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Adv 96 Int 11

The document discusses the performance and testing of various PLOT columns, including porous polymer and molecular sieve 13X zeolite columns, for analyzing light hydrocarbons and permanent gases. It highlights the importance of reproducibility, selectivity, and efficiency in column performance, detailing the testing methods and parameters used. Additionally, it provides specific product information and catalog numbers for different column types offered by Restek Corporation.

Uploaded by

Andrey Kovaltchuk (Indukoff)
Copyright
© © All Rights Reserved
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Download as PDF, TXT or read online on Scribd
13 views1 page

Adv 96 Int 11

The document discusses the performance and testing of various PLOT columns, including porous polymer and molecular sieve 13X zeolite columns, for analyzing light hydrocarbons and permanent gases. It highlights the importance of reproducibility, selectivity, and efficiency in column performance, detailing the testing methods and parameters used. Additionally, it provides specific product information and catalog numbers for different column types offered by Restek Corporation.

Uploaded by

Andrey Kovaltchuk (Indukoff)
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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available with the Q porous polymer or film and to calculate the number of plates

Molecular sieve 13X zeolite. Figure 2 per meter.


shows the analysis of light hydrocarbons PLOT
on a n MXT"-Q PLOT column and the Restek’s expanding line of PLOT columns
analysis of permanent gases on an MXT"- continue to bridge the gap from packed to
Columns
Msieve 13X PLOT column. capillary columns. Through continuing re-
search Restek now offers unbreakable and
COLUMN TO COLUMN REPRO- particle free porous Layer Open Tubular
Rt-S
DUClIBlLITY GUARANTEED capillary columns for the analysis of per- (fused silica)
Each porous polymer PLOT column is manent gases, light hydrocarbons and vola- 30m, 0.53mm ID cat.# 19712
tested with a hydrocarbon test mix to in- tile chemicals. 15m, 0.53mm ID cat.# 19713
sure proper phase thickness and selectiv- 30m, 0.32mm ID cat.# 19710
ity. Propane is used to calculate the parti- 15m, 0.32mm ID cat.# 19711
tion ratio which is monitored to insure a
reproducible film thickness. The number
of plates per meter is calculated and used Rt-Q
to evaluate column efficiency. Selectivity (fused silica)
is ensured by calculating the retention in- 30m, 0.53mm ID cat.# 19716
dices of acetylene and methyl acetylene. 15m, 0.53mm ID cat.# 19715
30m, 0.32mm ID cat.# 19718
Molecular sieve PLOT columns are all 15m, 0.32mm ID cat.# 19717
tested with a mixture of permanent gases.
In this test the peak height ratio of carbon
monoxide is used to determine a uniform
MXT"-Q
(SilcosteeP)
30m, 0.53mm ID cat.# 79716
15m, 0.53mm ID cat.# 79715
Figure 2 - MXT" PLOT columns give fast, efficient
separation of light hydrocarbons & permanent gases.
Rt-Msieve 13X
(fused silica)
30m, 0.53mm ID cat.# 19706
1. methane 15m, 0.53mm ID cat.# 19708
1. hydrogen
2. ethylene
3. acetylene
2. oxygen 30m, 0.32mm ID cat.# 19705
3. nitrogen 15m, 0.32mm ID cat.# 19707
4. ethane
4. methane
5. propylene
5. carbon monoxide
6. propane

MXT"-Msieve 13X
(Silcosteel")
4 5 30m, 0.53mm ID cat.# 79706

min. 1 min. 1
=k=-L
2 3
15m, 0.53mm ID cat.# 79708

30m, 0.53mm ID MXT-Q (cat.# 797 16) 30m, 0.53mm ID MXT-Msieve 13X (cat.# 79706)
100ul hydrocaro n 20u1 split inj. of permanent gases.
Rt-Alumina
Oven temp.: 50C isothermal Oven temp.: 40C isothermal (fused silica)
Inj. & det. temp.: 200°C Inj. & det. temp.: 200°C 30m, 0.53mm ID cat.# 19700
Carrier gas: hydrogen Carrier gas: helium 50m, 0.53mm ID cat.# 19701
Linear velocity: 6.5cm/sec. Linear velocity: 37cm/sec.
TCD (212 mA)
30m, 0.32mm ID cat-# 19702
FID sensitivity: 1.28 x l0-11 AFS Detector:
Split ratio: 10:1 Split ratio: 15:l 60m, 0.32mm ID cat.# 19703

Restek Corporation page 11 Advantage

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