Unit 2
Unit 2
CONCRETE
Structure
2.1 Introduction
Objectives
2.7 Soundness
2.8 Alkali Aggregate Reactivity -
2.8.1 Mortar Bar Expans~onTest
282 Chemcal Method
2.9 Summary
2.10 Key Words
2.1 1 Answers to S AQs
2.1 INTRODUCTION
In Unit 1. you studied about'tests of various cement and water. Now, you will be studying
in this unit about the various tests required to maintain quality of aggregales for concrete.
Aggregates are thc important corlsliluents in concrete. They impart body to the concrete,
rcduce shrinkage and effect economy. The mere fact that aggregates occupy 80 percent of
thc volurne of concrete, is a pointer to the impact of properties of aggregates on various
properties and characteristics of concrete. In fact concrete is considered as two-phase
material. i.e. paste phase and aggregate phase. This itself proves llie importance of
aggregates in concrete. Therefore, one of the major contributing factors to the quality of
concrete is the quality of the aggregates. It is, therefore, essential for us to assess the
quality of aggregates being incorporated in the concrete. IS : 2386-1963 lays down thc
various methods of test for aggregates for concrete. We will be studying these methods of
Lests in this unit.
Objectives
At the end of this Unit, you should be able to:
describe the procedure of different tests,
distinguish the purpose of different tests, and
identify the apparatus used for different tests.
- --
Testing for Conrrete Materials
2.2 TESTS FOR AGGREGATES
IS r 2386-1963 has grouped the test methods for aggregates into eight parts for
convenience of the engineers. These parts and their broad scope is given below
Part I Particle Size and Shape
Part I1 Estimation of Deleterious Materials (and Organic Impurities
Part 111 Specific Gravity. Density, Voids, Absorption and Bulking
Part IV Mechanical Properties
Part V Soundness
Part VI Measuring Mortar Making Properties of Fine Aggregate
Part VII Alkali Aggregate Reactivity
Part VIII Petrographic Examination
We will now exanline tliese methods of tests in general, though for detailed method, you
may refer to these codes directly when required in the field. We will be discussirig tests
listed in Part I to Part V and Part VII only.
I I SI.No.
Maximum Nominal
Size of Aggregate
Approximate Minimum
Weight of Sample
I
4) 40 or over 5000
The test sample is placed in container, added water and agitate. The wash water
containing the suspended and dissolved solids is sieved through a nest of two sieves,
the lowcr bcing 75-micron IS sieve and upper approximately 1.18 mm IS sieve. All
material retained or nested sieves shall be returned to the washed sample. The washed
aggregate shall be dried to constant weight at a temperature not exceeding 110 C and
weight to nearest 0.1 percent. The amount of percentage of material finer than 75
micron.
where,
R = original dry weight, and
C = dry weight after washing.
I't\tinp for Corrcrete M;rte~Sals 2.3.3 Determination of Flakiness Index
The flakiness index of aggregate is the percentage by weight of particles in it whose least
dimension (thickness) is less than three-fifths ot their mean dimension. The test is not
applicable to slzes smaller than 6.3 mm.
Test for Determination of Flakiness Index
This test is conducted by using a rnetal thickness gauge, of the description shown in Figurc
2.1. A sufficient quantity of aggregate,is taken such that a minimum number of 200 picces
of any fraction can be tested. Each fraction is gauged in turn for thickness on the metal
gauge. The total amount passing in the gauge is weighed to an accuracy of 0.1 per cenl of
the weight of the samples taken. The flakiness index is taken as the total weight of the
material passing the various thickness gauges expressed as a percentage of the total
weight of the sample taken. Table 2.3 shows the standard dimensions of tllickness and
length gauges.
Table 2.3 : Dimensions of Thickness and Length Gauges
(IS :2386 (Part-I) 1963)
-
- - -.
Size of Aggregate
GaugeThickncss * Gauge Cenith* ** I
Sieve (mm) Sieve (mm) (mm) (m m) I
Passing
of sieve-
Retain~d-
1
' 1 1
0 112.5 '5 20
6 3 , 10 .12.5, 1 1
1 1 25
4
All d m e n s i o n s in mm
I Figure 2.2 :Length Gauge
i
!
I size of matenal. The total amount retained by the gauge length shall be weighed to an
accuracy of at least 0.1 percent of the weight of the test samples taken. The elongation
index is the total weight of the material retained on the various length gauges
expressed as a percentage of the total weight of the sample gauged.
2.3.5 Determination of Angularity Number
One of the methods of expressing the angularity qualitatively is by a figure called
Angularity Number, as suggested by Shergold. This is based on the percentage voids in the
aggregate after compaction in a specified manner. The test gives a value termed the
angularity number. The method of determination is described in IS : 2386 (Part 1)-1963.
A quantity of single sized aggregate is filled into metal cylinder of three litres capacity.
