powder.
4. To plot the radial temperature distribution and to determine the thermal conductivity of
pipe insulation.
5. To determine the variation of temperature along the length of pin fin under forced
convection.
6. To determine the convective heat transfer coefficient for heated vertical cylinder loosing
heat to the ambient by free or natural convection.
7. To determine the convective heat transfer coefficient for a horizontal pipe through which
air flows under forced convection.
8. To determine the Emissivity of a grey surface at different temperatures.
9. To determine the value of Stefan Boltzmann constant for radiation heat transfer.
10. To study the condensation phenomenon and to determine overall heat transfer
coefficient.
11. To conduct test on a heat pipe and compare the temperature distribution and rate of heat
transfer with geometrically similar copper and stainless steel tubes.
12. To study the Shell and Tube Heat Exchanger.
 CH-14252: FLUID PARTICLE MECHANICS AND MECHANICAL OPERATIONS
LAB

L: T: P: Cr = 0:0:3:2

Objectives: To enable the students to develop a sound working knowledge on different types
of crushing equipments and separation characteristics of different mechanical
operation separators.

Prerequisites: Students would gain the practical knowledge and hands on various separation
techniques like filtration, sedimentation, screening, elutriation and crushing

List of Experiment

1. To determine the effect of initial concentration & initial suspension height on

sedimentation rates.
2. To study the batch settling process.
3. To study the operation of filter press in the laboratory and to evaluate specific cake
resistance and medium resistance.
4. Batch filtration studies using a plate and frame filter press.
5. Size distribution of sand particles using sieve shaker.
6. To study the characteristics of fluidized bed.
7. To study the characteristics of fixed bed.
8. To determine the efficiency of jaw crusher for crushing the material of known index.
9. To study the operation of a hammer mill.
10. To study effect of RPM on the power consumption of a ball mill (Variable/ Constant
speed).
11. To study the drying characteristics of a solid material under batch drying condition.
12. To study the reduction ratio in jaw crusher.
13. To study the separation characteristics of elutriator.

Text Books and References: 1. Mechanical operation lab manual of Chemical Engineering Dept., MNNIT
Allahabad.
 CY-14251: ORGANIC AND PHYSICAL CHEMISTRY LAB

L: T: P: Cr = 0:0:3:2

List of Experiment

1. Preparation & Physical Characterization of organic compounds.

2. Identification of functional groups of organic molecules.
3. Preparation of derivative of the functional groups
(a) Preparation of p- Nitro acetanilide from acetanilide (Nitration)
(b) Preparation of acetanilide from aniline (Acetylation)
4. Microwave synthesis of Aspirin-A green chemistry experiment.
5. Wet chemical method for the identification of organic dyes Malachite green,
Rosaniline and Indigo.
6. Preparation of buffer solution (AcOH & AcONa) of specific pH and its verification
By pH- metry.
7. Determination of distribution (partition) coefficient of I2 between CCL4 and water.
8. Kinetic study of hydrolysis of ethyl acetate by volumetric titration method.
9. Verification of Kohlrausch’s Ist law for strong electrolytes using conductometric
measurement.
10. Verification of Ostwald’s dilution law for week electrolytes using conductometric
measurement.
11. Determination of the strength of a strong acid by strong base using condctometric
titration.
12. Determination of sodium & Potassium by flame photometry.
13. To carry out the proximate analysis of a given sample of fuel.
 5th Semester Syllabus
CH-15101: CHEMICAL REACTION ENGINEERING-I

L: T: P: Cr = 3:1:0:4

Objectives: The objective is to enable understanding of engineering activity concerned with

the exploitation of Homogeneous chemical reactions on a commercial scale.
Prerequisites: Chemical reaction engineering is at the heart of virtually every chemical process.
It separates the chemical engineer from other engineers. This field studies the
rates and mechanisms of chemical reactions and the design of the reactors in
which they take place. This course applies the concepts of reaction rate,
stoichiometry and equilibrium to the analysis of chemical reacting systems.
Derivation of rate expressions from reaction mechanisms and equilibrium or
steady state assumptions for homogeneous reactions are taken into account.

LESSON PLAN
UNIT-1: Introduction: kinetics of reactions 4L

Introduction, Kinetics of homogeneous reactions: Concentration dependent & Temperature

dependent term of rate equation, searching for a reaction mechanism.
UNIT-2: Batch Reactor: Analysis of ratedata 6L

Constant-volume batch reactor, Varying-volume batch reactor, Dependency of rate

equation on temperature, Searching for a rate equation.
UNIT-3: Design of Ideal Reactor: For Single Reactions 10 L

Introduction to ideal reactors for a single reaction, Ideal batch reactor, Ideal mixed flow
reactor, and Ideal plug flow reactor, Size comparison of single reactors, Multiple reactor
systems, Recycle reactor, and Autocatalytic reactor.
UNIT-4: Design of Reactor:For Multiple Reactions 9L

Design for multiple Reactions: Reactions in parallel, reactions in series, and series - parallel
reactions.
UNIT-5: Heat Effects 4L

Temperature and pressure effects on single and multiple reactions.

UNIT-6: Flow Behavior of Reactors 9L

Non-ideal flow: Residence time distribution studies: C, E, and F curves, conversion

calculations directly from tracer studies. Models for non-ideal flow: one parameter models-
tank-in series and dispersion models, multi-parameter models.

Text Books and References: 1. O. Levenspiel, "Chemical Reaction Engineering", Wiley

Easter Ltd., New York.
2. H. Scott Fogler, “Elements of Chemical Reaction
Engineering”, PHI.
3. M. Davis and R. Davis, “Fundamental of Chemical Reaction
Engineering”,McCraw Hill, New York.
4. J.M.Smith, "Chemical Engineering Kinetics", McCraw Hill,
New York.
5. Lanny D. Schmidt, “The engineering of chemical reactions”
Oxford University Press, New York.
 CH-15102: MASS TRANSFER- II

L: T: P: Cr = 3:1:0:4

Objectives: The objective is to learn the mass transfer operations, where the composition of
the separated substances changes without involving chemical reactions.

LESSON PLAN
UNIT 1: Distillation: [4L]

Vapor- liquid equilibria: pressure-temperature-concentration phase diagrams, enthalpy-

concentration diagrams for ideal and non-ideal solutions, Raoults law and its
applications, concept of relative volatility, maximum and minimum boiling mixtures.

UNIT 2: Single stage distillation: [4 L]

Flash vaporization of a binary mixture, differential or simple distillation of a binary

mixture, steam distillation, principles of azeotropic and extractive distillations.

UNIT 3: Continuous distillation of binary mixtures: [8L]

Fractionating column: combination of rectification and stripping, Rectification on an ideal

plate, design calculations using McCabe Thiele and PonchonSavarit methods: total reflux
ratio, minimum and optimum reflux ratio, bottom plate and reboiler, open steam
distillation, tray efficiency, calculation of height and column diameter, bubble cap tray,
sieve tray, valve tray and packed columns. Introduction to multi-component distillation
system, multistage batch distillation
UNIT 4: Liquid - liquid extraction: [8L]

Principles of extraction, ternary liquid equilibria, effect of pressure and temperature,

triangular graphical representation concept of theoretical or ideal stage, single stage
operation, multistage continuous operation: co-current and cross current operations, stage
calculation, Analytical and graphical solutions of single and multistage operations for
miscible and immiscible systems, equipments: mixer settlers, plate column, spray and
packed column, etc.

UNIT 5: Solid - liquid extraction: [8L]

Theory, mechanism, types of leaching, solid - liquid equilibria, constant and variable
underflow, batch and continuous operations: single and multistage cross current and
counter current operations, equipments: percolation tank, agitated vessel, thinkers,
classifiers etc.

UNIT 6: Crystallization: [8L]

Principle and solubility curve of crystallization, theory of super saturation, nucleation and
crystal growth rate, controlled growth of crystals, equilibrium yield, Heat and mass
transfer rates in crystallization, classification and design of industrial crystallizers.

Text Books and References: 1. R.E. Treybal, "Mass Transfer Operations", McGraw Hill Book
Co., New York.
2. W.L. McCabe, J.C. Smith, P.Harriot, "Unit Operations of
Chemical Engineering", McGraw Hill Book Co., New York.
3.
 CH-15103: PROCESS DYNAMICS AND CONTROL

L: T: P: Cr = 3:1:0:4

Objectives: The objective is to learn the scientific and engineering principles underlying
process dynamics and control systems. It develops an insight into chemical
process control problems and makes familiar with industrial control systems

LESSON PLAN

UNIT-1: INTRODUCTION AND DYNAMICS OF PRPCESSES 12 L

Introduction to process control - Need of process control, process control strategies,

process control activities; Theoretical models of chemical processes - Modelling
principles, dynamic models and their solutions; Laplace transforms.

UNIT-2: FIRSTAND HIGHER ORDER SYSTEMS 8L

Development and properties of transfer functions, linearization of non-linear models

Response of first and second order processes, Dynamic response of more complicated
processes.

UNIT-3: FEEDBACK CONTROLLERS 7L

Concept & type of feedback control, block diagram representation, response of it,
Proportional controller, Proportional Integral (PI) controller and Proportional derivative
(PD) controller and PID controller.
UNIT-4: DESIGN AND STABILITY 8L

Influence of process design on process control, degrees of freedom for process control,
Selection of variables, Dynamic behavior and stability of closed loop system- closed loop
representation, transfer functions, stability analysis-Routh analysis

UNIT-5: 5L

Frequency response – Control system design, Root locus, Bode plot, Nyquist plot.

Text Books and References: 1. D. E.Seborg, T.F. Edgar and D.A. Mellichamp, "Process
Dynamics Control", Wiley,3rdEd. 2013.
2. G Stephanopopulas, "Chemical Process Control", Prentice-
Hall India, 1984.
3. D. R. Coughanowr, "Process System Analysis and Control",
2ndEd. McGraw Hill, 1991.
4. S. Sundaram "Process Dynamics and Control", Cengage
Publishers.
 CH-15104: CHEMICAL ENGINEERING THERMODYNAMICS-II

L: T: P: Cr = 3:1:0:4
Objectives: To present thermodynamic principles from a chemical engineering viewpoint.
Prerequisites: Students will learn laws of thermodynamics, thermodynamic property relations
and the behavior of fluids under PVT conditions, theory and application of
solution thermodynamics and chemical reaction equilibrium, compression and
refrigeration processes.

LESSON PLAN
UNIT-1: Fundamentals and Law of Thermodynamics: [8 L]
Terminologies of thermodynamics, variables and quantities of thermodynamics, Point and path
properties, heat and work, reversible and irreversible processes, phase rule, First law and internal
energy, statements of first law for the non flow and flow systems, enthalpy and heat capacity
limitations of the first law, Statements of the second law of thermodynamics, available and
unavailable energies, entropy function, applications of the second law. Zeroth law of
thermodynamics

UNIT-2: Thermodynamic Properties of Real Gases: [8 L]

The PVT behavior of fluids, laws of corresponding states and equation of states approaches to the
PVT relationships of non ideal gas problems, compressibility factors, generalized equations of
state, property estimation via generalized equation of state, fugacity and fugacity coefficients of
real gases.

UNIT-3Thermodynamics of Solutions: [10L]

Fundamental Property relation, Maxwell equation and consistency tests, The Chemical potential
and phase equilibria, Partial molar quantities, Gibbs-Duhem Equation, Criteria for thermodynamic
equilibrium, Phase equilibrium criteria, Ideal Solutions and Ideal Gas Mixtures, Concept of
Fugacity and Fugacity coefficient, Fugacity and Activity Coefficient Models, Non-ideal solutions,
Residual and excess properties, Solid-liquid equilibrium, solubility of gases in liquids, Liquid-
liquid equilibrium.

