Electrolysis Experiment
Electrolysis Experiment
Electrolysis Experiment
In electrolysis, components of water (a compound) are separated through the passage of an electric
current.
Materials needed:
Improvised electrolysis apparatus
• 5% sodium hydroxide (NaOH) solution
• Connecting wires (black and red insulation)
• 9V dry cell
• Plastic syringes will serve as “collecting syringe”
• Incense or bamboo stick
• Safety matches
Procedure:
1. Fill the sample container of the electrolysis apparatus half-full with 5% sodium hydroxide (NaOH)
solution.
2. Fill each electrolysis syringe with 5% sodium hydroxide (NaOH) solution up to the zero mark. To do this,
insert the tip of the ‘collecting syringe’ through the whole of the plastic straw and suck out the air.
Refer to figure 2. Initially, the plunger of the connecting syringe should be in the zero position. The
basic solution will rise and fill the electrolysis syringe as you pull the plunger of the collecting syringe”
3. Attach the connecting wires to the stainless screws. Attach the black wire to the negative (-) terminal of
the dry cell. Attach the red wire to the positive (-) terminal of the dry cell. The stainless screw that is
attached to the black wire is the negative electrode; while the stainless screw that is attached to the
red wire is the positive electrode.
4. Once the wires are connected with the dry cell, electrolysis will start. Electrolyze until6-8 ml of a gas is
obtained at the negative electrode.
5. Draw out the gas at the negative electrode with the collecting syringe. To do this insert the tip of the
collecting syringe into the straw on the side of the negative electrode. While drawing out the gas, you
will notice that the solution will rise up and fill the electrolysis syringe again. Make sure that the
collecting syringe will only contained the gas generated. However, take this chance to refill the
electrolysis syringe with the solution. When the level of the solution reaches zero mark in the
electrolysis syringe, slowly lower down the collecting syringe and immediately cover its tip with your
finger.
6. Inject the collected gas into an inverted test tube and again cover the mouth of the test tube and again
cover the mouth of the test tube with your thumb. Immediately test the gas collected with a lighted
match or a bamboo stick/incense.
7. Question: What happened when you placed a lighted match near the mouth of the test tube?
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8. Continue to electrolyze until 6-8Ml of the gas is obtained at the positive electrode.
9. Draw out the gas from the positive electrode and immediately inject into test tube held in upright
position. Immediately test the gas collected by thrusting a glowing (no flame) bamboo stick all the way
down towards the bottom of the test tube..
10. Note: Extinguish any flame from the burning stick but leave it glowing before thrusting it inside the test
tube.
11. Question: What happened when you thrust a glowing bamboo stick inside the test tube?
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Leader: ____________________
Members:
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