The aggregates are compacted in a standard manner and the percentage of void is found
out. If the void is 33 percent the angularity of such aggregate is considered zero. If the void
is 34 percent the angularity number of such aggregate is considered 11. In other words, if
the angularity number is zero, the solid volume of the aggregate is 67 percent and if
angularity number 1s 11, the solid volume of the aggregate is 56 percent. The normal
aggregates which are suitable for making the concrete may have angularity number
anylhing from zero to 11. Angularity number zero represents the most practicable rounded
aggregates and the angularity number 11 indicates the most angular aggregates that could
be tolerated for making concrete not so unduly llarsh and uneconomical.
Thc angularity number shall be calculated from the formula:
lOOW
An'gularity number = 67 - -
c GA
where,
W = mean weight in gm of [he aggregate in the cylinder,
Figure 2.3 :Sedimentation Pipette for Determination of Clay and Silt Content
Sedimentation pipette of the description shown in Figure 2.3 is used for determination of
clay and silt content. In the case of fine aggregate, approximately 300 gm of samples in the
air-dry condition, passing the 4.75 rnm IS Sieve, is weighed and placed in the screw
topped glass jar, together with 300 ml of the diluted sodium oxalate solution. The rubber
washer and cap are fixed. Care is taken to ensure water tightness. The jar is then rotated
about its long axis, with this axis horizontal, at a speed of 80 +_ 20 revolutions per minute
for a period of 15 minutes. At the end of 15 minutes the suspension is poured into 1000 ml
measuring cylinder and the residue washed by gentle swirling and decantation of
successive 150 ml portions of sodium oxalate solution, the washings being added to the Tests of
Aggregates for Concrete
cylinder until lhe volume is made upto 1000 ml. I
In the case of coarse aggregate the weighed sample is placed in a suitable container,
covered with a measured volume of sodium oxalate solution (0.8 gm per litre), agitated
vigorously to remove all f i e material adhered and the liquid suspension transferred to the
1000 ml measuring cylinder. This process is repeated till all clay material has been
transferred to the cylinder. The volume is made upto 1000 ml with sodium oxalate solution.
The suspension in the measuring cylinder is thoroughly mixed. The pipette A is then
gently lowered until the pipette touches the surface of the liquid, and then lowered a
further 10 cm into the liquid. Three minutes after placing the tube in position, the pipctte A
and the bore of tap B is filled by opening B and applying gentle suction at C. A small
surplus may be drawn up into the bulb between tap B and tube C, but this is allowed to run
away and any solid matter is washed out with distilled water from E. The pipette is then
removed from the measuring cylinder and its contents run into a weighed container. The
contents of the container IS dried at 100°C to 110' C to constant weight, cooled and
weighed.
The percentage of the f i e silt and clay or fine dust is calculated from the formula
where,
W, = weigh1 in gm of the original sample,
(weight C).
C
Specific Gravity = --
B-A
C
Apparent Sp. Gravity = -
C-A
Water absorption
= lOO(B-C)_
(Per cent of dry weight)
C
where,
A = the weight in gm of the saturated aggregate in water (A, -A,),
B = the weight in gm of the saturated surface-dry aggregate in air, 'and
C = the weight in gm of oven-dried aggregate in air.
2.5.2 Test for Determination of Bulk Density and Voids
Bulk density is the weight of material in a given volume. It is normally expressed in kg per
litre. A cylindrical rneasure preferably machined to accurate internal dimensions is used
for measuring bulk density. The size of the container for measuring bulk density is shown
in Table 2.5.
, Table 2.5: Size of Container for Bulk Density Test
Size of Largest Nominal Inside Inside Thickness
Particles Capacity Diameter Height of Metal
(cm) (cm)
4.75 and under 1s 17
Over 4.75to 40 I IS
Over 40 1 30
The cylindrical measure is filled about 113 each time with thoroughly mixed aggregate and
tamped with 25 strokes by a bullet ended tamping rod, 16 mm diameter and 60 cm long.
The measure is carefully struck off level using tamping rod as a straight edge. The net
weight of Uie aggregate in thc measure is determined and the bulk density is calculated in
kgllitre.
Net weight of the aggregate in kg
Bulkdensity =
Capacity of the container in litre
Percentage of voids = -
G s - y x 100
GJ
where,
G, = Specific gravity of aggregate, and
Tests of
y = bulk density in kgllitre.
Aggregates for C o ~ ~ c r e i e
2.5.3 Determination of Necessary Adjustment for Bulking of Fine
Aggregate (Field Method)
,The volume of sand increases when moisture is present and this phenomena is known as
bulking. The extent of bulking can be estimatcd by a simple field test. A sample of moist
fine aggregate is Cilled into a measuring cylinder in the normal manner. Note down the
level, say hi. Pour water into the measuring cylinder and completely inundate the sand and
shake it. Since the volume of the saturated sand is the same as that of the dry sand. the
inundated sand completely offsets the bulking effect. Note down the level of the sand say,
h,. Then h l - h2 shows the bulking of the sample of sand under test.
h i - h2
Percentage of bulking = -x 100
h2
The field test to find out the percentage of bulking is so simple that this could be
conducted in a very shoit time interval and the percentage of bulking so found out could be
employcd for correcting the volume of fine aggregate to be used. This can be considered as
'one of the important methods of field control to produce quality concrete. Since volume
hatching is not adopted for controlled concrete, the determination of the percentage of
moisture content is not normally required. The quantity of water could be controlled by
visual exanlination of the mix and by experience. The percentage of free moisture content
is required to be determined and correction made only when weigh hatching is adopted for
production of quality concrete.
