CBR_TEST
CBR_TEST
CBR_TEST
Designation: C150/C150M − 21
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C150/C150M − 21
C266 Test Method for Time of Setting of Hydraulic-Cement 4.1.1 This specification number and date,
Paste by Gillmore Needles 4.1.2 Type or types allowable. If no type is specified, Type
C451 Test Method for Early Stiffening of Hydraulic Cement I shall be supplied,
(Paste Method) 4.1.3 Any optional chemical requirements from Table 2, if
C452 Test Method for Potential Expansion of Portland- desired, and
Cement Mortars Exposed to Sulfate 4.1.4 Any optional physical requirements from Table 4, if
C465 Specification for Processing Additions for Use in the desired.
Manufacture of Hydraulic Cements
C563 Guide for Approximation of Optimum SO3 in Hydrau- 5. Ingredients
lic Cement 5.1 The cement covered by this specification shall contain
C1038/C1038M Test Method for Expansion of Hydraulic no ingredients except as follows:
Cement Mortar Bars Stored in Water 5.1.1 Portland Cement Clinker.
C1702 Test Method for Measurement of Heat of Hydration 5.1.2 Water or Calcium Sulfate, or Both—The amounts shall
of Hydraulic Cementitious Materials Using Isothermal be such that the limits shown in Table 1 for sulfur trioxide and
Conduction Calorimetry loss-on-ignition are not exceeded.
C1778 Guide for Reducing the Risk of Deleterious Alkali- 5.1.3 Limestone—The amount shall not be more than 5.0 %
Aggregate Reaction in Concrete by mass such that the chemical and physical requirements of
E29 Practice for Using Significant Digits in Test Data to this specification are met (see Note 3). The limestone, defined
Determine Conformance with Specifications in Terminology C51, shall be naturally occurring and consist of
IEEE/ASTM SI 10 American National Standard for Metric at least 70 % by mass of one or more of the mineral forms of
Practice calcium carbonate. If limestone is used, the manufacturer shall
report the amount used, expressed as a percentage of cement
3. Terminology mass, as determined using Annex A2, along with the oxide
3.1 Definitions: composition of the limestone.
3.1.1 For definitions pertinent to this specification, see
iTeh Standards
NOTE 3—This specification permits portland cement to contain
Terminology C219. limestone, but does not require that limestone be an ingredient in the
cement. Cement without ground limestone can be specified in the contract
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4. Ordering Information or order.
4.1 Orders for material under this specification shall include 5.1.4 Inorganic Processing Additions—The amount shall be
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the following: not more than 5.0 % by mass of cement. Not more than one
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Aluminum oxide (Al O ), max, %
2 3 C114
... 6.0 6.0 ... ... ...
Ferric oxide (Fe2O3), max, % C114 ... 6.0B 6.0B,C ... 6.5 ...
Magnesium oxide (MgO), max, % C114 6.0 6.0 6.0 6.0 6.0 6.0
Sulfur trioxide (SO3),D max, % C114
When (C3A)E is 8 % or less 3.0 3.0 3.0 3.5 2.3 2.3
When (C3A)E is more than 8 % 3.5 F F
4.5 F F
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TABLE 2 Optional Composition RequirementsA
Applicable Test II(MH) and III and
Cement Type I and IA II and IIA IV V Remarks
Method II(MH)A IIIA
Tricalcium aluminate (C3A),B max, % See Annex A1 ... ... ... 8 ... ... For moderate sulfate resistance.
Tricalcium aluminate (C3A),B max, % See Annex A1 ... ... ... 5 ... ... For high sulfate resistance.
A
These optional requirements apply only when specifically requested. Verify availability before ordering (see Note 2).
B
See Annex A1 for calculation.
