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© O INORGANIC
(lead
Phaymoceutic! (init typu
norqanjc) SCience) tor Syl PHARMACEUTICALS
preparation
oppr Nad

C
Histor labus:
ndtHeaVy
Chlorjda

chanistny

Sulphate
te of
(Impurities)

A
COmpounda
in for. Ipuritiea,
HU
of |ONIT-
whlch
(Acidifiers), norqanic
oF Chlorida
Phavmacopoia
of rd

R
(Eutiu)
Mutals,

dug L
slphat.
CHEMISTRY
It priniple
in
whch

E
,
Pharnaceuti
is Modified Sulphat
Sodium or sfudy 1"
mdicina 'involwe
th
Sourcul
invalved

W
obout
branch
BiCarbonak
,ron,
Antacids cal
it Scienca
in those
E Arsenie,
and CIQ
senl, in
test
thl of the
L L

PHARMACOPOEIA

(ommon
and Ihe publishad
U.sP)ek. of
(I-P about Cficial
qreek
Of
6.P by IF term
"oelia is sardocs
P

on
Govemnt.

book phaumacopoa
to be ward in do
thad sag.
H

q. Make defined
Inqiedients,
o opplicoble
Nom
ek. of whNch MaanA orms be
(ounty
peparotn
A

pharmakon'
Govemat.
definad
aa
dnugs as
Contoina and
to to
R

Coms
under
T pharmaceuticol
drugs
authorizd make"
depils as
IF is
-formulas ma from
conajn

information a th and
M

a
s}andard
quthority
"dnug" he book
a their
conplele (ON0qap
A

atda

of
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. • • • •
This
(940 INDIAN

In History Thu family on The If

Schedule for
tha (strength
(133?) in
deine
behal book

C
Indian of
India.
L0. and It
overall
Indian PHARMACOPOE1A
pharmote

uwelfa,
is
and standardi
qof

A
fisHy Rule the
of of an
f Phama
Development (identit, qualiiy
Phamacopotìa approval drags
utical official
inist 1945. tho

R
Eovernmant
the (opola
at control
Drug products

E
tast
under (purity), documut
legaly

India
of is ond
ommission
(pharmoceutiala)
of ealth publishud
the and

W
Cosmetic (safehy
acaptable.
India,.

Copany assUronca

Second espon

and
E )
(IP) by and sible
fct
L L

pharmacopoeia RCOMMUndad
- - • India.
refesenca from
publishd publich After
NOu,
these Now,
academic SourCus,
Uses, ist It in ad
contain
(1955)ie. (885)
independenta, Bonqal
P

information
of tha
edition dosagt
sfondard
dugs Indian
and tets, first
institutions.

comitee
Monogaphs,
H

th pharmorO
th
severol
and edition
several
of formula lp phormacopoeia.
for publicahion
bnsially B.P.
elated
19sS.
Indian
A

soraga in
laboratoy

(1949)-tu
potia
afmmd uhich uas was
am oF
pharmacopoua
R

subsancuA
(onditions
Usd
by .
ontains IP developrd made
addendum IPC (
of
indushry
was 1P).
au a
Indian
M

: official pharmacopoeio

publishd

uas ete..
/suppnu

and
to
A

in
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C
• •1" EbITIONS

Ltdition 2
6thfdihon 3RD
8th 7h Gh

A
dition edition
fdithion dition
dition tdition

R
2014 Q007 YEAR
1946 1995 19S5

E
19
q 66
Ediion

INDIAN

W
AddendUm Addendum ADDENDUM
Addendum
Addend AddendUM
Supplement Supplement
AddendUm Adderdum Addendum AddenduM Addendum

2022.
E PHARMACOPOEIA

um
L
2005
2002 2000
2008 199! 1989
2019 ol6 2o1S 20R
I960 OR
1945
L

SUPPLEMENT

EDITIONS
P H

No.

3 2 3 2
4 3 3 Of
Volumes
A R

MONO

1149
220 52 271 261 890 986

GRAPHS
M
A

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subsfanca,

manuacturing
orisa ,
and piengs whjch
which salts
jdextified. by

C
"procs
inorqank idatified
also exci
impurities drg impurities

-product,

A
may
of basicaly
easil during eagents, eke..
ynthusis easil
sforag.

R
those
those
thosa
it by caaayst
not
producad

ae
, test.

