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Please see the attached report for the testing conducted in early April.
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CARBON MONOXIDE AND PARTICULATE MATTER
EMISSIONS TEST REPORT
KA 905-24-01
To the best of my knowledge, all applicable field and analytical procedures
and all test data and plant operating data are true and correct.
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TABLE OF CONTENTS
1.0 INTRODUCTION......................................................................................... 1
APPENDICES
1.0 INTRODUCTION
Family Owned Funeral Group LLC owns and operates a human crematory unit
(EU-002) at the Forest Meadows facility at 725 NW 23rd Avenue in Gainesville,
Alachua County, Florida. This report describes:
Testing was conducted by Koogler and Associates, Inc. (Koogler) on April 5, 2024.
2.0 NOTIFICATION
1
Family Owned Funeral Group LLC KA
Gainesville, Florida Facility 905-24-01
Permit No. 0010057-009-AG June 7, 2024
The two sample ports used for sampling in the stack are located at 90 degrees to
one another in the circular stack. The ports are 48 inches (2.5 equivalent
diameters) above the secondary burner and 99 inches ( equivalent diameters)
upstream from the top of the stack. EPA Method 1 (40 CFR 60, Appendix A)
requires a minimum of 24 sampling points. Thus, 12 sample points were
selected on each of the two traverses.
2
Figure 1
USEPA METHOD 1
SOURCE INFORMATION
1 0.40
2 1.27
3 2.24 99" =A
4 3.36
5 4.75
6 6.76
7 12.24
8 14.25
9 15.64
10 16.76
11 17.73
12 18.60
48" =B
Family Owned Funeral Group LLC KA
Gainesville, Florida Facility 905-24-01
Permit No. 0010057-009-AG June 7, 2024
The CO reference method used for these measurements was EPA Method 10 as
described in 40 CFR 60, Appendix A. A schematic diagram of this sample train is
shown in Figure 2.
Stack gas composition (O2 and CO2) measurements, velocity measurements, and
stack gas moisture measurements were made in conjunction with the EPA Method
5 tests in accordance with EPA Methods 2, 3, and 4. Carbon monoxide emission
measurements were made in accordance with EPA Method 10. All EPA test
methods are described in 40 CFR 60, Appendix A and have been adopted by
reference by FDEP by Rule 62-204.800(8)(e), F.A.C.
A schematic diagram of the sampling train used for the particulate matter emission
measurement is shown in Figure 3.
4
Thermometer Flexible Line
Stack
Thermometer
Wall
Temperature
Sensor
Ice Bath
Probe
Heated Reverse-Type
Filter Pitot Tube
Silica Gel Empty Water
Pitot Manometer
Temperature Sensor
Probe
Pitot Tube
Impingers
KA
FIGURE 3
EPA Method 5 Particulate Matter Sampling Train
Family Owned Funeral Group LLC KA
Gainesville, Florida Facility 905-24-01
Permit No. 0010057-009-AG June 7, 2024
During the testing on April 5, 2024, Koogler conducted a single run for CO
emissions in accordance with EPA Method 10 and a single run for PM emissions
in accordance with EPA Method 5.
After the first run, it was noted that that the facility was operating above the
emission limit for CO set forth in 62-296.401 for incinerators (100 parts per million
by volume, dry basis, corrected to seven percent oxygen on an hourly basis). The
data associated with this test run are summarized in Figure 4 and Table 1.
While the hourly stack gas CO concentration averaged approximately 120 ppmvd
at 7% oxygen as shown in Table 1 (compared with an emission standard of 100
ppmvd at 7% oxygen), the 1-minute average stack gas CO concentrations ranged
7
Family Owned Funeral Group LLC KA
Gainesville, Florida Facility 905-24-01
Permit No. 0010057-009-AG June 7, 2024
from approximately
40 – 230 ppmvd at 7% oxygen; and were near or below the 1-hour CO stack gas
concentration limit of 100 ppmvd at 7% oxygen approximately 70% of the time
(See Figure 1).
During testing, the stack gas particulate matter concentration measured during the
single completed run was 0.013 gr/dscf corrected to seven percent oxygen. This
is roughly 16 percent of the emission limit of 0.08 gr/dscf corrected to seven
percent oxygen set forth in 62-296.401 for incinerators. The stack gas temperature
averaged 610 degrees F, and the stack gas moisture averaged 7.66 percent.
Results of the particulate matter emission measurement are summarized in Table
2.
7.0 CONCLUSION
Based upon the data reported herein, it can be concluded that the human
crematory unit owned and operated by Family Owned Funeral Group, LLC located
in Gainesville, FL as Forest Meadows was not operating within emissions limit for
CO set forth by their permit (0010057-009-AG) and 62-296.401 for incinerators.
The unit, however, was operating well within the established stack gas particulate
matter emission limit.
The facility is currently exploring options to have the unit serviced in an effort to
address the stack gas CO concentration issue, and to determine what part unit
settings (gas firing rate, primary and secondary combustion air, etc) play in
determining stack gas CO concentration and what part unit operating practices
play in this determination..
The Appendices of this report contains calculations, field and laboratory data
sheets, plant operating data, and project participants.
