The Formulation of Hibiscus Rosa- Sinensis, Cocos Nucifera, and Aloe Barbadensis

Miller Shampoo

Buriongan, Saira A.

Maygay, Daphen Claire

Palmaira, Vanessa Shane R.

Tomo, Kimberly M.

Quinoviva, Khrys Lhianne S.

S.Y. 2023-2024
 Chapter I
Introduction

Background of Study

Many individuals experience and struggling with their hair and scalp condition, such as

thinning hair, hair loss, breakage and slow growth. Some may suffer from dandruff and itchy

scalp. These hair and scalp problems can lead to discomfort (Staff, 2023). Shampoo is an

essential product used by individuals in their daily hygiene routine to maintain healthy hair and

scalp. A shampoo not only provides the cleaning of the scalp skin and hair as its primary

function, but in addition also serves to condition and beautify (Rathi et al., 2018).

The beneficial plants for hair and scalp are Hibiscus rosa- sinensis, Cocos nucifera, and

Aloe barbadensis miller. Hibiscus rosa- sinensis give nutrients for the hair and scalp as well as

antioxidants, vitamins, and mineral, that can stop hair loss. It has a high concentration of vitamin

C, which boosts the production of collagen, a protein that helps to strengthen hair. It also

includes amino acids, which help nourish follicles and encourage the growth of healthy hair

(Desk, 2023). However, according to Ayurveda (2021), that hibiscus leaf extracts are beneficial

for hair because they regulate the pitta dosha. The pitta dosha governs the body’s metabolism. An

imbalance between pitta and dosha is the source of excess heat build-up in the body. It damages

hair, making it thinner and leading early graying.

While Cocos nucifera can improve the health and condition of your hair. Coconut oil is

edible oil made from pressing the meat inside coconut, it is a common and effective moisturizing

ingredient in lotions and hair care products. It works by helping prevent protein loss in the hair
because it has caprylic acid C, myristic acid, and linoleic acid (Austin, 2023). However, coconut

oil is incredibly difficult to remove from hair. This is due to the oil's ability to cover the hair shaft

and its extreme density. Because of this, it could take several shampooing’s to completely

remove the oil (Foreo, 2022).

Then Aloe barbadensis miller is a great natural treatment for dry hair or an itchy scalp, it

has nourishing properties, and the vitamins and minerals that are present in the plant keep your

hair strong and healthy. Because of its antibacterial and antifungal, studies indicate that it helps

with dandruff (Ruggeri, 2023). However, if person have an allergy to an aloe vera can cause

specific side effects such as itching, burning sensation, rashes, and hives (Jangam, 2024).

The study aims to make a shampoo product using the Hibiscus Rosa- Sinensis, Cocos

Nucifera, and Aloe Barbedensis Miller because these natural ingredients are known for their

beneficial properties for hair and scalp.

Conceptual Framework

Independent Variable Dependent Variable

Concentration of Hibiscus rosa- Hair and scalp condition

sinensis, Cocos nucifera, and improvement in hair such as;
Aloe barbedensis miller extract prevent dandruff, less hairloss,
and hair growth

Control Variable

Applied method
• 5ml
• 10ml

Figure 1: The schematic diagram showing the relationship between the variables of the study.
Statement of the Problem

Hair significantly contributes to the beauty and appearance of both men and women, and

it plays a crucial role in boosting their confidence. However years passed, many individuals have

facing various challenges related to hair and scalp problems such as dandruff, hair loss, and other

hair issues.

Research Question

1. How does the effect of the combined formulation of Hibiscus rosa- inensis, Cocos

nucifera, and Aloe barbadensis miller in hair scalp problems?

2. Which common hair and scalp problems can effectively be addressed by the shampoo

product formulated from Hibiscus rosa- sinensis, Cocos nucifera, and Aloe barbadensis

miller?

3. Which is more effective between 5ml and 10ml concentration Hibiscus rosa- sinensis,

Cocos nucifera, and Aloe barbadensis miller shampoo in applying into hair and scalp?
Objective of the Study

1. determine the effect of the combined formulation of Hibiscus rosa- sinensis, Cocos

nucifera, and Aloe barbadensis miller on hair and scalp conditions:

2. determine the specific hair and scalp problems that can effectively addressed by the

shampoo product formulated from Hibiscus rosa- sinensis, Cocos nucifera, and Aloe

barbadensis miller; and

3. assess the comparative effectiveness in applying 5ml and 10ml concentrations of

Hibiscus Rorsa- sinensis, Cocos nucifera, and Aloe barbadensis miller shampoo in hair and

scalp problems.

