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    Chemical Experi 1

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    varinay1611
    This document provides details about the Chemical Experimentation I course, including instructor information, course objectives, textbook, and evaluation scheme. The course involves performing 22 organic chemistry experiments in two sections over the semester. Students will gain experience in synthesis, extraction, analysis, and purification techniques while developing safe lab practices. Evaluation is based primarily on laboratory work and reports, with tests assessing skills and learning outcomes.

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    Chemical Experi 1

    Uploaded by

    varinay1611
    18 views3 pages
    This document provides details about the Chemical Experimentation I course, including instructor information, course objectives, textbook, and evaluation scheme. The course involves performing 22 organic chemistry experiments in two sections over the semester. Students will gain experience in synthesis, extraction, analysis, and purification techniques while developing safe lab practices. Evaluation is based primarily on laboratory work and reports, with tests assessing skills and learning outcomes.

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    This document provides details about the Chemical Experimentation I course, including instructor information, course objectives, textbook, and evaluation scheme. The course involves performing 22 organic chemistry experiments in two sections over the semester. Students will gain experience in synthesis, extraction, analysis, and purification techniques while developing safe lab practices. Evaluation is based primarily on laboratory work and reports, with tests assessing skills and learning outcomes.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    18 views3 pages

    Chemical Experi 1

    Uploaded by

    varinay1611
    This document provides details about the Chemical Experimentation I course, including instructor information, course objectives, textbook, and evaluation scheme. The course involves performing 22 organic chemistry experiments in two sections over the semester. Students will gain experience in synthesis, extraction, analysis, and purification techniques while developing safe lab practices. Evaluation is based primarily on laboratory work and reports, with tests assessing skills and learning outcomes.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    of 3

    BIRLA INSTITUTE OF TECHNOLOGY AND SCIENCE, Pilani

    Pilani Campus
    AUGS/ AGSR Division

    SECOND SEMESTER 2023-24


    COURSE HANDOUT
    Date: 08.01.2024

    In addition to the part I (General Handout for all courses appended to the Timetable), this portion gives further
    specific details regarding the course.
    Course No : CHEM F242
    Course Title : Chemical Experimentation I
    Instructor-in-Charge : Indresh Kumar
    Tutorial/Practical Instructors: Dalip Kumar, Anil Kumar, Ajay Kumar Sah, Madhushree Sarkar, Paritosh
    Shukla, Indresh Kumar, Rajeev Sakhuja, Partha Sarathi Addy
    Student Instructors: ANUVASITA PARIKH, NANDINI ROY, PRIYANKA KUMARI PRASAD, TANK
    DISHABEN HARSUKHBHAI, SAKSHI BAJAJ, BORADE SOMNATH ARJUN,
    SAURAJIT GHOSH, PARMESHTHI PARIKH, RITU RANI, REENA JANGIR,
    PRIYANKA BHARDWAJ, NIDHI, GADEKAR AMOL BHAGWANRAO, ARUN
    PATEL, MAHIMA SAHU, SHRUTI SONI, SNEHA TAILOR, DIKSHA ROHILLA,
    SHUBHI SAINI, TARUN JANGIR, NITIKA, VINEETA CHATURVEDI, DIVYA,
    ARPIT.
    1. Course Description: This course is based on laboratory experiments in organic chemistry. This course is
    available for second-year M.Sc. Chemistry students.
    2. Scope and Objective of the Course: The course’s main objective is to provide students with a firsthand
    experience of basic techniques used in an organic chemistry laboratory. Broadly, the experiments include
    qualitative organic analysis, detection of known and unknown functional groups, chemical separation of a
    mixture of two compounds, examples of single-step and two-step organic syntheses, extraction of organic
    compounds from natural sources or from drugs, chromatographic separation of the pure compound from a
    mixture obtained in a multistep reaction, etc.

    3. Textbooks: Vogel's Textbook of Practical Organic Chemistry, 5th Ed.


    4. Reference Books: Reference sources for each experiment will be specified as necessary.
    5. Course Plan: The students will perform several experiments in qualitative, synthetic organic chemistry, including
    single-step and multi-step synthesis, extraction of natural products, and training in chromatographic separation, with an
    emphasis on individual planning and execution of the experiments. The students will be divided into two sections (I & II),
    and each section will conduct a set of experiments (Lab I or Lab-II experiments) in the first half semester, and thereafter,
    interchanging of the students will proceed during the second half of the semester. Selected 22 experiments will be discussed
    and performed in the class.