8
TABLE 1
APPENDICES
APPENDIX A
Carbon Monoxide and Particulate Matter
Calculations and Field Data Sheets
Family Owned Funeral Group LLC
Gainesville, Florida Facility 905-24-01
Permit No. 0010057-009-AF June 7, 2024
Appendix A-1
CO Calculations
Pollutant: O2 CO2 CO
Method: 3A 3A 10
Instrument Span 25 25 125
Zero Gas Cylinder ID CC308074 CC308074 CC308074
Low Gas Cylinder ID N/A N/A N/A
Mid Gas Cylinder ID EB0133348 EB0133348 EB0017922
Span Gas Cylinder ID CC70314 CC70314 CC251941
Info
Zero Gas Concentration (CV, zero) 0 0 0
Low Gas Concentration (CV, low) N/A N/A N/A
Mid Gas Concentration (CV, mid and CM,A) 10.05 10.01 45.3
Span Gas Concentration (CS and CV, span) 20.12 20.48 98.49
Calibration Gas Concentration (CV, cal) 10.05 10.01 45.3
Zero Gas Start 07:20 (0.000) 07:20 (-0.017) 07:20 (0.016)
Zero Gas Stop 07:21 (0.000) 07:21 (-0.028) 07:21 (-0.004)
Zero Gas Response(Cdir, zero) 0.000 -0.023 0.006
1
Zero Gas Accuracy (ACEzero) 0.000% < 2% 0.110% < 2% 0.006% < 2%
Pre-Sampling Calibrations
Direct Loop (System Loop for HCs)
2
Zero Gas Accuracy (SBzero) 0.000% < 5% 0.623% < 5% 0.320% < 5%
Calibration Gas Start 08:54 (10.083) 08:54 (9.165) 08:58 (42.920)
Calibration Gas Stop 08:55 (10.080) 08:55 (9.460) 08:59 (42.943)
Calibration Gas Response (CS, cal) 10.082 9.313 42.932
Calibration Gas Accuracy2(SBcal) 0.108% < 5% 3.948% < 5% 0.648% < 5%
1. Method 7E, Section 12.2, Equation 7E-1 (2% of span plus analyzer calibration error)
References and Formulas 2. Method 7E, Section 12.3, Equation 7E-2 (5% of span)
3. Method 25A, Section 8.4 (5% of predicted values from 2-point calibration curve zero-span)
Pollutant: O2 CO2 CO
Method: 3A 3A 10
Start 10:15 (14.788) 10:15 (4.313) 10:15 (61.613)
Compliance 1
Stop 11:16 (15.668) 11:16 (3.545) 11:16 (87.715)
Stack Gas Response (Cavg) 15.319 3.896 44.841
1,2
Corrected Stack Gas Response (Cgas) 15.325 3.931 48.047
Zero Gas Start 11:25 (0.000) 11:25 (0.590) 11:25 (-0.588)
Stack Gas Analysis 1 Zero Gas Stop 11:26 (0.000) 11:26 (0.543) 11:26 (-0.607)
Zero Gas Response (Cs, zero) 0.000 0.567 -0.598
Average Zero Gas Response (C0) 0.000 0.336 -0.454
3
Zero Gas Accuracy (SB zero) 0.000% < 5% 2.877% < 5% 0.613% < 5%
System Loop
4,5
Zero Gas Drift (Dzero) 0.000% < 3% 2.254% < 3% 0.293% < 3%
Calibration Gas Start 11:30 (10.010) 11:30 (9.453) 11:35 (41.635)
Calibration Gas Stop 11:31 (10.010) 11:31 (9.523) 11:36 (41.507)
