SAILO
SAILO
SAILO
Procedure
i) Fill the burette with solution A
ii) Using pipette, pipette 25cm³ of solution B and place in a conical flask
iii) Add 2 drops of phenolphthalein indicator and titrate with solution A until the
pink colour disappears
iv) Record your results in the table below
v) Repeat the titrations two more times and complete the table below.
I II III
Final burette reading
Initial burette reading
Volume of solution A
used(cm³)
Procedure
vi) Fill the burette with solution A
vii) Using pipette, pipette 25cm³ of solution B and place in a conical flask
viii) Add 2 drops of methyl orange and titrate with solution A
ix) Record your results in the table below
x) Repeat the titrations two more times and complete the table below.
I II III
Final burette reading
Initial burette reading
Volume of solution A
used(cm³)
You are required to determine the value of X in the formula of the carbonate
Procedure
i) Using pipette, pipette 25cm3of solution B and place in a conical flask
ii) Add 2 drops of methyl orange indicator
iii) Fill the burette with solution A
iv) Titrate solution B using solution A and fill the table below
v) Repeat two more times and complete the table below
I II III
Final burette reading
Initial burette reading
Volume of solution A
used(cm³)
EXPERIMENT 4
Procedure
i) Using a clean measuring cylinder, measure 50cm3 of solution R and transfer in
100cm3plastic beaker.
ii) Add all solid A at once into the moments of the beaker, stir until
effervescence stops.
iii) Transfer this solution into a 250cm3 volumetric flask and add distilled water
up to the mark. Label this solution as B
iv) Fill the burette with solution Q
v) Pipette 25.0cm3 of solution B into a conical flask. Add 2 drops of
phenolphthalein indicator.
vi) Titrate solution B using solution Q.
vii) Record your results in the table
viii) Repeat the titration two more times and complete the table below.
I II III
Final burette reading
Initial burette reading
Volume of solution Q
used(cm³)
Calculate the:
i) Average volume of solution Q used.
EXPERIMENT 5
You are provided with:
0.4M solution of acid A(phosphoric acid)
Solution B containing 10.0g of NaOH in 250cm3 of solution.
You are required to determine the basicity of the acid A
Procedure
Pipette 25.0cm3portions of solution B and titrate against solution A in a burette using
phenolphthalein indicator and fill in the table
I II III
Final burette reading
Initial burette reading
Volume of solution A
used(cm³)
EXPERIMENT 6
Procedure
Using pipette, pipette 25cm3of solution Y and place in a conical flask
Add 2 drops of methyl orange indicator
Fill the burette with solution X
Titrate solution Y using solution X and fill the table below
Repeat two more times and complete the table below
I II III
Final burette reading
Initial burette reading
Volume of solution X
used(cm³)
a) Calculate the:
i) Average volume of solution X used.
ii) Determine the molar mass of solid Y and hence work out the molar
mass of A in the compound Na2A
EXPERIMENT 7
You are required to determine the value of x in the formula of the acid.
The dibasic acid reacts with sodium hydroxide as follows:
2NaOH + CH2)X (COOH2) _________2H2O + CH2)X (COONa)2
Procedure
Pipette 25.0cm3of sodium hydroxide solution and titrate against the acid solution in a
burette using phenolphthalein indicator and fill in the table.
I II III
Final burette reading
Initial burette reading
Volume of acid used(cm³)
EXPERIMENT 8
You are required to standardize the potassium manganate (VII) solution using the
ammonium iron (II) sulphate, solution B
Procedure
I II III
Final burette reading
Initial burette reading
Volume of solution A (cm³)
c) Calculate the number of moles of iron (II) ions in the 25ml of solution B.
d) Using the ionic equation for the reaction between manganate (VII) and iron (II)
ions given below, calculate the concentration of manganate (VII) ions in solution
A in moles per litre.
Reagents:
Experiments 1
0.2M HCL
0.1MNaOH
Phenolphthalein indicator
Experiment 2