UNIT-4: Chemical Reaction Equilibrium: [10 L]

The reaction Coordinate, Application of equilibrium criteria to chemical reactions, the standard
Gibbs free energy change and the equilibrium constant, Effect of temperature on equilibrium
constant, Evaluation of equilibrium constants, Relation of equilibrium constants to composition,
Heat effects, industrial reactions (NH3 synthesis etc), free energy calculations, Homogeneous and
heterogeneous reaction systems, multiple reactions, partially miscible and immiscible systems,
Azeotropes, retrograde condensation, thermodynamic diagrams, Multi reaction Equilibria.

UNIT-5: Compression and Refrigeration Cycle: [6 L]

Thermodynamic aspects of compression process, classification of compression processes, basic
equation for change of state of gases, the work expression for different situations, the effect of
clearance volume, multistage compression, convergent divergent flow, Ejectors. Definitions of
refrigeration, Reverse Carnot cycle, Vapor compression and vapor absorption cycle, Gas
refrigeration.
Text Books 1. J. M. Smith and Van Ness, "Introduction to Chemical Engineering Thermodynamics",
& McGraw Hill, New York.
References 2. Rao. Y.V.C. “Chemical Engineering Thermodynamics”, Universities Press.
: 3. K.V.Narayanan, “A text book of Chemical Engineering Thermodynamics", PHI Learning
Private Limited, New Delhi.
4. B.F. Dodge, "Chemical Engineering Thermodynamics", McGraw Hill, New York.
5. S.I. Sandler, “Chemical and Engineering Thermodynamics, Wiley.
 HS-1501: PRINCIPLES OF MANAGEMENT

L: T: P: Cr = 3:1:0:4

Objectives: The emphasis on teaching of Humanities and Social Sciences for the overall intellectual and
social development of the students of technology is an important feature of the
undergraduate curriculum at MNNIT, Allahabad. This education intends to expand the
students’ horizon of knowledge by exposing them to areas of study which make them
sensitive to a wide range of human problems and social phenomena. Such a holistic
education, it is hoped, would enable them to appreciate their role in national reconstruction
by responding to the challenges of the time.
Prerequisites: Knowledge on the principles of management is essential for all kinds of people in all kinds
of organizations. After studying this course, students will be able to have a clear
understanding of the managerial functions like planning, organizing, staffing, leading and
controlling. Students will also gain some basic knowledge on international aspect of
management.
LESSON PLAN
Unit I: Introduction to Management: 5L
Definition of Management – Science or Art – Management and Administration, Functions of
Management – Types of Business Organization. Levels of management and Managerial skills

Unit II: School of Management Thoughts: 6L

Evolution of Management thoughts, classical approach, neo- classical approach, contribution of
Taylor, Weber and Fayol, modern approach.

Unit III: 8L
Planning Nature & Purpose – Steps involved in Planning ,Objectives, Setting Objectives, Process of
Managing by Objectives, Strategies, Policies & Planning Premises Forecasting Decision-making.

Unit IV: 11 L
Organizing Nature and Purpose – Formal and informal organization – Organization Chart – Structure
and Process – Departmentation by difference strategies – Line and Staff authority – Benefits and
Limitations – De-Centralization and Delegation of Authority – Staffing – Selection Process -
Techniques – HRD – Managerial Effectiveness. Directing: Scope – Human Factors – Creativity and
Innovation – Harmonizing Objectives – Leadership – Types of Leadership Motivation – Hierarchy of
needs – Motivation theories – Motivational Techniques – Job Enrichment – Communication – Process
of Communication – Barriers and Breakdown – Effective Communication – Electronic media in
Communication.

Unit V: Controlling: 5L
System and process of Controlling – Requirements for effective control – The Budget as Control
Technique – Information Technology in Controlling – Use of computers in handling the information –
Productivity – Problems and Management – Control of Overall Performance ; Coordination.

Unit-VI: 5L
Organizational Behavior: Organizational change, Conflict Management and Stress Management.
Functional management: Human Resource Management, Financial management, marketing
Management.

Text Books & 1 Tripathy PC And Reddy PN, “Principles of Management”, Tata McGraw-Hill.
References: 2. Decenzo David, Robbin Stephen A, “Personnel and Human Reasons Management”,
Prentice Hall of India.
3. JAF Stomer, Freeman R. E and Daniel R Gilbert, “Management”, Pearson Education,
Sixth Edition.
4. Fraidoon Mazda, “Engineering Management”, Addison Wesley.
5. Harold Kooritz& Heinz Weihrich “Essentials of Management”, Tata McGraw-Hill.
6. Joseph L Massie “Essentials of Management”, Prentice Hall of India, (Pearson) Fourth
 CH-15251: MASS TRANSFER LAB

L: T: P: Cr = 0:0:3:2
List of Experiment

1. Diffusion of an organic vapour in air.

2. Mass transfer with/without chemical reaction

3. Adsorption studies of dyes on activated carbon

4. Studies on forced draft Cooling Tower.

5. Drying of Solid in tray dryer under forced draft condition.

6. VLE curve for CCl4- toluene mixture

7. Study of bubble cap multistage batch type distillation column.

8. To study the characteristics of steam distillation using turpentine oil as a feed stock.

9. To study the performance of Swenson Walker crystallizer.

10. Extraction of acetic acid from its mixture with toluene using water
 CH-15252: PROCESS DYNAMICS & CONTROL LAB

L: T: P: Cr = 0:0:3:2
List of Experiment

1. To study the dynamic response of liquid level in two tank interacting liquid level system.
2. To study the dynamic response of liquid level in two tank non-interacting liquid level
system.
3. To study of current to pressure (I to P) and pressure to current (P to I) converter.
4. To study the dynamic behavior of a first order system.
5. To study the characteristics and working principle of the RF-capacitance type level
transmitter.
6. To study the characteristics and working principle of the differential pressure transmitter.
7. To study the characteristics and working principle of the current to pressure converter
and control valve.
8. To study the performance of cascade controller.
9. To study the performance of on-off/P/PI/PID controllers on level process.
10. To study the performance of on-off/ P/PI/PD/PID controllers on flow process.
11. Study of control valve characteristics .
12. Study of U-tube manometer.
 CH-1553: PROCESS SIMULATION LAB

L: T: P: Cr = 0:0:3:2

List of Experiment

1. Modeling and Simulation of CSTR using programming language.

2. Modeling and Simulation of PFR using programming language. .
3. Modeling and Simulation of Shell and Tube/Plate Type Heat Exchanger using
programming language.
4. Modeling and Simulation of Multi component distillation column using programming
language.
5. Modeling and Simulation of Reactive/Extractive/Azeotropic distillation column using
programming language.
6. Modeling and Simulation of Absorption unit using programming language.
7. Steady State and Dynamic simulation of Heat Exchanger using ASPEN HYSYS.
8. Steady State and Dynamic simulation of CSTR using ASPEN HYSYS.
9. Steady State and Dynamic simulation of PFR using ASPEN HYSYS.
10. Steady State and Dynamic simulation of Multi component distillation Column using
ASPEN HYSYS.
11. Steady and Dynamic simulation of Reactive/Extractive/Azeotropic distillation Column
using ASPEN HYSYS.
12. Steady State and Dynamic simulation of Absorption unit using ASPEN HYSYS.
 6th Semester Syllabus
CH-16101: CHEMICAL REACTION ENGINEERING-II

L: T: P: Cr = 3:1:0:4

Objectives: The objective is to develop an insight into the heterogeneous reaction systems
with a view to tackle real industrial challenges and to develop understanding
about reactor analysis and design for heterogeneous systems.
Prerequisites: Reaction engineering ties together virtually all elements of Chemical
Engineering, from thermodynamics and chemical kinetics to mass and energy
balances to mass and heat transfer. This field studies the rates and mechanisms
of heterogeneous chemical reactions and the design of the reactors such
reactions via synthesischemical kinetics, transport phenomena, and mass &
energy balances. Derivations of rate expressions from reaction mechanisms for
heterogeneous reactions arealso taken into account.

LESSON PLAN

UNIT-1: GENERAL CONSIDERATIONS: 6L

Introduction to design for Heterogeneous Reacting Systems: Rate equation for
heterogeneous reactions, contacting pattern for two-phase systems. Mixing of fluids: Self
mixing of single fluids, mixing of two miscible fluids

UNIT-2: NON-CATALYTIC FLUID-PARTICLE REACTIONS SYSTEM: 7L

Models for non-catalytic fluid-particle reaction systems, limitations, and selection. Fluid-
particle reactors design.

UNIT-3: NON-CATALYTIC FLUID- FLUID REACTIONS SYSTEM: 7L

Rate equations for instantaneous, fast, intermediate, slow, and infinitely slow
reactions.slurry reaction kinetics, fluid-fluid reactors design.

UNIT-4: CATALYSIS AND CHARACTERISTICS OF CATALYST: 8L

Introduction to catalysis, catalyst: definition and properties, promoters, inhibitors.
poisons, solid catalyzed reaction system, the rate equation for surface kinetics, pore
diffusion resistance, porous catalyst particles, turn over frequency.

UNIT-5: REACTORS AND KINETICS OF SOLID CATALYZED REACTIONS: 10 L

Kinetics and mechanism of heterogeneous catalytic reactions, evaluation and elimination
of internal and external diffusion resistances, effectiveness factor, heat effects, controlling
resistances, rates of chemisorptions, adsorption isotherms, and reactor for solid catalyzed
reaction systems.

UNIT-6: CATALYST DEACTIVATION: 4L

Mechanism of catalyst deactivation, the rate and performance equations.

Text books and references:

1. O. Levenspiel, "Chemical Reaction Engineering", Wiley Easter Ltd., New York.
2. H. Scott Fogler, “Elements of Chemical Reaction Engineering”, PHI.
3. M. Davis, “Fundamental of Chemical Reaction Engineering”, McCraw Hill, New York.
4. J.M.Smith, "Chemical Engineering Kinetics", McCraw Hill, New York.
5. Lanny D. Schmidt, “The engineering of chemical reactions” Oxford University Press, New
York.
 CH-16102: TRANSPORT PHENOMENA

L: T: P: Cr = 3:1:0:4
Objectives: To provide an overview of mass, momentum and energy transport phenomena.
Prerequisites: This course provides knowledge about applying balance equations on
fundamental quantities mass, momentum and energy transport at molecular,
microscopic and macroscopic level, and to determine velocity, temperature and
concentration profiles.

LESSON PLAN
UNIT-1: Laminar Flow: 8L
Viscosity and the Mechanisms of Momentum Transport, Velocity distribution in Laminar
flow - Shell momentum balances -Flow through tubes, surfaces, Flow of non-Newtonian
fluids.
UNIT-2: Equation of Motion: 10 L
Vector and tensor, Equation of change for isothermal process – One dimensional equation
of motion and continuity - Euler and Navier - Stokes equation, Dimensional analysis of
equation of change.
UNIT-3: Turbulent Flow: 6L
Velocity distribution in turbulent flow - Semi empirical expressions for Reynolds stress,
Inter-phase transport in isothermal system - Ergun's equation.
UNIT-4: Heat Transfer Analysis: 8L
Thermal Conductivity and Mechanisms of energy transport,Temperature distribution in
solids and fluids in laminar flow - Equations of change for multi component systems.

UNIT-5: Mass Transfer Analysis: 6L

Diffusivityand the mechanism of Mass Transport, Concentration distribution in solids and
in fluids, laminar flow - Equations of change for multi component systems.
UNIT-6: Computational Fluid Dynamics 4L
Introduction, applications and software.