Hypothesis of the Study

H₀: The combined formulation of Hibiscus rosa- sinensis, Cocos nucifera, and Aloe

barbadensis miller in a shampoo product will not significantly improve hair and scalp conditions,

including dandruff prevention, reducing hair loss, and promoting hair growth.

Hₑ: The combined formulation of Hibiscus rosa- sinensis, Cocos nucifera, and Aloe

barbadensis miller in a shampoo product will significantly improve hair and scalp conditions,

including dandruff prevention, reducing hair loss, and promoting hair growth.

Significance of the study

This study aims to determine the effectiveness of the shampoo product that formulated

from Hibiscus rosa- sinensis, Cocos nucifera, and Aloe barbadensis miller.
Scope and Delimitation

This study will only focus and limited only to the effectiveness of the researchers

shampoo product formulated from Hibiscus rosa-sinensis, Cocos nucifera, and Aloe barbadensis

miller and will not include other shampoo product.

Definition of Terms

Concentration - The amount of a substance per defined space (Google.com n.d). In this

study, concentration is considered as manipulated amount of Hibiscus rosa- sinensis, Cocos

nucifera, and Aloe barbadensis miller.

Hibiscus rosa - sinensis – refers to a large showy asiatic or small tree having large single

or double red to deep-red flowers (Google.com n.d). In this study, Hibiscus rosa - sinensis is

considered as one of the main ingredients in making the shampoo product.

Cocos nucifera – is commonly called coconut or coconut palm, is a tall tree that is native

to tropical islands in the Western Pacific (Google.com n.d). In this study, Cocos nucifera is

considered as one of the main ingredients in making the shampoo product.

Aloe barbadensis miller - known as Aloe Vera in renowned for its remarkable properties

in promoting health, skin care, and medical benefits (Google.com n.d). In this study, Aloe

barbadensis miller is considered as one of the main ingredients in making the shampoo product.

Dandruff - Common condition then causes the skin on the scalp to flake (Google.com

n.d). In this study, dandruff prevention is one of the expected outcomes of the researchers for the

product they will develop.

 Hairloss - Disorder caused by an interruption in the bodies cycle of hair production

(Google.com n.d). In this study, hair loss is the one of the expected outcomes of the researchers

for the product they will develop.

Applied Method – Tools to help answer questions when there are constraints of time,

dollars, and freedom of action (Google.com n.d). In this study, applied method can be considered

as measurements of concentration.
 Chapter II
Review of Related Literature

Hibiscus rosa - sinensis

The saponins in Hibiscus Rosa-Sinensis is the natural cleansing instrument that works

for hair cleansing in addition of amino acids stimulate the keratin production which gives

structure for hair (Binu, 2021). Dermatologist mentioned in their Journal of Emerging

Technologies and Innovative Research, that people who has low porosity hair, using Hibiscus

Rosa-Sinensis can be a potential solution to hair and scalp problems because Hibiscus Rosa-

Sinensis is rich in amino acids, antioxidants, vitamin C, mucilage fiber, flavonoids, and moisture.

Fresh Hibiscus Rosa-Sinensis flower has anti-inflammatory, antioxidant properties,

and a high level of vitamin C that is essential for collagen production and hair growth, which

helps to improve hair growth and scalp health (Kiran, 2023). According to Arshiya Syeda (2023),

that the natural coloring pigments in our body, antioxidants, and vitamins present in hibiscus are

said to help in producing melanin, and hibiscus has been used as a natural dye to cover gray hair

traditionally. It helps prevent premature graying of hair and is a good hair conditioner. When the

first traces of gray hair appear, they should begin using hibiscus for hair, use on a regular basis to

delay premature graying. So that their natural hair color may be preserved and harm to the hair

pigment can be avoided the antioxidants in hibiscus, which fight free radicals (Sushimita, 2023).