Autoclave expansion, max, % C151/ 0.80 0.80 0.80 0.80 0.80 0.80 0.80 0.80 0.80 0.80
C151M
iTeh Standards
[1740] [1450]
3 days 12.0 10.0 10.0 8.0 10.0 8.0 24.0 19.0 ... 8.0
[1740] [1450] [1450] [1160] [1450] [1160] [3480] [2760] [1160]
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7 days 19.0 16.0 17.0 14.0 17.0 14.0 ... ... 7.0 15.0
[2760] [2320] [2470] [2030] [2470] [2030] [1020] [2180]
28 days ... ... ... ... ... ... ... ... 17.0 21.0
[2470] [3050]
inorganic processing addition shall be used at a time. For amounts used or greater and the total amount of organic
amounts greater than 1.0 %, they shall have been shown to processing additions used shall not exceed 1.0 % by mass of
meet the requirements of Specification C465 for the inorganic cement.
processing addition in the amount used or greater. If an 5.1.6 Air-entraining Addition (for Air-entraining Portland
inorganic processing addition is used, the manufacturer shall Cement Only)—The interground addition shall conform to the
report the amount used, expressed as a percentage of cement requirements of Specification C226.
mass, along with the oxide composition of the processing
addition (see Note 4). 6. Chemical Composition
NOTE 4—These requirements are based on data and recommendations 6.1 Portland cement of each of the ten types shown in
by Taylor.3 Section 1 shall conform to the respective standard chemical
5.1.5 Organic Processing Additions—They shall have been requirements prescribed in Table 1. In addition, optional
shown to meet the requirements of Specification C465 in the chemical requirements are shown in Table 2.
NOTE 5—The standard composition requirements in Table 1 require
reporting of equivalent alkalies. Cements with a maximum of 0.60 %
3
Taylor, P., “Specifications and Protocols for Acceptance Tests on Processing equivalent alkalies were historically designated as “low-alkali cements”
Additions in Cement Manufacturing,” NCHRP Report 607, Transportation Research and recommended for use with aggregates susceptible to alkali-silica
Board, Washington, DC 20008, pp. 96. Available at www.trb.org. reaction (ASR). However, low-alkali cements (in the absence of other
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TABLE 4 Optional Physical RequirementsA
Applicable
Cement Type I and II IA and IIA II(MH) II(MH)A III IIIA IV V
Test Method
Early stiffening, final penetration, min, % C451 50 50 50 50 50 50 50 50
Heat of hydration:
Isothermal Conduction Calorimetry:
3 days, max, kJ/kg [cal/g] C1702 ... ... 335 [80]B 335 [80]B ... ... 200 [50]C ...
7 days, max, kJ/kg [cal/g] ... ... ... ... ... ... 225 [55]C ...
Strength, not less than the values shown:
Compressive strength, MPa [psi] C109/C109M
28 days 28.0 22.0 28.0 22.0 ... ... ... ...
[4060] [3190] [4060] [3190]
Sulfate resistance,D 14 days, max, % expansion C452 . . .E . . .E . . .E . . .E ... ... ... 0.040
Gillmore test: C266
Initial set, min, not less than 60 60 60 60 60 60 60 60
Final set, min, not more than 600 600 600 600 600 600 600 600
A
These optional requirements apply only when specifically requested. Verify availability before ordering (see Note 2).
B
The limit for the sum of C3S + 4.75(C3A) in Table 1 shall not apply when the cement complies with this limit.
C
The limits of C3S, C2S, C3A, and Fe2O3 in Table 1 shall not apply when the cement complies with this limit.
D
When the sulfate resistance is specified, it shall be instead of the limits of C3A, C4AF + 2(C3A), and Fe2O3 listed in Table 1.
E
Cement meeting the high sulfate resistance limit for Type V is deemed to meet the moderate sulfate resistance requirement of Type II and Type II(MH).
mitigation measures) may not be effective in mitigating ASR. Guidance on 9.1.9 Sulfate Resistance—Test Method C452 (sulfate expan-
formulating concrete mixtures, including calculating alkali loading using sion).
equivalent alkali content of cement to minimize the potential for ASR, is
provided in Guide C1778. 9.1.10 Time of Setting by Gillmore Needles—Test Method
NOTE 6—The limit on the sum, C3S + 4.75(C3A), in Table 1 provides C266.
control on the heat of hydration of the cement and is consistent with a Test 9.1.11 Calcium Sulfate (Expansion of) Mortar—Test
Method C1702 three-day heat of hydration limit of 315 kJ/kg [75 cal ⁄g].
iTeh Standards
Method C1038/C1038M.
