Technovit Polymer Embedding Catalog
Technovit Polymer Embedding Catalog
Technovit Polymer Embedding Catalog
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EMBEDDING
CORPORATE EMBEDDING
Kulzer Technovit®
Pioneer in sample preparation Resins that set standards in quality and processing
Essential aspects for the materialographic As far back as the early fifties, the idea was born to High-quality resins with reliable properties The resins from Kulzer meet the highest requirements.
transfer the expertise in resin technologies to the field of They are used as embedding resins for materialographic
examination are to make reliable statements and easy handling are the prerequisites for examinations or as aids in materialography and production
materials testing.
about the characteristics of the samples to precise material testing. Kulzer has been a processes. They thus occupy a permanent place in the
This was the birth of Kulzer Technik and “Technovit”
be examined. In 1953, Kulzer Technik introduced the fast-curing resin leader in the development and manufacture everyday life of modern laboratories and manufacturing
processes.
Perfectly prepared samples support the
Technovit – an important basic material for of resin products of the highest quality for
materialographic tests – to the market. In the course of the Technovit – the resin with many faces
analysis of cause and effect. many decades.
last almost 70 years, the product range of Technovit resins The umbrella brand "Technovit" stands for a wide range of
has been continuously expanded and adapted to changing resin products of different technologies. The focus is on the
You will find Kulzer Technik to be a reliable requirements. application for material testing.
partner in the field of materialography. In addition to the product range of Technovit resins, Kulzer Gap-free embedding, transparency, time-saving and easy
We offer you free, individual advice and Technik offers a complete program of grinding and handling, as well as a maximum of impression accuracy
polishing media as well as a matching equipment series and form stability are the outstanding features that are
work with you to develop preparation
for materialography. specifically required in "materialography." Kulzer Technik
methods for new tasks. Convince yourself meets these requirements with its complete product range.
Minimal preparation steps and perfect preparation
of the quality of our products in your The components are coordinated in such a way that from
In addition to classical materialographic applications, these
products can also be used for industrial manufacturing
laboratory. the cutting of the samples to the final polishing step,
processes, toolmaking, prototype construction (spouts,
efficient, time- and thus cost-saving preparation takes
fasteners) or in the restoration sector.
place – naturally at the highest quality level! Our goal is to
always offer you up-to-date and high-quality products and All Technovit products originate from our own research and
solutions for your individual working environment. development laboratories.
Customized solutions
In addition to our standard program, we are also happy to
provide you with our know-how for customized products.
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EMBEDDING COLD EMBEDDING RESINS EMBEDDING
Technovit 4004 | Technovit 4006 | Technovit 4006 SE All-rounder for daily use Mixing ratio is 1:2:2 by volume or 1:2:3 by weight
EN ISO 604: 2003
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EMBEDDING COLD EMBEDDING RESINS COLD EMBEDDING RESINS EMBEDDING
Quantities and mixing ratios Technovit 4002 IQ (without sample), example for 3:2 Quantities and mixing ratios of Technovit 4004 (without sample)
25 mm* 30 mm* 40 mm* 50 mm* Mixing ratios PDR LIQ 25 mm* 30 mm* 40 mm* 50 mm* Mixing ratios PDR LIQ
20 g 25 g 45 g 70 g 30 g powder with 20 g liquid approx. 60% approx. 40% 13 g 18 g 32 g 48 g 25 g powder with 15 g liquid approx. 62.5% approx. 37.5%
12 g powder 15 g powder 27 g powder 42 g powder 30 g powder with 19 ml liquid 8 g powder 11 g powder 20 powder 30 g powder 25 g powder with 16 ml liquid
8 g liq. 10 g liq. 18 g liq. 28 g liq. 5 g liq. 7 g liq. 12 g liq. 18 g liq.
* Kulzer embedding forms. The mixing ratios mentioned are basic values and can be varied slightly depending on the application requirements. * Kulzer embedding forms. The mixing ratios mentioned are basic values and can be varied slightly depending on the application requirements.
