BS ISO 16468:2015

BSI Standards Publication

Investment castings (steel,

nickel alloys and cobalt
alloys) — General technical
requirements
BS ISO 16468:2015 BRITISH STANDARD

National foreword
This British Standard is the UK implementation of ISO 16468:2015. It
supersedes BS ISO 16468:2005 which is withdrawn.
The UK participation in its preparation was entrusted to Technical
Committee ISE/111, Steel Castings and Forgings.
A list of organizations represented on this committee can be
obtained on request to its secretary.
This publication does not purport to include all the necessary
provisions of a contract. Users are responsible for its correct
application.
© The British Standards Institution 2015.
Published by BSI Standards Limited 2015
ISBN 978 0 580 76505 6
ICS 77.140.80
Compliance with a British Standard cannot confer immunity from
legal obligations.
This British Standard was published under the authority of the
Standards Policy and Strategy Committee on 31 October 2015.
Amendments/corrigenda issued since publication
Date Text affected
 BS ISO 16468:2015

INTERNATIONAL ISO
STANDARD 16468

Second edition
2015-10-01

Investment castings (steel, nickel

alloys and cobalt alloys) — General
technical requirements
Pièces moulées en cire perdue (acier, alliages de nickel et alliages de
cobalt) — Exigences techniques générales

Reference number
ISO 16468:2015(E)

© ISO 2015
BS ISO 16468:2015
ISO 16468:2015(E)


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© ISO 2015, Published in Switzerland
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Contents Page

Foreword......................................................................................................................................................................................................................................... iv
1 Scope.................................................................................................................................................................................................................................. 1
2 Normative references....................................................................................................................................................................................... 1
3 Terms and definitions...................................................................................................................................................................................... 1
4 Materials and manufacture........................................................................................................................................................................ 2
4.1 Melting process....................................................................................................................................................................................... 2
4.2 Remelting process................................................................................................................................................................................. 2
5 Inspection and testing..................................................................................................................................................................................... 2
5.1 General requirements........................................................................................................................................................................ 2
5.2 Sampling........................................................................................................................................................................................................ 2
6 Retests.............................................................................................................................................................................................................................. 8
7 Cleaning and dressing...................................................................................................................................................................................... 8
8 Quality.............................................................................................................................................................................................................................. 8
9 Production welds.................................................................................................................................................................................................. 8
10 Supplementary requirements................................................................................................................................................................. 8
10.1 General............................................................................................................................................................................................................ 8
10.2 Agreed manufacturing procedure........................................................................................................................................... 8
10.3 Magnetic particle inspection........................................................................................................................................................ 8
10.4 Radiographic inspection.................................................................................................................................................................. 8
10.5 Liquid penetrant inspection......................................................................................................................................................... 9
10.6 Ultrasonic inspection.......................................................................................................................................................................... 9
10.7 Inspection of weld preparation................................................................................................................................................. 9
10.8 Prior agreement relating to major finishing welds.................................................................................................. 9
10.9 Impact test at low temperatures.............................................................................................................................................. 9
10.10 Hardness test............................................................................................................................................................................................. 9
10.10.1 Brinell......................................................................................................................................................................................... 9
10.10.2 Rockwell................................................................................................................................................................................... 9
10.10.3 Vickers....................................................................................................................................................................................... 9
10.11 Specified ferrite range in austenitic and austenitic ferritic stainless steels........................................ 9
10.12 Unspecified elements...................................................................................................................................................................... 10
10.13 Test material removed from castings................................................................................................................................ 10
10.14 Tensile test blocks and specimen locations for castings................................................................................... 10
10.15 Weld maps (sketches)..................................................................................................................................................................... 10
10.16 Chemical analysis — Testing frequency.......................................................................................................................... 10
10.17 Tensile test — Testing frequency ......................................................................................................................................... 10
10.18 Inspection documents.................................................................................................................................................................... 10
10.19 Marking....................................................................................................................................................................................................... 10
10.20 Decarburization................................................................................................................................................................................... 10
10.21 Metallurgical cleanliness.............................................................................................................................................................. 10
Bibliography.............................................................................................................................................................................................................................. 12