2.5.4 Determination of Surface Moisture in Fine Aggregate (Field
Method)
In this test the container is filled upto the mark with water and the weight in grams
determined. It is now emptied and enough water is placed to cover the sample. The sample
of fine aggregate is now introduced into the container and the entrained air is removed.
The container is then filled to the original mark and weight in grams determined.
Then V,=Mc+Ms-M
where,
Vs = weight in gm of water displaced by the sample,
M,. = weight in gm of container filled upto the, mark with water,
M, = weight in gm of the sample, and
M = weight in gm of the sample and container filled to the mark with water.
Then,
where,
PI = %age surface moisture in terms of saturated surface dry fine aggregate,
V , = weight in gm of water displaced,
Vd = the weight of sample (M,) divided by the specific gravity on saturated
and surface dry basis, determined as prescribed, and
P?, = %age surface moisture in terms of the weight of wet fine aggregate.
Test sample and abrasive chargc is placed in the Los Angeles abrasion testing machine and
the machine is rotatcd at a speed of 20 to 33 revlmui. For gradings A, B, C and D. the
machine is rotated for 500 revolubons. For gradings E, F and G , it is rotated 1000
revolutions. At the completion of the above number of revolution, the matcrial is
discharged from the machine and a preliminary separation of thc sample 11ladeon sieve
coarser than 1.7 rmn IS Sieve. Finer portion is then sieved on a 1.7 rnm IS sleve. The
material coarser than 1.7 mmIS Sieve is washed, dried in an oven at 105 to 110'C to a
substantially constant weight and accurately weighed to the nearest gram.
The difference between the original weight and the final weight or test sample is
expressed as a percentage of the original weight of the test sample. This value is reported
as the percentage of wear. The percentage of wear should not be more than 16 per cent for
concrete aggregates.
SAQ 1
i) What test is conducted to determine Soundness of aggregate'? HOWis it .
conducted?
ii) What is aggregate crushing value and how is it determined?
iii) How do you determine angularity number of aggregate?
iv) Descrihe the field method for determination of necessary adjustment for
bulking of fine aggregate.
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2.7 SOUNDNESS
Soundness refers to the ability of aggregate to resist excessive changes in volume as a
result of changcs in physical conditions. These physical conditions that affect the
soundness of aggregate are the freezing and thawing, variation in temperature, alternate
wetting and drying under normal conditions and wetting and drying in salt water.
Aggregates which are porous, weak and containing any undesirable extraneous matters
undergo excessive volume change when subjected to the above conditions. Aggregates Terts of
Aggreg3tes for Co~~rrete
which undergo more than the specified amount of volume change is said to be unsound
aggregates. If concrete is liable to be exposed to the action of frost, the coarse and fine
aggregate wh~chare going to be used should be subjected to soundness test.
2.7.1 Soundness Test
The soundness test consists of alternative immersion of carefully graded and weighed test
sample in a solution of sodium or magnesium sulphate and oven drying it under specified
conditions. The accumulation and growth of salt crystals in the pores of the particles, is
thought to produce disruptive internal forces similar to the action of freezing of water or
crystallisation of salt. Loss in weight, is measured for a specifed number of cycles.
Soundness test is specified in IS 2386 (Part V). As a general guide. it can be taken that the
average loss of weight after 10 cycles should not exceed 12 percent and 18 percent when
tested with sodiun~sulphate and ~nagnesiumsulphate respectively.
Figurc 2.4 :Illustration of Division Between Imocuous and Deleterious Aggregates on Basis of Reduction in
Alkalinity Test
Te*tingforConcreteMaterids VIII-1963). Generally, a potentially deleterious reaction is indicated if the plotted test
result falls to the right of the boundary line of Figure 2.4 and if plotted result falls to the
left side of the boundary line, the aggregate may be considered as innocuous. The above
chemical test also be employed for finding out the effectiveness of adding a particular
proportion of pozzolanic material to offset the alkali-aggregate reaction.
SAQ 2
i) What do you understand by the term "Alkali Aggregate Reactivity" and how
is it determined by Chemical Method?
ii) Which sieves are used generally in sieve-analysis?
iii) How do you determine the aggregate abrasion value? What are the
recommended limits for different situations?
iv) What is "Sedimentation Method" and what is its objective?
I
2.9 SUMMARY
In this unit we have discussed about method of tests for aggregates for concrete. These
tests are given in great detail in IS : 2386 - 1963 in Parts I to V and VII and cover the
aspects of particle size and shape, deleterious materials and organic impurities, specific
gravity, density, voids, absorption and bulking, mechanical properties, soundness and
alkali aggregate reactivity. These tests are conduct to determine the suitablity of aggregate
for concrete.