Text Books and References: 1. J.L. Stuart., 'Transport Phenomena", John Wiley, New York.
2. R. B. Bird, W. Stewart and E. N. Lightfoot, "Transport
Phenomena", Wiley, New York.
3. C. J. Geankopolis, "Transport Processes in Chemical
Operations", Prentice Hall of India, New Delhi.
4.
 CH-16103: ENVIRONMENTAL POLLUTION MONITORING AND CONTROL

L: T: P: Cr = 3:1:0:4
Objectives: The aim of this course is to create awareness in every engineering graduate
about the importance of environment, the effect of technology on the environment
and ecological balance and make them sensitive to the environment problems in
every professional endeavour that they participates.

Prerequisites: At the end of this course the student is expected to understand what constitutes
the environment, what are precious resources in the environment, how to
conserve these resources, what is the role of a human being in maintaining a
clean and useful environment for the future generations and how to maintain
ecological balance and preserve bio-diversity. The role of government and non-
government organization in environment managements.

LESSON PLAN
UNIT-1: INTRODUCTION 6L
Ecology & Environment, Biodiversity, Interaction of man and environment, Overall
picture of environmental pollution, Ambient air and water quality criteria, Standards and
Acts-Indian, EPA& EURO, Effects and control of noise, thermal and radioactive
pollution.

UNIT-2: AIR POLLUTION 10 L

Types of pollutants – Natural and manmade air pollutants, Dispersion of pollutant in the
atmosphere, Gaussian dispersion model, Meteorological factors, Stability and inversion of
atmosphere, Plume behaviour, Control of air pollution from stationary and mobile
sources, Methods of measuring and sampling of gaseous and particulate pollutants in
ambient air and industrial waste gases, measurement of smoke density and visibility.
Control of gaseous pollutants - SOx, NOx, H2S, VOCS, Auto exhaust. Stack design,
Classification, selection and design of equipment’s like cyclones, electrostatic
precipitators, bag filters, wet scrubbers, settling chambers.

UNIT-3: WATER POLLUTION 10 L

Waste water characteristics – Physical and chemical composition, Biochemical oxygen
demand (BOD), Pathogenic bacteria and chemical toxicity. Types of pollutants in waste
water of chemical industries, Methods of sampling, preservation of samples and analysis.
Methods for the treatment of liquid wastes to control pollution, Classification viz.
physical, chemical and biological methods, Selection and design of equipment like
hydrocyclone, settling tanks, filters, ion- exchange.

UNIT-4: SOLID WASTE MANAGEMENT 6L

Characterization of solid wastes, Problems of collection and handling, Various processing
techniques used in solid waste management such as compaction, incineration,
Composting, landfills and biological processing, Solid waste as resource material.

UNIT-5: POLLUTION ABATEMENT IN CHEMICAL INDUSTRIES 6L

Pollution abatement in important chemical industries like fertilizers, petroleum refineries
and petrochemicals, Pulp and Paper, Pharmaceuticals, Tannery, Sugar, Distillery, food
 processing, cement and electroplating.

UNIT-6: MISCELLANEOUS 4L
Soil pollution, Marine pollution, Noise pollution, Thermal pollution and Nuclear hazards,
carbon trading.

Text Books and References: 1. Howard S. Peavy, D. R. Rowe & C. Tchobonoglous

“Environmental Engineering”, McGraw Hill.
2. Metcalf & Eddy, “Waste Water Engineering Treatment,
Disposal & Reuse”, Tata McGraw Hill.
3. Werner Strauss, ‘Air Pollution Control: Measuring and
monitoring air pollutant’ Wiley.
4. Werner Strauss, ‘Air Pollution Control part –II’ Wiley.
5. Pandey G. N. and Carney G. C., "Environmental
Engineering ". Tata McGraw Hill.
5.
 CH-16104: PROCESS EQUIPMENT DESIGN

L: T: P: Cr = 3:1:0:4

Objectives: To impart the information about design of process equipments and develop
understanding about pressure vessel design and storage tank design.

LESSON PLAN
UNIT 1 7L
Nature of process equipments, general design procedure, basic considerations in design,
standards codes and their significance, equipment classification and their selection, design
pressure, design temperature, design stress, review of fabrication techniques and
environmental considerations in design procedure.

UNIT 2 8L
Proportioning of pressure vessels, selection of L/D ratio, optimum proportions of vessels.
Design of unfired pressure vessels subjected to combined loading, purging of vessels.
Selection and design of various heads such as flat, hemispherical, elliptical and conical,
opening/nozzles, manholes, nozzle reinforcement design, etc. Flanged joints, classification
of flanges, design of non standard flanges, types of gaskets, their selection, and design.

UNIT 3 8L
Various types of storage vessels and applications, atmospheric vessels, vessels for storing
volatile and nonvolatile liquids, storage of gases, losses in storage vessels, various types of
roofs used for storage vessels, manholes, nozzles and mountings. Design of cylindrical and
spherical storage vessels; should include base plates, shell plates, roof plates, wind girders,
curb angles for self supporting and column supported roofs.

UNIT 4 9L
Types of agitators, their selection, applications, baffling, power consumption which
includes twisting moment, equivalent bending moment, design of blades etc. Reaction
vessels-Introduction, classification, heating systems, design of vessels, study and design of
various types of jackets like plain, half coil, channel.

UNIT 5 9L
Design of heat transfer equipments such as heat exchangers with and without phase change,
evaporators, crystallizers.Design of mass transfer equipments such as distillation columns,
absorption columns, extraction columns, dryers and cooling towers.

TEXT BOOKS AND REFERENCES:

1. S. D. Dawande, “Process Design of Equipments”, Central Techno Publications, 2005.
2. M.V. Joshi, V. V. Mahajani, “Process Equipment Design”, Macmillan India Ltd., 2000.
3. B.C. Bhattacharyya, “Introduction to Chemical Equipment Design”, CBS Publishers &
Distributors, 2003.
4. D. Q. Kern, “Process Heat Transfer”,Tata McGraw-Hill, 2004.
5. J.M. Coulson, J. F. Richardson, R. K. Sinnott, “Coulson and Richardson's Chemical
Engineering: Chemical Engineering Design”Vol.6, Butterworth – Heinemann, 2004.
6. E. Ludwig, "Chemical Process Equipment Design", Gulf Pub., 2002.
7. Indian standards Institution, ‘Code for unfired pressure vessels’, IS – 2825.
 CH-16105: CHEMICAL TECHNOLOGY
L: T: P: Cr = 3:0:0:3

Objectives: To impart the knowledge on unit processes and unit operations involved in the
large scale manufacture of different chemical industries.
Prerequisites: This course provides a detailed understanding of manufacturing of various
chemical compounds and the related industries.

LESSON PLAN
UNIT -1: 5L

Chlor-alkali Industries: Manufacture of Soda ash, Manufacture of caustic soda and

chlorine - common salt.

UNIT -2: 5L
Sulphur and Sulphuric acid: Manufacture of sulphuric acid&Oleum.

UNIT -3: 5L
Cement: Types and Manufacture of Portland cement

UNIT -4: 5L
Industrial Gases: Hydrogen, Producer Gas & Water-Gas.

UNIT -5: 5L
Manufacture of paints and Pigments.

UNIT-6: 5L
Nitrogen industries :- Ammonia, Nitric Acid, Nitrogenous & mixed fertilizers

UNIT-7: 5L
Pulp& paper Industry

UNIT-8 5L
Petrochemicals:- Formaldehyde, Ethylene Glycol , Styrene, Butadiene.

Text Books and References:

1. G.T.Austin, "Shreve's Chemical Process Industries", McGraw
Hill Book Co., New York.
2. R.GopalRao, "Dryden's Outlines of Chemical Technology",
Affiliated East-West Publishers.
 6.
CH-16251: CHEMICAL TECHNOLOGY LAB

L: T: P: Cr = 0:0:3:2
List of Experiment

1. To determine the aniline point and mixed aniline point of a given oil sample.
2. To determine viscosity of a given sample by Tar viscometer.
3. To determine Conradson carbon residue (CCR) content in a given oil sample.
4. To determine asphaltenes content in a residual fuel oil sample.
5. To determine the calorific value of a given sample by using bomb calorimeter.
6. To determine the flash point of a given oil sample by using Pensky-Martens apparatus.
7. To determine the flash point and fire point of a given oil sample by using Cleveland open
cup apparatus.
8. To determine pour point and cloud point of a given oil sample.
9. To carry out proximate analysis of a given sample.
10. To carry out distillation characteristics of a lighter oil fraction via ASTM D86 method.
11. To prepare soap via saponification process.
12. To prepare tooth powder.
13. To prepare pigment of three different colours.
 CH-16252 CHEMICAL REACTION ENGINEERING LAB

L: T: P: Cr = 0:0:3:2

List of Experiment

1. To study the kinetics and determine the reaction rate constant (k) for the given
saponification reaction in a multiple reactor (Cascade CSTRs) at fixed temperature.
2. To determine the effect of temperature on rate constant (k) of saponification in a
multiple reactor (Cascade CSTRs).
3. To study the kinetics and determine the reaction rate constant (k) for the given
esterification reaction in a multiple reactor (Cascade CSTRs) at fixed temperature.
4. To determine the effect of temperature on rate constant (k) of esterification reaction in a
multiple reactor (Cascade CSTRs).
5. To study the kinetics and determine the reaction rate constant (k) for the given
saponification reaction in a multiple reactor (Combined CSTR & PFR) at fixed
temperature.
6. To determine the effect of temperature on rate constant (k) of saponification in a
multiple reactor (Combined CSTR & PFR).
7. To study the kinetics and determine the reaction rate constant (k) for the given
esterification reaction in a multiple reactor (Combined CSTR & PFR) at fixed
temperature.
8. To determine the effect of temperature on rate constant (k) of esterification reaction in a
multiple reactor (Combined CSTR & PFR).
9. To determine the activation energy for a non catalytic homogeneous reaction in CSTR.
10. To determine the activation energy for a catalytic homogeneous reaction CSTR.
11. To study the effect of different kinds of packing in a packed bed reactor.
12. To study the residence time distribution in a CSTR at constant flow rate. To plot the exit
time distribution of the reactor and thereby obtain E-curve, F-curve and mean residence
time, t.
13. To study the residence time distribution in a CSTR with varying flow rates. To plot the
exit time distribution of the reactor and thereby obtain E-curve, F-curve and mean
residence time, t.
14. To study the flooding characteristics and pressure drops in a trickle bed reactor.
15. RTD studies in a packed bed reactor.
 CL-16253 ENVIRONMENTAL ENGINEERING LAB

L: T: P: Cr = 0:0:3:2

List of Experiment

1. To study the increase in loss of head with respect to time in the filter bed.
2. To study the effect of parameters like pH and temperature on adsorbents.
3. To study change in alkalinity of wastewater by bubbling acidic gas.
4. To check the acidity and alkalinity of water resources.
5. To calculate the amount of solids in a suspension.
6. To measure COD level in wastewater.
7. To measure the conductivity of various wastewater.
8. To plot the pressure drop profile through the filter bed.
9. To measure the sediment removal efficiency and relating this to the hydraulic
characteristics of a sedimentation tank.
10. To study the characteristics of anaerobic digester.
11. To determine the effect of velocity of water for separation of equal sized particles of
different densities.
 7th Semester Syllabus
CH-17101: PETROLEUM REFINING ENGINEERING

L: T: P: Cr = 3:1:0:4

Objectives: To impart information about the importance of crude oil in energy mix and to
acquaint the students about various processes in petroleum refining industry.

LESSON PLAN

UNIT 1 [7L]
World and Indian petroleum refining scenario, composition of crude oil, classification of crude oil,
UOP Characterization factor, types of refineries, various petroleum products, Indian specifications,
testing methods and their significance.