Calibration Gas Response (Cs, cal) 10.010 9.488 41.571
Average Calibration Gas Response (CM) 10.046 9.400 42.251
3
Calibration Gas Accuracy (SBcal) 0.249% < 5% 3.089% < 5% 2.030% < 5%
4,5
Calibration Gas Drift (Dcal) 0.356% < 3% 0.859% < 3% 1.381% < 3%
1. Method 7E, Section 12.6, Equation 7E-5b.
2. Method 25A, Section 12.1, Equation 25A-1. (as propane)
References and Formulas 3. Method 7E, Section 12.3, Equation 7E-2 (<5% error of span)
4. Method 7E, Section 12.5, Equation 7E-4 (<3% drift of span from start of run)
5. Method 25A, Section 13.1.2 [same methodology as Equation 7E-4] (<3% of span)
Pollutant: O2 CO2 CO
Method: 3A 3A 10
Timestamp - label pollutants here: O2 CO2 CO
04/05/2024 07:10 20.842 0.158 1.420
04/05/2024 07:11 14.348 0.137 1.463
04/05/2024 07:12 0.043 0.092 1.286
04/05/2024 07:13 0.000 0.077 1.194
04/05/2024 07:14 -0.005 0.067 1.183
04/05/2024 07:15 -0.010 0.053 1.180
04/05/2024 07:16 -0.013 0.035 1.066
04/05/2024 07:17 -0.020 0.007 0.988
04/05/2024 07:18 -0.020 -0.003 0.903
04/05/2024 07:19 0.000 -0.003 0.168
04/05/2024 07:20 0.000 -0.017 0.016
04/05/2024 07:21 0.000 -0.028 -0.004
04/05/2024 07:22 0.000 -0.038 -0.010
04/05/2024 07:23 0.000 -0.025 -0.003
04/05/2024 07:24 9.087 9.427 -0.164
04/05/2024 07:25 20.167 19.870 -0.536
04/05/2024 07:26 20.173 20.655 -0.563
04/05/2024 07:27 20.180 21.220 -0.577
04/05/2024 07:28 20.180 21.635 -0.580
04/05/2024 07:29 20.180 21.960 -0.598
04/05/2024 07:30 20.187 22.222 -0.611
04/05/2024 07:31 20.143 21.128 -0.625
04/05/2024 07:32 20.120 20.553 -0.617
04/05/2024 07:33 20.120 20.703 -0.639
04/05/2024 07:34 20.113 20.755 -0.622
04/05/2024 07:35 10.227 13.007 -0.487
04/05/2024 07:36 10.057 12.720 -0.485
04/05/2024 07:37 10.060 10.123 -0.469
04/05/2024 07:38 10.060 10.119 -0.496
04/05/2024 07:39 8.717 10.798 -0.658
04/05/2024 07:40 0.020 3.533 -0.151
04/05/2024 07:41 0.000 3.092 -0.139
04/05/2024 07:42 0.000 2.780 -0.139
04/05/2024 07:43 0.000 2.552 -0.019
04/05/2024 07:44 0.000 2.373 -0.004
04/05/2024 07:45 0.000 2.233 -0.026
04/05/2024 07:46 0.038 2.122 6.098
04/05/2024 07:47 0.000 2.005 42.238
04/05/2024 07:48 0.000 1.905 42.739
04/05/2024 07:49 0.000 1.817 43.165
04/05/2024 07:50 0.000 1.730 45.469
04/05/2024 07:51 0.000 1.650 45.579
04/05/2024 07:52 0.005 1.575 43.827
04/05/2024 07:53 14.798 1.550 16.228
04/05/2024 07:54 20.583 1.513 2.100
04/05/2024 07:55 14.522 1.457 4.642
04/05/2024 07:56 0.005 1.355 14.243
04/05/2024 07:57 0.000 1.297 14.250
04/05/2024 07:58 0.000 1.247 14.229
04/05/2024 07:59 0.000 1.198 14.215
04/05/2024 08:00 0.000 1.152 14.227
04/05/2024 08:01 0.000 1.108 14.232
04/05/2024 08:02 0.000 1.065 14.224
04/05/2024 08:03 0.000 1.023 14.231
04/05/2024 08:04 0.000 0.985 14.218
04/05/2024 08:05 0.000 0.947 14.212
04/05/2024 08:06 0.000 0.912 14.193
04/05/2024 08:07 0.000 0.875 14.234
04/05/2024 08:08 0.000 0.840 14.224
04/05/2024 08:09 0.013 0.810 13.304
04/05/2024 08:10 18.220 0.827 3.179
04/05/2024 08:11 20.718 0.827 0.591
04/05/2024 08:12 20.713 0.808 0.320
04/05/2024 08:13 20.715 0.790 0.132
04/05/2024 08:14 20.138 1.048 1.787
04/05/2024 08:15 20.722 0.762 0.153
04/05/2024 08:16 20.730 0.737 0.112
04/05/2024 08:17 20.730 0.710 0.105
04/05/2024 08:18 20.732 0.687 0.067
04/05/2024 08:19 20.738 0.665 0.095
04/05/2024 08:20 20.740 0.645 0.063
04/05/2024 08:21 20.740 0.625 0.035
04/05/2024 08:22 20.740 0.608 0.047
04/05/2024 08:23 20.740 0.588 0.026
04/05/2024 08:24 20.762 0.572 0.013
04/05/2024 08:25 20.780 0.555 0.012
04/05/2024 08:26 12.462 0.520 32.181
04/05/2024 08:27 0.012 0.472 102.023
04/05/2024 08:28 0.002 0.443 102.078
04/05/2024 08:29 0.000 0.402 100.823
04/05/2024 08:30 0.000 0.375 98.256
04/05/2024 08:31 0.000 0.358 98.304
04/05/2024 08:32 0.000 0.338 98.258
04/05/2024 08:33 0.000 0.320 98.307
