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    Speedwave Entry Vessel Cleaning

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    agansh01

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    © All Rights Reserved
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    Speedwave Entry Vessel Cleaning

    Uploaded by

    agansh01
    5 views2 pages

    Original Title

    Speedwave-Entry-Vessel-Cleaning

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    © © All Rights Reserved

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    Copyright:

    © All Rights Reserved
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    5 views2 pages

    Speedwave Entry Vessel Cleaning

    Uploaded by

    agansh01

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    of 2

    APPLICATION NOTE | SPEEDWAVE ENTRY S.

    1/2

    Environment, Geology
    Cleaning of Microwave Digestion Vessel

    Summary Blank digestion for basic cleaning of new digestion vessels.

    Method
    Equipment
    Type Manufacturer
    speedwave Entry Berghof Products + Instruments GmbH
    DAP-60K Berghof Products + Instruments GmbH
    Reagents Acid Volume
    HNO3 (65%) 9.0 mL
    HCI (37%) 1.0 mL
    Procedure
    Put 9.0 mL of HNO3 and 1.0 mL of HCl into the digestion vessel. Close the vessel and heat in
    the microwave with the following program.
    Temperature Program** Step T [°C] Ta [min] Time [min] Power [%]
    1 170 5 5 90
    2 200 1 15
    3 75 1 10
    4
    5
    Note: To avoid foaming and splashing wait until the vessels have cooled to room temperature (about 20 min). Carefully open the digestion vessel in a
    fume hood wearing hand, eye and body protection since a large amount of gas will be produced during the digestion process.

    Analysis
    Blank concentrations of new DAP-60+ vessels after 3 subsequent blank digestions.
    Element 1. Digestion* 2. Digestion* 3. Digestion*
    Li µg/l 0.2 <0.025 <0.025
    Be µg/l <0.25 <0.25 <0.25
    Mg µg/l 20.1 5.0 1.9
    Al µg/l 19.8 <0.25 <0.25
    V µg/l <0.025 <0.025 <0.025
    Cr µg/l 2.6 0.3 <0.05
    Mn µg/l 0.6 0.04 <0.05
    Co µg/l 0.1 <0.025 <0.025
    Ni µg/l 1.3 0.1 <0.025
    Cu µg/l 0.53 <0.025 <0.025
    APPLICATION NOTE | SPEEDWAVE ENTRY | ENVIRONMENT, GEOLOGY S. 2/2

    Zn µg/l 12.5 2.3 0.3


    As µg/l <0.025 <0.025 <0.025
    Sr µg/l 0.2 <0.025 <0.025
    Ag µg/l 0.2 <0.025 <0.025
    Cd µg/l 0.08 <0.025 <0.025
    Ba µg/l 0.5 <0.05 <0.05
    Pb µg/l 0.6 0.1 <0.05
    Bi µg/l <0.025 <0.025 <0.025
    U µg/l <0.001 <0.001 <0.001
    Fe µg/l 7.5 0.4 <0.25
    * mean values of 6 digestions

    Note: This application serves only as a guide line and may need to be optimized for your sample.
    ** The program “Cleaning Vessel” is preinstalled on the controller.

    Berghof Products + Instruments GmbH | Harretstrasse 1 | 72800 Eningen | www.berghof.com

    53-0202-87-00-01-003 | Speedwave-Entry-Vessel-Cleaning, Änderungen und Irrtümer vorbehalten, Printed in Germany

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