NOTE 7—There are cases where performance of a cement is improved
with SO3 in excess of the Table 1 limits in this specification. Guide C563
10. Inspection
is one of several methods a manufacturer can use to evaluate the effect of
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sulfate content on cement characteristics. Whenever SO3 content of a
10.1 Inspection of the material shall be made as agreed upon
cement exceeds Table 1 limits, Test Method C1038/C1038M results
between the purchaser and the seller as part of the purchase
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provide evidence that excessive expansion does not occur at this higher
sulfate content. contract.
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C150/C150M − 21
12.2 When limestone is used, the manufacturer shall state in provided in the shipping documents accompanying the ship-
writing the amount thereof and, if requested by the purchaser, ment of packaged or bulk cement. All packages shall be in
shall supply comparative test data on chemical and physical good condition at the time of inspection.
properties of the cement with and without the limestone (see NOTE 10—With the change to SI units, it is desirable to establish a
Note 8). The comparative tests do not supersede the normal standard SI package for portland cements. To that end 42 kg [92.6 lb]
testing to confirm that the cement meets chemical and physical provides a convenient, even-numbered mass reasonably similar to the
requirements of this specification. The amount of limestone in traditional 94-lb [42.6 kg] package.
cement shall be determined in accordance with Annex A2.
14. Storage
NOTE 8—Comparative test data may be from qualification tests per-
formed by the manufacturer during formulation of the cement with 14.1 The cement shall be stored in such a manner as to
limestone. permit easy access for proper inspection and identification of
each shipment, and in a suitable weather-tight building that
12.3 At the request of the purchaser, the manufacturer shall
will protect the cement from dampness and minimize ware-
report the chloride content as determined using Test Methods
house set.
C114, in percent by mass of the cement, in the manufacturer’s
report (see Note 9). 15. Manufacturer’s Certification
NOTE 9—Chlorides in concrete come from multiple ingredients and 15.1 Upon request of the purchaser in the contract or order,
cement chloride content may be required to estimate concrete chloride a manufacturer’s report shall be furnished at the time of
content. Requirements for concrete chloride content are provided in
building codes and other documents. shipment stating the results of tests made on samples of the
material taken during production or transfer and certifying that
13. Packaging and Package Marking the cement conforms to applicable requirements of this speci-
13.1 When the cement is delivered in packages, the words fication.
“Portland Cement,” the type of cement, the name and brand of NOTE 11—Guidance on preparing the manufacturer’s report is provided
the manufacturer, and the mass of the cement contained therein in Appendix X1.
shall be plainly marked on each package. When the cement is
iTeh Standards
16. Keywords
an air-entraining type, the words “air-entraining” shall be
16.1 hydraulic cement; portland cement; specification
plainly marked on each package. Similar information shall be
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ANNEXES
(Mandatory Information)
ASTM C150/C150M-21
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A1. CALCULATION OF POTENTIAL CEMENT PHASE COMPOSITION
A1.1 All values calculated as described in this annex shall properly qualified under the requirements of Test Methods C114.
be rounded in accordance with Practice E29. When evaluating
A1.3 When the ratio of percentages of aluminum oxide to
conformance to a specification, round values to the same
ferric oxide is 0.64 or more, the percentages of tricalcium
number of places as the corresponding table entry before
silicate, dicalcium silicate, tricalcium aluminate, and tetracal-
making comparisons. The expressing of chemical limitations
cium aluminoferrite shall be calculated from the chemical
by means of calculated assumed phases does not necessarily
analysis as follows:
mean that the oxides are actually or entirely present as such
Tricalcium silicate (C3S) = (4.071 × % CaO) – (7.600 × % SiO2)
phases. – (6.718 × % Al2O3) – (1.430 × % Fe2O3) – (2.852 × % SO3)