04/05/2024 08:34 0.000 0.305 98.404
04/05/2024 08:35 0.000 0.287 98.445
04/05/2024 08:36 0.000 0.272 98.408
04/05/2024 08:37 0.000 0.257 98.510
04/05/2024 08:38 0.000 0.243 98.635
04/05/2024 08:39 0.000 0.228 98.477
04/05/2024 08:40 0.000 0.215 98.444
04/05/2024 08:41 0.000 0.203 98.508
04/05/2024 08:42 0.002 0.190 65.524
04/05/2024 08:43 0.000 0.177 42.940
04/05/2024 08:44 0.000 0.167 43.516
04/05/2024 08:45 0.000 0.157 43.624
04/05/2024 08:46 0.003 0.145 40.875
04/05/2024 08:47 0.957 0.138 7.541
04/05/2024 08:48 0.015 0.127 -0.273
04/05/2024 08:49 0.005 0.120 -0.281
04/05/2024 08:50 0.000 0.110 -0.314
04/05/2024 08:51 0.000 0.100 -0.305
04/05/2024 08:52 9.823 1.530 -0.373
04/05/2024 08:53 19.247 2.183 -0.362
04/05/2024 08:54 10.083 9.165 -0.664
04/05/2024 08:55 10.080 9.460 -0.691
04/05/2024 08:56 5.633 5.355 15.435
04/05/2024 08:57 0.035 0.792 42.684
04/05/2024 08:58 0.012 0.607 42.920
04/05/2024 08:59 0.000 0.490 42.943
Pollutant: O2 CO2 CO
Method: 3A 3A 10
04/05/2024 09:00 10.825 0.447 23.408
04/05/2024 09:01 20.845 0.445 -0.147
Method 7E, Section 12.2, Equation 7E-1 (2% of span plus analyzer calibration error)
- Example calculation based on O2, Pre-Sampling Calibrations, Direct Loop, Mid Gas Accuracy - NOT APPLICABLE
Method 7E, Section 12.5, Equation 7E-4 (3% drift of span from start of run)
- Example calculation based on O2, Stack Gas Analysis 1, Compliance 1, Calibration Gas Drift - NOT APPLICABLE
C S,final - C dir C S,i - C dir |(C S,final - C dir ) - (C S,i - C dir )| |C S,cal,final - C S,cal,i | |10.010 - 10.082|
D cal = |Sb cal, final - Sb cal, i | = - = = = = 0.356%
CS CS CS CS 20.120
Appendix A-2
CO Field Data Sheets
Family Owned Funeral Group LLC
Gainesville, Florida Facility 905-24-01
Permit No. 0010057-009-AF June 7, 2024
Appendix A-3
PM Calculations
STACK DATA SUMMARY
Δ𝐻
𝑃
Absolute Meter Gas Pressure Pm = 13.6 inHg
𝑃
𝑃
Absolute Flue Gas Pressure Ps = 13.6 inHg
V lc = 66.00 ml
V w(std) = 3.112 scf
17.636 ∗ 𝑌 ∗ 𝑉𝑚 ∗ Pm
Dry Gas Meter Volume Sampled V m(std) = 𝑇 dscf
YC = 1.002
Vm = 37.229 dcf
Pm = 30.13 inHg
Tm = 528.30 °F
V m(std) = 37.520 dscf
.
.
100
Moisture Content at Stack Gas, at Saturated Condition B ws(sat) = 10 ∗ %
𝑃
Ts = 1069.71 °F
Ps = 30.01 inHg
B ws(sat) = 100.00 %
𝑉
Moisture Content of Stack Gas, Measured B ws = 𝑉 𝑉 %
Dry Molecular Weight Md = 0.440 %𝐶𝑂2 0.320 %𝑂2 0.280 %𝑁2 %𝐶𝑂 lb/lb-Mole
%CO2 = 3.9 %
%O2 = 15.3 %
%N2 & %CO = 80.8 %
Md = 29.2360 lb/lb-Mole
𝑇
85.49 ∗ 𝐶 ∗ 𝛥𝑝 𝑎𝑣𝑔 ∗
Average Stack Gas Velocity vs = 𝑃 ∗𝑀 ft/sec
Cp = 0.840
√(Δp) avg = 0.3778 √(inH 2 O)
Ts = 1069.71 °F
Ps = 30.01 inHg
Ms = 28.3766 lb/lb‐Mole
vs = 30.41 ft/sec
𝑇 𝑃
60 1 𝐵 𝑣𝐴
Dry Volumetric Flow Rate Q sd = 𝑇 𝑃 dscfm
Ts = 1069.71 °F
B ws = 7.6590% %
vs = 30.41 ft/sec
30.01 inHg
Ps =
2
As = 1.96 ft
Q sd = 1633.9 dscfm
Q = 3576.2 acfm
𝑉 𝑌 ∆𝐻
100𝑇 𝐾 𝑉 𝑃
Percent Isokinetic of Sampling Rate I = 𝑇 13.6 %
60𝜃𝑣 𝑃 𝐴
Ts = 1069.71 °F
V lc = 66.00 ml
YC = 1.002
Vm = 37.229 dcf
EXAMPLE CALCULATIONS
Tm = 528.300 °F
Pm = 30.13 inHg
θ = 60.0 minutes
vs = 30.41 ft/sec
Ps = 30.01 inHg
2
An = 0.00075 ft
I = 100.3 %
Family Owned Funeral Group LLC
Gainesville, Florida Facility 905-24-01
Permit No. 0010057-009-AF June 7, 2024
Appendix A-4
PM Field Data Sheets
USEPA METHOD 1
CYCLONIC FLOW CHECK
Date: 4/5/2024
Pitot ID: 9146
2 3 1
2 4 0
2 5 0
2 6 4
2 7 7
2 8 2
2 9 5
2 10 1
2 11 1
2 12 0
USEPA METHOD 2
PRELIMINARY FLOW
Date: 4/5/2024
Pitot ID: 9146
Pitot Tube Coefficient: 0.840
Barometric Pressure: 30.02 in Hg
Stack Static: -0.2 in H2O
Assumed Moisture: 5 %
Oxygen: 16 %
Carbon Dioxide: 3 %
2 2 0.07 560
2 3 0.12 560
2 4 0.22 560
2 5 0.28 560
2 6 0.36 560
2 7 0.30 560
2 8 0.25 560
2 9 0.12 560
2 10 0.06 560
2 11 0.03 560
2 12 0.03 560
MULTIPLE METHODS
ISOKINETIC DATA SHEET