UNIT 2 [7L]
Dehydration and desalting of crude oil, descriptive account of atmospheric distillation, vacuum
distillation, various straight-run products, properties and applications, treatment techniques for the
straight-run products.

UNIT 3 [9L]
Thermal conversion processes, reactions involved in thermal conversion processes, free radical
mechanism, thermal cracking, coil visbreaking, coil-soaker visbreaking, delayed coking, fluid
coking, flexi coking.

UNIT 4 [9L]
Catalytic conversion processes, reactions involved in catalytic conversion processes, carbonium
ion mechanism, catalytic cracking, fixed bed catalytic cracking and fluidized catalytic cracking,
deep catalytic cracking, hydrocracking, catalytic reforming, isomerisation, alkylation.

UNIT 5 [8L]
Heavy oil and petroleum residue upgrading, petroleum coke gasification, fixed bed gasifier,
fluidized bed gasifier, entrained bed gasifier, Fischer-Tropsch synthesis for the production
transportation fuels from synthesis gas.

Text Books and References: 1. J.H. Gary, G.E. Handwerk, M.J. Kaiser, “Petroleum
Refining:Technology and Economics”, Marcel Dekker
Publication, 2007.
2. J.G. Speight, “The Chemistry and Technology of
Petroleum”, Marcel Dekker Publication, 2006.
3. W.L. Nelson, “Petroleum Refinery Engineering”, McGraw
Hill Publication, 1958.
4. B. K. BhaskaraRao, “Modern Petroleum Refining
Processes”, Oxford and IBH Publishing Company, 1990.
5. R. Prasad, “Petroleum Refining Technology”, Khanna
Publishers, 2002.
 CH-17102: OPTIMIZATION OF CHEMICAL PROCESSES

L: T: P: Cr = 3:1:0:4

Objectives: The present course aims the study of optimization techniques for designing any
chemical process, and the principles for developing an executive system.
Prerequisites: Numerical methods and other UG level chemical engineering courses

LESSON PLAN
UNIT 1 [8 L]
Introduction to optimization; formulation of objective function; basic concepts-functions,
regions, necessary and sufficient conditions for an extreme of an unconstrained
function; one dimensional search: scanning and bracketing; Newton, quasi-Newton and
secant methods; region elimination method, polynomial approximation methods.

UNIT 2 [8 L]
Unconstrained multivariable optimization: Direct methods-random search, grid search,
univariate search, simplex method, conjugate search direction and Powell’s method;
Indirect method-gradient and conjugate gradient methods Newton's method, movement in
search direction, secant method.

UNIT 3 [10 L]
Linear programming: Basic concept in linear programming; Graphical solution; simplex
method; Standard LP from; Obtaining first feasible solution; Sensitivity analysis. Non
linear programming: Lagrange multiplier method; Quadratic programming; penalty
function and augmented Lagrangian methods; Successive quadratic programming;
Optimization of dynamic process.

UNIT 4 [9L]
Optimization of staged and discrete processes: Dynamic programming; integer
and mixed integer programming; Nontraditional optimization techniques: Simulated
annealing; Genetic algorithms; Differential evolution.

UNIT 5 [6 L]
Application of optimization in the design of separation process, chemical reactor and large
scale process plant.

Text Books and References: 1. Onwubolu, G.C.; Babu, B.V., “New Optimization
Techniques in Engineering; Springer-Verlag, Germany,
(2004).
2. Edgar, T.F., Himmelblau, D.M., Lasdon, L.S.,
“Optimization of Chemical Processes” second edition,
McGraw-Hill (2001).
3. Babu, B.V. “Process Plant Simulation”, Oxford University
Press, India (2004).
4. Jana A.K., “Chemical Process Modeling and Computer
Simulation” PHI, New Delhi (2011)
 8th Semester Syllabus
CH-18101: HAZARDS AND SAFETY IN CHEMICAL INDUSTRIES

L: T: P: Cr = 3:1:0:4

Objectives: To introduce awareness on the importance of plant safety and hazards analysis.
Introduction: Students learn about implementation of safety procedures, risk analysis and
assessment, fire and explosion models, hazard identification, HAZOP.
LESSON PLAN

UNIT-1: INTRODUCTION 4L
Safety terminology, Safety programs, Safety policy, Safety committee: structure and
functions, Psychological factors in industrial safety, Accident and loss statistics.

UNIT-2: INDUSTRIAL HYGIENE AND OCCUPATIONAL HEALTH 7L

Definition of Industrial Hygiene, Govt. regulations and evaluation, Concept of
threshold: TLV, OSHA, FAR, Fatality rate, Occupational health hazards:
toxicological studies, Dose versus response, Personal protective equipment (PPE),
Material safety data sheet (MSDS), Ergonomics: definition, aims andscope,
application ofergonomics in industry for safety, health andenvironment.
UNIT-3: PAST ACCIDENT ANALYSIS 6L
Past accident analysis of Flixborough, Bhopal gas tragedy, Three mile island
Chernobyl accident, Fukushima Daiichi,Port Wentworth, Pasadena,
Jacksonville,Feyzin disaster, Seveso accident analysis.
UNIT -4: FIRE AND EXPLOSION 6L
The fire triangle, Potable fire extinguishers, Effects of explosion, Explosions:
deflagration, detonation, TNT& TNO, Confine & unconfined explosion, Over
pressure, Flash fire, Jet fire, Pool fire, VCE, BLEVE, Fire ball.
UNIT-5: SAFETY MANAGEMENT 6L
Process safety management, Risk management and its tools, Safety health and
environment(SHE)management, Safety audit, Safety report: preparation
andassessment, Safety surveys and review,Emergency response and preparedness.

UNIT-6: HAZARD AND RISK ANALYSIS 7L

Hazard identification, Comprehensive risk analysis, Preliminary hazard analysis,
FMEA, HAZOP study, Checklists/ What if analysis, Event tree and fault tree
analysis, Hazards and their control in: textile industry, fertilizer industry and
petroleum refineries, etc.

Text Books and References: 1. K. V. Raghavan and A. A Khan, "Methodologies in Hazard

 Identification and Risk Assessment", Manual by CLRI.
2. V. C. Marshal, "Major Chemical Hazards", Ellis Hawood
Ltd., Chichester, United Kingdom.
3. Kletz, "Risk Analysis Hazops” Institute of Engineers, U.K.
4. Frank P. Less, "Loss Prevention in Process Industries", Vol.
I, II & III Butterworth, London
 CH-18102: PLANT DESIGN AND ECONOMICS

L: T: P: Cr = 3:1:0:4

Objectives: To impart information about overall plant design for a particular process for the
manufacture of particular product considering various aspects such as site
selection, plant layout, material of construction, and economic principles involved
in construction of a process plant.

LESSON PLAN

UNIT 1: Methods of Process Design [6L]

General design considerations, material and fabrication selection, hierarchy of chemical

process design, economic design criteria, nature of process synthesis and analysis.

UNIT 2: Cash Flow and Investments [8L]

Cash flow for industrial operations, factors effecting investment and production cost,
estimation of capital investments, cost factors in capital investment, production costs,
fixed charges, plant overhead costs, financing, interest and investment cost, present worth
and discount annuities, cost due interest on investment, taxes and insurances, type of
taxes.

UNIT 3: Depreciation and Profitability [8L]

Depreciation, types of depreciation, services life, methods for determining depreciation,

profitability, alternative investments and replacements, profitability standards, discounted
cash flow, capitalized cost, pay out period, alternative investments, analysis with small
investments, increments and replacements.

UNIT 4: Optimization of process flow sheets [9L]

Objectives, Introduction, General formulation of the optimization problem, Objective

function and decision variables, equality and inequality contraints, lower and upper
bounds Linear Programming, Non linear programming with a single variable.

UNIT 5: Process Integration [8L]

Process heuristics, sequences of ordinary distillation columns for ideal mixtures, Heat exchange
networks synthesis and utilities, energy targets.

Text Books and References: 1. M.S. Peters, K.D.Timmerhaus, “Plant Design and Economics
for Chemical Engineering”, McGraw-Hill, 1991.
2. W.D. Seider, J.D. Seader, D.R. Lewin, “Process Design
Principles: Synthesis, Analysis, and Evaluation”, John Wiley,
1999.
3. Perry's Chemical Engineer's Handbook, McGraw-Hill, 2007.
 Section - 2

SYLLABUS OF
PROFESSIONAL ELECTIVES
 Professional Electives – I & II

CH-17331: INTRODUCTION TO BIOCHEMICAL ENGINEERING

L: T: P: Cr = 3:1:0:4
Objectives: This course introduces the basic aspects of biochemical engineering and
bioprocess technology and their commercial implications to the students from
various disciplines.

LESSON PLAN
6L
UNIT-1: Introduction to microbiology and biochemistry, classification and characteristics of
microorganism, Essential chemicals of life - lipids, sugars and polysaccharides, RNA
and DNA, amino acids and proteins.
12 L
UNIT-2: Enzymes and their classification, enzyme kinetics, immobilization of enzymes and
whole cells, immobilized enzyme kinetics

10 L
UNIT-3: Cell metabolism, regulation, stoichiometry, end products, cell growth kinetics,
product formation kinetics, thermal death kinetics, media and air sterilization
5L

UNIT -4: Transport phenomena in cellular systems, oxygen transfer rates, mass transfer
coefficient and interfacial area, mechanical agitation and power requirement
8L

UNIT-5: Bioreactors: Type, design, operation and scale-up, instrumentation and control.
Down-stream processing, environmental concerns

Text Books and References: 1. J.E. Bailey, D.F. Ollis, “Biochemical Engineering Fundamentals”
2nd Ed., McGraw Hill International Edition, 1987.
2. M.L. Shuler, F.Kargi “Bioprocess Engineering: Basic Concepts” 2nd
Ed., Prentice-Hall, 2003
3. H.W. Blanch, D.S. Clark, “Biochemical Engineering” Marcel
Dekker, Inc., 1997.
4. P.F. Stanbury, A.Whitaker, “Principles of Fermentation
Technology,” 2nd edition, Elsevier, (1995)
 CH-17332: ALTERNATIVE ENERGY SOURCES

L: T: P: Cr = 3:1:0:4
Objectives: To impart information about alternative energy resources, their principles,
potential, limitations and to motivate them for search of new energy resources.

LESSON PLAN

UNIT-1: INTRODUCTION 5L
Definition, Concepts of non conventional energy resources, Criteria for assessing the
potential of NCES, Classification of NCES, Solar, Wind, Geothermal, Biomass,
Ocean energy sources, Limitations

UNIT-2: PRINCIPLES OF SOLAR RADIATION 8L

Definition, Energy available from Sun, Solar radiation data, solar constant,
extraterrestrial and terrestrial solar radiation, solar radiation on titled surface,
instruments for measuring solar radiation and sun shine, solar energy conversion into
heat
UNIT-3: SOLAR ENERGY CONVERSION 9L
Flat plate and concentrating collectors, classification of concentrating collectors,
orientation and thermal analysis, advanced collectors, solar storage and thermal
conversion, photovoltaic energy conversion

UNIT -4: WIND ENERGY 6L

Sources and potentials, horizontal and vertical axis windmills, performance
characteristics, Betz criteria

UNIT-5: OCEAN ENERGY AND GEOTHERMAL ENERGY 8L

Resources, types of wells, methods of harnessing the energy, potential in
India.OTEC, Principles utilization, setting of OTEC plants, thermodynamic cycles.
Tidal and wave energy: Potential and conversion techniques, minihydel power plants,
and their economics.

