CP 2 - Investigating PH
CP 2 - Investigating PH
CP 2 - Investigating PH
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Investigating pH (neutralisation)
Aim
Investigate the change in pH on adding powdered calcium hydroxide or calcium oxide to a fixed
volume of dilute hydrochloric acid.
Equipment list
● 25 cm3 measuring cylinder or volumetric pipette and pipette filler
● Beaker
● Glass rod
● Universal indicator or pH probe
● Spatula
Chemicals required
● Hydrochloric acid
● Powdered calcium hydroxide or calcium oxide
Method
1. Using the measuring cylinder or volumetric pipette, add 25 cm3 of dilute hydrochloric acid to
a beaker.
2. Add a few drops of universal indicator. Compare the initial colour of the solution to a pH
colour chart and record the pH. Alternatively, a pH probe can be used.
3. Add calcium hydroxide or calcium oxide (one level spatula at a time) to the beaker, stirring
and recording the pH between additions.
4. Stop adding calcium hydroxide/calcium oxide when the pH remains constant.
Key points
● The equations for the reactions, depending on which base is used, are:
CaO + 2HCl → CaCl2 +H2O
Ca(OH)2 + 2HCl → CaCl2 + 2H2O
● A volumetric pipette offers greater accuracy than a measuring cylinder when measuring the
volume of hydrochloric acid.
● Stirring the solution before taking a pH reading ensures the reaction is complete and that
the pH is consistent throughout the mixture.
● Using a pH probe instead of universal indicator offers greater accuracy.
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Diagram
Safety Precautions
● Safety glasses must be worn.
● Hydrochloric acid is corrosive in high concentrations. Wash hands immediately after any
contact with the skin.
● Calcium hydroxide may cause skin and eye irritation so wear gloves and safety goggles.
Wash hands immediately after any contact with the skin.
● Clear up any spillages or broken glassware immediately.
Analysis of results
The starting pH and final pH can be recorded to investigate the effect of adding calcium
hydroxide/calcium oxide to hydrochloric acid.
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