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First 2 Eliminated: 1.8 2 F (X) 0.0131798245614035 X 0.0711578947368421 R 0.990886123262293

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Janki Bhagat
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18 views18 pages

First 2 Eliminated: 1.8 2 F (X) 0.0131798245614035 X 0.0711578947368421 R 0.990886123262293

Uploaded by

Janki Bhagat
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as XLSX, PDF, TXT or read online on Scribd
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Concentration(

SrNo Absorbance 1 Absorbance 2 Absorbance 3


ppm)
1 5 0.048 0.018 0.046 5
2 10 0.077 0.1 0.114 10
3 20 0.164 0.211 0.218 20
4 60 0.616 0.631 0.714 60
5 100 1.213 1.218 1.44 100
6 110 1.412 1.376 1.579 110
7 150 1.797 1.826 1.915 150
8 180 1.877 1.848 1.981 180

first
2 eliminated

2
1.8 f(x) = 0.0131798245614035 x − 0.0711578947368421
1.6 R² = 0.990886123262293
1.4
1.2
1
0.8
0.6
0.4
0.2
0
0 20 40 60 80 100 120 140 160

SE of Intercept 0.012
SD of Intercept 0.02683281573
Lod 6.7082039324994
Loq 20.327890704544
Mean sd rsd Concentration

0.037333 0.016773 44.92766 9.03030303030303 6.75757575757576


0.097 0.018682 19.25932 11.2272727272727 12.969696969697
0.197667 0.029366 14.85608 17.8181818181818 21.3787878787879 All 5 10 20 60 100 110 1
0.653667 0.052786 8.075328 52.0606060606061 53.1969696969697
1.290333 0.129639 10.04696 97.2878787878788 97.6666666666667 2
f(x) = 0.0116870511646831 x + 0
1.8
1.455667 0.108316 7.440982 112.363636363636 109.636363636364 R² = 0.977403911287657
1.6
1.846 0.06149 3.330977 141.530303030303 143.727272727273
1.4
1.902 0.069936 3.676955 147.590909090909 145.393939393939
1.2
1
0.8
0.6
0.4
0.2
0
0 20 40 60

SUMMARY OUTPUT

Regression Statistics
Multiple R 0.995432631202279
R Square 0.990886123262293
Adjusted R Square 0.987848164349724
140 160 Standard Error 0.0725382671073121
Observations 5

ANOVA
df SS MS
Regression 1 1.71623282164 1.716233
Residual 3 0.01578540058 0.005262
Total 4 1.73201822222

Coefficients Standard Error t Stat


Intercept -0.071157894736842 0.07194851531 -0.989011
X Variable 1 0.0131798245614035 0.00072977453 18.06013
All 5 10 20 60 100 110 150 180
2
f(x) = 0.0116870511646831 x + 0.00729864713660877
1.8 R² = 0.977403911287657
1.6
1.4
1.2
1
0.8
0.6
0.4
0.2
0
0 20 40 60 80 100 120 140 160 180 200

F Significance F
326.1684 0.000370284

P-value Lower 95% Upper 95%Lower 95.0%


Upper 95.0%
0.395571 -0.30013018 0.157814 -0.30013 0.157814
0.00037 0.010857356 0.015502 0.010857 0.015502
Concentration(
SrNo Absorbance 1 Absorbance 2 Absorbance 3
ppm)
1 5 0.023 0.018 0.046 5
2 10 0.077 0.1 0.114 10
3 20 0.213 0.211 0.218 20
4 60 0.616 0.631 0.714 60
5 100 1.213 1.218 1.44 100
6 110 1.412 1.376 1.579 110
7 150 1.797 1.826 1.915 150
8 180 1.877 1.848 1.981 180

first
2 eliminated

2
1.8 f(x) = 0.0130674089068826 x − 0.0579986504723347
1.6 R² = 0.990579232856485
1.4
1.2
1
0.8
0.6
0.4
0.2
0
0 20 40 60 80 100 120 140 160

SE of Intercept 0.071948515313
SD of Intercept 0.16088177112
Lod 40.220442780004
Loq 121.88012963637
Mean sd rsd Concentration

0.029 0.014933 51.49374 7.13636363636364 6.75757575757576


0.097 0.018682 19.25932 11.2272727272727 12.969696969697
0.214 0.003606 1.684837 21.530303030303 21.3787878787879 All 5 10 20 60 100 110 1
0.653667 0.052786 8.075328 52.0606060606061 53.1969696969697
1.290333 0.129639 10.04696 97.2878787878788 97.6666666666667 2
f(x) = 0.0116756586308616 x + 0
1.8
1.455667 0.108316 7.440982 112.363636363636 109.636363636364 R² = 0.977502060587912
1.6
1.846 0.06149 3.330977 141.530303030303 143.727272727273
1.4
1.902 0.069936 3.676955 147.590909090909 145.393939393939
1.2
1
0.8
0.6
0.4
0.2
0
0 20 40 60

SUMMARY OUTPUT

Regression Statistics
Multiple R 0.995432631202279
R Square 0.990886123262293
Adjusted R Square 0.987848164349724
140 160 Standard Error 0.0725382671073121
Observations 5

ANOVA
df SS MS
Regression 1 1.71623282164 1.716233
Residual 3 0.01578540058 0.005262
Total 4 1.73201822222

