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Bab 4 Iso

1) The document presents results from experiments analyzing standard solutions and samples using spectroscopy. Tables show absorbance measurements for standard solutions with different concentrations and sample solutions. 2) Graphs of the standard solutions show a linear relationship between concentration and absorbance. Graphs of Freundlich and Langmuir isotherm models also show linear relationships for sample solution adsorption. 3) The results were used to calculate adsorption capacity and efficiency for different sample solutions, ranging from 94.47% to 98.90% efficiency.

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Akidah Tahir
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29 views4 pages

Bab 4 Iso

1) The document presents results from experiments analyzing standard solutions and samples using spectroscopy. Tables show absorbance measurements for standard solutions with different concentrations and sample solutions. 2) Graphs of the standard solutions show a linear relationship between concentration and absorbance. Graphs of Freundlich and Langmuir isotherm models also show linear relationships for sample solution adsorption. 3) The results were used to calculate adsorption capacity and efficiency for different sample solutions, ranging from 94.47% to 98.90% efficiency.

Uploaded by

Akidah Tahir
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as DOCX, PDF, TXT or read online on Scribd
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BAB IV

HASIL DAN PEMBAHASAN

A. Hasil Pengamatan

1. Tabel Pengamatan

Tabel IV.1 Hasil Pengamatan Larutan Standar


x y
No. Larutan x.y x2 y2
(mg/L) (Adsorbansi)

1 Standar 1 0,5 0,0466 0,0233 0,25 0,00217156

2 Standar 2 1 0,0728 0,0728 1 0,00529984

3 Standar 3 2 0,1483 0,2966 4 0,02199289

4 Standar 4 4 0,3342 1,3368 16 0,11168964

5 Standar 5 8 0,6865 5,4920 64 0,47128225

n=5 Σ = 15,5 Σ =1,2884 Σ =7,2215 Σ = 85,25 Σ =0,61243618

Tabel IV.2 Hasil Pengamatan Larutan Contoh


No. Larutan x (mg/L) y (Adsorbansi) Panjang
Gelombang (nm)

1 Sampel 1 30 0,1325 655

2 Sampel 2 45 0,0779 655

3 Sampel 3 60 0,0833 655

4 Sampel 4 75 0,1238 655

5 Sampel 5 90 0,0739 655


Tabel IV.3 Hasil Perhitungan Efektivitas Adsorpsi Larutan Sampel
Konsentrasi Kapasitas Efektivitas
No. Larutan Adsorbansi
Sisa Adsorpsi Adsorpsi

1 Sampel 30 ppm 0,1325 1,657163837 0,005668567 94,47 %

2 Sampel 45 ppm 0,0779 1,027839229 0,000879443 97,71 %

3 Sampel 60 ppm 0,0833 1,090080124 0,011781983 98,18 %

4 Sampel 75 ppm 0,1238 1,556886839 0,014688622 97,92 %

5 Sampel 90 ppm 0,0739 0,981734862 0,017803653 98,90 %

Tabel IV.4 Persamaan Freundlich


No. Larutan Ce Qe x (log Ce) y (log Qe)

1 Sampel 30 ppm 1,657163837 0,0056685672 0,2193654476 -2,246526698

2 Sampel 45 ppm 1,027839229 0,0008794432 0,0119251894 -3,055792197

3 Sampel 60 ppm 1,090080124 0,0117819839 0,0374584213 -1,928781572

4 Sampel 75 ppm 1,556886839 0,0146886226 0,1922570476 -1,833018926

5 Sampel 90 ppm 0,981734862 0,0178036530 -0,008005786 -1,749490878

Tabel IV.5 Persamaan Langmuir


No. Larutan Ce Qe x (1/Ce) y (1/Qe)

1 Sampel 30 ppm 1,657163837 0,0056685672 0,6034406361 176,4114219

2 Sampel 45 ppm 1,027839229 0,0008794432 0.9729148020 1137,083099

3 Sampel 60 ppm 1,090080124 0,0117819839 0.9173637588 84,87534938

4 Sampel 75 ppm 1,556886839 0,0146886226 0.6423074400 68,07990287

5 Sampel 90 ppm 0,981734862 0,0178036530 1,0186049601 56,16824816


2. Grafik
a. Larutan Standar

Larutan Standar
0.8
0.8000
0.7
0.7000
f(x) =f(x)
0.0864548387096774 x − 0.00924999999999998
= 0.0864548387096774 x − 0.00924999999999998
0.6
0.6000 R² = 0.998496213958368
R² = 0.998496213958368
Y (Absorbansi)

0.5
Adsorbansi (Y)

0.5000
0.4
0.4000 Absorbansi
Adsorbansi
0.3 LinearLinear
(Adsorbansi)
0.3000 (Ab-
sorbansi)
0.2
0.2000
0.1000
0.1
0.0000
0
0 0
1 12 2 3 3 44 55 6 6 7 78 9
8 9
Konsentrasi
Konsentrasi (mg/L) X (ppm)

Grafik IV.1 Larutan Standar


b. Larutan Contoh

Larutan
Konsentrasi ContohContoh
Larutan
0.14
10.0000
0.129.0000
8.0000 f(x) = 0.0499799756097561 x − 1.67587743902439
f(x) = 0.000732285714285714
0.17.0000 x + 0.0452857142857143
Y (Absorbansi)

R² = 0.959203989732364
R² = 0.253501624285846
Adsorbansi (Y)

0.086.0000 Absorbansi
5.0000 Adsorbansi
Linear
0.064.0000 (Ab-
Linear (Adsorbansi)
sorbansi)
0.043.0000
2.0000
0.021.0000

0
0.0000
0 100 20 5030 100 15060 200
40 50 70 250 90 100
80
Konsentrasi (mg/L) X (ppm)
Konsentrasi

Grafik IV.2 Larutan Contoh


c. Grafik Isoterm Adsorpsi Freundlich

Isoterm Adsorpsi
Persamaan Freundlich
Freundlich
0.25 0.0000
-1.0000 0.0000 1.0000 2.0000 3.0000
0.2 -0.5000

0.15 -1.0000
Persamaan Freundlich
Log Ce
Log Ce
log Qe

0.1 -1.5000 Linear (Persamaan


Linear (Log Ce)
Freundlich)
-2.0000
f(x) = 9.14285714285715E-05 x + 0.0674285714285714
0.05 R² = 0.00087491455912525
f(x) = 0.207928803173391 x − 2.46900705578348
-2.5000 R² = 0.748566526578363
0
0 10 20
-3.0000 30 40 50 60 70 80 90 100
-0.05
logKonsentrasi
Ce X (ppm)

Grafik IV.3 Isoterm Adsorpsi Freundlich


d. Grafik Isoterm Adsorpsi Langmuir

Isoterm Adsorpsi
Persamaan Langmuir
Langmuir
0
450.0000
0 10 20 30 40 50 60 70 80 90 100
400.0000
-0.5
350.0000 f(x) = 166.519500856621 x + 120.739080767104
R² = 0.870853610830886
-1
300.0000
f(x) = − 0.0141904761904762 x − 1.08714285714286
250.0000
R² = 0.210808480576108 Persamaan Langmuir
-1.5
Log Qe
1/Qe

200.0000 Linear (Persamaan


Log Qe
Langmuir)
150.0000
-2 Linear (Log Qe)
100.0000
-2.5
50.0000
-3 0.0000
0.00000.50001.00001.50002.0000
-3.5
1/Ce
Konsentrasi X (ppm)

Grafik IV.4 Isoterm Adsorpsi Langmuir

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