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EMBEDDING COLD EMBEDDING RESINS COLD EMBEDDING RESINS EMBEDDING
Quantities and mixing ratios of Technovit 4006/4006 SE (without sample) Quantities and mixing ratios of Technovit 4071 (without sample)
25 mm* 30 mm* 40 mm* 50 mm* Mixing ratios PDR LIQ 25 mm* 30 mm* 40 mm* 50 mm* Mixing ratios PDR LIQ
13 g 18 g 32 g 48 g 25 g powder with 15 g liquid 63% 37% 13 g 18 g 32 g 48 g 25 g powder with 15 g liquid approx. 63% approx. 37%
8 g powder 11 g powder 20 powder 30 g powder 25 g powder with 14 ml liquid 8 g powder 11 g powder 20 powder 30 g powder 25 g powder with 14 ml liquid
5 g liq. 7 g liq. 12 g liq. 18 g liq. 5 g liq. 7 g liq. 12 g liq. 18 g liq.
* Kulzer embedding forms. The mixing ratios mentioned are basic values and can be varied slightly depending on the application requirements. * Kulzer embedding forms. The mixing ratios mentioned are basic values and can be varied slightly depending on the application requirements.
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EMBEDDING COLD EMBEDDING RESINS EMBEDDING
bubble-free
cost-effective
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EMBEDDING COLD EMBEDDING RESINS COLD EMBEDDING RESINS EMBEDDING
Gap-freeembeddings
Gap-free embeddingsfor
forSEM
SEM exami- Technovit 5071 – gentle removal
nations in combination
examinations with Technovit
in combination with of sensitive samples.
Technovit
EPOX. EPOX.
Thermally separable: If the samples are heat resistant, Technovit Chemically separable: Dissolution rate for a sample block
5071 can be softened by heating the sample block to 150 °C. The (approx. 27 g resin) in 100 ml acetone at room temperature
sample block can also be heated to 150 °C. Simple geometric ca 11 h, at 50 °C approx. 4 h.
shapes can thus be removed again without much effort.
Quantities and mixing ratios of Technovit 5000 (without sample) Quantities and mixing ratios of Technovit 5071 (without sample)
Mixing ratios PDR LIQ 25 mm* 30 mm* 40 mm* 50 mm* Mixing ratios PDR LIQ
25 g powder with 15 g liquid 63% 37% 13 g 18 g 32 g 48 g 25 g powder with 15 g liquid approx. 63% approx. 37%
25 g powder with 14 ml liquid 8 g powder 11 g powder 20 powder 30 g powder 25 g powder with 16 ml liquid
5 g liq. 7 g liq. 12 g liq. 18 g liq.
* Kulzer embedding forms. The mixing ratios mentioned are basic values and can be varied
slightly depending on the application requirements. * Kulzer embedding forms. The mixing ratios mentioned are basic values and can be varied slightly depending on the application requirements.
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EMBEDDING COLD EMBEDDING RESINS COLD EMBEDDING RESINS EMBEDDING
Quantities and mixing ratios of Technovit EPOX (without sample) Hardness (Shore D) [MPa] Technovit EPOX
Embedding Quantity without sample Ambient tem- Max. curing Time to max. Time to end mea- Product Curing at EPOX EPOX
form perature temperature temperature surable temp. Regular Fast
Technovit EPOX Resin & Technovit EPOX Hardener regular Shore D (20 h) Room temperature 71 73
25 mm* 12 g (8 g resin / 4 g hardener) 20 °C 30 °C 120 min ca. 18 h Shore D (2 d) Room temperature 78 79
30 mm* 18 g (12 g resin / 6 g hardener) 20 °C 35 °C 110 min ca. 18 h Shore D (7 d) Room temperature 79 80
40 mm* 30 g (20 g resin / 10 g hardener) 20 °C 45 °C 105 min ca. 18 h Shore D (14 d) Room temperature 80 81
50 mm* 45 g (30 g resin / 15 g hardener) 20 °C 65 °C 100 min ca. 18 h Shore D (21 d) Room temperature 80 81
40 mm* 30 g (20 g resin / 10 g hardener) 23 °C 48 °C 105 min ca. 18 h Shore D (20 h) 50 °C 79 80
40 mm* 30 g (20 g resin / 10 g hardener) 50 °C 100 °C 40 min ca. 3 h Mixing ratio: 100 g resin / 50 g hardener
Technovit EPOX Resin & Technovit EPOX Hardener fast
25 mm* 12 g (8 g resin / 4 g hardener) 20 °C 37 °C 90 min ca. 10 h
30 mm* 18 g (12 g resin / 6 g hardener) 20 °C 57 °C 80 min ca. 10 h
40 mm* 30 g (20 g resin / 10 g hardener) 20 °C 110 °C 70 min ca. 10 h
50 mm* 45 g (30 g resin / 15 g hardener) 20 °C 144 °C 60 min ca. 10 h
40 mm* 30 g (20 g resin / 10 g hardener) 23 °C 120 °C 60 min ca. 9 h
40 mm* 30 g (20 g resin / 10 g hardener) 50 °C 140 °C 40 min ca. 2 h
* Kulzer embedding forms. The mixing ratios mentioned must be adhered to exactly and are a prerequisite for this product for flawless curing.
