JOURNAL OF

AOAC Table of Contents

INTERNATIONAL
A Peer-Reviewed Journal Publishing July/August 1993 VOL. 76, No. 4 JAINEE 76(4)703-944 (1993)
Basic and Applied Research in the
Analytical Sciences Related to Foods,
Drugs, Agriculture, and the Environment
95A New Products
101A For Your Information
EDITORIAL BOARD
105A Books in Brief
Claire Franklin 107A Cumulative Author Index
Chairman and Editor-in-Chief
Dieter Arnold
James Ault
Franklin E. Barton II
Richard A. Durst

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J. Richard Gorham
Anant V. Jain CHEMICAL CONTAMINANTS MONITORING
James Lichtenberg
W. Harvey Newsome 703 Total Organochlorine Content of Fish from the Great Lakes
Joseph Sherma W. Harvey Newsome, Paul Andrews, Henry B.S. Conacher, R.R. Rao, and A.
James T. Tanner Chatt
David L. Terry
707 Organochlorine Pesticides and Polychlorinated Biphenyl Congeners in
JOURNAL EDITORS
Commercial Fish from the Great Lakes
Agricultural Materials W. Harvey Newsome and Paul Andrews
Rodney J. Noel
Drugs, Cosmetics, Forensic Materials DAIRY PRODUCTS
Joseph Westheimer
711 Liquid Chromatographic Method for Determination of Iodine in Milk:
Food Chemical Contaminants
Albert E. Pohland Collaborative Study
Residues and Trace Elements David Sertl and William Malone
Joseph Sherma
DRUG RESIDUES IN ANIMAL TISSUES
Food Composition and Additives
James F. Lawrence
720 Simultaneous Determination of Xylazine and Its Major Metabolite,
Chemical Contaminants Monitoring
2,6-Dimethylaniline, in Bovine and Swine Kidney by Liquid
James D. MacNeil
Chromatography
Statistical Analysis
David C. Holland, Robert K. Munns, Jose E. Roybal, Jeffrey A. Hurlbut, and
George W. Latimer, Jr Austin R. Ix>ng
Food Biological Contaminants
George J. Jackson 725 Liquid Chromatographic Method for Determination of Sulfamethazine
Residues in Milk: Collaborative Study
JOURNAL STAFF
JohnD. Weber and Michael D. Smedley
Publications Director: Krystyna A. Mclver
Managing Editor: Robert E. Rathbone ENVIRONMENTAL ANALYSIS
Assistant Editor: Scott Reardon
Production: Thomas McMullan 730
Advertising:
Pararosaniline as a New Chromogen for the Extractive Spectrophotometric
Christine Barger
Subscriptions: Mark Stewart
Determination of Trace Amounts of Hydrogen Sulfide in Air
B.S.M. Kumar and N. Balasubramanian
AOAC BOARD OF DIRECTORS
President: Henry B.S. Conacher
President-Elect: Arvid Munson
Secretary/Treasurer: Alan R. Hanks
Copyright, 1993, by AOAC International, Inc. All rights reserved. The Journal of AOAC
Immediate Past
International (ISSN 1060-3271) is published bimonthly by AOAC International, Suite 400,
President: Edgar R. Elkins 2200 Wilson Blvd, Arlington, VA 22201 -3301 USA. Subscriptions for Vol. 76 (1993) are: '
Directors: Paul R. Beljaars Members, $120.00 in U.S., $158.00 outside U.S.; Nonmembers, $175.00 in U.S., $213.00
George H. Boone outside U.S. Second class postage paid at Arlington, VA, and additional mailing offices. Ab-
Eugene J. Klesta stracted or indexed in AGRICOLA, Analytical Abstracts, Biological Abstracts, Cambridge Sci-
Raymond Matulis entific Abstracts, Chemical Abstracts, Current Advances in Ecological Sciences, Current
Albert E. Pohland Contents, and others. Printed in USA.
P. Frank Ross
POSTMASTER: Send address changes to AOAC International, Suite 400,2200 Wilson
Executive Director: Ronald R. Christensen Blvd, Arlington, VA 22201-3301 USA.
 FEEDS

735 Rapid Determination of Supplemental Vitamin E Acetate in Feed Premixes by

Capillary Gas Chromatography
Svatomir Kmostak and David A. Kurtz

741 Influence of Water on the Near Infrared Spectra of Model Compounds

James B. Reeves III

FERTILIZERS

749 Comparison of Texas Liquid Sampler with Missouri Bottle for Sampling
Liquid Fertilizers: Collaborative Study
George W. Latimer, Jr

FOOD ADDITIVES

754 Simultaneous Determination of Flavor Enhancers Inosine 5'-Monophosphate

and Guanosine 5'-Monophosphate in Food Preparations by Derivative

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Spectrophotometry
Isabel Durdn-Merds, Francisco Salinas, Arsenio Muhoz De La Pena, and
Miguel Lopez Rosas

760 Gas Chromatographic/Mass Spectrometric Determination of Benzene in

Nonstick Cookware and Microwave Susceptors and Its Migration into
Foods on Cooking
Sue M. Jickells, Mark R. Philo, John Gilbert, and Laurence Castle

765 Liquid Chromatographic Method for the Determination of Nine Phenolic

Antioxidants in Butter Oil: Collaborative Study
B. Denis Page

FOOD COMPOSITION

780 Comparison of Kjeldahl Method for Determination of Crude Protein in Cereal

Grains and Oilseeds with Generic Combustion Method: Collaborative
Study
Ronald C. Bicsak

787 Combustion Method for Determination of Crude Protein in Meat and Meat
Products: Collaborative Study
Marcia King-Brink and Joseph G. Sebranek

