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    System Precision Report

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    Riad Manamanni
    The document reports on a system precision test where six injections of caffeine were made. The results met the specifications with %RSD for area less than 0.5%, %RSD for height less than 1.1%, and standard deviation for retention time less than 1 second.

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    System Precision Report

    Uploaded by

    Riad Manamanni
    15 views3 pages
    The document reports on a system precision test where six injections of caffeine were made. The results met the specifications with %RSD for area less than 0.5%, %RSD for height less than 1.1%, and standard deviation for retention time less than 1 second.

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    © © All Rights Reserved

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    The document reports on a system precision test where six injections of caffeine were made. The results met the specifications with %RSD for area less than 0.5%, %RSD for height less than 1.1%, and standard deviation for retention time less than 1 second.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    15 views3 pages

    System Precision Report

    Uploaded by

    Riad Manamanni
    The document reports on a system precision test where six injections of caffeine were made. The results met the specifications with %RSD for area less than 0.5%, %RSD for height less than 1.1%, and standard deviation for retention time less than 1 second.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    of 3

    SYSTEM PRECISION REPORT

    AC Q U I SI TI O N I N F O R M ATI O N

    System Name: Del_Patrol2 Acquired By: Jennb


    Project Name: SQT_PATrol_TUV_CM_rev C Column serial Number: 11581505610K
    Sample Set Method: 020 System Precision Sample Kit 1 Expiration date: 10/22/2010 12:00:00 AM
    Processing Method System Precision PM Sample Kit 1 Lot Number: N070015
    Report Method Name: System Precision Report Build Version: Empower 2 Software Build 2154 SPs
    User Name: System Installed:
    Sample Set Feature Release 5
    Id: 10377 DB ID:
    Result 847558692
    Set Id 10390
    Sample Set Name: System Precision Sample Set Start Date: 10/25/2010 5:51:34 PM

    In the System Precision qualification, six (6) injections of Caffeine are made.

    The SD for the Caffeine peak RT should be < or = 1.0 seconds, the %RSD for Area should be < or = 0.5 %
    and the %RSD for Height should be < or = 1.1 %.

    Caffeine Area and Height Results Table

    Area %RSD Area Area %RSD Height %RSD Height Height %RSD
    Specification %RSD Pass Fail Specification %RSD Pass Fail
    1 %RSD < or = 0.5 0.1 PASS %RSD < or = 1.1 0.2 PASS

    Caffeine Retention Time (RTsec) Results Table

    Retention time (sec) Retention time (sec)


    Retention time (sec)
    Standard Deviation Standard Deviation
    Standard Deviation
    Specification Pass Fail
    1 SD RT < or = 1.0sec 0.0 PASS

    Printed 8:30:17 AM US/Eastern 11/17/2010 Page: 1 of 3


    SYSTEM PRECISION REPORT

    AC Q U I SI TI O N I N F O R M ATI O N

    System Name: Del_Patrol2 Acquired By: Jennb


    Project Name: SQT_PATrol_TUV_CM_rev C Column serial Number: 11581505610K
    Sample Set Method: 020 System Precision Sample Kit 1 Expiration date: 10/22/2010 12:00:00 AM
    Processing Method System Precision PM Sample Kit 1 Lot Number: N070015
    Report Method Name: System Precision Report Build Version: Empower 2 Software Build 2154 SPs
    User Name: System Installed:
    Sample Set Feature Release 5
    Id: 10377 DB ID:
    Result 847558692
    Set Id 10390
    Sample Set Name: System Precision Sample Set Start Date: 10/25/2010 5:51:34 PM

    System Precision Chromatograms


    Caffeine - 0.953

    1.00
    AU

    0.00
    Caffeine - 0.952

    1.00
    AU

    0.00
    Caffeine - 0.952

    1.00
    AU

    0.00
    Caffeine - 0.953

    1.00
    AU

    0.00
    Caffeine - 0.952

    1.00
    AU

    0.00
    Caffeine - 0.951

    1.00
    AU

    0.00
    0.00 0.20 0.40 0.60 0.80 1.00 1.20 1.40 1.60 1.80 2.00 2.20
    Minutes

    Printed 8:30:17 AM US/Eastern 11/17/2010 Page: 2 of 3


    SYSTEM PRECISION REPORT

    AC Q U I SI TI O N I N F O R M ATI O N

    System Name: Del_Patrol2 Acquired By: Jennb


    Project Name: SQT_PATrol_TUV_CM_rev C Column serial Number: 11581505610K
    Sample Set Method: 020 System Precision Sample Kit 1 Expiration date: 10/22/2010 12:00:00 AM
    Processing Method System Precision PM Sample Kit 1 Lot Number: N070015
    Report Method Name: System Precision Report Build Version: Empower 2 Software Build 2154 SPs
    User Name: System Installed:
    Sample Set Feature Release 5
    Id: 10377 DB ID:
    Result 847558692
    Set Id 10390
    Sample Set Name: System Precision Sample Set Start Date: 10/25/2010 5:51:34 PM

    System Precision Peak Results

    Name: Caffeine
    Inj Vol RT Retention time Height Points
    Vial Injection Name Area Result Id
    (ul) (min) (sec) (µV) Across Peak
    1 6 1 10 Caffeine 0.953 57.18 2495668.59 1611216.77 54 10424
    2 6 2 10 Caffeine 0.952 57.13 2492075.36 1610091.17 54 10425
    3 6 3 10 Caffeine 0.951 57.07 2497832.71 1615197.14 54 10426
    4 6 4 10 Caffeine 0.953 57.18 2491935.83 1609450.82 54 10427
    5 6 5 10 Caffeine 0.952 57.09 2497452.47 1612504.54 53 10428
    6 6 6 10 Caffeine 0.952 57.09 2490695.24 1606722.34 53 10429
    Mean 57.12 2494276.70 1610863.80
    Std. Dev. 0.04 3092.59 2875.40
    % RSD 0.12 0.18

    Printed 8:30:17 AM US/Eastern 11/17/2010 Page: 3 of 3

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