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EMBEDDING COLD EMBEDDING RESINS EMBEDDING
Technovit 4021 2 component Routine embedding, black 2 5–6 min / 82 Vacuum not possible
Properties and application Self-curing odourless 99 °C Pressure possible
embedding and production of sections and thin sections
embedding of complex-shaped, fine plastic parts Technovit 4071 2 component Routine embedding green- 2 5–7 min / 85 Vacuum not possible
3-component embedding resin based on HEMA
Self-curing transparent 108 °C Pressure necessary
optimal infiltration and thus stabilization of fragile
Technovit 5000 2 component conductive copper-brown 1 7–12 min / 85 Vacuum not possible
materials Self-curing SEM examinations 125 °C Pressure necessary
ensures optimal infiltration of porous materials
Technovit 5071 2 component separable for SEM examina- green- 2 8–10 min / 84 Vacuum not possible
no temperature load
Self-curing tions transparent 112 °C Pressure necessary
the pointed shape distributes the cutting forces evenly and
thus protects the blade and sample Technovit Epox fast 2 component porous materials, workpieces transparent 20 10 h / 79 Vacuum possible,
Technovit 7100 – ideal for microtomy. Self-curing with low hardness 57 °C Pressure possible
Technovit Epox regular 2 component porous materials, materials transparent 20 18 h / 78 Vacuum possible,
Self-curing with low hardness 35 °C Pressure possible
Thin sections down to 1 µm Technovit 7100 3 component for microtome sections transparent 7 75 min / -- --
This unique, easy-to-use 3-component HEMA-based resin Self-curing 38 °C
allows thin sections down to 1 µm. This property makes
Technotherm 2000 1 component low shrinkage creamy white -- 10–15 min / 90 --
Technovit 7100 an indispensable embedding resin for
fusing fibre-reinforced 160–180 °C
difficult resin samples, textiles, paper, fibres, polymer
materials and their combinations. Technotherm 3000 1 component conductive black -- 10–15 min / 89 --
fusing SEM examinations 160–180 °C
Infiltration – preservation of structural details
In addition to the optimum infiltration and good cutting Technotherm 4000 1 component Target preparation, transparent -- 10–15 min / -- --
properties, the high tolerance to most polymer materials is fusing colourless 90–180 °C
particularly noteworthy.
Smooth plastic samples can be embedded directly,
while porous materials (sponges, textile samples, etc.)
are infiltrated for stabilization
Paper is impregnated with the very low-viscosity Technovit
Embedding forms and "cradle" use
7100 embedding solution within a very short time, so that
Polyethylene embedding form, 25 mm diameter, and All Technovit resins are resistant to the most
matching "cradle" insert (makes it possible to reduce the
additional infiltration is generally unnecessary.
cutting resistance and thus simplify cutting).
common etching agents used in metallography.
See table on page 37.
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EMBEDDING LIGHT-CURING EMBEDDING RESINS LIGHT-CURING EMBEDDING RESINS EMBEDDING
Technovit® 2000 LC – Liquid Technovit® 2000 – Inside Cure Technovit 2000 LC Fixing Paste Modulus of elasticity [MPa]
EN ISO 604: 2003
approx. 2000–3000
The light-curing Technovit 2000 LC Fixing Paste is used
The light curing Brings "light into the darkness”
for positioning the samples in the embedding form. It can be
Order no.: Technovit 2000 LC
Light-curing, 1-component embedding resin Special additive for shaded areas modelled like modelling clay and ground and polished after
The liquid enables highly transparent embeddings. The Technovit 2000 Inside Cure is a special additive that 64708496 Technovit 2000 LC Liquid 1000 ml
hardening. Due to its high hardness, the fixing paste is also
polymerization (Time: 2x 10 min) takes place in semi- enables the polymerization of Technovit 2000 LC in shadow 66053974 Technovit 2000 Inside Cure 40 ml
ideally suited as edge protection.
