Inolab Cond 730
Inolab Cond 730
Inolab Cond 730
1 Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
1.1 Keyboard . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
1.2 Display . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
1.3 Sockets. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
2 Safety . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
2.1 Authorized use . . . . . . . . . . . . . . . . . . . . . . . . . 10
2.2 General safety instructions . . . . . . . . . . . . . . . . 10
3 Commissioning . . . . . . . . . . . . . . . . . . . . . . . . . 13
3.1 Scope of delivery . . . . . . . . . . . . . . . . . . . . . . . 13
3.2 Initial commissioning . . . . . . . . . . . . . . . . . . . . 13
4 Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
4.1 Switch on the instrument . . . . . . . . . . . . . . . . . 17
4.2 Measuring. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
4.2.1 Conductivity / Specific resistance . . . . . 21
4.2.2 Salinity . . . . . . . . . . . . . . . . . . . . . . . . . . 22
4.2.3 TDS (total dissolved solids) . . . . . . . . . . 23
4.2.4 Printing/transmitting measured values . 24
4.3 Determining/setting up the cell constant [C] . . . 25
4.3.1 Determining the cell constant
(calibrating) ................... 25
4.3.2 Setting the cell constant manually . . . . . 29
4.4 Setting up the temperature compensation TC . 32
4.5 Storing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36
4.5.1 Manual storage . . . . . . . . . . . . . . . . . . . 36
4.5.2 Switching on AutoStore (Int 1). . . . . . . . 38
4.5.3 Outputting the data storage . . . . . . . . . . 40
4.5.4 Clearing the storage . . . . . . . . . . . . . . . 46
4.6 Data transmission. . . . . . . . . . . . . . . . . . . . . . . 47
4.6.1 Data transmission interval (Int 2). . . . . . 47
4.6.2 Recorder (analog output) . . . . . . . . . . . 49
4.6.3 PC/external printer (RS232 interface) . . 50
4.6.4 Operation with MultiLab pilot . . . . . . . . . 51
4.7 Configuration . . . . . . . . . . . . . . . . . . . . . . . . . . 52
4.8 Reset . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 57
3
Contents Cond 730
6 What to do if... . . . . . . . . . . . . . . . . . . . . . . . . . . 63
7 Technical data. . . . . . . . . . . . . . . . . . . . . . . . . . 67
8 Lists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 73
4
Cond 730 Overview
1 Overview
The compact inoLab Cond 730 precision conductivity meter
lets you perform conductivity measurements rapidly and reli-
ably.
The inoLab Cond 730 provides the highest degree of oper-
ating comfort, reliability and measuring safety for all applica-
tions.
4
3
Co
nd
73
0
1 Keypad
2 Display
3 Sockets
4 Printer*
Note
The measuring instrument can also be delivered as part of
a set.
Information on this and other accessories is available in the
WTW catalog LABORATORY AND FIELD INSTRUMENTATION or
via the Internet.
5
Overview Cond 730
1.1 Keyboard
12
1 11
2 10
3 9
4 8
7
5
6
6
Cond 730 Overview
1.2 Display
Status line
Sensor symbol
Measured value display
Function and
temperature display
1.3 Sockets
Connectors:
1 Conductivity measuring cell
2 RS 232 interface/analog output
3 Plug-in power supply
Caution
Only connect measuring cells to the instrument that cannot
feed excessive voltages or currents (> SELV and > circuit
with current limiter). Almost all commercial measuring cells
- especially WTW measuring cells - meet these require-
ments.
7
Overview Cond 730
8
Cond 730 Safety
2 Safety
This operating manual contains basic instructions that you
must follow during the commissioning, operation and main-
tenance of the instrument. Consequently, all responsible
personnel must read this operating manual before working
with the instrument.
The operating manual must always be available within the
vicinity of the instrument.
Target group This measuring instrument was developed for use in the lab-
oratory.
Thus, we assume that, as a result of their professional train-
ing and experience, the operators will know the necessary
safety precautions to take when handling chemicals.
Symbols used
Caution
indicates instructions that have to be followed to prevent
damage to your instrument.
Warning
indicates instructions that have to be followed to protect
yourself and the instrument from dangerous electrical volt-
age.
Note
Indicates notes that draw your attention to special features.
Note
Indicates cross-references to other documents, e.g. appli-
cation reports, operating manuals of measuring cells, etc.
9
Safety Cond 730
Function and The smooth functioning and operational safety of the instru-
operational safety ment can only be guaranteed if the generally applicable
safety measures and the specific safety instructions in this
operating manual are followed.
Caution
The instrument is only allowed to be opened by personnel
authorized by WTW.