Plant: Forest Meadows Funeral Home and Cemetary Project Number: 905-24-01 Run No.: 1 Start Time: 10:15
Source Name: EU-002: Human Crematory Unit Location: 725 NW 23rd Ave, Gainesville, FL 32609 Run Date: 4/5/2024 End Time: 11:16
Test Type: PM Test Operators: KM, SG Test Observers
Preliminary and Assumptions Equipment Identification Sample Moisture Data Leak Checks
Est. Moisture: 5 % Pitot ID: 9512 Pitot Corr.: 0.840 Moisture in: grams Pre Mid Post
Est. Meter Temp: 65 °F Probe Length (ft): 7 Impinger ID: Type: Contents: Initial: Final: DGM Lk Rate (cfm): 0.011 0.006
Probe ID:
Est. Stack Temp: 600 °F KAS-7 Material: SS Impinger 1: MOD H2O 0.0 62.0 Volume Correction(cf):
Support Measurements Stack TC ID: KAKI-62 Filter Box: Impinger 2: STD H2O 0.0 0.0 DGM Vac (in Hg): 10 7
O2 Concentration: 15.30 % Meter Box Meter Y: 1.002 Impinger 3: MOD Empty 0.0 0.0 Pitots Lk Check Pass: Yes Yes
CO2 Concentration: 3.90 % No.: KA-11 Delta H: 1.820 Impinger 4: Temperature Control
Stack Static: -0.20 in H2O Nozzle Diameter(In.): 0.370 Impinger 5: Low High Target
Nozzle ID:
Barometric Pres.: 30.02 in Hg SS-.37 Material: SS Impinger 6: Probe Set Points 223 273 248
Molecular Weight (dry): 29.24 lb/lb-mole Filter No. 1: 2361 Filter No. 2: Silica Imp.: MOD Silica 0.0 4.0 Filter Set Points 223 273 248
Est. Mol. Weight (wet): 28.67 lb/lb-mole Silica ID: 109 Filter Holder ID: R-1 Total Moisture Gain (V LC) 66.0 grams Aux Set Points 50 68 59
Sampling Time Sampling Target DGM Actual DGM Reading Velocity Head Stack Dry Gas Meter Target Orifice Pressure Actual Orifice Pressure Probe Aux Final exit
Traverse Distance From Filter Temperature Pump Vacuum
Port (Begin) Time (End) Reading (Vm) (Vm) (ΔP) Temperature Temperature Differential (ΔH) Differential (ΔH) Temperature Temperature Temperature
Point Stack Wall
3
min min ft3 ft in H2O °F °F in H2O in H2O °F °F °F °F in Hg
1 01 18.60 0.0 2.5 127.350 0.10 582 64 0.96 0.96 249 240 64 2
1 02 17.73 2.5 5.0 128.7 128.600 0.10 603 64 0.94 0.94 246 240 62 2
1 03 16.76 5.0 7.5 129.9 129.800 0.17 605 64 1.59 1.59 240 240 57 3
1 04 15.64 7.5 10.0 131.5 131.400 0.26 604 65 2.44 2.44 258 241 56 4
1 05 14.25 10.0 12.5 133.5 133.500 0.32 605 65 3.00 3.00 249 247 56 4
1 06 12.24 12.5 15.0 135.9 136.000 0.38 603 66 3.57 3.57 248 252 56 4
1 07 6.76 15.0 17.5 138.6 138.700 0.17 608 66 1.59 1.59 244 252 57 3
1 08 4.75 17.5 20.0 140.4 140.400 0.15 607 67 1.41 1.41 244 250 58 3
1 09 3.36 20.0 22.5 142.0 142.000 0.05 618 67 0.46 0.46 240 243 58 2
1 10 2.24 22.5 25.0 142.9 143.100 0.05 575 68 0.48 0.48 264 242 59 2
1 11 1.27 25.0 27.5 144.1 144.100 0.05 605 68 0.47 0.47 247 242 59 2
1 12 0.40 27.5 30.0 145.0 145.100 0.06 618 68 0.56 0.56 244 241 59 2
2 01 18.60 30.0 32.5 146.1 146.100 0.05 600 69 0.47 0.47 248 249 61 2
2 02 17.73 32.5 35.0 147.0 147.000 0.04 627 69 0.37 0.37 257 248 60 2
2 03 16.76 35.0 37.5 147.8 147.800 0.05 627 70 0.46 0.46 244 248 59 2
2 04 15.64 37.5 40.0 148.7 148.700 0.08 633 70 0.74 0.74 243 240 58 3
2 05 14.25 40.0 42.5 149.9 149.800 0.35 633 70 3.23 3.23 248 244 58 5
2 06 12.24 42.5 45.0 152.3 152.200 0.39 628 71 3.62 3.62 246 251 56 6
2 07 6.76 45.0 47.5 154.8 154.900 0.26 629 71 2.41 2.41 257 252 57 5
2 08 4.75 47.5 50.0 157.0 157.000 0.24 623 72 2.24 2.24 243 248 57 5
2 09 3.36 50.0 52.5 159.1 159.100 0.14 621 73 1.31 1.31 257 247 58 4
2 10 2.24 52.5 55.0 160.7 160.700 0.04 581 73 0.39 0.39 255 245 59 3
2 11 1.27 55.0 57.5 161.6 161.600 0.20 580 73 1.95 1.95 256 240 59 4
2 12 0.40 57.5 60.0 163.5 163.500 0.20 626 74 1.87 1.87 248 241 58 4
165.4 164.579
Appendix A-5
Relinquished by:
Signature Date Time
Received by:
Signature Date Time
Relinquished by:
Signature Date Time
Laboratory:
Received by: Kyle Miller 4/8/2024 6:00
Signature Date Time
Chain of Custody
APPENDIX B
Calibrations
KOOGLER & ASSOCIATES, Inc.