Hibiscus has been linked to headaches, ringing in the ear, nausea, and dermatitis. It may also

cause blood pressure to drop, and hibiscus may dangerous to those who are sensitive or allergic

to Hibiscus Rosa Sinensis and to members of the Malvaceae plant family (Metcalf, 2023).
Cocos nucifera

Cocos nucifera has packed with fatty acids and a lauric acid a type of saturated fat

abundant used to restore luster to dry, tame frizz, relieve dandruff, protect and restore the

damaged hair (Wong, 2023). Lauric acid is the main medium-chain fatty acid found in coconut

oil. Because of this coconut oil has long and straight structure that makes it easier for the hair

shaft to absorb it deeply (West, 2021). Coconut oil can be absorbed by the hair, because it is very

notorious hair care product. It works well as a detangler, heat protectant, deep conditioner, deep

cleansing and lice treatment. It might also aid in hair growth and the management of dandruff

(Shoemaker, 2022). Coconut oil has the ability to make fine hair appear oily, lifeless, and heavy,

refrain from building up because it might make coarse hair tight in certain individuals. Coconut

oil may also result in blocked pores (Wong, 2023). Despite the fact that coconut oil is fantastic

for hair, using too much of it might result in oily hair since it builds up on the scalp and make

hair appear oily (Foreo, 2022).

Aloe barbadensis miller

Aloe vera is a plant that has gel-like inside of thick leaves and according to National

Cancer Institute (NCI), it is composed of water, carbohydrates polymers, and these are the

ingredients that make it ideal for managing hair and scalp problem (Cavallo, 2023). An aloe vera

contains an abundance of strong antioxidants called polyphenols, which neutralized harmful free

radicals in the body. Aloe vera gels are typically regarded as skin safe, however aloe vera can

cause excessive oil production or dryness if it is used excessively or overly (Memon, 2022).

Vitamins A, C, and E can be found in aloe vera. These three vitamins support healthy cell growth

and lustrous hair by aiding in cell turn over. Aloe vera gel also contains folic acid and vitamin
B12. These two elements together can prevent hair loss (Watson, 2023).

Lane mentioned that Aloe barbadensis miller has benefits for hair that can heal the scalp

problems. Aloe barbadensis miller is a humectant substance that help hydrate the skin, nails and

hair because humectants attract water. The examples of humectants are hyaluronic acid and

glycerin (Wicks, 2022). Vitamins A, C, and E can be found in aloe vera. These three vitamins

support healthy cell growth and lustrous hair by aiding in cell turn over. Aloe vera gel also

contains folic acid and vitamin B12. These two elements together can prevent hair loss.

Additionally, the common product that individuals apply to their skin after being in the sun is

aloe vera. This is as a result of its cooling qualities and high collagen content. Aloe vera's high

vitamin content makes it possible that it could also help your hair heal from sun damage (Watson,

2023). In general, there are no risk associated with administering aloe vera topically. For certain

people, it could be triggering an allergy, leading to a skin rash (WebMd, 2024).

 Chapter III
Methodology

This chapter discuss in detail the research design and approach process in this study, the

population and sampling procedures, extraction procedure, Plant materials and research locale.

Research Design

The researchers will be using an experimental method with the scientific approach,

where a set of variables are kept constant while the other variables are being measured as the

subject of experiment. It will support the study in terms of determining the observation to the

efficacy of the product formulated by Hibiscus rosa-sinensis, Cocos nucifera, and Aloe

barbadensis miller in hair treatment.

Research Locale

The study will be developed at Science Laboratory of La Purisima High School Wao,

Lanao del Sur. This strategy can ensure the study’s easier and more successful development.

Figure 2: The Research Locale Map

Materials and Reagents

The materials will be use in this study are blender, mortar and pestle, cheesecloth or fine

mesh strainer, pot, clean containers for storing the extract, funnel, and filter paper.

The reagent will be using in this study is ethanol (ethyl alcohol) to enhance the

extraction and pH adjuster to aim specific pH range for their final extraction.

Plant Material

The plant materials are Hibiscus rosa-sinensis commonly called as Gumamela, Cocos

nucifera commonly called as Coconut and Aloe barbadensis miller commonly referred as Aloe

vera were collected at Purok 4 Manila group Wao, Lanao del Sur. Plants were identified by the

researchers.

Extraction of Plant Material

Hibiscus rosa-sinensis first, dry and grind the flowers and leaves into a fine powder.

After that mix 10g of this powder with a 75milliliters of ethanol and let it lie for 24 hours at

room. Then, use a rotary evaporator to evaporate ethanol, concentrating the extract to obtain

the flavonoids. Grate the fresh Cocos nucifera meat, use a cold press extractor to press the

grated coconut and obtain the oil. Mix the gel from Aloe barbadensis miller with ethanol and

set it for 24 hours, then filter and use a rotary evaporator to concentrate the extract.
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