E
ie. Mateial
: ae
-their Inpurities to
ae during related"
ak
impurities
inpurities ek. process.
.
Inpurities

These
impuritie
these
basiall
hu mefal
liat
during raus-

W
Fngnts Irorgaric
ba Ucing
drug-
cad hiovy
produ
Organic these
and
These om
EL
these

i) ii)
L

p
Substacas

toxicahy

and
of ek-
Phaamacoutical
qualihy
P

Impurities
types
) Iron,cloridu
pharacouticalA
(-foreign
TrPES
aue olution
H

thte
an
Unwanted t
AND
frsenic,
A

also
also cf
loues

SoURCES
in mainl
Inpurities Impuritie
R

present impue) ad Impuritie

may alcjum,
ae Solven

pharmaceutiols

Impurities
Impuritie. Subrjuce

Ihorganic
|: ead, Residval
Of Orqonie
M

Impurities a Jnpuaihies
it They
-foreiqn Types
whih make
A

• e4
1) 11) 11)
O

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ocured

sourcUs raus
producs

Manufacture.

wich
impuvities

C
frorm
acidertally ek.
orious produt.
drug
matrial
siler

A
q,
manufacturi Sonetinu,

in from coppu,
in
IMPuRITI Souru in -Adulerotion

R
impurities USed end
or employed
azads ra
obainsd
excipiests elated lead,
Method
th

E
CÔmmon
Cotaminate
ng fiom
Nanufoctuing Materias
duri Materials
Of The Usad Envivonnt
Of
Accdeutal
be naterial,
or

W
ttocs
SoURCES may ProQSSU storog
aS MOst Dofect
Renqent

Such
E
Raw kuo
tho
vIn) V) 0
L
i) ii) ii) iv) v) v)
L

typu eke.
inpurities pur
proceus
i.e. of
impurities
distillatica
whjch Iprohibikel
furchond
method
teo in
io
Carbon
P

impurities
manufachuring
nto those
(etfet): those chamjcal

ateqorised
ie. thu steel.
stop substancu. %)
H

nethod
ae improves

those
ae bosIall than manufoctue

tneir by Thesa
A

These
-
hysjcal
: kMOved tmpurities
less
during
tnpurities

als0 Of basially
of fdding
R

which
Soluent: foncions
these Solvents. basis
may
and to
prodvcad
ba onstvuctive
substancu.

Destructive
which iron
M

May chomjally
Residual Impurties thu
tha
from
on
A

It
•
€
iü) )

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Naß, inpurity
bodies, USe.
subfarcus
contomination
not emain
-
tery. toxict
occured
ond
prodvctsL to
we chapor . ynfit

C
insect of properties
chongk, efe
always subsancOS
.
which amnoUnt Cause
wSe taste
toxlc
and
at dust, wth

A
mrobial
inpurity odouv,
pysical unhuaienc
inpuities t mical
accidenty
Sonme
odulkakd a
pollute the active.

R
te. thun
Somtjmus, cf
conjaminaion,
Color,
sorage.
intabilitiy, f
eKCOs. t shelf-ufe
Somthm,, of

E
erro may phusical thuroapurticlly subsanc
omoUnt
is So effts
mixed maerial,
t
padking kBr
during ete.
Changes
choical in

W
Acidertol exponsve lite toxC
mal |cyoun. tu hu thu
aH present
Cross
storog making
anj A a Cawce aller make educs
nd
E May

(Vii) e in
(vii) is
L
manufocturing
impurities
ocUed
latim/exipients.
L

prodvct.
ek.
Hs,
inpusty aUSe ete
not ar
pH ocurs
- So, meallic
inpurities
impu may Gasel
sons peSSUR, erro.
ae oxidahon. tlundt
-
P

final manufacturing.
pecipitate
ials. during
Containation
thy solvent preducts.e
conguninohe Manufachuring
these qlau,
mater
.
manufactuing
formu Sonetims,
tenp. Overall
H

mixing,
oCus
atMosçhae,
f
murcuy Rsdue e
dirt,
procu.
eaguts h
A

to defects l.e.
improper
tinal
qros(eror)
and >
-
Hozavdy during
îno -frogments
Ouring elaled
Ammoniakd du to of
chemical
R

propavl from
in from ener
in to mixing
Contaminoton
bu du as
Used Dus Manufocturing

Evionmat
may oriso
ocCUS Processes
such
playtie
M

Rengort washad
to
Dafects to to
also due
e .It Ouu Due
A

• •
VD
iv)
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passed.
ofPassad
insolvbla

hlorida
of-failed masue
ldertifyinq

test which

C
is NO
solution

Soltion soluble +
lint solution is
which

A
and to
eacion,
budity
pRCipuatu
Agcl
Stordard for
than Turbudit
impuritie
with
test CHLORIDE
test