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Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www.iso.org/directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www.iso.org/patents).
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation on the meaning of ISO specific terms and expressions related to conformity
assessment, as well as information about ISO’s adherence to the WTO principles in the Technical
Barriers to Trade (TBT) see the following URL: Foreword - Supplementary information
The committee responsible for this document is ISO/TC 17, Steel, Subcommittee SC 11, Steel castings.
This second edition replaces the first edition (ISO 16468:2005), which has been technically revised
with the following changes:
— Clause 2, two standards added;
— 3.3, revised;
— 3.4, deleted;
— 10.6, reference made to ISO 4992-1 and ISO 4992-2.

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 BS ISO 16468:2015
INTERNATIONAL STANDARD ISO 16468:2015(E)

Investment castings (steel, nickel alloys and cobalt

alloys) — General technical requirements

1 Scope
This International Standard specifies technical requirements for castings (steel, nickel alloys, and
cobalt alloys) produced by the investment-casting process. The International Standards specifying
metallurgical material requirements for steel, nickel alloy, and cobalt alloy casting grades are listed in
the Bibliography.
The requirements stated in this International Standard form an integral part of the material
specification. In cases of conflict, the requirements of this specification take precedence over the
individual material specification requirements.

2 Normative references
The following documents, in whole or in part, are normatively referenced in this document and are
indispensable for its application. For dated references, only the edition cited applies. For undated
references, the latest edition of the referenced document (including any amendments) applies.
ISO 4986, Steel castings — Magnetic particle inspection
ISO 4987, Steel castings — Liquid penetrant inspection
ISO 4990, Steel castings — General technical delivery requirements
ISO 4992-1, Steel castings — Ultrasonic examination — Part 1: Steel castings for general purposes
ISO 4992-2, Steel castings — Ultrasonic examination — Part 2: Steel castings for highly stressed components
ISO 4993, Steel castings — Radiographic inspection
ISO 6506-1, Metallic materials — Brinell hardness test — Part 1: Test method
ISO 6507-1, Metallic materials — Vickers hardness test — Part 1: Test method
ISO 6508-1, Metallic materials — Rockwell hardness test — Part 1: Test method (scales A, B, C, D, E, F,
G, H, K, N, T)
ISO 10474, Steel and steel products — Inspection documents
ISO 11970, Specification and approval of welding procedures for production welding of steel castings
ISO 13520, Determination of ferrite content in austenitic stainless steel castings

3 Terms and definitions

For the purposes of this document, the following terms and definitions apply.
3.1
primary heat
master
mother heat
melt
quantity of metal processed in a single furnace or refining vessel at one time, in such a manner, as to
produce the desired composition and properties

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3.2
sub-heat
melt
production heat
daughter heat
portion of a primary heat remelted for pouring into castings
3.3
investment casting
lost wax casting
metal casting that is produced in a ceramic shell or mould using an expendable pattern
Note 1 to entry: The expendable pattern may consist of wax, plastics, or other material, and is removed prior to
filling the mould with liquid metal.

4 Materials and manufacture

4.1 Melting process

Primary heats shall be made by the electric furnace process, with or without separate refining, such
as argon-oxygen-decarburization (AOD), vacuum-oxygen-decarburization (VOD), vacuum-induction-
melting (VIM), etc., unless otherwise specified in the individual specification or agreed upon between
the purchaser and manufacturer. Primary heats may be used directly for producing castings or
converted into ingot, bar, shot, or other suitable form, for later remelting as a sub-heat.

4.2 Remelting process

Sub-heats shall be produced from primary-heat metal in suitable batch sizes by an electric induction
furnace, with or without atmosphere protection, such as vacuum or inert gas, unless otherwise specified
in the individual specification or agreed upon between the purchaser and manufacturer. Revert (gates,
sprues, risers, and rejected castings) shall not be remelted except in primary heats. Additions of up to
5 %, by mass, are permitted for compositional adjustments and deoxidation.