UNIT-6: NEW ENERGY SOURCES 4L

Cavitations Energy, Fuel Cells, Hydrogen, electrochemical energy conversion

Text Books and References: 1. G.D. Rai, NonConventional Energy Sources, Khanna Publishers.
2. Twidell&Wier, Renewable Energy Resources, CRC Press( Taylor &
Francis)
3. Ashok Desai V, Non-Conventional Energy, Wiley Eastern Ltd, 1990.
4. K.M., Mittal Non-Conventional Energy Systems, Wheeler
Publishing Co. Ltd, 1997.
5. R, Ramesh, K.U. Kurnar, Renewable Energy Technologies, Narosa
Publishing House, New Delhi, 1997.
 CH-17333: POLYMER SCIENCE AND TECHNOLOGY

L: T: P: Cr = 3:1:0:4
Objectives: To impart the knowledge of basic fundamental of polymer science and technology,
reaction engineering and manufacturing of polymers, processing of polymers into
plastics, fibers and elastomers.

LESSON PLAN
UNIT-1: CHARACTERISTICS AND ANALYSIS OF POLYMERS 8L
The science of large molecules, Theory of polymer solutions, Average molecular
weight, molecular weight distribution, Methods for determination of molecular
weight and size, Polymer degradation, Analyzing and testing of polymers.

UNIT-2: POLYMER MATERIAL STRUCTURE AND PROPERTIES 8L

Morphology in crystalline polymers, Polymer structure and physical properties,
mechanical properties of polymers.Reheologicalstudies: Deformation, flow and melt
characteristics, Temperature dependence of viscosity, Simple linear viscoelastic
models

UNIT-3: REACTION ENGINEERING 8L

Condensation and Addition polymers, Kinetics of step growth polymerization, radical
and ionic chain polymerizations, Co-polymerization, Coordination polymerization.

UNIT -4: INDUSTRIAL POLYMERS 8L

Polymerization techniques,Manufacturing processes and applications: Hydrocarbon
plastics, and elastomers, other carbon chain polymers, Thermosetting resins

UNIT-5: PROCESSING OF POLYMERS 8L

Plastics, fibers and elastomers: Extrusion, injection molding, blow molding,
Rotational molding, compression and transfer molding, thermoforming, spinning of
fibers.

Text Books and References: 1. F.W. Billmeyer, "Text Book of Polymer Science", 3rd Edn.,
Wiley Inter Science.
2. F. Rodriguez, "Principles of polymer systems", 4th Edn.,
Taylor and Francis, Washington.
3. “Encyclopedia of Polymers Science and Technology", John
Wiley-Inter Science.
4. J.R. Fried, “Polymer Science and Technology”, Prentice
Hall, Inc
 CH-17334: FOOD TECHNOLOGY AND ENGINEERING

L: T: P: Cr = 3:1:0:4
Objectives: To impart information about various food processes and unit operations for the
manufacture, packaging, preservation of food products considering various
aspects such as nutrition retention, stability and shell life.

LESSON PLAN
UNIT-1: FOOD PROCESS ENGINEERING -FUNDAMENTALS: 5L
Fundamentals of food process engineering, application of quantitative methods of
material and energy balance in food engineering practice.

UNIT-2: UNIT OPERATIONS IN FOOD INDUSTRY 10 L

Refrigeration and freezing, types of freezing, freezers, evaporation and dehydration
operations in food processing. Basic Principles of Food Preservation; Preservation of food by
removal or supply of heat, dehydration, irradiation, addition of chemicals and fermentation;
CA/MA storage; Water activity and food stability.

UNIT-3 FOOD CANNING TECHNOLOGY: 7L

Fundamentals of food canning technology, Heat sterilization of canned food, containers -
metal, glass and flexible packaging, Canning procedures for fruits, vegetables, meats,
poultry marine products.

UNIT-4: EXTRUSION AND RHEOLOGY 8L

Basics and Principles of Extrusion, Cold extrusion and extrusion cooking, Single and twin
screw Extruders, Introduction to rheology, types of fluids, Newtonian and non Newtonian
fluids, viscoelastic liquids and solids, burger model, creep test, types of rheometer

UNIT-5 IMPROVEMENT OF NUTRITIVE QUALITY: 8L

Process such as fortification, enrichment, germination fermentation, inactivation of
nutritional factors, stabilization of nutrients and increasing the availability of nutrient

Text Books and References: 7. 1. Food Microbiology by WC Frazier; Tata McGraw Hill, Delhi
8.
9. 2. Introduction to Food Engineering by R. Paul Singh, Dennis R.
3. Heid, J.L. and Joslyn, M.A.,5th ed., Academic Press, Elsevier.
10.
11. 3. Fundamentals of Food Processing Operation, The AVI
Publishing Co; Westport, 1967.
12.
13. 4. Food Process Engineering by Heldman, D.R., The AVI
Publishing Co; Westport, 1975.
14.
15. 5. Food Science by Potter, Norman N., Hotchkiss, Joseph H.,
Fifth Edition, Springer, 1995.
 CH-17335: FERTILIZER TECHNOLOGY

L: T: P: Cr = 3:1:0:4
LESSON PLAN

UNIT-1 : 7L
Importance of fertilizers for sustainable agricultural activities, Elements required for
plants growth, Classification of fertilizers industries in India, Role of co-operative
initiatives in fertilizer industry, General function of each of nitrogen, phosphorus, and
potassium fertilizers. Nitrogen fixation from the air.

UNIT-2: 8L
Processes for manufacturing of raw materials for nitrogen, phosphorus, and potassium
based fertilizers, viz. ammonia, nitric acid by ammonia oxidation process, phosphoric
acid from phosphate rock by strong sulphuric acid process, potassium chloride from
sylvinite. Mining of phosphate rock.

UNIT-3: 8L
Manufacturing of urea, biuret formation in urea synthesis, ammonium carbamate,
ammonium nitrate, ammonium sulphate, reactions involved and process conditions in
each of these fertilizers.

UNIT-4: 8L
Processes for manufacture of potassium nitrate, potassium sulphate, Recovery of
Potassium salts. Specification and storage of potassium chloride. Specification and
storage of potassium nitrate.

UNIT-5: 9L
Manufacturing of single super phosphate, triple super phosphate, calcium phosphate,
sodium phosphate, mono-ammonium phosphate, di-ammonium phosphate, bio-
fertilizers, plant growth promoting rhizobacteria, root colonization.

Text Books and References: 1. G. T. Austin, “Shreve’s Chemical Process Industries”,

McGraw-Hill, 1984.
2. L. J. Carpentire, "New Developments in Phosphate Fertilizer
Technology", Elsevier, 1971.
3. M. Sitting, M.G. Rao, “Dryden’s outlines of Chemical
technology”, East-West Press, 2010.
 CH-17336: TWO PHASE FLOW AND HEAT TRANSFER

L: T: P: Cr = 3:1:0:4
LESSON PLAN

UNIT-1: INTRODUCTION 6L
Introduction to two phase flow: type and applications,Flow Patterns in Adiabatic Flow,
Flow Pattern Transitions in Adiabatic Flow, Flow Patterns in Diabatic Flow, Void
Fraction and Slip Ratio, Methods of identifications for two-phase flow, Measurement
technique in two phase flow. Introduction to two phase flow problems in process industry.

UNIT-2: MODELING OF TWO-PHASE FLOW: 8L

Homogeneous Model/Drift Flux Model, Separate-Phase/ Two-Fluid Model, Models for
Flow Pattern Transition, Models for Bubbly Flow, Models for Slug Flow, Models for
Annular Flow, Models for Stratified Flow in Horizontal Pipe, Models for Transient Two-
Phase Flow.

UNIT-3: PRESSURE DROP IN TWO-PHASE FLOW: 8L

Local Pressure Drop, Analytical Models for Pressure Drop Prediction: Bubbly Flow, Slug
Flow, Annular Flow, Stratified Flow; Empirical Correlations for various flow types,
Pressure Drop in Rod Bundles, Pressure Drop in Flow Restriction.

UNIT-4: POOL BOILING HEAT TRANSFER: 8L

Introduction to two phase heat transfer, Modes of pool boiling, boiling curve, Heat
transfer mechanism in pool boiling: bubble nucleation, growth and departure from a
Heated Surface, Bubble emission Frequency, Waiting Period, Correlation of Nucleate
Boiling Data, Pool Boiling Crisis, Film Boiling in a Pool; Forced convection boiling,
Burnout.

UNIT-5: HEAT TRANSFER IN CONDENSATION: 6L

Type of condensation, Film condensation, Drop-wise condensation, Condensation on a
vertical plate, Condensation on tubes and spheres.

UNIT-6: ENHANCED HEAT TRANSFER: 4L

Introduction to enhanced heat transfer, Techniques for enhanced heat transfer: Active
Techniques, Passive techniques and compound techniques.

Text Books and References: 1. L. S. Tong and Y. S. Tang, “Boiling Heat Transfer and Two-
Phase Flow”, Second Edition, Taylor& Francis.
2. S. G. Kandlikar, "Handbook of Phase Change: Boiling and
Condensation" Taylor & Francis.
Jean J. Ginoux, Two phase flow and heat transfer.
3. Bergles, Collier & Hewitt, Two phase flow and heat transfer
 in the power and process industries.

16. CH-17337: ADVANCED PROCESS CONTROL

L: T: P: Cr = 3:1:0:4
17.
Objectives: The objective of this course is to provide a fundamental understanding to develop
a technology for chemical processes.

LESSON PLAN
UNIT-1 Frequency Response: 8L
Review of control system design in Laplace, time, and frequency domains, controller
design using Laplace, time and frequency response-Analysis of some common loops
Bode diagrams for Ist&IInd order system, Bode stability criteria, Zigler- Nichols and
Cohen-coon Tuning rules and Nyquist Plots

UNIT-2 Design of Controllers for Difficult & Complex Dynamics: 8L

Inverse response systems - controller design - design of inverse response compensator,
Time delay systems - controller design - Smith predictor method

UNIT-3 Complex Dynamics: 6L

Dynamics and Control of complex processes. Theoretical analysis of complex processes
like jacketed kettle, absorber and heat exchanger

UNIT-4 Multivariable Systems: 6L

Feed forward control, cascade and ratio control - Introduction to stage space methods-
Design of controllers using state-space methods - Introduction to multiloop systems-
Relative gain analysis.

UNIT-5 Controllers Design and Art of Process Control: 6L

Degrees of freedom analysis - Introduction to distillation system - Controller design for
mutliloop systems. Interaction and pairing of control loops, the art of process control.

UNIT-6 Design of Digital Controllers: 8L

Supervisory control systems-Digital computer control - sampling & filtering of
continuous measurements, Developments of discrete time models - Dynamic response of
discrete time systems. Analysis of sampled data control System-Design of digital
controllers.

Text Books and References: 1. D. E.Seborg, T.F. Edgar and D.A. Mellichamp, "Process
Dynamics Control", Wiley,3rdEd. 2013.
2. G Stephanopopulas, "Chemical Process Control", Prentice-Hall
India, 1984.
3. D. R. Coughanowr, "Process System Analysis and Control",
2ndEd. McGraw Hill, 1991.
4. Ogunnauike and W.H.Ray, "Process Dynamics, Modeling and
Control" Oxford Press.1994.
5. W.L.Luybin,“Process modeling, simulation and control for
 chemical Engineers” McGraw Hill,1973.

CH-17338: MATHEMATICAL METHODS IN CHEMICAL ENGINEERING

L:T:P = 3:1:0 = 4
Objectives: The present course aims to help the student to learn, different mathematical
technique to solve and analyze different classes of Chemical Engineering
problem.
Prerequisites: Knowledge of basic chemical engineering courses and general mathematics for
applying in chemical engineering problems.

LESSON PLAN
UNIT:1 [8 L]
Modeling, simulation, types of equation, vectors, metrics, norms, inner products, normed
linear space, dimension of vector spaces, applications, gram-schmidtortho-normalisation.