R
choridu
Tur used
HNO
soldion keoct
the

E
of basially acid. Nibrae

silver
torbidity ion on AqNO;
solution solution
cWorida) quarthity is
cf foR
standard of lvey
based nitric
nútrate

W
Turbdili
Torbiditi -foYm
TESt is
Stardakd I+
test
Principle is
the 4hair d.
thon
E LIMIT
It Stlwer whjch
th It
If in
L
• If, If, •

staudard solution
L

thiu,
impuritie basically

ldenhify substoncu.
- ck teut
Somi COde)
of
in
P

amount of
that
o ae
ae soltion.
to of cost
H

quavtitatie qvatity principle

desiqnud in /opales
which fo
pesont
of teut ffurbidit,
A

(dekermination)
te turbidt
Cylindes
standard
CoMpae
teats
Small Laghty
test inet the
Nessters
R

oR
thoco
control) on the
TESTS
quardilative

These
ak based with
compae
for
Împurities.
M

whjch

LIMIT
and Used
soluhion

These
is
A

Solution

Test
It we
•
.
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thun Control
vse uoUitie
mOe
thu
for soktion,
Stundard
soltion,
min.
for
in B le
asid
to

C
-& ady is
ylindu silve S
Som is
Culindr ud
sut soltion
solution
ard
sandard stand

A
and and
to Of
NeSsler Nessler

Dilujed test teat

tet

R
test of
1
of limet
obsemodon imt of turbidity

(onpare urbidiy

E
sol of
turbidity
the
Siver fo both
(AgNO3) the
A asida tubidit
in -A pAssel -faled
ylinder
linder

W
Som
|Set
thu
of h

NAHak
h
than Sample
Sarmple
to + im tu thon
Nessler
E Nessler

Duted
Add If
Teat
If
L
- -
L

qlinde, Nac.
SOUUT]ON
du compakd
teot (HNO3)
chJoridu(pp) tat -s) cworida
turbodii) thu
Nütole,
ylindes
MeasUring limi
P

pepar
on solution.
STANDARD

hun all SodjUm

depunds
Silyer (N2sser
H

fer
appars which , Sama
to cylinder
Silver Afardard
acid,
Of
A

hove
is lorid), ee..

torbiditi, so. Nürie

Solution Nessles's (q) aad
we
R

SOLÚTION
HNO2)
of rod
A)
- water
ylinder substanco
thjs, Ntic
formation Afandad
Glass D.
cf (

f :
M

aMount Procdure for Appadus : TEST

tes (Nessles
Chemials
Specified + of of
Degee
Nou,
with Jm
to
A

10
• • O
• •
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wafer
which Salurotion Sulphat
prerenSypr)

SOLÚTION
so
sot" alohol as dist.
in w/ Barium
,
std. pesart

C
eaget tesf -) o.\0897. Hy m
sulphate-fte
fte te. Cylinder
4s
pepae
witth
witr - STANDARO

sulphae
tha(senstisl)of

A
of of
is sulphate in
Compared
Compared k,soy
(Nossler Sm
soluion. of Added
(Roch 2m

R
, to m
cloridu 1
haue of
ßaium
clorida

E
is Sulphaa
incHtase
Sandard watct
we phate
torbidit sulphae. SOLUTION
Barium -a)
Borium ths, spxified
of Cylindu sul Rarjum
m

W
:
-form y5
ProcadUHe cOf
potascivm In
covtajns, a
his this, Subsfanca Kagent
(Nessler
in
E well
TEST of of
Addual
tnen qm
1 S
L
In th
•

cortrlling
L

chlovida, u
qenat
make sulphát
so
ohich turbidity
0cdlc) in
wich
impurity
24
which
P

nd -for Aolvbl
usad except +
HNÔ, so
solution used in foum
HOction, Basoy
) di).(HI peipiatt
H

sulphale
add inpuritie bosially
wjth ppt
in
SULPHATE

jnsoluble
(Nitric
A

make
Heact
the
of HI
the sulphát
oher
R

is on
HNO, to is pHSence
BaCly
a foR idenhifying
based
Sod test dlorid
Rarium
dissolve thuy SubsfancL