5 Inspection and testing

5.1 General requirements

The general requirements for inspection and testing shall be in accordance with ISO 4990, except as
described in 5.2.

5.2 Sampling

5.2.1 If castings are poured directly from one or more primary heats, then the samples for chemical
and other required testing shall also be poured directly from each of the primary heats.

5.2.2 Unless otherwise specified by the purchaser, test blocks may be taken from castings, may be cast
integrally with the castings, or may be cast in separate moulds of the same type and materials as those
used for the castings. Samples for the determination of the chemical composition may be cast in other
types of mould.

5.2.3 If castings are poured from a sub-heat, then the samples for chemical and other required tests
shall also be poured from a sub-heat of the same primary melt, but not necessarily from the same sub-
melt as the castings. The sub-melt used for the test samples shall be produced using the same practices
and additions as used for the castings.

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5.2.4 Examples of test blocks which may be used for mechanical testing are shown in Figure 1, except
when 10.14 is specified. The test block in Figure 1 d) may be employed only for austenitic alloy castings
with a ruling thickness less than 65 mm.
Dimensions in millimetres

a)

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b)

c)

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d)

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e)

f)

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g)

h)
Key
t taper
a alternative

Figure 1 — Test blocks

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6 Retests
In addition to the requirements of ISO 4990, if any specimen shows defective machining or develops
flaws, it may be discarded and another specimen substituted from the same primary heat.

7 Cleaning and dressing

All the castings shall be cleaned and dressed sufficiently to determine compliance with the requirements
of Clause 8. Additional dressing may be agreed at the time of the enquiry and order.
If the pattern is supplied by the purchaser, or is produced using a die supplied by the purchaser, the
dimensions of the casting shall be as produced by the pattern or die.

8 Quality

8.1 Visual standards for acceptance shall be agreed between the purchaser and manufacturer.
ISO 11971 may be used to specify visual surface standards. Other surface conditions shall meet the visual
acceptance standards specified in the order. Unacceptable visual surface discontinuities shall be removed
and their removal verified by visual examination.

8.2 When additional inspection is desired, 10.3, 10.4, 10.5, 10.6, or 10.7 may be specified.

9 Production welds
Production welding shall be in accordance with the requirements of ISO 11970.

10 Supplementary requirements

10.1 General
One or more of the following supplementary requirements may be applied when specified in the enquiry
and order. Additional supplementary requirements may also be found in ISO 4990. Details of these
supplementary requirements shall be agreed upon by the manufacturer and purchaser at the time of
the enquiry and order. The specified tests shall be carried out before delivery of the castings.

10.2 Agreed manufacturing procedure

At the time of enquiry and order, the purchaser may require prior approval of the manufacturing process.

10.3 Magnetic particle inspection

Castings shall be inspected for surface and near-surface discontinuities by magnetic particle
inspection. The inspection shall be in accordance with ISO 4986. The extent of inspection and the basis
for acceptance shall be agreed upon between the manufacturer and the purchaser.

10.4 Radiographic inspection

Castings shall be inspected for internal defects by means of X-rays or gamma rays. The procedure shall
be in accordance with ISO 4993. The extent of inspection and the basis for acceptance shall be agreed
upon between the manufacturer and purchaser.

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10.5 Liquid penetrant inspection

Castings shall be inspected for surface discontinuities by means of liquid penetrant inspection. The
inspection shall be in accordance with ISO 4987. Areas to be inspected, methods and types of liquid
penetrants to be used, developing procedure, and the basis for acceptance shall be agreed upon between
the manufacturer and purchaser.

10.6 Ultrasonic inspection

Castings shall be inspected for internal defects by means of ultrasonic inspection. The procedure shall
be in accordance with ISO 4992-1 or ISO 4992-2. The extent of inspection and the basis for acceptance
shall be agreed upon between the manufacturer and purchaser.

10.7 Inspection of weld preparation

Surfaces prepared for welding shall be inspected, using the same methods and acceptance criteria as
specified for the casting, to verify removal of discontinuities.

10.8 Prior agreement relating to major finishing welds

The requirements related to major finishing welds shall be in accordance with ISO 4990.