UNIT:2 [8 L]
Matrices, Eigenvalues, eigen vectors, Rayleigh’s quotient, linear algebric eq. ODE, IVP,
non self adjoint systems.

UNIT:3 [8 L]
Classification of PDE, boundary conditions, developing PDE in Chemical Engineering
systems, Infinite dimensional spaces, Fourier series, Cartesian coordinate, cylindrical &
spherical coordinate systems, Fourier series & finite Fourier transforms.

UNIT:4 [8 L]
Application on ODE & PDE, maximum principles, energy methods, Fredhalm alternative,
monotone iteration method, numerical analysis, method of continuation.

UNIT:5 [8 L]
Linear stability of a dynamic system, bifurcation theory, Landau-Hopf scenario, period
doubling cascades, Ruelle- Takens scenario, characteristic of trajectories.

Text Books and References: 1. S. Pushpavanam, “Mathematical Methods in Chemical

Engineering” PHI, New Delhi, 1998.
2. S K Gupta, “Numerical Methods for Engineers” New Age
International, New Delhi, 1995.
3. C.F. Gerald and P.O. Wheatley, “Applied Numerical Analysis”,
5th edition, Addison-Wesley, 1998.
4. K J Beers, “Numerical Methods for Chemical Engineering:
Applications in MATLAB”CambridgeUniv Press, 2006.
5. B. Wayne Bequette, “Process Dynamics Modeling, Analysis, and
Simulation,” Prentice-Hall-International, Inc., 1998.
18.
 CH-17339: INTERFACIAL SCIENCE AND ENGINEERING

L:T:P = 3:1:0 = 4
Objectives: This course is aimed at introducing the basic concepts and tools for the analysis
of colloidal and interfacial properties and their applications in adhesion,
particle-aggregation, wetting, detergency, oilrecovery, flotation, nucleation, bio-
surfaces, chromatography, paints, composite materials.
Prerequisites: Basic knowledge of physics and chemical engineering
LESSON PLAN
UNIT:1 [10L]
Effects of confinement and finite size; Concepts of surface and interfacial energies and
tensions; Apolar (van der Waals) and polar (acid-base) components of interfacial
tensions.Young-Laplace equation of capillarity; examples of equilibrium surfaces;
multiplicity, etc.Stability of equilibrium solutions; Contact angle and Young's equation;
Determination of a polar (vander Waals) and acid-base components of surface/interfacial
tensions.Free energies of adhesion; Kinetics of capillary and confined flows.

UNIT:2 Intermolecular, nanoscale and interfacial forces [10 L]

Van der Waals, Electrostatic double layer, Acid-base interactions including hydrophobic
attraction and hydration pressure.

UNIT:3 Mesoscale Thermodynamics, Mesoscale Phenomena in Soft Matter [8L]

Gibbs treatment of interfaces; concept of excess concentration; variation of interfacial
tensions with surfactant concentration.Adhesion, wetting, nucleation, flotation, patterning
of soft material by self - organization and other techniques.

UNIT:4 Stability of Nanoparticle Dispersions, Nanofluidics [8 L]

DLVO and DLVO like theories and kinetics of coagulation plus general principles of
diffusion in a potential field/Brownian movement.Stability of thin ( < 100 nm) films; self-
organization in confined systems; meso-patterning.

Unit:5 Advanced and Functional Interfaces [4 L]

Superhydrophobicity, functional coatings, structural colors, nano-adhesives;
nanocomposites.

Text Books and References: 1. Hiemenz, , Paul C. "Principles of Colloid and Surface
Chemistry", Marcel Dekker, any edition starting with the 2nd
edition, 1986.
2. Adamson, Arthur W. Physical Chemistry of Surfaces" Wiley,
5th edition, 1990.
3. Hunter, Robert J. "Foundations of Colloid Science",
Clarendon, Oxford, Volume 1, 1989.
4. Russel, W. B., Saville, D. A. andSchowalter, W. R.
''Colloidal Dispersions", Cambridge University Press, 1989.
5. Israelachvili, Jacob N.'' Intermolecular and Surface Forces'',
Academic Press, 1992 or later editions.
6. Oss, C. J. Van ''Interfacial Forces in Aqueous Media'',
 Marcel Dekker or Taylor & Francis, 1994.

CH-17340: BIOENERGY ENGINEERING

L: T: P: Cr = 3:1:0:4

LESSON PLAN
UNIT 1 [7L]
Biomass sources, characteristics & preparation, chemical composition and properties of
different biomass materials, energy plantations, pretreatment techniques for the utilization
of biomass, size reduction, briquetting of loose biomass, drying, storage and handling of
biomass.

UNIT 2 [7L]
Biogas technology, feedstock for biogas production, aqueous wastes containing
biodegradable organic matter, animal residues, microbial and biochemical aspects,
operating parameters for biogas production. Kinetics and mechanism,dry and wet
fermentation, digesters for rural application, high rate digesters for industrial waste water
treatment.

UNIT 3 [8L]
Bio-ethanol and bio-diesel technology: production of fuel ethanol by fermentation of
sugars, gasohol as a substitute for leaded petrol, trans-esterification of oils to produce bio-
diesel.

UNIT 4 [9L]
Pyrolysis and gasification of biomass, thermo-chemical conversion of ligno-cellulose
biomass, biomass processing for liquid fuel production, pyrolysis of biomass, pyrolysis
regime, effect of particle size, temperature, and products obtained. Thermo-chemical
gasification principles, effect of pressure, temperature and of introducing steam and
oxygen, design and operation of fixed and fluidized bed gasifiers.

UNIT 5 [9L]
Combustion of biomass and cogeneration systems, theory, calculations and design of
equipments, cogeneration in biomass processing industries. Case studies: combustion of
rice husk, use of bagasse for cogeneration.

Text Books and References: 1. A.Chakraverthy, “Biotechnology and Alternative

Technologies for Utilization of Biomass or Agricultural
Wastes”, Oxford & IBH publishing 1989.
2. K.M. Mital, “Biogas Systems: Principles and Applications”,
New Age International Publishers Pvt. Ltd., 1996.
3. D.L. Klass, G.M. Emert, “Fuels from Biomass and Wastes”,
Ann Arbor Science Publication, 1985.
19.
 CH-17341: ELECTROCHEMICAL ENGINEERING

L: T: P: Cr = 3:1:0:4

Objectives: To impart necessary basic knowledge in order to understand, analyze and solve
problems related to electrochemical processes.
Introduction: Students will learn and have the knowledge on electrical double layer,
Electrocatalysis and different typesof electrochemical techniques.The students
will have a practical ability to analyze electrochemical design models, thermal
behavior of reactors and electrochemical reactors.

LESSON PLAN

UNIT-1: INTRODUCTION TO ELECTROCHEMICAL ENGINEERING 5L

Introduction, Methods of measurement - Steady state techniques, Non-steady state
techniques, Eliminating IR drop.
UNIT-2: ELECTROCHEMICAL TRANSFER PROCESS 6L
Electrochemical transfer processes, Mass transport, Charge transport and heat
transfer.
UNIT-3: ELECTROCHEMICAL REACTION ENGINEERING 6L
Electrochemical thermodynamics and electrode kinetics, Kinetics in electrochemical
Reactors.
UNIT -4: SEPARATION PROCESSES IN ELECTROCHEMICAL CELLS 5L
Separation Systems in electrochemical cells, Materials and corrosion

UNIT-5: THERMAL BEHAVIOR OF REACTORS 6L

General aspects of thermal behavior in electrochemical reactor, Thermal behavior
under CSTR conditions, the estimation of heat losses; the thermal behavior under
PFR conditions; Thermal behavior of batch electrochemical reactors.

UNIT-6: ELECTROCHEMICAL TECHNIQUES 6L

Ion selective electrodes: Principles of potentiometry and
amperometry,Potential step method (chronoamperometry) under diffusion
control derivation of Cottrellequation for a planar and spherical electrode.

Text Books and References: 1. J.C. Kuriakose and J. Rajaram, Chemistry in Engineering and
Technology, Vol.1 & 2, Tata McGraw Hill Publishing Company (P)
Ltd., New Delhi, 1996.
2. Geoffrey A., Electrochemical Engineering Principles, Prentice hall
publications
3. Allen J. Bard and Larry R. Faulkner, Electrochemical Methods:
Fundamentals and Applications
4. Carl H. Hamann, Andrew Hamnett and Wolf
VielstichElectrochemistry , Wiley publications
 CH-17342: INDUSTRIAL CATALYSIS

L: T: P: Cr = 3:1:0:4

LESSON PLAN

UNIT-1 INTRODUCTION TO CATALYSIS: 4L

General properties of homogeneous and heterogeneous catalysis, Classification of catalysts
and supports.

UNIT-2 GEOMETRIC AND ELECTRONIC FACTORS IN CATALYSIS: 6L

Adsorption and reaction kinetics in catalytic (heterogeneous) system.

UNIT-3CATALYST PREPARATION: 6L
Preparation and evaluation of industrial catalysts.

UNIT-4 KINETICS OF HETEROGONOUS REACTIONS: 8L

Reaction engineering applied to catalytic homogeneous and heterogeneous chemical
reactions. Theories of heterogeneous catalysis

UNIT-5 CATALYST POISONING: 6L

Catalyst poisoning and deterioration (sintering) origination of catalyst.

UNIT-6 ELECTRO CATALYSIS AND FUEL CELL: 8L

Photo catalysis for the removal of air and water pollutants and conversion of solar energy,
Polyfuctional catalysts.

Text Books and References: 1. Fundamentals of Industrial Catalytic Processes by C. H.

Bartholomew, Robert J. Farrauto , Wiley-AIChE; 2 edition
2. Concepts of Modern Catalysis and Kinetics by I. Chorkendorff,
J. W. Niemantsverdriet , Wiley-VCH; 2nd edition
3. Handbook of Industrial Catalysts by Lloyd, Lawrie, Springer
publications
4. Industrial Catalysis: A Practical Approach by Jens Hagen,
Wiley-VCH; 2 edition
20.
 Professional Elective – III & IV

CH-1831: INTRODUCTION TO NANOTECHNOLOGY

L: T: P: Cr = 3:1:0:4

Objectives: The objective of this course is to make students familiar with the basic
fundamental of nanotechnology, important concepts in Nanotechnology and its
applications.
Introduction: Enabling the students to learnthe properties behaviour, implementation of
nanotechnology and synthesis of nonmaterial for the future developments

LESSON PLAN

UNIT-1: FUNDAMENTALS AND OVERVIEW OF NANOSCIENCEOF 6L

NANOTECHNOLOGY
Definitions, history and current practice, Properties of nano-particles, Overview of
current industry applications, Nano-scale science and engineering principles.Different
classes of nano-materials:Metal and semi-conductor nanomaterials, Quantum dots,
Wells and wires, Molecule to bulk transitions, Bucky balls and Carbon nanotubes.

UNIT-2: CARBON NANOSTRUCTURES 6L

Carbonmolecules, Carbon clusters, Carbon nanotube technologies (CNT): Carbon
nano-tube applications, Fabricating carbon nano-tubes and nano-wall structures, Key
applications of CNT.
UNIT-3: SYNTHESIS OF NANOMATERIALS 6L
Top-down (Nanolithography, CVD), Bottom-up (Sol-gel processing, chemical
synthesis), Physical Vapor deposition, Wet deposition techniques,Self-assembly
(Supramolecular approach), Molecular design and modeling.

UNIT -4: CHARACTERIZATION 5L

TEM, SEM and AFM technique, Fluorescence Microscopy and Imaging

UNIT-5: NANOFABRICATION 5L
Nanolithography, Thin film processes, semiconductors, MEMS:Overview and history
of development, Industry applications: Challenges and future development.