10
Cond 730 Safety
Obligations of the The operator of this measuring instrument must ensure that
operator the following laws and guidelines are observed when using
dangerous substances:
EEC directives for protective labor legislation
National protective labor legislation
Safety regulations
Safety datasheets of the chemical manufacturer.
11
Safety Cond 730
12
Cond 730 Commissioning
3 Commissioning
3.1 Scope of delivery
Laboratory measuring instrument, inoLab Cond 730
Plug-in power supply
Operating manual and short manual
4 x type AA Mignon 1.5 V batteries
13
Commissioning Cond 730
Warning
The line voltage on site must lie within the input voltage
range of the original plug-in power supply unit (see chapter
7 TECHNICAL DATA).
Caution
Use original plug-in power supplies only
(see chapter 7 TECHNICAL DATA).
2
1
14
Cond 730 Commissioning
Note
You can also perform measurements without a plug-in
power supply. However, the functions of the integrated
printer can only be used with connected plug-in power sup-
ply.
15
Commissioning Cond 730
16
Cond 730 Operation
4 Operation
4.1 Switch on the instrument
Note
The instrument has an energy saving feature to avoid
unnecessary battery depletion.
The energy saving feature switches the instrument off if no
key has been pressed for an hour.
The energy saving feature is not active:
17
Operation Cond 730
18
Cond 730 Operation
4.2 Measuring
Preparatory Perform the following activities when you want to measure:
activities
1 Connect the measuring cell to the instrument.
2 Adjust the temperature of the test solutions or
measure the current temperature if the measurement
is made without a temperature probe.
3 Calibrate the instrument with the measuring cell or
check the cell constant set up.
4 Select the measuring mode by pressing m.
Caution
When connecting an earthed PC/printer, measurements
cannot be performed in earthed media as incorrect values
would result.
The RS232 interface is not galvanically isolated.
Note
The conductivity meter automatically recognizes the type of
the temperature probe used. As a result, you can connect
electrodes with the NTC30 or Pt1000.
19
Operation Cond 730
Note
The current AutoRead measurement (with acceptance of
the current value) can be terminated at any time by
pressing g.
20
Cond 730 Operation
Conductivity
Specific resistance
21
Operation Cond 730
4.2.2 Salinity
To measure the salinity, proceed as follows:
22
Cond 730 Operation
Note
Also refer to Application Report ... 084 KONDUCTOMETRICAL
DETERMINATION OF THE TOTAL DISSOLVED SOLIDS (TDS).
23
Operation Cond 730
Note
To print, you must switch on the printer using the Print key
o (Print LED lights up green)*.
To transmit to the interface, you must connect the interface
cable. The integrated printer is then switched off automati-
cally.
Note
If you connect a recorder (analog output), the output to the
digital interface is switched off.
24
Cond 730 Operation
25
Operation Cond 730
Note
If error message E3 appears see chapter 6 WHAT TO DO IF...
26
Cond 730 Operation
Note
This method of automatically determining the cell constant
by calibrating in the 0.01 mol/l KCL control standard can
only be used for measuring cells with a cell constant in the
range 0.450 ... 0.500 cm-1 or 0.800 ... 1.200 cm-1.
Calibration protocol The calibration protocol contains the calibration data of the
current calibration. You can call up the calibration protocol
by outputting the data storage (section 4.5.3).
Note
You can automatically print out a calibration protocol after
the calibration. To do so, switch on the printer (Print LED
lights up green) before calibrating*. After a valid calibration,
the protocol is printed.
CALIBRATION PROTOCOL
14.04.99 11:37
Device No.: 99990000
CALIBRATION CONDUCTIVITY
Cal Time: 14.04.99 / 11:37
Cal Interval: 180d
Cal Std.: 0.01 mol/l KCL
40.0 °C
Conduct./Tref25: 1413µS/cm
Cell Const : 0.975 1/cm
Probe : +++
27
Operation Cond 730
Calibration interval The flashing sensor symbol reminds you to calibrate regu-
(Int 3) larly. After the selected calibration interval (Int 3) expires,
the sensor symbol flashes. Measurements can continue.
Note
To ensure the high measuring precision of the measuring
system, perform a calibration after the calibration interval
expires.
Setting the The calibration interval (Int 3) is set to 180 days in the facto-
calibration interval ry. The interval can be changed (1 ... 999 days):
28
Cond 730 Operation
Setting the fixed cell 1 Press the c key repeatedly until CELL appears on
constant the display.
