orrimnt Name/No.
Paga
Dote
Ate ualitatiue Semimiero aralycis of mixtue s
comtaining eatica6. k anions.
PHYSICAL 00SERVATIONA
) Salablity
) Appeananca -
DAY TEST FOR AcID RADICALS
erperiment Obseruatron rberence
1.
Q6sent.
Jo theat a pirch of the AcelounlaK gas ailk
(may be)
dense, askill funck ashen a
LaR tha mouth o tke fest teabe.
TEST RoR INTEREERING RADICALS
Experiment O6ser vatfon Znterenee
Tut fort phosphate: he No canarty yeloL2 -PO
absent
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EpetmentManetNo: Poge :
Date :
Ekpoimant Obseruafior îngenereo
ad.senf amneniumnalybdate
Valatil vapouts AO
abser
H80 khcat them.
WETTEST FOR AcID RADICALS
t Preparation of Sadh axiract:
Le takeakout 19 finey poadcncod sample niduo and about
flask Cie add
14a ankydhous aookant cartonater în a100 me conical
by_euaporatien, ce kilter the content auo! cash the reidue
aatore
aatE Amall_poretion chstilled ssatere. he bilrate ath thes ceashing
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Name/ No
Eeient Poge
Dato
Bxperiments Obsert vatlons 7rserehes
eauy chite ppt
-present
HE. DA bail tha mixtute. to epe!
Ball slution.
Aa purple calourafin s abzent
Sodium nitcoprusside. ges,
8. Test or So, 8 Ta Rml t So absent
Soda extract, aeada o'5 ml Colourcatian.
4. Test fort Halide, rcadica!
hcolahle n HNOg
ue aeidiy Rm o Soda extract
dl. NHOH.
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EnertNsme/Na
Page: 4
Date :
Experimcnts Dbsercvafions I"7enenet
s. Test sort Nitrate Ronl t No kroon ting NOg
bgent .
HC2, cO, beileal e ard add
Rml frashy pnepana fesly
soae esa) the midue ndr
tha fost fube..
TEST FOR MIXTURES QE ACID RADICALS !
Obserc vations In7enenee
Expeniments
1 Nitrode amd Nitrite
A) NO We take agutous NO abrent.
LAolattioy thes sample cna
seot plate ad ado ong duep
hle boileo the a No rtedcolouratfon, NO absent
l6)NO
sutphamie acio/ ureA and
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tanelentNaseINa
Poge :
Date
Experti nnent Obsercvatfo Insenenees
ntteate comyplately art then cesled
enapthylamins.ant atkad fllousel
8.Chloruc, Bromide and lodido:
Na uialcd colouraten I" abeent.
A5onl of Soda extracB is
Rthen chaken aftor gradual
Ne yellsish brcoun
gnaskual adttion ef Ch csater colour Ppart
NH, OH but irsoluble
Hpresert) aud filtened. Then
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eriet Narme /No Paqe :
Date
Experiment obseruatios) Irference
CoNCLUSIDNI Baced .on to abaue orpeninentt ae fod Wiat the
DRY TEST FOR GASIC RADICALS R
Experimert Dbserv afion 2n6enen ce
( Ray be)
Lumineus Bunser flama. F) Qshito sub limate céthined. ) NH, call.
2. Flame test& A pinch ot
the saupb oith cone. He)
Aeotesl n anon- lummas Jlne ( )Btuisk ghen blame ppears. () Cet gatt.
fakec .
8. Hootng on a charcif blecki )Keddish -salf.
A pmes Hhe samplk is mikeMite esidue: gloc) on ) A, Ca, S, Ba
attk deukle theguatity&eatig. |g, Mn - salt.
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ment Nare No Page
Ex periment 0bsertva tion Zgerence
Na, Ca aud heated the mixhrt ena
hasueng flara.
Ce - ceyporno
(mey be)
4 6lue uhen cotd.
flame, kocaAad finst cellk upk
finally metls to fotm a eolourlass Celenless sken hot,
kead &touched wsi fe Banple md
cold.
hen the hedtucig tlamli
6. Cobal! NHrate teet Tue ashite
iteside Charoaf bleck test is Coleua ful
awater mass pmoduceo.
eunlaol by ast 3-Sdaeps f Cmay be)
saadd, then apai keated
tlames
Streng pungort shmey NH, Satl.
6. lTest fer NH, : Salt + Na, og t|
NH g26. Cmay be)
heat
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Foeriment Name /
Date
WET TEST FOR BASLS RADICAL6:
radicals Naaa Greup anaysis
Dbscvafier Inkerene
Experiment
test for-ptoup C) shet penfenag
areup ()
)gatt co 8arcmcsl anc/ H,S is elackPl oresent.
asscme.
Gnep ( )
Abue flhate, kikd teremUe MSt eshite pt Present.
assumtd.
ancup C)
a6sent.
breup ()
abcErt.
Nay H(Po) Caahte Pot.
6) Rboe fllate t
e inslalo ke assen eo. prtsent ,
so/, Senatoh
o
test tube eith a glaSs
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Serimeot Nane /No Page
Date:
NHyc A Aleos ill Re so beLO alolloc., lu ohsen tation arco
follows -
Thel cehite pot may te ef ALoHs
2minakes uotil evoltien of coASes. ond thenfller il.
fert
) lolourless filtrak mo contain NaALO,
Solid Nl, co aut bofI 7, ashite seltinous Ppt.
8) FiHate t
formed.
11 Cerfims the prasent of n .
teco parts.
shite Ppt. fermed.
1! cerfirne the pesent of mgt,
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Page
Experiment Name/No
Dote:
J) Rnd paret + foo areAs of magneeen aagent t NaoH co/ Hl
alkacine Alueppt obtaincd
|TEST OR NH
Expenlment Dbsercvatien Infenence
1o
NH, pretent.
Yelleus ppt.
fortm
Cobalfntrite som
NHt pre SCnt
fon mada |& confrmes,
Nessler neagent
20
Hence the kmple contains follezong radicals -
i) Acid tadfeals :
) Gasic rasicals : CuRt, AL3, Mgt an
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