TEST
+
di.
M

This c bidity 2
Soy
is is
cavte -turbid. Priniple:
jum th
Why forms
IF they LIMIT and It
bar
A

bi in tur
O
-
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problem

basically thesa
whjch coloed substonus test. which

C
ceoate
Convert during
problQms Solution.
pomanqonake). color
ke
for
SuLPHATES

A
foR
used an Colorle furbldty.
Somuims
purple
which duty
bidty. w
TEStS those
tut. test Cubstanu

R
basialy
tut, tubi
Into
tuts qives
limit (potassivm

overcomi
for tu

E
LIMIT AND becavee
limt in
Aubsfancas
clear
disturbana
Ubsfonce
those (olod of kunoy
CHLORIDE
during is
Modied
CHLORIDE
formation
Subsfancus,

W
MODIEIED
tet qu
KMnOy
ae to Colord)
These we this,
Bccurs (Hate
USed This (olored
These
foR
E
in So.
- in In
L
e

Jader. um solubion,
L

last Bacle
and m
of of
soluhon ssi ualet
of is
is n M (S pota
with solutjon
turbidity wighed ft o-s
ieagent
-for wafer. standard
s of (10om
P

keaguiSn)of
ith mixed
w/N solion
asida
to Rasoy teatcd
uplo
l0892.
of is test
is
H

the addad
sulphale of
usm wlt diluted
on.
Set chuck -fe of
oF solut
o. 0.0181%, turbidit
Ond sulphale
A

passed.
upto
of turbidit
s Sm wejghd
of Basoy al
HcI m
tuvaidty
R

1gm then th and(Sn)of these

1
pepae of
dilute
- the tet
for waler,
soluion s 20m the
- oF thun
asede solution kgsOy than
limit
the
M

hn Sond If
odd phalt.
dishiled to
Standotd
cuck alcchol
Oddad HCI, Result
less
Set then,
Test
thin
add
A

sul

•
•
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sah Standad sa Tet

4)

C
A
+

R E
SULPHATE

W
E
SULPHATE fOR TEST LIMIT
L
foR GRAM DIA RovaH
bath ethanol.
kMnOy turbjduly
+
L

2kOH
).
(chdoiot
substane
ol water a
etnan 24,0 for coloed
nognaium
of
of procadue
tet San
+ 97.
P

2Mnozt in above
qm on
HO inteofeono
with for cin
1S hat Of lit colorles

3H, (olorless
H

used
tea
Oissolve
usater, furthor
eOted
&
a
)
Redox rxn
m
also color
A

SOmo
CHtale
into
4 &dd 6o
sulphate
dist. follaus
ehonol)
: upto
29H,0H (purplu
is KMhOy
Reducing
is
R

ICMnoy
procadue
which
it
fet
ogut of Convert
dilue SULPHATE

kMnOy. and tor

m (Worid.
+ of This teAt
color preparation Subsfanca
M

Sõ
Conpound
AKMNOy
and al we
t, Purple
in
-hen fOR
.. liti
and So,
A

for Cool

. •
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diamte
quoytily
APPARATUS
tube diamser
sáde
2HU an qas papu,
arSenjc
dupnda Spying
clip qlass
uith solution through
intenal tor

C
t external
hole
(ftsHy),
stain) compod
long cWorida
GUTZEIT
sovtion colors.

solution. mm 2mm Test

(Yellow Dm Bmm) pasud

A
200 6-5
Hq tet these
mruric

is

R
of A sfardod
staio qa
Chloridu) of
arsing
(Mecurlc

E
yellou) idensb
Hqch
to
of eachd

sfaun)
the
t

W
theso andenked
qas) Apparotus: tat.
wattr tube.
ftsH
CArsL yellow Rubbr Cork and
CNovidu
MOrcuric

2
Nou,
E paper
for During
for is the
which
hole
Hole exit
M
L
• (I in -
mercuric
ancs.
L

3H,0
is
whjch with
idertifying Stain.
state acid)
substancu.
and subs +
educhion
AsH,1 througn
P

adicine in ad (AYsina) yellow

((ArseneoUS
rable eaction, HftsOz

arseneouS
ARSENIC
undesi SHn/H,
H

Rodschon
for acid. passed
in by aa
in
presut Reduchon
produce
tmpurities
purities the gas
A

hydrochloride
used known
GHho
qas
arsin Sud
-foR
on
R

is substanca 4 +
4 well based in rsin and
ocid)
cortolling
arsenc
ad)
TEST
fest into
HaftsOy paper
AsOz (Arsenedus
and (Arsenic
is Prináple:
is
M

