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    Pr 10 Che Xii Salt Al2(So4)3

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    arefa shadab

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    Pr 10 Che Xii Salt Al2(So4)3

    Uploaded by

    arefa shadab
    1 views4 pages

    Copyright

    © © All Rights Reserved

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    © All Rights Reserved
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    1 views4 pages

    Pr 10 Che Xii Salt Al2(So4)3

    Uploaded by

    arefa shadab

    Copyright:

    © All Rights Reserved
    Download as DOC, PDF, TXT or read online from Scribd
    Download as doc, pdf, or txt
    of 4

    | CHEMISTRY| PRACTICAL NOTES

    Expt. No- Date


    -

    Identification of cation & anion of the given unknown salt

    Aim of the experiment: To identify cation & anion of the given unknown
    salt.

    Salt number:

    Colour: White

    Structure: Crystalline

    Solubility: Water

    Dry test for basic radicals

     Test tube heating:

    Experiment Observation Inference


    A pinch of salt was White residue was Al 3+
    may be present.
    taken in a clean and glown on heating. A
    dry test tube and was swelling of salt took
    heated strongly. place.

     Charcoal Cavity Test:

    Experiment Observation Inference


    A pinch of salt was An infusible Al 3+
    may be present.
    taken in a charcoal incandescent white
    cavity & it was heated residue was obtained.
    in an oxidizing flame
    with a blowpipe.

     Cobalt Nitrate Test:

    Experiment Observation Inference


    One drop of cobalt Blue mass was Al 3+
    may be present.
    nitrate was added to obtained.
    the above infusible
    incandescent white
    mass obtained in a
    charcoal cavity &
    heated again in
    oxidizing flame by

    ODM Educational Group Page 1


    | CHEMISTRY| PRACTICAL NOTES

    using a blowpipe.

    I. Dry test for acid radicals

    Experiment Observation Inference


    A pinch of salt was No effervescence took CO , SO32-, S2-, NO2-
    3
    2-

    taken in a clean and place. are absent.


    dry test tube and 1 ml
    of dilute H2SO4 was
    added to it.
    II.

    Experiment Observation Inference


    A pinch of salt was No effervescence took Cl , Br , I- , NO3- are
    - -

    taken in a clean and place. absent.


    dry test tube and 1 ml
    of Conc. H2SO4 was
    added to it.

    I. Wet test for acid radicals

    Experiment Observation Inference


    2 ml of salt solution A white ppt. was SO 4
    2-
    may be present.
    was taken in a clean formed.
    test tube and 1 ml of
    BaCl2 solution was
    added to it.

    II. Confirmatory test for SO42-

    Experiment Observation Inference


    To the above Precipitate was SO 4
    2-
    was confirmed.
    precipitate Ammonium dissolved.
    acetate solution was
    added to it in excess.

    Wet test for basic radicals


     Test for Gr-I basic radicals
    ODM Educational Group Page 2
    | CHEMISTRY| PRACTICAL NOTES

    Experiment Observation Inference


    1 ml of salt solution No precipitate was Gr-I basic Pb2+ radical
    was taken in a clean obtained. is absent.
    test tube and 1 ml of
    dil. HCl was added.

     Test for Gr-II basic radicals

    Experiment Observation Inference


    H2S gas was passed No precipitate was Gr-II basic radicals
    through the above obtained. (pb2+, Cu2+, Cd2+, As3+)
    solution. are absent.

     Test for Gr-III basic radicals

    Experiment Observation Inference


    1 ml of salt solution A gelatinous white Gr-III basic radicals
    was taken in a clean precipitate was formed. (Fe3+, Al3+) may be
    test tube then solid present.
    ammonium chloride
    was added till
    saturation &
    ammonium hydroxide
    solution was added till
    alkaline.

     Confirmatory test for Al3+

    Experiment Observation Inference


    In the above Bluish white precipitate Al3+ is confirmed.
    precipitate one ml of floating in a colorless
    dil. HCl was added. solution called the Lake
    Then few drops of blue test.
    litmus solution and
    NH4OH solution in
    excess were added
    dropwise.

    ODM Educational Group Page 3


    | CHEMISTRY| PRACTICAL NOTES

    Conclusion

    The given salt contains acid radicals SO 42- and basic radical Al3+. So, the
    given unknown salt is Al2 (SO4)3.

    ODM Educational Group Page 4

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