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Salt Analysis Rough Draft

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Kirtan Patel
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68 views3 pages

Salt Analysis Rough Draft

Uploaded by

Kirtan Patel
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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SNO ‘Analysis of anions |Small amount of salt + A drop of Conc. HCI form a paste. Take the: paste at the charred end of the ‘splinter and introduce it near the Bunsen flame Action of dil. HCI: Small amount of salt + 1mL of dil. [Action of MnO2 and Conc. H2SO4: [Small amount of salt in a dry test tube + pinch of MnG2 + Conc. H2S04 and gently heat it [Action of Canc. H2SO4 and copper| turning: small amount of salt in a dry], lest tube + few copper turnings + Conc. H2SO4. Gently heat it Action of dil. NaOH solution: Small lamont of a salt + dil.NaOH solution | land gently heat it. : [Chromyl chloride test: Test for halides: 1 ml of sodium carbonate extract |+dil. HNO, + 1ml of AgNOs, and shake it {Test with barium chloride: {One mi of the sodium carbonate: extract + dil. Aceticacid + 1ml of bariumchloride solution and shake [Test with leadacetate: ml of the sodium carbonate extract, + Im| of dil acetic acid and heat it + 1 iml of Lead Acetate [Brown ring test: ‘imi of the sodium carbonate extract |+ dil. H_SO, + freshly prepared ferrous sulphate solution then add iConc. H,SO, along the sides of the test tube. imonium molybdate test: 1 mi of the extract + dil HNO, + about} ml each of ammonium molybdate jand Cone. HNO; Test with sodium nitro bruside: ‘Imi of the sodium carbonate extract) + 1ml of dil aommonia. + few drops of sodium nitro bruside. Preparation of salt solution: To a small amount of salt in a test tube add 2 to 3mi of water, shake it and gently heat it. This ‘solution is called “original solution”. IGROUP O imi of the original salt solution add jabout 1ml each of Nessler's reagent [Take about 1 ml of the salt solution in ja test tube Add about 1ml of dil HCI, (GROUP Ill To about imi of the salt solution add about Imi each of 4 [NH,CI, NH,OH and shake it well [GROUP V To the salt solution add ml each of NH,Cl, NH,OH and |(NH,),CO; and shake it well. (GROUP VI To the original salt solution add 1ml each of NH,Cl, 7 |NH.OH and NH.H;PO,, and scratch ithe sides of the test tube. Result: The Anion Present The cation Present The Given simple salt

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