    Topic Exp No. Experimental Detail Learning Outcomes

    Lab-I 1 Chemoselective reduction of organic • Safe laboratory practices and


    Experiments: compound handling of glassware, equipment,
    and reagents.
    Synthesis, 2 Multicomponent reaction (Biginelli Reaction)
    extraction, • Findings of limiting reagent and
    3 Coumarin synthesis using microwave percent yield of a single or a multi-
    estimation, and
    irradiation step synthesis.

    1
    BIRLA INSTITUTE OF TECHNOLOGY AND SCIENCE, Pilani
    Pilani Campus
    AUGS/ AGSR Division

    purification 4 Oxidation of Organic Compounds (Synthesis • Understanding reaction monitoring


    techniques of bezil from benzoin) and product purification techniques
    like distillation, recrystallization,
    5 Synthesis of benzilic acid from benzil using aqueous extraction, thin layer, and
    grinding technique column chromatography.

    6 Cycloaddition reaction (Diels-Alder Reaction) • Utilization of characterization


    techniques like mp, IR, NMR, etc.
    under heating or microwave conditions
    • Understanding the mechanism of
    7 Separation/purification of an organic
    some simple organic reactions
    compound using column chromatography
    • Proper documentation of
    8 Isolation of curcumin from curcuma longa laboratory work

    9 Nucleophilic Aromatic Substitution

    10 Purification of compounds by Column


    Chromatography (from exp-8)

    1 Elemental Analysis of Known Organic


    Compounds (4 Compounds, common)

    2-3 Functional group analysis of known compounds • Safe laboratory practices and
    (12 Compounds, common) handling of glassware, equipment,
    Lab-II and reagents.
    Experiments*: Non-nitrogenous functional groups: Alcohol,
    Phenol, Aldehyde, Ketone, Alkene, Alkyne • Preliminary observation of general
    Qualitative physical characteristics of organic
    (unsaturated compounds), Carbohydrate,
    Analysis of compounds
    Carboxylic acid, and Ester
    Organic
    Understanding of the organic
    Compounds Nitrogenous functional groups: Amine, Amide, compounds chemical separation and
    Nitroaromatics purification techniques like
    distillation, extraction, etc.
    4-5 Complete analysis (Elemental analysis &
    functional group determination) of unknown • Learning of elements and
    compounds, & mp determination (min. of two functional group analysis.
    compounds by each student)
    • Utilization of characterization
    6 Separation of the mixture by Separation techniques like mp, IR, and NMR
    Technique-I: A mixture of water-soluble • Proper documentation of
    components and the water-insoluble component laboratory work
    will be separated by water and identification of
    residue by elemental & functional group analysis
    (one mixture to each student)

    7-8 Separation of the mixture by Separation


    Technique-II & Technique-III: A mixture of
    acidic/basic and neutral components will be
    separated, and identification of acidic/basic and

    2
    BIRLA INSTITUTE OF TECHNOLOGY AND SCIENCE, Pilani
    Pilani Campus
    AUGS/ AGSR Division

    neutral components will be by elemental and


    functional group analysis (two different types of
    mixtures to each student)

    9 Separation of the mixture by Separation


    Technique-IV: A mixture of acid and base
    components will be separated, and their analysis
    (elemental and functional group) will be
    performed (one mixture to each student)

    10 Separation of the mixture by Separation


    Technique-V: A mixture of solid/liquid or
    liquid/liquid will be separated and a detailed
    analysis of both the components will be
    performed via elemental and functional group
    analysis (one mixture to each student)

    *
    In a qualitative analysis of compounds/mixtures, NMR and IR will be provided to characterize the compounds.
    6. Evaluation Scheme:
    Component Weightage (%) Date & Time
    Laboratory Work & Reports 84 Continuous

    Lab tests I and II 16 To be announced

    6a. Marks Distribution: Each Lab experiment will be of 14 Marks.


    The distribution of marks is as follows:

    Lab-I Experiments: Attendance (2), Lab quiz (3), Lab cleaning (1), NMR (2), record book (6).
    Lab-II Experiments: Attendance (2); Lab quiz (3); Performance (6), Other evaluation components (3).
    7. Notices: All notices concerning the course will be displayed on Nalanda.

    8. Make-up Policy: No makeup or buffers policy will be applied to this course.

    Instructor-in-charge
    CHEM F242

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