10.9 Impact test at low temperatures

The requirements related to the impact test at low temperatures shall be in accordance with ISO 4990.

10.10 Hardness test

10.10.1 Brinell

Brinell hardness tests at specified locations of the castings shall be carried out in accordance with
ISO 6506-1, and shall be reported.

10.10.2 Rockwell

Rockwell hardness tests at specified locations of the castings shall be carried out in accordance with
ISO 6508-1, and shall be reported.

10.10.3 Vickers

Vickers hardness tests at specified locations of the castings shall be carried out in accordance with
ISO 6507-1, and shall be reported.

10.11 Specified ferrite range in austenitic and austenitic ferritic stainless steels

10.11.1 The chemical composition of the melt shall be controlled such that the ferrite content,
as determined by the chemical composition procedure of ISO 13520, shall be in conformance with the
specified ferrite content range.

10.11.2 The specified ferrite content shall be as agreed upon between the manufacturer and the
purchaser. If both minimum and maximum ferrite contents are specified, the minimum specified range of
ferrite content shall be 10 %. The minimum specified ferrite content shall not be lower than the percent
necessary to achieve the minimum mechanical properties required for the alloy.

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10.11.3 Should the purchaser wish to have the ferrite content determined by either the magnetic
response or metallographic methods, the purchaser should impose these requirements at the time of the
enquiry.

10.12 Unspecified elements

Chemical analysis and limits for elements not specified for the grade ordered shall be as agreed upon
between the manufacturer and purchaser.

10.13 Test material removed from castings

In addition to the tests required by the material specification, test material shall be removed from the
casting. The properties and location of the test material shall be agreed upon between the manufacturer
and purchaser.

10.14 Tensile test blocks and specimen locations for castings

10.14.1 Test blocks may be cast integrally with the shell in which the castings are produced or in
separate shells. Test blocks shall be heat treated together with the castings they represent.

10.14.2 The dimensions of the test block, the number and locations of the specimens, and the
limits for the mechanical properties shall be agreed upon between the manufacturer and purchaser.

10.15 Weld maps (sketches)

The requirements related to weld maps shall be in accordance with ISO 4990.

10.16 Chemical analysis — Testing frequency

The frequency of chemical analysis shall be as agreed upon between the purchaser and manufacturer.

10.17 Tensile test — Testing frequency

The frequency of tensile tests shall be as agreed upon between the purchaser and manufacturer.

10.18 Inspection documents

Documents for specific inspection and testing shall be supplied in accordance with ISO 10474.

10.19 Marking
The castings shall be marked for identification, or traceability, or both. The content of the marking
and the method of marking, including size, location, and style, shall be as agreed upon between the
purchaser and the producer.

10.20 Decarburization
A casting or block shall be evaluated for the degree and depth of decarburization. The test method,
location and preparation of samples, and the basis for acceptance shall be agreed upon between the
purchaser and manufacturer.

10.21 Metallurgical cleanliness

10.21.1 The details of the method for inspection and the basis for acceptance shall be agreed
upon between the purchaser and manufacturer.

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10.21.2 It is realized that the foundry may be unable to perform the inspection for metallurgical
cleanliness prior to shipment, or that the purchaser may wish to defer inspection until after additional
work or machining has been performed on the casting. However, the foundry is responsible for the
castings under the final inspection required in 10.21.1.

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Bibliography

[1] ISO 4991, Steel castings for pressure purposes

[2] ISO 9477, High strength cast steels for general engineering and structural purposes
[3] ISO 11971, Steel and iron castings — Visual examination of surface quality
[4] ISO 11972, Corrosion-resistant cast steels for general applications
[5] ISO 11973, Heat-resistant cast steels and alloys for general applications
[6] ISO 12725, Nickel and nickel alloy castings
[7] ISO 13521, Austenitic manganese steel castings
[8] ISO 13583-2, Centrifugally cast steel and alloy products — Part 2: Heat resistant materials
[9] ISO 14737, Carbon and low alloy cast steels for general applications

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ICS 77.140.80
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