THERMOCOUPLE CALIBRATION
DATE: April 17, 2023
"K" TYPE TESTER: Will Sands
122 Degree F 212 Degree F 392 Degree F
NIST Probe Difference Difference NIST Probe Difference Difference NIST Probe Difference Difference Pass
Probe ID (Fo) o
(F ) (Fo) %R (Fo) (Fo) (Fo) %R (Fo) (Fo) (Fo) %R Y/N
Secondary Standard Thermocouple with Hand Held OMEGA (HH 509 R) s/n 51001062
KAK # 1 122.0 122.0 0.0 0.0 212.0 212.0 0.0 0.0 392.0 392.0 0 0.0 YES
Last Impinger Thermocouples (Method 2, Section 10.3 Criteria = ±1.5%R)
KAK-2 122.0 122.0 0.0 0.0 212.0 212.0 0.0 0.0 392.0 392.0 0.0 0.0 YES
KAK-3 122.0 121.0 -1.0 0.2 212.0 212.0 0.0 0.0 392.0 392.0 0.0 0.0 YES
KAK-5 122.0 121.0 -1.0 0.2 212.0 212.0 0.0 0.0 392.0 392.0 0.0 0.0 YES
KAK-6 122.0 121.0 -1.0 0.2 212.0 212.0 0.0 0.0 392.0 392.0 0.0 0.0 YES
KAK-7 122.0 122.0 0.0 0.0 212.0 212.0 0.0 0.0 392.0 392.0 0.0 0.0 YES
KAK-9 122.0 122.0 0.0 0.0 212.0 212.0 0.0 0.0 392.0 392.0 0.0 0.0 YES
KAK-10 122.0 122.0 0.0 0.0 212.0 213.0 1.0 -0.1 392.0 392.0 0.0 0.0 YES
KAK-15 122.0 122.0 0.0 0.0 212.0 211.0 -1.0 0.1 392.0 392.0 0.0 0.0 YES
KAK-11 122.0 121.0 -1.0 0.2 212.0 212.0 0.0 0.0 392.0 392.0 0.0 0.0 YES
KAK-16 122.0 121.0 -1.0 0.2 212.0 211.0 -1.0 0.1 392.0 392.0 0.0 0.0 YES
KAK-17 122.0 121.0 -1.0 0.2 212.0 210.0 -2.0 0.3 392.0 392.0 0.0 0.0 YES
Stack Thermocouples (Method 2, Section 10.3 Criteria = ±1.5%R)
KAK-35 122.0 121.0 -1.0 0.2 212.0 212.0 0.0 0.0 392.0 392.0 0.0 0.0 YES
KAK-36 122.0 119.0 -3.0 0.5 212.0 212.0 0.0 0.0 392.0 392.0 0.0 0.0 YES
KAK-38 122.0 122.0 0.0 0.0 212.0 212.0 0.0 0.0 392.0 392.0 0.0 0.0 YES
KAK-48 122.0 121.0 -1.0 0.2 212.0 212.0 0.0 0.0 392.0 391.0 -1.0 0.3 YES
KAK-50 122.0 121.0 -1.0 0.2 212.0 214.0 2.0 -0.3 392.0 392.0 0.0 0.0 YES
KAK-61 122.0 122.0 0.0 0.0 212.0 212.0 0.0 0.0 392.0 392.0 0.0 0.0 YES
KAK-63 122.0 122.0 0.0 0.0 212.0 211.0 -1.0 0.1 392.0 392.0 0.0 0.0 YES
KAK-64 122.0 122.0 0.0 0.0 212.0 211.0 -1.0 0.1 392.0 392.0 0.0 0.0 YES
KAK-65 122.0 121.0 -1.0 0.2 212.0 211.0 -1.0 0.1 392.0 392.0 0.0 0.0 YES
KAK-66 122.0 121.0 -1.0 0.2 212.0 211.0 -1.0 0.1 392.0 392.0 0.0 0.0 YES
KAK-69 122.0 120.0 -2.0 0.3 212.0 210.0 -2.0 0.3 392.0 392.0 0.0 0.0 YES
KAK-70 122.0 123.0 1.0 -0.2 212.0 212.0 0.0 0.0 392.0 392.0 0.0 0.0 YES
KAK-71 122.0 121.0 -1.0 0.2 212.0 212.0 0.0 0.0 392.0 392.0 0.0 0.0 YES
KAK-72C 122.0 122.0 0.0 0.0 212.0 212.0 0.0 0.0 392.0 392.0 0.0 0.0 YES
KAK-80 122.0 122.0 0.0 0.0 212.0 212.0 0.0 0.0 392.0 392.0 0.0 0.0 YES
KAK-108 122.0 123.0 1.0 -0.2 212.0 212.0 0.0 0.0 392.0 392.0 0.0 0.0 YES
KAK-100 122.0 121.0 -1.0 0.2 212.0 212.0 0.0 0.0 392.0 392.0 0.0 0.0 YES
KAK-110 122.0 122.0 0.0 0.0 212.0 212.0 0.0 0.0 392.0 392.0 0.0 0.0 YES
KAK-119 122.0 119.0 -3.0 0.5 212.0 212.0 0.0 0.0 392.0 392.0 0.0 0.0 YES
Stack Thermocouples (Method 2, Section 10.3 Criteria = ±1.5%R)
KAKI-51 122.0 122.0 0.0 0.0 212.0 214.0 2.0 -0.3 392.0 392.0 0.0 0.0 YES
