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    CoA TDS1000 - LRAD7678

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    Laboratorium BBIHP

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    © All Rights Reserved
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    CoA TDS1000 - LRAD7678

    Uploaded by

    Laboratorium BBIHP
    13 views2 pages

    Original Title

    CoA TDS1000_LRAD7678

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    13 views2 pages

    CoA TDS1000 - LRAD7678

    Uploaded by

    Laboratorium BBIHP

    Copyright:

    © All Rights Reserved
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    of 2

    Document 20550009 Version 2.

    Certificate of Analysis - Certified Reference Material


    Total Dissolved Solids 1000 mg/L Calibration Standard
    Product no.: TDS1000-100ML
    Lot no.: LRAD7678
    Expiry Date: January 2027
    Manufacturing Date: January 2024
    Storage: ROOM TEMPERATURE (2 °C to 30 °C)
    Solvent/Matrix: DI WATER
    Certificate version: LRAD7678.01 (Note: Certificates may be updated due to
    the availability of new data. Check our website at:
    www.sigma-aldrich.com for the most current version.)

    Certified Values:

    Certified Raw Material Raw Material


    Analyte Units Value Purity,% Lot

    TOTAL DISSOLVED SOLIDS mg/L 1000 ± 3 99.99 20K305207


    Additional Information: SAMPLE PREPARATION
    The sample is ready to use.
    No sample preparation is required.
    Metrological traceability: Traceable to the SI and higher order standards from NIST through an unbroken
    chain of comparisons. The balance used to weigh raw materials is accurate to
    +/-0.0001 g and calibrated regularly using mass standards traceable to NIST. All
    dilutions were performed gravimetrically. Additionally, individual analytes are
    traceable to NIST SRMs where available and specified above.
    Measurement method: Where applicable, the assigned value is based on a purity determination by mass
    balance and gravimetrically prepared value.
    Intended use: Intended for R&D and Analytical Use only. Not for drug, household or other uses.

    Packaging: 100 ML IN HDPE BOTTLE


    Instructions for handling Use on the as is basis. The internal pressure of the container may be slightly
    and correct use: different from the atmospheric pressure at the user`s location. Open slowly and
    carefully to avoid dispersion of the material.
    Health and safety All chemical reference materials should be considered potentially hazardous and
    information: should be used only by qualified laboratory personnel. Please refer to the Safety
    Data Sheet for detailed information about the nature of any hazard and
    appropriate precautions to be taken.
    Accreditation: Sigma-Aldrich RTC is accredited by the US accreditation authority ANAB as a
    registered reference material producer AR-1470 in accordance with ISO 17034.
    Certificate issue date: 03 JAN 2024

    Andy Ommen - QC Manager Scott Stetler - QA Manager

    Sigma-Aldrich RTC, 2931 Soldier Springs Rd. Laramie, WY 82070, USA;


    Tel. 1 307-742-5452; Fax 1 855-831-9211; www.sigmaaldrich.com
    Sigma-Aldrich RTC is a subsidiary of Merck KGaA, Darmstadt, Germany.

    Certificate Page 1 of 2 Certificate version 01


    Details on metrological This standard has been gravimetrically prepared using balances that have been
    traceability: fully qualified and calibrated to ISO 17025 requirements. All calibrations utilize
    NIST traceable weights which are calibrated externally by a qualified ISO 17025
    accredited calibration laboratory to NIST standards. Qualification of each balance
    includes the assignment of a minimum weighing by a qualified and ISO 17025
    accredited calibration vendor taking into consideration the balance and installed
    environmental conditions to ensure compliance with USP tolerances of NMT
    0.10% relative error. Fill volume to predetermined specifications is
    gravimetrically verified throughout the dispensing process using qualified and
    calibrated balances. Further traceability to a corresponding Primary Standard may
    be achieved through a direct comparison assay. Where a Primary Standard is
    available, the assay value will be included in the specified section of the COA.

    Associated uncertainty: Ucrm - Uncertainty values in this document are expressed as Expanded
    Uncertainty (Ucrm) corresponding to the 95% confidence interval. Ucrm is
    derived from the combined standard uncertainty multiplied by the coverage factor
    k, which is obtained from a t-distribution and degrees of freedom. If k is not
    provided, assume a value of 2.0. The components of combined standard
    uncertainty include the uncertainties due to characterization, homogeneity, long
    term stability, and short term stability (transport). The components due to
    stability are generally considered to be negligible unless otherwise indicated by
    stability studies. The mathematical representation of the Ucrm calculation is as
    follows:
    2 2 2
    𝑈𝑐𝑟𝑚 = 𝑢𝑐ℎ𝑎𝑟𝑎𝑐𝑡𝑒𝑟𝑖𝑧𝑎𝑡𝑖𝑜𝑛 + 𝑢ℎ𝑜𝑚𝑜𝑔𝑒𝑛𝑒𝑖𝑡𝑦 + 𝑢𝑠𝑡𝑎𝑏𝑖𝑙𝑖𝑡𝑦 × 𝑘

    Homogeneity assessment: Homogeneity was assessed in accordance with ISO Guide 35. Completed units
    were sampled using a random stratified sampling protocol. The results of
    chemical analysis were then compared by Single Factor Analysis of Variance
    (ANOVA). The uncertainty due to homogeneity was derived from the ANOVA.
    Heterogeneity was not detected under the conditions of the ANOVA.
    Stability assessment: Significance of the stability assessment will be demonstrated if the analytical
    result of the study and the range of values represented by the Expanded
    Uncertainty do not overlap the result of the original assay and the range of its
    values represented by the Expanded Uncertainty. The method employed will
    usually be the same method used to characterize the assay value in the initial
    evaluation.

    Certificate of analysis revision history:

    Certificate version Date Reason for version


    LRAD7678.01 03 JAN 2024 Original release date
    Disclaimer: The purchaser is required to determine the suitability of this product for
    any particular application. Sigma-Aldrich RTC makes no warranty of any kind, express
    or implied, other than its products meet all quality control standards set by
    Sigma-Aldrich RTC. We do not guarantee that the product can be used for any
    particular application.
    The vibrant M, Supelco, TraceCERT and Sigma-Aldrich are trademarks of Merck KGaA, Darmstadt, Germany or its affiliates.
    All other trademarks are the property of their respective owners. Detailed information on trademarks is available via
    publicly accessible resources. © 2018 Merck KGaA, Darmstadt, Germany and/or its affiliates. All Rights Reserved.

    Certificate Page 2 of 2 Certificate version 01 LRAD7678

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