0.010 cm-1
29
Operation Cond 730
30
Cond 730 Operation
31
Operation Cond 730
Note
ips Select the following temperature compensations to work
with the test samples given in the table:
32
Cond 730 Operation
33
Operation Cond 730
34
Cond 730 Operation
Switching off the To switch off the temperature compensation proceed as fol-
temperature lows:
compensation
1 Press the c key repeatedly until LF tc appears on
the display.
35
Operation Cond 730
4.5 Storing
The conductivity meter has an internal data storage device.
Up to 800 data records can be stored in it.
A complete data record consists of:
Memory location
Date
Time
Measured value
Temperature
I.D. number
Manual storage
Switching on the AutoStore function (Int 1), see page 38.
36
Cond 730 Operation
2 Confirm with g.
The display changes to the input of the I.D. number.
StoFull message This message appears if all 800 memory locations are full.
37
Operation Cond 730
Note
If the AutoStore function is active, the setting of the data
transmission interval (int 2) is ineffective (see page 47).
38
Cond 730 Operation
39
Operation Cond 730
Note
The AutoStore function is interrupted if you perform other
functions, e.g. output data storage.
After completing the other function, the AutoStore function
continues. However, as a result, gaps can occur in the
recording of the measured values.
display
printer/interface
Outputting to the 1 Press the r key repeatedly until Sto disp appears
display on the display.
40
Cond 730 Operation
41
Operation Cond 730
Note
If you want to find a specific parameter (e.g. date), proceed
as follows:
42
Cond 730 Operation
Outputting to the 1 Press the r key repeatedly until Sto SEr appears
interface on the display.
Note
You can cancel the transmission by pressing m or g.
43
Operation Cond 730
No. 1:
01.01.99 00:04
2.40 mS/cm 25 °C
Tman
nLF
Tref25 C = 0.475 1/cm
Ident : 1
No. 2:
10.01.99 10:09
2.40 mS/cm 25.3 °C
Tauto
nLF
Tref25 C = 0.475 1/cm
Ident : 1
No. 3:
12.01.99 01:48
2.40 mS/cm 21.6 °C
Tauto
nLF
Tref25 C = 0.475 1/cm
Ident : 1
44
Cond 730 Operation
45
Operation Cond 730
Note
The Clear store function only appears if data records have
already been stored in the storage. Otherwise, the conduc-
tivity meter automatically changes to the measuring mode.
Note
The calibration data remain in the storage and can be called
up via the calibration protocol.
46
Cond 730 Operation
Note
The setting of the interval (Int 2) only has an effect when the
storage interval (AutoStore function) is switched off.
47
Operation Cond 730
Note
If the AutoStore function is active, the data transmission is
performed according to the setting of the storage interval
(Int1). Set the storage interval (Int 1) to OFF to activate the
data transmission interval (Int 2).
Note
You can also set the data transmission interval (Int 2) in the
Configuration menu (see page 52).
48
Cond 730 Operation
1 Free
Socket assignment 2 Plug coding
1 2
3 Ground
4 3 4 Analog output
RS 232
(internal resistance < 5 Ohm)
REC
Note
Activate the analog output by connecting 2 and 3 or use the
original cable.
49
Operation Cond 730
Note
The RS232 interface is not galvanically isolated.
If it is connected to an earthed PC/printer, measurements
cannot be made in earthed media as this would give incor-
rect results!
1 CTS
Socket assignment
2 RxD
1 2
3 Ground
4 3 4 TxD
RS 232
REC
50
Cond 730 Operation
Note
More detailed information can be found in the MultiLab pilot
operating manual.
51
Operation Cond 730
4.7 Configuration
You can adapt the conductivity meter to your individual
requirements. To do this, the following parameters can be
called up/changed (the status on delivery is marked in bold):
Note
You can leave the configuration menu at any time. Parame-
ters that have already been changed are stored.
To do this, press the m key.
52
Cond 730 Operation
Baud rate
Calibration
interval
53
Operation Cond 730
ARng (AutoRange)
Conductivity
54
Cond 730 Operation
Temperature unit
55
Operation Cond 730
56
Cond 730 Operation
4.8 Reset
You can reset (initialize) measuring and configuration
parameters separately from one another.
Measuring mode
Cell constant 0.475 cm-1 (calibrated)
0.475 cm-1 (set up)
Temperature nLF
compensation
Reference temperature
Temperature coefficient of 2.000 %/K
the linear temperature
compensation
TDS factor 1.00
Note
When the measuring parameters are reset, the calibration
data are lost. After the parameters have been reset, cali-
brate!
57
Operation Cond 730
Resetting
configuration
parameters
58
Cond 730 Maintenance, cleaning, disposal
Note
See the relevant operating manual of the measuring cell for
instructions on maintenance.