METALS AND OTHER ELEMENTS

794 Determination of Free and Bound Cd, Zn, Cu, and Ag Ions in Lobster
(Homarus americanus) Digestive Gland Extracts by Gel
Chromatography Followed by Atomic Absorption Spectrophotometry
and Polarography
Chiu L. Chou, John F. Uthe, and Robert D. Guy

798 Determination of Metals in Foodstuffs by Atomic Absorption

Spectrophotometry after Dry Ashing: NMKL Interlaboratory Study of
Lead, Cadmium, Zinc, Copper, Iron, Chromium, and Nickel
Lars Jorhem

MICROBIOLOGICAL METHODS

814 Detection of Salmonella in Dry Foods Using Refrigerated Pre-Enrichment and

Enrichment Broth Cultures: Interlaboratory Study
Jean-Yves D'Aoust, Anne M. Sewell, and Paula Greco

92A JOURNAL O F AOAC INTERNATIONAL VOL. 76, No. 4,1993

822 AutoMicrobic System for Biochemical Identification of Listeria Species
Isolated From Foods: Collaborative Study
Loralyn Harris and John Humber

831 Comparison of MICRO-ID Listeria Method with Conventional Biochemical

Methods for Identification of Listeria Isolated From Food and
Environmental Samples: Collaborative Study
Don L. Higgins and Barbara J. Robison

838 Total Bacterial Count in Raw Milk Using the BactoScan 8000
J.L. Rodriguez-Otero, M. Hermida, A. Cepeda, and C. Franco

MYCOTOXINS

842 Ochratoxin A in Cow's Milk and in Human Milk with Corresponding Human
Blood Samples
Anna Breitholtz-Emanuelsson, Monica Olsen, Agneta Oskarsson, Ira
Palminger, and Karl Hult

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PESTICIDE FORMULATIONS

847 Rapid and Accurate Method for Determination of Niclosamide Released from
Molluscicidal Formulations
Laila H. Emara

PESTICIDE AND INDUSTRIAL CHEMICAL RESIDUES

851 Determination of Methyl 2-Benzimidazolecarbamate in Wine by Competitive

Inhibition Enzyme Immunoassay
Rodney J. Bushway, Lance R. Paradis, Lewis B. Perkins, Titan S. Fan,
Barbara E.S. Young, and Paul E. Walser

857 Optimization of Experimental Conditions for the Supercritical Carbon Dioxide

Extraction of Pesticide Residues from Grains
Jerry W King, Marvin L. Hopper, Ronald G. Luchtefeld, Scott L. Taylor, and
William L. Orton

864 Evaluation of Soxtec Extraction Procedure for Extracting Organic Compounds

from Soils and Sediments
Viorica Lopez-Avila, Karin Bauer, June Milanes, and Werner F. Beckert

881 Liquid Chromatographic Method for Determination of Diquat and Paraquat

Herbicides in Potatoes: Collaborative Study
Brian L. Worobey

PESTICIDE RESIDUES IN ANIMAL TISSUES

888 Supercritical Fluid Extraction of Poultry Tissues Containing Incurred Pesticide

Residues
Janet M. Snyder, Jerry W. King, Loyd D. Rowe, and Julie A. Woerner

TOXICITY TESTING

893 Evaluation and Application of a Bioluminescent Bacterial Genotoxicity Test

Thomas S.C. Sun and Henry M. Stahr

VETERINARY ANALYTICAL TOXICOLOGY

899 pH Method for Determination of Cholinesterase in Whole Blood:

Collaborative Study
Paula Martin Imerman

JOURNAL O F AOAC INTERNATIONAL VOL. 76, No. 4,1993 93A

 VITAMINS AND OTHER NUTRIENTS

902 Rapid Determination of Cholesterol in Single and Multicomponent

Prepared Foods
Sami M. Al-Hasani, Jan Hlavac, and Mark W. Carpenter

TECHNICAL COMMUNICATIONS

907 Extension of a Liquid Chromatographic Method for ./V-Methylcarbamate

Pesticides in Cattle, Swine, and Poultry Liver
M. SherAli, Jerry D. White, Ralph S. Bakowski, Nancy K. Stapleton, Kay A.
Williams, Robyn C. Johnson, Evan T. Phillippo, Robert W Woods, and
Richard L. Ellis

910 Determination of Selenium in Feeds, Premixes, Supplements, and Injectable

Solutions by Hydride-Generated Inductively Coupled Plasma Atomic
Emission Spectrometry
Kim A. Anderson and Brandon Isaacs

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913 Fast Atom Bombardment Mass Spectrometric Analysis of Base Hydrolyzed
y-Lactone
Randall J. Baker

918 Automated Beer Analyzer Method for Determination of Alcohol Content and
Original Gravity of Beer: Summary of Collaborative Study
Peter W. Gales and Mark Schwiesow

920 Citrate Insoluble P2O5: Problems with Ammoniated Fertilizers

Joseph E. Gliksman

923 Enzymatic-Gravimetric Determination in Foods of Dietary Fiber as Sum of

Insoluble and Soluble Fiber Fractions: Summary of Collaborative Study
Roger Mongeau and Rene Brassard

926 International Harmonized Protocol for Proficiency Testing

of (Chemical) Analytical Laboratories
Michael Thompson and Roger Wood

941 Discriminating Between Adult Mandibles of Oryzaephilus surinamensis and

Oryzaephilus mercator Using Setal Brush Length
MarkM. Wheeler

94A JOURNAL OF AOAC INTERNATIONAL VOL. 76, No. 4,1993