COnverted is
Ibis harmful t
Arsenie
LIMIT firstl Hg chlorido

Zinc Then,
and
A

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auidu procvc sfain is dak placa

wih solution
fad

Soktion
yelow in/ it.
passad.ReyulH
it

C
Heact A Aoe du
mjn. nl
imudiaedy
tut thun
papr stajn ef uith

A
qas b
the Ho /dianaer
in ,
Ahould washd
yelaw water
arsing sfain
Icaap -for

R
Hqc
conpord
intensity yellow
produu-
papr with
tut

E
0cide
wjth Sanding.
be
timit
Ahould thn
solution
corido
these
of ba
teoct
and infensit should

W
min. AST)
stajn lRss,han
:
PRautions
paper on tube
qas Compare
o tsonjc
auway
the 4o
yellow
E sfain
arsin Hqch tha H
lcaep -for IF
-
L
- •

Aolution KT
L

cubstanca.
chorida
SOLUmON
tu 3olution
of Zinc(AST)

KI
o on /qm
colors Snch
dependa sandard 1M
stannous
P

stain
sfain lodid)
present
stundard
STANDARO

in of of
presunt of
yellow (potasium
H

Intensity
sm
is arsonie
of of qM
sain
Add
impurities and Im Sm
1o
A

producus
x
yellous
test 4sTseu
paper. -heir qenerotor
ce prepaed chNorida
R

KT ot
/gm) Snclz

asendc
both
SoLUTION

qas of of opared 1M
Hey
chlorida
sfannous
Pepored zine
intnsity solution lodido)
indensit in wh
asin
M

Procedure:
of
of placed (S)
+ (potasiom
TEST
rcUrie botte
of
amoUnt and
Now,
-Test of qm
A

Add
Tu ahd
5
jo
- - •

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thioglyolic

water
Solufion ). m.
as SoLÚT|ON fee]. acid make

uel w/ and aside Mn

with 50 other

C
207. acaic upto
Stondard
iron to lkalin. 5
as diluted of kaep
aMMonia for each
(MerCopto
STANDARD
test solution
of drops

A
n. acd + (onpared
)
pepoed
o 2m Solution
Of (iron 2
Cihic
upto Add Add ake

R
Add acd
2 of
. • is
|

E
to thicglçoli
acid) color
w/u Make
ftee]
Soluion. in m. aside min
is t Sd
have SOLÜTTON discolved volume
207. acahie
ypto
Vo alkalina Developed
Ciron S
to keep
with

W
amnmonio solutn for
we of of (Nercopto

Stardard
acid diops
Procodue then
tirsHy. is up +
2m
TEST Solution
Sample
water
E
made 2
Add iric Make
acid Add
•Add
L
. .
acid]
24*
solution.
Color
L

idetifying

iron +
bufer, thoglycolate
0cehic a purple 00c HSHC
which is
of
(nerapto
P

in color
(oDelex
complex
inpurities
of
for citate
intensity

in purple
CO0
Used soluhion.
Iron
H

reochion aminonjum
acid thioglycolae
thioglycolae

«
is ivon this impurities
A

IRON colic
sjandard
test thiogly
the of
the Thioqlycolic
R

CHSH
fOR of intensity

lint cortralling iron

on iron acid
presence

with with
TEST based
forms olor. of +2
:
M

Tbs
•Principle react the CoMpared
Amount
LIMIT
and is the purple
which
TIhen 2fe Iron
A

It is in
In

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C=S
tn Soluion

color N=NN-NH
aád and
isted. „N=N.
is water
as ciric
ammonas
coplex solution

C
in uell funnel. AYogm) m)
violet
go
end
Dithizone-lead
as
color. NA-N,

A
Sample separcting átrote
test
is the Solutions.
Gmplex
udium

R
prepartd
aronium
at
alkalin
of
Compar
color

E
(le) quantity
both
dihzon
Pb ue solution, in
resulting +
first solution: of
Dithizone
transferred
we ,NHB 2SNEN

W
- knouun
lead
m
last
his, Sfandasd
.Procadure
the
E Test Add
and A
At
So In
L
i)
imMmedjakely

idertifying
L

solution.
(ditizon),
lead dithizon
od
then CNoroforM
test
compared which
solution,
P

of for in
diphenytiocarbazona

impurities
lead
color Used in colot.
reacion,
H

test.
standard
be form
io
should Colot
purple is
limü LEAD
A

test legd in
to
than the
solution ed in
of solution
R

/Result foR qreen

minutes.
liit the on
intensity (less) passed is
controling
TEST based with which
the
Observation
This alkaling
is within5
is
:
M

is thic, •Principle teact Oithizone

Salution LIMIT complex

the Sample
is
and
A

If In It is in
•

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solutiar solution. water.

innse
transfesed
ahd

developad
ftee
seconds
lauer. f
test sfandard
mOHe HNÖ,

C
(1ead

is Pb
chlorofoam O. a
30 dil.