59
Maintenance, cleaning, disposal Cond 730
Caution
Make sure that the poles of the batteries are the right way
round.
The ± signs in the battery compartment must correspond to
the ± signs on the batteries.
Only use leakproof alkaline manganese batteries.
60
Cond 730 Maintenance, cleaning, disposal
2
3
Note
Only use original WTW rolls of printer paper. Information on
this is given in the WTW catalog, LABORATORY AND FIELD
INSTRUMENTATION or via the Internet.
You can also use HQ thermal paper that remains legible for
at least 10 years.
61
Maintenance, cleaning, disposal Cond 730
5.2 Cleaning
Occasionally wipe the outside of the measuring instrument
with a damp, lint-free cloth. Disinfect the housing with iso-
propanol as required.
Caution
The housing is made of synthetic material (ABS). Thus,
avoid contact with acetone or similar detergents that contain
solvents. Remove any splashes immediately.
5.3 Disposal
Packing The measuring instrument is sent out in a protective trans-
port packing.
We recommend: Keep the packing material. It protects the
instrument against damage during transport.
Batteries This note refers to the battery regulation that applies in the
Federal Republic of Germany. We would ask end-consum-
ers in other countries to follow their local statutory provi-
sions.
Note
In compliance with §14 of the BATTERY REGULATION, we
would like to point out that this instrument contains batteries.
Batteries that have been removed must only be disposed of
at the recycling facility set up for this purpose or via the retail
outlet.
It is illegal to dispose of them in household refuse.
62
Cond 730 What to do if...
6 What to do if...
Cause Remedy
LoBat – Batteries almost depleted – Replace batteries
(see section 5.1.1
CHANGING THE
BATTERIES)
63
What to do if... Cond 730
to Cause Remedy
display – Timeout of the interface – Check connected
instrument
64
Cond 730 What to do if...
65
What to do if... Cond 730
66
Cond 730 Technical data
7 Technical data
67
Technical data Cond 730
Accuracy No compensation:
(± 1 digit) Accuracy ± 0.5 %
Non-linear compensation :
Accuracy Test sample temperature
± 0.5 % 0 °C ... 35 °C
according to EN 27 888;
± 0.5 % 35 °C ... 50 °C
extended nLF function according to
WTW measurements
Linear compensation :
Accuracy Test sample temperature
± 0.5 % 10 °C ... 75 °C
(the accuracy percentage always refers
to the measured value!)
SAL Range 0.0 ... 42.0
Accuracy Test sample temperature
± 0.1 5 °C ... 25 °C
± 0.2 25 °C ... 30 °C
TDS [mg/l] 1
T [°C] NTC 30:
Accuracy ± 0.1
PT 1000:
Accuracy Operating temperature
± 0.5 0 °C ... 15 °C
± 0.1 15 °C ... 35 °C
± 1 35 °C ... 55 °C
T [°F] NTC 30:
Accuracy ± 0.2
PT 1000:
Accuracy Operating temperature
± 0.9 32 °F ... 59 °F
± 0.2 59 °F ... 95 °F
± 1.8 95 °F ... 131 °F
68
Cond 730 Technical data
69
Technical data Cond 730
70
Cond 730 Technical data
71
Technical data Cond 730
72
Cond 730 Lists
8 Lists
This chapter provides additional information and orientation
aids.
Specialist terms The glossary briefly explains the meaning of the specialist
terms. However, terms that should already be familiar to the
target group are not described here.
Index The index helps you find the topics that you are looking for.
73
Lists Cond 730
Abbreviations
Conductivity value
ABS Plastic housing
AR AutoRead (drift control)
ARng Automatic range switching
Measuring instrument measures with high-
est resolution
AutoStore Automatic storing
Baud Baud rate
C Cell constant cm-1
Cal Calibration
CELL Cell constant
disp Display
Output of the data storage on the display
E3 Error message
(see chapter 6 WHAT TO DO IF...)
Ident I. D. number
InI Initialization
Resets individual basic functions to
the status they had on delivery
Int Interval
Lin Linear temperature compensation
LoBat Low Battery
Batteries are almost empty
nLF Non-linear temperature compensation
OFL Overflow
Display range exceeded
Sal Salinity
SELV Safety Extra Low Voltage
Sto Clr Clear storage
74
Cond 730 Lists
75
Lists Cond 730
Glossary
With the value of the cell constant you can roughly descri-
be the application range of a conductivity measuring cell.
The cell constant is determined through calibration in one
or several calibration solutions.
