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    (Aluminum Sulphate) Systematic Analysis of Simple Salt No - 10

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    (Aluminum Sulphate) Systematic Analysis of Simple Salt No - 10

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    sharang1234567890
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    ( Aluminum Sulphate )Systematic Analysis of Simple Salt No . 10

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    10 views5 pages

    (Aluminum Sulphate) Systematic Analysis of Simple Salt No - 10

    Uploaded by

    sharang1234567890
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    © All Rights Reserved
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    of 5

    SYSTEMATIC ANALYSIS OF SIMPLE SALT (SALT NO.

    10)
    PRELIMINARY TEST

    1)PHYSICAL EXAMINATION

    a) Note the colour of the white Cu2+, Fe2+, Fe3+ absent


    salt
    b) Note the odour of the no specific odour NH4+, and CH3COO- may be
    salt absent

    2)DRY HEATING TEST

    Heat a pinch of salt in a dry test


    tube and note the following
    observation

    a)Gas evolved No gas evolved CO32- may be absent

    b) sublimation No sublimate formed Aluminum chloride , iodide may


    be absent

    Lead nitrate , barium nitrate ,


    c) Descrepitation No cracking sound observed potassium chloride , potassium
    iodide may be absent

    Zn 2+may be present

    d) colour of the residue Yellow when hot and white


    when cold

    3)FLAME TEST
    Prepared a paste of the salt with No characteristic flame Cu2+, Ba2+ , Sr2+ , Ca2+ may be
    conc. HCl and performed the absent
    flame test

    4)COBALT NITRATE TEST

    To the salt solution added a few Green residue is absent Zn 2+,Al 3+, Mg 2+ may be absent
    drops of cobalt nitrate solution ,
    dipped filter paper in it and
    introduced it in a luminous flame

    5)DILUTE SULPHURIC ACID TEST

    Treated a pinch of the salt with No gas evolved CO32- absent


    dil. H2SO4 and warmed

    6)CONCENTRATED SULPHURIC
    ACID TEST

    Treated a pinch of the salt with


    conc. H2SO4 and warmed No reddish brown gas evolved NO3- absent

    7)KMnO4 TEST

    To a pinch of salt added dil H2SO4 No decolourisation Cl- , Br-, I- , Fe2+ are absent
    and then add a drop of KMnO4
    solution

    8)COPPER CHIPS TEST

    Heated a pinch of salt with No reddish brown gas NO3- absent


    conc. H2SO4 and a few copper
    chips
    9)MnO2 TEST

    Heat a pinch of solid salt with MnO2 No greenish yellow gas Cl- absent
    evolved which bleaches
    And conc. H2SO4 moist blue litmus paper

    10)BaCl2 TEST

    Boil small amount of a salt with dil. White ppt is formed which SO4– may be present
    HCl in a test tube. Filter the contents is insoluble in Dil.HCl
    and to the filtrate added few drops of

    BaCl2 solution.

    CONFIRMATORY TEST FOR ACID RADICAL


    BaCl2 TEST

    Boil small amount of a salt with dil. White ppt is formed which SO4–2may be confirmed
    HCl in a test tube. Filter the contents is insoluble in Dil.HCl
    and to the filtrate added few drops of

    BaCl2 solution

    IDENTIFICATION OF BASIC RADICAL

    11)SODIUM HYDROXIDE (NaOH)TEST

    Heat a pinch of solid salt with No gas evolved NH4+ absent

    NaOH solution .

    PREPARATION OF ORIGINAL SALT


    SOLUTION :
    Prepare original salt solution by
    dissolving a pinch of salt in 10-15ml
    of distilled water.

    GROUP SEPERATION

    a) To a few drops of original solution No precipitate formed Group zero absent (NH4+)
    added 1ml of nessler’s reagent and
    excess of NaOH solution .

    b)To a few drops of original solution No precipitate formed Group I absent


    added 2ml of dil. HCl
    (Pb2+)

    c) To a few drops of original solution No precipitate formed Group II absent


    added 2ml of dil. HCl and then
    passed H 2S gas . (Cu2+)

    d) To a few drops of original solution Gelatinous white Group III present


    added 1ml of NH4Cl and 2 ml of precipitate formed
    NH4OH (Fe3+ , Al 3+) present

    CONFIRMATORY TEST FOR BASIC RADICAL

    a)LAKE TEST :

    Dissolved the above white ppt in Dil. Blue ppt floating in the Al 3+ confirmed
    HCl , add to it 2 drops of blue litmus
    solution . to this added NH4 OH drop colurless solution
    wise till blue colour develops

    b) add sodium hydroxide solution and


    warm.
    White gelatinous ppt Al 3+ confirmed
    formed

    RESULT :

    –2
    ACID RADICAL : SO4

    BASIC RADICAL: Al 3+

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