A
lead ptoceduk bt
layer ba
for in Should with
ot obfained
cNoroform
Solution
of

R
funnel.
should washd
solution Same
of /chemicolk

E
(color)
/Result:
seperahing )
sdution
Solution
color
th standad
th should

follow of
shake
reaqents

W
th caution:
Observaiorn
Sfandad color thh
cbserve a Nou, fest
Glqssuwa
Nou).
E n
The
than

Pre All
AI|
L
ii)
chlorofornm

n
tronsfer
L

qrean. lopo etonol

soluion.
in
to for add
jn. dittyzon
v/u of
2m make Uçed become ettas
ditzn the
Sm also
P

and Gmmonia
ad %
% ma
discard

and
is add
cyanlde i
extrocts
and lo
soution of zong of
H

30ng
hydiochloride
unil
N ution solution
huylvoclor
ed adding
ithi
ditzon) and
potassjum 30
A

soluton
phunol dithizona sepavator. sol
combined
solutton dithjzone)
with acid
by
R

hytroxlamine
above
of
alkaline
o second seconds this
drops 5
the
the acd
md th Sandard
M

Combine in
2 solutión
Shako 4 Now,
extoct Ditje lauyer.
Nou,
Add Add
o 30
A

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solvto stadard(1eac)

3-4
solvtion Le. SOLUON in
solution Cylindes. ate
Mo watr buhuen
Stondord mlion'
dd.
bo

C
soluhon
nd
stondad
acid
not m 3S
standard adjustd
S Necsler
should DARD aetic
of per of upto

A
intensit as pats in ammonia

soution STAN 2 Solutin

leod dil. Volum
with t:. Somm is
Take

R
leod as
as pH by
vse thon usae•
solution
tet well
well
sampd
)woler
th lindy
beten

E
Compase
in /
sOLUTION
we soluhion.
expRssad acid
lead m
test test,
as of m cy
quartity Nosley
in(2s gatic
adjustcd SS
tect
foL :

W
ammonia
we ProceduR
upto
dissclued dil.
of this 20Dpm
Prepore TEST n
Nouw, is Specific 3-4)by
Color
Voluma
E ,so is
In It
• pH
in dil.
•
is
•
L
.
Zin(2n),
L

Calor.of
(Ha), acidic
is elk-. which
eoct
chenical
for it sulpkida 2H*
Concentaion,.

METALS Mercury

Used and (G), an

P

slver is /byoun
in Sulphidu
inpurities. t
densit reaction
(M) in
those chtomjUM
basiall
utal
(0), M,s
H

(Hs) eddish
HEAvY Cobal mtals
divn tal
are louw

mtallie
high ead (B),
A

(fs), Suphide
heavy torms fid'c
is Slpkad
thos at Cadnjum,

fOR hove poisonous)

on
Bismuth
test
R

Aysenic
- based Mutaltydroqen

Hydroqen which
the Metals which of bs
TEST
Principle:
- solution
determining
li exomples is M+
Mdiym,
M

Heav ents ot
LIMIT This
toxjc) It
elem wth 2
a
A

• . •

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doesnot )ud
solution,(Na,s)Used.

Vsed.
:
qives qivea
thods
ths
solution,
which

C
who ,s which

substances,
otr CoMPLETED
solutin

A
substance
subsfancs
colorless
phama

by

R
b
colorles coloyles
Catuell

porformd
ormLd
those clear
hose
hose

E
UNIT-I

@
clear clear
for tor qive
for

W
also
A: R: C:
Mehod
Mathod
Mithod
is
EL L

in
freshly om D
CHydroqen S standard,
adiust is
Sfaudard

fo So| Solution solution

upto water.
asid
P

of tp olation

(HS
in
Volum |lceop produced
Sfandasd
adding test in
producad
1o Sulphide]
H

ptepaed Standard
Make

soluhions.

Color
by color
. in passed.
A

he produced
•
color
Conpake of
Son intensity
s nin both
R

(Hys fou test

sulphideJ upto water. th in
aside Reslt Color solutjon
Of prodvced
prepared
Solution

than linit
kep
Observotion
adding
M

volu the
(Hydroqen

freskly Test less then

olor Test
Make
sammple
IF
A

OTest
by •
•

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