KAKI-52 122.0 122.0 0.0 0.0 212.0 213.0 1.0 -0.1 392.0 392.0 0.0 0.0 YES
KAKI-61 122.0 122.0 0.0 0.0 212.0 212.0 0.0 0.0 392.0 392.0 0.0 0.0 YES
KAKI-62 122.0 121.0 -1.0 0.2 212.0 213.0 1.0 -0.1 392.0 392.0 0.0 0.0 YES
KAKI-71 122.0 122.0 0.0 0.0 212.0 212.0 0.0 0.0 392.0 392.0 0.0 0.0 YES
KAKI-72 122.0 122.0 0.0 0.0 212.0 212.0 0.0 0.0 392.0 392.0 0.0 0.0 YES
KAKI-81 122.0 122.0 0.0 0.0 212.0 212.0 0.0 0.0 392.0 392.0 0.0 0.0 YES
KAKI-82 122.0 122.0 0.0 0.0 212.0 211.0 -1.0 0.1 392.0 392.0 0.0 0.0 YES
30B Thermocouples
30B1 122.0 122.0 0.0 0.0 212.0 210.0 -2.0 0.3 392.0 392.0 0.0 0.0 YES
30B2 122.0 122.0 0.0 0.0 212.0 212.0 0.0 0.0 392.0 392.0 0.0 0.0 YES
30B3 122.0 122.0 0.0 0.0 212.0 212.0 0.0 0.0 392.0 392.0 0.0 0.0 YES
30B4 122.0 122.0 0.0 0.0 212.0 213.0 1.0 -0.1 392.0 392.0 0.0 0.0 YES
Dioxin Furan Trap Thermocouples
KAK DF 1 122.0 122.0 0.0 0.0 212.0 212.0 0.0 0.0 392.0 392.0 0 0.0 YES
KAK DF 3 122.0 122.0 0.0 0.0 212.0 212.0 0.0 0.0 392.0 392.0 0 0.0 YES
KAK DF 5 122.0 122.0 0.0 0.0 212.0 212.0 0.0 0.0 392.0 392.0 0 0.0 YES
KAK DF 6 122.0 122.0 0.0 0.0 212.0 212.0 0.0 0.0 392.0 392.0 0 0.0 YES
KAK DF 8 122.2 122.0 -0.2 0.0 212.0 212.0 0.0 0.0 392.0 392.0 0 0.0 YES
KAK DF 10 122.0 122.0 0.0 0.0 212.0 212.0 0.0 0.0 392.0 392.0 0 0.0 YES
KAK DF 11 122.0 122.0 0.0 0.0 212.0 212.0 0.0 0.0 392.0 392.0 0 0.0 YES
Criteria:
Method 2 Section 10.3, Temperature Sensors.
10.3.1 After each field use, calibrate dial thermometers, liquid-filled bulb thermometers, thermocouple-potentiometer systems, and other sensors at a temperature within 10 percent of the average absolute
stack temperature. For temperatures up to 405 °C (761 °F), use an ASTM mercury-in-glass reference thermometer, or equivalent, as a reference. Alternatively, either a reference thermocouple and
potentiometer (calibrated against NIST standards) or thermometric fixed points ( e.g., ice bath and boiling water, corrected for barometric pressure) may be used. For temperatures above 405 °C (761 °F), use
a reference thermocouple-potentiometer system calibrated against NIST standards or an alternative reference, subject to the approval of the Administrator.
10.3.2 The temperature data recorded in the field shall be considered valid. If, during calibration, the absolute temperatur e measured with the sensor being calibrated and the reference sensor agree within
1.5 percent, the temperature data taken in the field shall be considered valid. Otherwise, the pollutant emission test shall either be considered invalid or adjustments (if appropriate) of the test results shall be
made, subject to the approval of the Administrator.
Method 4 Section 10.1 Reference Method. Calibrate the metering system, temperature sensors, and barometer according to Method 5,
Sections 10.3, 10.5, and 10.6, respectively.