UNIT-6: APPLICATIONS 5L
Solar energy conversion and catalysis, Molecular electronics and printed electronics,
Liquid crystalline systems, Linear and nonlinear optical and electro-optical properties,
Applications in displays and other devices, Advanced organic materials for data
storage, Photonics, Plasmonics, Chemical and biosensors, Nano-medicine and Nano-
biotechnology.

Text Books and References: 1. Hari Singh Nalwa, “Nanostructured Materials and
Nanotechnology”, Academic Press, 2002
2. A.Nabok, “Organic and Inorganic Nanostructures”, Artech House,
2005
3. C.Dupas, P.Houdy, M.Lahmani, Nanoscience: “Nanotechnologies
 and Nanophysics”, Springer- Verlag Berlin Heidelberg, 2007
4. Charles Poole,Introduction to Nanotechnology, Frank Owens, Wiley
India Pvt Ltd 2007.
5. Lynn E. Foster, Nanotechnology Pearson Released: 2007

CH-18332: INTRODUCTION TO PROCESS INTENSIFICATION

L:T:P = 3:1:0 = 4
Objectives: This course is aimed to provide the knowledge leading compact, safe, energy-
efficient and environment-friendly novelequipments and processes.

LESSON PLAN
UNIT I [6 L]
Need of process intensification, process intensifying equipments and methods, examples of
their application on the commercial scale.
NIT II [10 L]
Use of high gravity fields, higee reactor, spinning disc reactors,micro-channel heat exchangers.

UNIT III [10 L]

Monolithic catalyst and reactors,reverse flow reactor, micro-reactors.

UNIT IV [10 L]
Concept and principle, reactive- distillation, extraction, precipitation adsorption,
absorption, fermentation-pervaporation, adsorptive distillation, membrane reactors and
bioreactors.

UNIT V [4 L]
Industrial practice (methodology, application) PI by improvement in existing plant and
process synthesis, pi by plants safety.

Text Books and References: 1. Stankiewicz,A.;Moulijn, J.A. “Re-engineering the chemical

processing plant: process intensification” Marcel Dekker,
Inc., New York, 2004.
2. Mizrahi,J. “Developing an industrial chemical process: an
integrated approach” CRC Press, 2002.
3. Keil,F.J.“Modeling of Process Intensification” Wiley-VCH
Verlag Germany, 2007
4. Reay,D.;Ramshaw,C.; Harvey, A.“Process
Intensification”Elsvier, 2013
5. Boodhoo,K.; Harvey,A. “Process Intensification for Green
Chemistry”, Wiley, 2013.
21.
 CH-18333: ADVANCE SEPARATION PROCESSES

L: T: P: Cr = 3:1:0:4
Objectives: To impart the knowledge of advance separation techniques such as membrane
separation, advance adsorption, chromatography, Thermal separation, adductive
and advanced crystallization and foam separation.

LESSON PLAN

UNIT 1: MEMBRANE SEPARATION PROCESSES: [15 L]

Principle,classification, structure& characteristics of membranes, membrane modules and
application, reverse osmosis, ultrafiltration, microfiltration, nanofiltration, dialysis, gas
separation and pervaporation processes, ion selective membranes and their application in
electro-dialysis, liquid membranes, membrane reactors.

UNIT 2: ADSORPTION TECHNIQUE: [8L]

Adsorbents, molecular sieves, Single component adsorption and multi component
adsorption equilibrium calculation, Langmuir, BET and Gibbs isotherms, pressure and
temperature swing adsorption techniques, parametric Pumping: Batch, continuous and
semi-continuous pumping, thermal, pH and heatless parametric pumping.

UNIT 3: CROMATOGRAPHY SEPARATION: [5L]

Principle, classification and techniques of chromatography, chromatographic column,
development of gradient-elution separations, equipment and commercial processes.

UNIT 4: THERMAL SEPARATION: [4L]

Thermal diffusion: basic rate law, theory of thermal diffusion phenomena for gas and
liquid mixtures, equipments design and applications, zone melting: equilibrium diagrams.

UNIT 5: ADDUCTIVE AND EXTRACTIVE CRYSTALLIZATION: [4 L]

Molecular addition compounds, Clathrate compounds and Adducts; Equipments;
Applications.

UNIT 6: FOAM AND BUBBLE SEPARATION: [4L]

Principle, Classification and separation techniques, surface adsorption, Nature of foams,
apparatus, Applications and Controlling factors.

Text Books and References: 1.H.M. Schoen, “New Chemical Engineering Separation
Techniques", Inter Science Publications New York.
2. C. Loeb, R. E. Lacey, "Industrial Processing with Membranes",
Wiley Inter Science.
3. J.M. Coulson, J.F. Richardson, "Chemical Engineering", Vol.-
2, Butterworth - Heinemann London.
4. J.D. Seader, E.J. Henley, "Separation Process Principles”,
John wiley& Sons Inc,
5. K. Sattler, H. J. Feindt, “Thermal Separation Process”, VCH
6. J. J. Mketta, "Unit operation Handbook” (vol-1,
MassTransfer),CRC Press.
7. R.W. Rousseau, “Handbook of separation Process
Technology”, Wiley-India.
22.
 CH-18334: PROCESS MODELING AND SIMULATION

L: T: P: Cr = 3:1:0:4
LESSON PLAN
UNIT-1: 8L
Introduction to modeling and simulation, classification, Uses of mathematical models,
Principles of model formulation, Fundamental laws- continuity equation, energy equation,
equations of motion, Transport equations, equations of state, equilibrium and kinetics,
Introduction to process simulators and mathematical tools.

UNIT-2: 6L
Numerical solution of model equations with linear and non linear algebraic equations in
one and more than one variables, ordinary differential equations in one and more than one
variables

UNIT-3: 6L
Numerical solutions of model equations with partial differential equations using finite
difference method, Model parameters estimation: Introduction, method of least squares,
curve fitting, etc.

UNIT-4: 7L
Lumped Parameter Models: Formulation and solution techniques for vapor-liquid
equilibrium models, batch and continuous distillation column, mixing tank, stirred tank
with heating, CSTR with multiple reactions. N- CSTRs in series, Non-isothermal CSTR.

UNIT-5: 7L
Steady State Distributed Parameter Models: Formulation and solution of split boundary
value problems - shooting technique, quasi-linearization techniques, counter current heat
exchanger, tubular reactors.

UNIT-6: 6L
Unsteady State Distributed Parameter Models: convective problems, diffusive problems,
combined convective and diffusive problems.

Text Books and References: 1. K. M. Hangos and I. T. Cameron, “Process Modeling and
Model Analysis”, Academic Press, 2001.
2. W.L. Luyben, “Process Modelling, Simulation and Control for
Chemical Engineers”, 2nd Edn., McGraw Hill Book Co., New
York, 1990.
3. W. F. Ramirez, “Computational Methods for Process
Simulation”, Butterworths, 1995.
4. Process Dynamics: Modeling, Analysis and Simulation, B
Wayne Bequette, Prentice Hall. International Inc.
5. Computational Methods for Process Simulation, 2nd ed., W F
Remirez, Butterworth-Heinemann.
6. Roger E. Franks, “Modeling and Simulation in Chemical
Engineering”, JohnWiley and Sons, 1972.
7. Mark E. Davis, “Numerical Methods and Modeling for
Chemical Engineers”, John Wiley & Sons, 1984.
8. Singiresu S. Rao, “Applied Numerical Methods for Engineers
and Scientists” Prentice Hall, Upper Saddle River, NJ, 2001
9. Seinfeld and Lapidus, “Mathematical Methods in Chemical
Engineering”, Prentice Hall, 1974.
 23.
CH-18335: INTRODUCTION TO MULTIPHASE FLOW

L: T: P: Cr = 3:1:0:4
LESSON PLAN
UNIT- I: Flow past immersed bodies: 6L

Drag and drag coefficients, flow through beds of solids, motion of particles through
fluids, fluidization, types of fluidization and applications.

UNIT-2: Two-phase flow: 4L

Two–phase flow through pipes, Lockhart-Martinelli parameters and their application in

analysis of two-phase flows.

UNIT-3: Interaction of fluids: 6L

Mixing of a single fluid; degree of segregation, early and late mixing of fluids, models for
partial segregation, mixing of two miscible fluids, Gas-liquid flow phenomenon, Types of
regimes formation – trickle, pulse, bubble, dispersed bubble, spray regime etc.

UNIT-4: Types of Multiphase-Reactors: 8L

Various types of multiphase reactors e.g. packed bed, packed bubble column, trickle bed
reactor, three phase fluidized bed reactor, slurry bubble column, stirred tank reactor.
Characteristics of above mentioned reactors such as; fluid flow phenomena and flow
regimes, flow charts/ correlations, pressure drop, liquid hold up etc, Reactors involving
Newtonian and non-Newtonian fluids.

UNIT-5: RTD in Multiphase Flow systems: 9L

Non Ideal Flow: Residence time distribution of fluid in vessel, E, F & C Curve, Mean and
variance, the Dirac delta function, residence time, linear and non-linear processes, models
for non ideal flow, dispersion model, N tanks in series model, model for small deviations
from plug flow and long tails, conversion in a reactor using RTD data, diagnosing ills of
operating multiphase reactors, models for multiphase reactors, Two parameter model, PD
model, three parameter models, PE Model.

Text Books and References: 1. Levenspiel O, “Chemical Reaction Engineering”, 3rd Ed, John
Wiley & Sons, Singapore (1999).
2. Fogler H Scott, “Elements of Chemical Reaction Engineering”,
3rd ed, Prentice Hall Inc. (1999).
3. Shah Y.T., “Gas-Liquid-Solid Reactor Design”, McGraw Hill
Int. New York, 1979.
4. Westerterp K.R., van Swaaij W.P.M., and Beenackers A.A.C.M.,
“Chemical Reactor Design and
Operation”, John Wiley & Sons, 1993.
5. Doraiswamy L.K., and Sharma M.M., “Heterogeneous
Reactions: Volume 2 Fluid- Fluid-Solid Reaction”, John Wiley
& Sons, 1984, Singapore.
24.
 CH-18336: ENERGY ENGINEERING

L: T: P: Cr = 3:1:0:4
LESSON PLAN
UNIT-1: Coal 6L
Classification, properties, washing and storage, combustion, carbonization, liquefaction
and gasification, briquetting of pulverized coal, proximate and ultimate analysis, merits
and demerits of solid, liquid and gaseous fuels.

UNIT-2: Liquid fuels 8L

Properties, handling, storage and transportation, combustion characteristics and associated
problems, fuel specification and standards, Origin of petroleum, classification and
refining of crude petroleum, knocking, octane rating and cetane rating of fuels ,Gaseous
fuels: Manufacture, properties and characteristics of natural gas, CNG, LPG, coal gas,
coke oven gas, producer gas and water gas

UNIT-3: Alternate energy sources 7L

Biomass combustion and pyrolysis, bio-gas production, Solar energy- Flat plate collector,
analysis and construction of solar water heater, solar pond, solar desalination and solar
space heating and cooling. Geothermal energy sources and their harnessing, energy from
wind and tides, energy storage and distribution

UNIT-4: Combustion process 6L

Nature of combustion, mechanism of combustion reactions, chain reaction – hydrogen-
oxygen reaction, velocity of flame propagation, limits of inflammability, structure of
flame, kinematics of liquid and solid fuel combustion.

UNIT-5: Energy conservation measures 5L

Waste heat recovery, use of low grade hot streams, condensate and flue gases,
improvement in heat energy, steam trap

UNIT-6: Energy auditing 8L

Mapping of distribution of energy supply and demand in a chemical plant, identification
of energy intensive areas, energy auditing and acts.