Conductivity The conductivity value is a sum parameter for the ion con-
centration of a test sample.
76
Cond 730 Lists
77
Lists Cond 730
78
Cond 730 Lists
Index
A initialize . . . . . . . . . . . . . . . . . . . . . . 57
analog output . . . . . . . . . . . . . . . . . 49 interval
authorized use . . . . . . . . . . . . . . . . 10 calibration (Int 3) . . . . . . . . . . . . 28
AutoRange . . . . . . . . . . . . . . . . . . . 54 data transmission (Int 2) . . . . . . 47
AutoRead . . . . . . . . . . . . . . . . . . . . 20 storing (Int 1) . . . . . . . . . . . . . . . 38
AutoStore . . . . . . . . . . . . . . . . . . . . 38
K
B keys . . . . . . . . . . . . . . . . . . . . . . . . . 6
batteries
replacing . . . . . . . . . . . . . . . . . . 59 L
battery compartment . . . . . . . . . . . . 60 linear temperature compensation . . 34
baud rate, setting . . . . . . . . . . . . . . 53 LoBat . . . . . . . . . . . . . . . . . . . . . . . 63
C M
calibration . . . . . . . . . . . . . . . . . . . . 25 manual storing . . . . . . . . . . . . . . . . 36
interval . . . . . . . . . . . . . . . . . . . . 28 measuring . . . . . . . . . . . . . . . . . . . . 19
protocol . . . . . . . . . . . . . . . . . . . 27 measuring precision . . . . . . . . . . . . 28
calibration evaluation . . . . . . . . . . . 27 MultiLab pilot . . . . . . . . . . . . . . . . . 51
cell constant . . . . . . . . . . . . . . . 18, 25
commissioning . . . . . . . . . . . . . . . . 13 N
condition on delivery . . . . . . . . . . . . 57 non-linear temperature
Conductivity . . . . . . . . . . . . . . . . . . 21 compensation . . . . . . . . . . . . 33
conductivity . . . . . . . . . . . . . . . . . . . 54
O
conductivity/resistance . . . . . . . . . . 49
operation . . . . . . . . . . . . . . . . . . . . 17
D operational safety . . . . . . . . . . . . . . 10
data record . . . . . . . . . . . . . . . . . . . 36 output data storage . . . . . . . . . . . . 40
data transmission (interval) . . . . . . . 48
P
date, setting . . . . . . . . . . . . . . . 13, 55
paper roll
display . . . . . . . . . . . . . . . . . . . . . . . . 7
replacing . . . . . . . . . . . . . . . . . . 59
drift control . . . . . . . . . . . . . . . . . . . 20
place of the instrument . . . . . . . . . . 17
E plug-in power supply
energy saving feature . . . . . . . . . . . 17 connecting . . . . . . . . . . . . . . . . . 14
error messages . . . . . . . . . . . . . . . . 63 printing
calibration protocol . . . . . . . . . . 27
I measured values . . . . . . . . . . . . 24
initial commissioning . . . . . . . . . . . . 13 printing measured values . . . . . . . . 24
79
Lists Cond 730
R
recorder output . . . . . . . . . . . . . . . .49
reference temperature . . . . . . . . 54, 58
reset . . . . . . . . . . . . . . . . . . . . . . . . 57
RS232 interface . . . . . . . . . . . . . . . .50
S
safety . . . . . . . . . . . . . . . . . . . . . . . . .9
safety precautions . . . . . . . . . . . . . . .9
salinity . . . . . . . . . . . . . . . . . . . . . . .49
salinity measurement . . . . . . . . . . .22
scope of delivery . . . . . . . . . . . . . . .13
sockets . . . . . . . . . . . . . . . . . . . . . . .7
Specific resistance . . . . . . . . . . . . .21
storing . . . . . . . . . . . . . . . . . . . . . . .36
switching on . . . . . . . . . . . . . . . . . . .13
T
TDS . . . . . . . . . . . . . . . . . . . . . . 23, 49
technical data . . . . . . . . . . . . . . . . .67
temperature compensation . . . . . . .32
linear . . . . . . . . . . . . . . . . . . . . . .34
non-linear . . . . . . . . . . . . . . . . . . 33
setting . . . . . . . . . . . . . . . . . . . . .32
switch off . . . . . . . . . . . . . . . . . . 35
temperature probe . . . . . . . . . . . . . .19
temperature unit . . . . . . . . . . . . . . .55
time, setting . . . . . . . . . . . . . . . . 13, 55
total dissolved solids
measurement . . . . . . . . . .23
transmit data . . . . . . . . . . . . . . . . . . 47
80