Method 5 Section 10.5 Temperature Sensors. Use the procedure inSection 10.3 of Method 2 to calibrate in-stack temperature
sensors. Dial thermometers, such as are used for the DGM and condenser outlet, shall be calibrated against mercuryin -glass thermometers.
Post-Test Thermocouple Calibration
Parameters: PM
Tolerance ± 2 °F 0.0
Date: 4/5/2024
Meter Box: KA-11
Y c: 1.002
0.95 * Yc: 0.952
1.05 * Yc: 1.052
Average Yqa:
Result: VERIFY
Run Yc Yqa
1 1.002 1.0293
2 1.002 #VALUE!
3 1.002 #VALUE!
DATE: 9/16/2023 METER SERIAL #: KA-11 BAROMETRIC PRESSURE (in Hg): 29.95 29.95 29.95 IF Y VARIATION EXCEEDS 2.00%,
METER PART #: KA10 CRITICAL ORIFICE SET SERIAL #: PJ 40-73 ORIFICE SHOULD BE RECALIBRATED
FACTOR VACUUM DGM READINGS (FT 3) DGM DGM TIME (MIN) DGM DH (1) (2) (3) Y
ORIFICE # RUN # (AVG) (in Hg) INITIAL FINAL NET (Vm) Orifice INITIAL FINAL AVG q (in H2O) Vm (STD) Vcr (STD) Y VARIATION (%) DH@
1 0.5916 14 138.698 144.821 6.123 72 72 72 72 8.00 1.9 6.1125 6.1473 1.006 1.81
63 2 0.5916 14 144.821 150.185 5.364 72 72 74 73 7.00 1.9 5.3448 5.3789 1.006 1.80
3 0.5916 14 150.185 155.540 5.355 72 74 74 74 7.00 1.9 5.3258 5.3789 1.010 1.80
AVG = 1.007 0.49
1 0.4525 15 155.540 160.881 5.341 72 74 74 74 9.00 1.1 5.3015 5.2897 0.998 1.78
55 2 0.4525 15 160.881 166.216 5.335 72 74 75 74.5 9.00 1.1 5.2906 5.2897 1.000 1.78
3 0.4525 15 166.216 172.144 5.928 72 75 75 75 10.00 1.1 5.8732 5.8774 1.001 1.77
AVG = 0.999 -0.30
1 0.3364 17 172.144 177.440 5.296 72 75 75 75 12.00 0.65 5.2412 5.2433 1.000 1.90
48 2 0.3364 17 177.440 183.182 5.742 72 75 75 75 13.00 0.65 5.6826 5.6802 1.000 1.90
KA11_Meter_Cal_09182023
Family Owned Funeral Group LLC
Gainesville, Florida Facility 905-24-01
Permit No. 0010057-009-AF June 7, 2024
APPENDIX C
Calibration Gas Certificates
Airgas Specialty Gases
Airgas USA LLC
630 United Drive
Durham, NC 27713
Airgas.com
CERTIFICATE OF ANALYSIS
Grade of Product: EPA PROTOCOL STANDARD
Part Number: E03NI60E15A0286 Reference Number: 122-402029840-1
Cylinder Number: CC70314 Cylinder Volume: 159.6 CF
Laboratory: 124 - Durham (SAP) - NC Cylinder Pressure: 2015 PSIG
PGVP Number: B22021 Valve Outlet: 590
Gas Code: CO2,O2,BALN Certification Date: Feb 12, 2021
Expiration Date: Feb 12, 2029
Certification performed in accordance with “EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)” document EPA
600/R-12/531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical
uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a
mole/mole basis unless otherwise noted. The results relate only to the items tested. The report shall not be reproduced except in full without approval of the laboratory. Do
Not Use This Cylinder below 100 psig, i.e. 0.7 megapascals.
ANALYTICAL RESULTS
Component Requested Actual Protocol Total Relative Assay
Concentration Concentration Method Uncertainty Dates
CARBON DIOXIDE 20.00 % 20.48 % G1 +/- 0.6% NIST Traceable 02/12/2021
OXYGEN 20.00 % 20.12 % G1 +/- 1.0% NIST Traceable 02/12/2021
NITROGEN Balance
CALIBRATION STANDARDS
Type Lot ID Cylinder No Concentration Uncertainty Expiration Date
NTRM 12061508 CC354696 19.87 % CARBON DIOXIDE/NITROGEN +/- 0.6% Jan 11, 2024
NTRM 08010202 1D003076 23.20 % OXYGEN/NITROGEN +/- 0.4% Jun 01, 2024
ANALYTICAL EQUIPMENT
Instrument/Make/Model Analytical Principle Last Multipoint Calibration
Horiba VA-5001 CO2 BF89GV17 Nondispersive Infrared (NDIR) Feb 04, 2021
Horiba MPA510 O2 41499150042 Paramagnetic Feb 04, 2021
Signature on file
Approved for Release Page 1 of 1
Family Owned Funeral Group LLC
Gainesville, Florida Facility 905-24-01
Permit No. 0010057-009-AF June 7, 2024
APPENDIX D
Project Participants
PROJECT PARTICIPANTS