Coefficients Standard Error t Stat


Intercept -0.071157894736842 0.07194851531 -0.989011
X Variable 1 0.0131798245614035 0.00072977453 18.06013
All 5 10 20 60 100 110 150 180
2
f(x) = 0.0116756586308616 x + 0.00920292950869694
1.8 R² = 0.977502060587912
1.6
1.4
1.2
1
0.8
0.6
0.4
0.2
0
0 20 40 60 80 100 120 140 160 180 200

F Significance F
326.1684 0.000370284

P-value Lower 95% Upper 95%Lower 95.0%


Upper 95.0%
0.395571 -0.30013018 0.157814 -0.30013 0.157814
0.00037 0.010857356 0.015502 0.010857 0.015502
0.1 0.023
0.2 0.222 Chart Title
0.3 0.42
0.8
0.4 0.565
0.5 0.7222 0.7 f(x) = 1.7414 x − 0.13198
R² = 0.99492615783299
0.6

0.5

0.4

0.3

0.2

0.1

0
0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 0.45 0.5 0.55

SE of Intercept 0.023813
SD of Intercept 0.053247
Lod 0.044971
Loq 0.305769
0.5 0.55

SUMMARY OUTPUT

Regression Statistics
Multiple R 0.99745985274245
R Square 0.99492615783299
Adjusted R0.99323487711065
Standard E0.02270444890324
Observatio 5

ANOVA
df SS MS
Regression 1 0.303247396 0.303247
Residual 3 0.001546476 0.000515
Total 4 0.304793872

Coefficients Standard Error t Stat


Intercept -0.13198 0.023812626902549 -5.542438
X Variable 1.7414 0.0717977715531617 24.25423
F Significance F
588.2679 0.000154

P-value Lower 95%Upper 95%Lower 95.0%Upper 95.0%


0.011579 -0.207762 -0.056198 -0.207762 -0.056198
0.000154 1.512907 1.969893 1.512907 1.969893
Sr No Level Conce before spiking Conc of std added conce after spiking Absorbance
1 80% 60ppm 48ppm 108 1.362
2 80% 60ppm 48ppm 108 1.366
3 80% 60ppm 48ppm 108 1.367
4 100% 60ppm 60ppm 120 1.574
5 100% 60ppm 60ppm 120 1.574
6 100% 60ppm 60ppm 120 1.576
7 120% 60ppm 72ppm 132 1.738
8 120% 60ppm 72ppm 132 1.754
9 120% 60ppm 72ppm 132 1.763
Concen after calculation % Recovery Mean SD RSD
108.575757575758 100.533109 Absorbance and Concentration
108.878787878788 100.813692 100.7435 0.200436 0.198956
108.954545454545 100.883838 2
124.636363636364 103.863636 1.8 f(x) = 0.0130674089068826 x − 0.05799865047
124.636363636364 103.863636 103.9057 0.087477 0.084189 1.6
R² = 0.990579232856485
124.787878787879 103.989899 1.4
137.060606060606 103.833792 1.2
138.272727272727 104.752066 104.6182 0.959264 0.916919 1
138.954545454545 105.268595 0.8
0.6
0.4
0.2
0
0 20 40 60 80 100
nce and Concentration

0.0130674089068826 x − 0.0579986504723347
.990579232856485

40 60 80 100 120 140 160


Sr No Time Interval Level Conce before spiking Conc of std added conce after spiking
1 Morning
2 Noon 80% 60ppm 48ppm 108
3 Evening
4 Morning
5 Noon 100% 60ppm 60ppm 120
6 Evening
7 Morning
8 Noon 120% 60ppm 72ppm 132
9 Evening
Abs @ Morning Concentration Mean SD RSD
1.481 117.590909091 Absorbance and Concentration
1.487 118.045454545 117.99495 0.381305 0.323153
1.491 118.348484848 2
1.644 129.939393939 1.8 f(x) = 0.0130674089068826 x − 0.057998650472334
1.65 130.393939394 130.54545 0.69433 0.531868 1.6
R² = 0.990579232856485
1.662 131.303030303 1.4
1.829 143.954545455 1.2
1.837 144.560606061 144.43434 0.430776 0.29825 1
1.84 144.787878788 0.8
0.6
0.4
0.2
0
0 20 40 60 80 100
Concentration

9068826 x − 0.0579986504723347
56485

60 80 100 120 140 160


Sr No Time Interval Level Conce before spiking Conc of std added conce after spiking
1 Day 1
2 Day 2 80% 60ppm 48ppm 108
3 Day 3
4 Day 1
5 Day 2 100% 60ppm 60ppm 120
6 Day 3
7 Day 1
8 Day 2 120% 60ppm 72ppm 132
9 Day 3
Absorbance Concentration Mean SD RSD
1.423 113.196969697 Absorbance and Concentration
1.439 114.409090909 114.20707 0.925773 0.810609
1.447 115.015151515 2
1.644 129.939393939 1.8 f(x) = 0.0130674089068826 x − 0.057998650472334
1.666 131.606060606 131.17677 1.088205 0.829572 1.6
R² = 0.990579232856485
1.671 131.984848485 1.4
1.838 144.636363636 1.2
1.839 144.712121212 144.93939 0.460815 0.317937 1
1.849 145.46969697 0.8
0.6
0.4
0.2
0
0 20 40 60 80 100
Concentration

9068826 x − 0.0579986504723347
56485

60 80 100 120 140 160

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