Text Books and References: 1. Fuel and Combustion – Smith N.L. &Stainson K.W.
2. Principles of Solar and Energy Handbook: Kreider J.F., Frank
and Kreith, F
3. Unconventional energy sources: G.D. Rai, Khanna Publishers.
4. Renewable Energy Resources: John Twidell and Tony Wein
5. Industrial Energy Conservation: A hand book for engineers
and managers - Reay D.A.
6. Fuels & Combustion: Samir, Sirkar, Orient Longman Pub. 2nd
ed. Mumbai.
7. Solar Energy Engineering – S.P. Sukhatma, 2nd ed, TMH Pub,
Ltd. New Delhi
 8. Fuels Combustion & Refractory- O.P.Gupta,
KhannaPublishers .
25.
CH-18337: SCALE-UP IN PROCESS INDUSTRIES

L: T: P: Cr = 3:1:0:4
LESSON PLAN

UNIT-1: Introduction [4 L]
Introduction to pilot plants and Models, Process Development, Process study, the principle
of similarity and similarity criteria

UNIT-2: Pilot Plants and Plant Models [8 L]

Dimensional analysis and its application in scaling-up or scaling-down the chemical
process plant, Project engineering, Practical consideration; Safety considerations,
successful plant operations and case studies.

UNIT-3: Mathematical Equations [8 L]

Mathematical Equations representing the Mechanical, Thermal, Diffusional and chemical
processes and derivation of the dimensionless groups from these differential equations.Rate
of chemical reaction of Homogeneous and Heterogeneous chemical reactions.

UNIT-4: The Regime Concept [8 L]

The Regime Concept, Laupichleir's study of catalytic water gas reaction, chemical dynamic
and mixed regime, Effect of temperature on physical and chemical reactions. Similarly
criteria for the principle types of regime and scale equations.

UNIT-5 Scale up of Heat Transfer Equipments [6 L]

Scale-up methods for Heat-Transfer equipment e.g.-Heat Exchangers, Steam or vapor
Heaters, Evaporators, Condensers and Coolers.

UNIT-6 Scale up of Miscellaneous Equipment [8 L]

Scale-up methods for mixing equipment and other miscellaneous equipment used in
chemical process industries.

Text Books and References: 1. R.E. Johnstone and M.W. Thring, "Pilot Plants, Models and
Scale-up methods in Chemical Engineering ", McGraw Hill
Book Company, New York, 1957.
2. Bisio&Kabel, "Scale-up in Chemical Industry".
3. D.G. Jordan, "Chemical Process Development", Vol. I & II,
Interscience Publishers, 1988.
26.
 CH-18338: SOLID WASTE MANAGEMENT

L: T: P: Cr = 3:1:0:4

LESSON PLAN
UNIT 1 [8L]
Philosophy and organization, status of solid waste management, composition of an
integrated waste management strategy, evolution of solid waste management, legislation
and government agencies.

UNIT 2 [8L]
Types of solid waste, Sources of solid waste, physico-chemical properties of solid waste,
materials flow in society, reduction in raw materials usage, reduction in solid waste
quantities, reuse of solid waste materials,

UNIT 3 [8L]
Generation of solid waste, onsite handling, storage, and processing, collection of solid
wastes, transfer and transport, processing techniques and equipment, hazardous waste and
their management, process management issues.

UNIT 4 [8L]
Recovery of resources from solid waste, Energy recovery methods: chemical and biological
methods.Land filling, ocean disposing, source reduction, recycling, incineration,
composting.

UNIT 5 [8L]
Case studies on major industrial solid waste generation units,coal fired power plant, textile
industry, brewery, distillery, oil refinery. Use of refuse-derived fuels.

Text Books and References: 1. G. Tchobanoglous, H.Theisen, R.Eliassen, “Solid Wastes:

Engineering Principles and Management Issues”, McGraw-
Hill, 1977.
2. H.S. Peavy, D.R. Rowe, G. Tchobanoglous, “Environmental
Engineering”, McGraw-Hill, 1985.
3. S. K. Garg, R. Garg, R. Garg, “Environmental Science and
Ecological Studies”, Khanna Publishers, 2006.
27.
 CH-18339: INDUSTRIAL CORROSION AND SURFACE COATING

L: T: P: Cr = 3:1:0:4

LESSON PLAN

UNIT-1 INTRODUCTION: 10L

Survey of paint industry and its scope in India.Pigments and their classification. Methods
of manufacture: white, colored, metallic and luminous pigments.

UNIT-2 CLASSIFICATION OF PAINTS: 10L

Oil, emulsion, and water soluble paints and their manufacturing processes; Drying oils;
Natural and synthetic resins; Solvents and plasticizers.

UNIT-3 DEFINITION AND CLASSIFICATIONOF VARNISH: 10L

Oleoresinious and spirit varnishes; Manufacture of different types of varnishes. Ceramic
coating: Glazing and enameling.

UNIT-4 METALLIC COATING: 10L

Electroplating, Galvanizing, Tinning, Polymeric coating; Protective and decorative
coatings, Powder Coating.

Text Books and References: 1. Noel, H., “Out of Paint Technology”, Charles Griffin and
Co., Ltd.
2. Morgans, W.M., “Outlines of Paint Technology”, Vol.I,
Charles Griffin and Co.
3. Bidlack, C. and Edgar W. P., “Paints and Varnish Production
Manual”, Chapman & Hall Ltd.
4. Turner, G.P.A., “Introduction to Paint Chemistry Principles
of Paint Technology”, Oxford University Press.
28.
 CH-18340: INDUSTRIAL ENZYME ENGINEERING AND FERMENTATION
TECHNIQUES
L: T: P: Cr = 3:1:0:4

LESSON PLAN

UNIT-1 BASIC CONCEPTS OF ENZYME: 6L

Mechanism of Enzyme Action and kinetic of reaction: Concept of active sites, and energetic
of enzyme substrate complex formation, Specificity of enzyme action, Estimation of
Michaelis-Menten Parameter

UNIT-2 STABILITY OF ENZYMES: 6L

pH, Temperature, Mechanical forces, Heterogeneous system.

UNIT-3 PRODUCTION AND PURIFICATION OF ENZYMES: 8L

Extract from plant, animal and microbial sources, Methods of characterization of enzymes,
Development of enzymatic assays.

UNIT-4 ENZYME IMMOBILIZATION: 8L

Physical and chemical techniques for enzyme immobilization adsorption, Matrix entrapment,
Encapsulation, cross linking, covalent binding, Advantages and disadvantages of different
immobilization techniques.

UNIT-5 APPLICATIONS OF ENZYMES: 6L

Classification of enzymes, Commercial application of enzymes in food, Pharmaceutical and
other industries, Enzymes for analytical and diagnostic application.

UNIT-6 MASS TRANSFER EFFECTS IN IMMOBILIZED ENZYMES: 6L

Analysis of film and pore diffusion effects on kinetics of immobilized enzyme reaction,
Formulation of dimensionless groups, Calculation of effectiveness factors

Text Books and References: 1. Price N C and Stevens L, “Fundamentals of Enzymology: The
Cell and Molecular Biology of Catalytic Proteins”, 3rd Edition,
Oxford University Press (2003).
2. Bailey and Ollis, “Biochemical Engineering Fundamentals”,
McGraw Hill (1996)
3. Lehninger, A L “Principles of Biochemistry”, Butterworth
Publishers, New York (1993)
4. Conn E E and Stump P K,“Outlines of Biochemistry” John
Wiley and Sons, New York (1987)
5. Stanbury P F and Whitaker A, “Principles of Fermentation
Technolgy”, Pergamon Press (1995)
29.
 CH-18341: ADVANCES IN FLUIDIZATION ENGINEERING
L: T: P: Cr = 3:1:0:4

LESSON PLAN

UNIT 1 [7L]
Introduction to fluidization, types of fluidization, industrial applications of fluidized beds,
cracking and reforming of hydrocarbons, gasification, carbonization, gas - solid reactions.

UNIT 2 [8L]
Gross behavior of fluidized bed, minimum and terminal velocities in fluidized beds,
design of distributors, voidage in fluidized beds, variation in size distribution with height,
viscosity and fluidity of fluidized beds, power consumption, bed expansion.

UNIT 3 [8L]
Davidson's model, frequency measurements, bubble behavior, bubbles in ordinary
bubbling bed model for bubble phase,emulsion phase, experimental findings, bubbling
bed model for emulsion phase interchange co-efficient.

UNIT 4 [8L]
Flow pattern of gas through fluidized beds, bubbling bed model for gas inter-change
interpretation of gas mixing data, heat and mass transfer between fluid and solid,
experiment findings on heat and mass transfer, heat and mass transfer rates from bubbling
bed model.

UNIT 5 [9L]
Heat transfer between fluidized beds and surfaces, theories of bed heat transfer,
comparison of theories, model for entrainment and application of the entrainment model
to elutriation.Principles of semifluidization, production of various bed parameters,
industrial applications,design of fluidized bed reactors.

Text Books and References: 1. D. Kunii, O.Levenspiel, “'Fluidization Engineering”, John

Wiley& Sons, 1992.
2. J.F. Davidson, D. Harrison, “Fludization”, Academic Press,
1971.
3. C. K. Gupta, D. Sathiyamoorthy, “Fluid Bed Technology in
Materials Processing”, CRC Press, 1998.
4. F.A. Zenz, D.F. Othmer, “Fludization and Fluid Particles
Systems”, Reinhold Publishing, 1960.
30.
 CH-18342: UPSTREAM HYDROCARBON ENGINEERING

L: T: P: Cr = 3:1:0:4

LESSON PLAN

UNIT 1 [8L]
World exploration and production (E&P) scenario, Indian exploration and production
(E&P) scenario, petroleum Exploration basics, concept of source, reservoir, migration,
stratigraphic and combinational traps, primary and secondary migration, techniques of
petroleum exploration, geochemical, gravity, magnetic, electrical and seismic method of
hydrocarbon exploration.

UNIT 2 [8L]
Basics of drilling fluid, functions of drilling fluid, classification of drilling fluids, properties
of drilling fluids, nature of drilling fluid, generic drilling fluid system. Drilling fluids
equipment related to pressure and separation. Formulations of drilling fluid, separation of
drilled solids from drilling fluid, various rheology models of drilling fluids.

UNIT 3 [8L]
Bulk volume, grain Volume, effective pore volume and net volume, porosity,
compressibility, Darcy’s Law. Absolute and Effective Permeability, Permeability
averaging, Transmissibility, Measurements of Permeability heterogeneity, Darcy’s law of
directional permeability, rock fluid interactions.

UNIT 4 [8L]
Enhanced oil recovery methods,correlation of capillary pressure to rock
properties,wettability, capillary pressure, equivalent height and transition zone, mobility,
relative mobility and flow capacity.

UNIT 5 [8L]
Composition of natural gas, properties, fields & reserves in world and in India, energy
scenario, major natural gas producing industries of India and their contribution to Indian
economy, techniques of utilization, specifications of natural gas for transportation in
pipelines, concept of gas to liquid (GTL).

Text Books and References: 1. J. J. Milson, A. Eriksen, “Field Geophysics”, John Wiley and
Sons, 2011
2. J. W. Amyx, D.H. Bass, R. L.Whiting, “Petroleum Reservoir
Engineering”, McGraw Hill, 1960.
3. D. L. Katz, R. L. Lee, “Natural Gas Engineering-Production
and Storage”, McGraw-Hill, 1990.
4. W.L. Nelson, “Petroleum Refinery Engineering”, McGraw
Hill Publication, 1958.
5. G.D. Hobson, W. Pohl, “Modern Petroleum Technology”,
Wiley & Sons Publication, 1973.
31.