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PDF 08 0247

This document provides information about the crystalline structure of elemental sulfur. It includes the orthorhombic unit cell parameters, space group, density, molecular weight, and volume. It also lists the strongest diffraction lines and provides the indexed diffraction pattern, including miller indices, intensities, and d-spacings. This replaces an earlier reference pattern for sulfur.

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Luis Arturo Lopez Cruz
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101 views2 pages

PDF 08 0247

This document provides information about the crystalline structure of elemental sulfur. It includes the orthorhombic unit cell parameters, space group, density, molecular weight, and volume. It also lists the strongest diffraction lines and provides the indexed diffraction pattern, including miller indices, intensities, and d-spacings. This replaces an earlier reference pattern for sulfur.

Uploaded by

Luis Arturo Lopez Cruz
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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PDF#08-0247: QM=Indexed(I); d=Guinier(114.

6mm); I=Densitometer
Sulfur, syn
S Yellow
Radiation=CuKa1 Lambda=1.5405 Filter=
Calibration= 2T=11.498-69.346 I/Ic(RIR)=
Ref: de Wolff, P., Technisch Physische Dienst, Delft, The Netherlands.
ICDD Grant-in-Aid
Orthorhombic - Powder Diffraction, Fddd (70) Z=128 mp=112.8$DE
CELL: 10.45 x 12.84 x 24.46 <90.0 x 90.0 x 90.0> P.S=oF128 ($GA) (S)
Density(c)=2.076 Density(m)=2.070 Mwt=32.06 Vol=3281.99 F(30)=29.7(0.023,44/0)
Ref: Ibid.

Strong Lines: 3.85/X 3.21/6 3.44/4 3.33/3 3.11/3 3.08/2 2.84/2 5.76/1 2.62/1 2.42/1
NOTE: Validated by calculated pattern 24-733.
Other data 21-1066.
To replace 1-478.

2-Theta d(�) I(v) h k l Theta 1/(2d) 2pi/d n^2


11.498 7.6900 3.0 1 1 1 5.749 0.0650 0.8171
15.370 5.7600 9.0 1 1 3 7.685 0.0868 1.0908
15.588 5.6800 4.0 0 2 2 7.794 0.0880 1.1062
18.469 4.8000 2.0 2 0 2 9.234 0.1042 1.3090
21.187 4.1900 2.0 1 1 5 10.593 0.1193 1.4996
21.873 4.0600 11.0 2 2 0 10.937 0.1232 1.5476
22.723 3.9100 12.0 1 3 1 11.362 0.1279 1.6070
23.082 3.8500 100.0 2 2 2 11.541 0.1299 1.6320
24.921 3.5700 9.0 1 3 3 12.460 0.1401 1.7600
25.879 3.4400 45.0 0 2 6 12.939 0.1453 1.8265
26.346 3.3800 5.0 2 2 4 13.173 0.1479 1.8589
26.749 3.3300 29.0 3 1 1 13.375 0.1502 1.8868
27.769 3.2100 72.0 0 4 0 13.884 0.1558 1.9574
28.680 3.1100 31.0 3 1 3 14.340 0.1608 2.0203
28.966 3.0800 22.0 1 3 5 14.483 0.1623 2.0400
29.159 3.0600 3.0 0 0 8 14.580 0.1634 2.0533
31.452 2.8420 24.0 0 4 4 15.726 0.1759 2.2108
33.305 2.6880 3.0 3 3 1 16.652 0.1860 2.3375
33.497 2.6730 3.0 2 4 2 16.748 0.1871 2.3506
34.182 2.6210 21.0 1 3 7 17.091 0.1908 2.3972
34.276 2.6140 6.0 4 0 0 17.138 0.1913 2.4037
34.896 2.5690 12.0 3 3 3 17.448 0.1946 2.4458
35.876 2.5010 12.0 2 4 4 17.938 0.1999 2.5123
37.057 2.4240 22.0 3 1 7 18.528 0.2063 2.5921
37.376 2.4040 3.0 4 0 4 18.688 0.2080 2.6136
37.850 2.3750 6.0 4 2 2 18.925 0.2105 2.6456
37.999 2.3660 7.0 3 3 5 19.000 0.2113 2.6556
39.347 2.2880 10.0 0 2 10 19.674 0.2185 2.7461
40.700 2.2150 3.0 2 0 10 20.350 0.2257 2.8367
42.070 2.1460 7.0 1 1 11 21.035 0.2330 2.9279
42.780 2.1120 18.0 3 1 9 21.390 0.2367 2.9750
43.080 2.0980 4.0 2 2 10 21.540 0.2383 2.9948
43.983 2.0570 4.0 5 1 1 21.991 0.2431 3.0545
44.346 2.0410 4.0 2 4 8 22.173 0.2450 3.0785
45.233 2.0030 4.0 3 5 3 22.617 0.2496 3.1369
45.594 1.9880 8.0 4 0 8 22.797 0.2515 3.1606
46.358 1.9570 4.0 2 6 2 23.179 0.2555 3.2106
47.149 1.9260 4.0 4 4 4 23.574 0.2596 3.2623
47.834 1.9000 16.0 5 1 5 23.917 0.2632 3.3069
49.041 1.8560 4.0 3 1 11 24.521 0.2694 3.3853
49.554 1.8380 4.0 1 5 9 24.777 0.2720 3.4185
49.989 1.8230 8.0 2 4 10 24.995 0.2743 3.4466
51.252 1.7810 26.0 2 6 6 25.626 0.2807 3.5279
52.100 1.7540 18.0 5 3 5 26.050 0.2851 3.5822
53.044 1.7250 18.0 6 0 2 26.522 0.2899 3.6424
53.955 1.6980 18.0 1 3 13 26.977 0.2945 3.7003
55.114 1.6650 5.0 6 2 2 27.557 0.3003 3.7737
55.367 1.6580 5.0 2 0 14 27.683 0.3016 3.7896
55.768 1.6470 14.0 3 5 9 27.884 0.3036 3.8149
56.705 1.6220 14.0 6 2 4 28.353 0.3083 3.8737
57.283 1.6070 14.0 4 0 12 28.642 0.3111 3.9099
57.518 1.6010 5.0 6 0 6 28.759 0.3123 3.9245
57.754 1.5950 10.0 4 6 4 28.877 0.3135 3.9393
59.052 1.5630 5.0 4 4 10 29.526 0.3199 4.0200
59.938 1.5420 5.0 3 7 5 29.969 0.3243 4.0747
60.414 1.5310 5.0 0 0 16 30.207 0.3266 4.1040
61.119 1.5150 5.0 3 5 11 30.560 0.3300 4.1473
61.615 1.5040 5.0 1 7 9 30.807 0.3324 4.1777
62.258 1.4900 5.0 2 8 4 31.129 0.3356 4.2169
62.963 1.4750 5.0 6 2 8 31.482 0.3390 4.2598
63.637 1.4610 5.0 7 1 3 31.818 0.3422 4.3006
64.727 1.4390 11.0 4 4 12 32.363 0.3475 4.3664
65.494 1.4240 11.0 0 8 8 32.747 0.3511 4.4123
65.753 1.4190 5.0 7 1 5 32.877 0.3524 4.4279
67.251 1.3910 6.0 3 5 13 33.625 0.3595 4.5170
68.881 1.3620 6.0 5 7 3 34.441 0.3671 4.6132
69.346 1.3540 11.0 7 3 5 34.673 0.3693 4.6405

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