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Act 10

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Abigail Mae P.

Yanong
CHM121.2 - A56

ACTIVITY 10

A. Preparation of 0.01M EDTA Solution


Weigh accurately 0.9306 g disodium salt EDTA, C10H14N2Na2O8.2H20 (MW: 372.24g/mol)
and 0.025 g MgCl2.6H20 into a clean 100ml beaker.

Dissolve the solids in water, transfer the solution to a clean 250ml volumetric flask and dilute to
the final volume of the flask.

Mix the solution thoroughly and label the solution.

B. Determination of Total Hardness in Water

Obtain the water to be analyzed from the instructor. Measure 50-mL and transfer into each of
three 250-mL Erlenmeyer flasks. Then to the first sample, add 1.0 ml of the buffer solution and 5
drops of the Eriochrome Black T Indicator solution.

Titrate the solution with the prepared 0.01M EDTA solution to a color change of wine -red to
pure blue. And record the volume of EDTA solution consumed in reaching the end point of the
titration.

Repeat the procedure (2-4) on the other two portions of the water. Then, calculate the total
hardness of the water as parts per million(ppm) of calcium carbonate.

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