64712762 Technovit 2000 LC Cover Varnish 100 ml
transparent PE embedding forms in the Technotray POWER areas or on the inside of the sample (porous materials, inner
Perfect positioning aid also for all other embedding systems 66005103 Technovit 2000 LC Fixing Paste 4g
light polymerization unit at max. 90 °C. areas of pipe sections, etc.).
with the aid of the Technovit Blue LED.
By working in several layers or using a special irradiation Properties and application
Technovit 2000 LC Covering Varnish
programme, the polymerization temperature can be lowered much wider range of applications, as it is suitable for all
The Technovit 2000 LC Covering Varnish is used to prevent
even further (to approx. 50 °C). The material reaches its final sample types
a dispersion layer on the reverse side of the sample so
hardness after cooling to room temperature after which the for infiltration of porous samples
that a crystal-clear, hard and dry surface is created after
sample can be mechanically processed. same application as a standard product – no change to
polymerization has completed. It is applied to the sample in
Properties and application work processes, documentation, etc.
a layer a few millimetres thick after half the polymerization
flawless mixing
complete consumption – no mixing residues time. Sample markings can also be securely affixed in this
add the complete bottle of Inside Cure to the
variable pot time, as polymerization is only initiated by way.
using blue light bottle of Technovit 2000 LC Liquid, shake – ready; all
low polymerization temperature of approx. 90 °C
application parameters remain unchanged
approx. 50 °C also achievable with the irradiation
programme
alcohol and acid resistant
Temperature max. 60 °C
Lamp on off on off on off on off on off on off on off on
4 min 10 min 30 sec 10 min 30 sec 10 min 30 sec 10 min 30 sec 10 sec 20 min -- -- -- --
Temperature max. 50 °C
Lamp on off on off on off on off on off on off on off on
1 2 3 4 2 min 10 min 30 sec 10 min 30 sec 10 min 30 sec 10 min 30 sec 10 min 30 sec 10 min 2 min 10 min 20 min
1 – Put Technovit fixing paste onto the bottom of the embedding form. Irradiation program: 3 lamps below, 1 lamp above, 40 mm embedding form (full)
2 and 3 – Sample positioning
4 – Cure the fixing paste with the Technovit Blue LED; embed the sample as usual
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EMBEDDING LIGHT-CURING EMBEDDING RESINS LIGHT-CURING EMBEDDING RESINS EMBEDDING
Technovit 2000 LC or
Technovit 2021 LC FAST
Technotray POWER unit
incl. consumables and accessories
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EMBEDDING ACCESSORIES ACCESSORIES EMBEDDING
Technical specifications Technomat – perfect for fast-curing resins Spoon, spatula, mixing cup
The Technomat is a space-saving, compact pressure device. Aids for the removal and mixing of all powder-liquid systems.
Supply voltage 230 volt, 50 Hz The pressurization is 2.0 bar. Polymerization in the Techno- Embedding forms
Power max. approx. 60 Watt mat creates bubble-free and thus higher-quality samples. Polyethylene forms for embedding materialographic
Light 6 lamps each 9 watts
This device a must-have, especially for embedding with the samples. The smooth surfaces and high strength ensure
Lamp type Fluorescent tubes / LED strip
clear, fast-curing Technovit varieties 4004 and 4006. easy release and long service life. The standardised sizes
Timer with 3 time settings 5 min, 10 min
and continuous operation. Continu- of 15, 25, 30, 40 and 50 mm enable efficient further
ous operation switches off after 30 Technical specifications processing of the samples in automatic or manual grinding
min and polishing machines.
Pressurization 2.0 bar
automatically.
Safety valve 2.8–3.3 bar Cover LAM
Interior dimensions W x D x H: 170 x 160 x 120 mm
Pressure connection 3–10 bar Protective film for covering prepared samples. The Cover
Auto-start when pushing in the drawer
Dimensions L x W x H: 340 x 340 x 255 mm LAM protects against contamination and tarnishing.
Interior high-quality aluminium reflectors
Weight approx. 4 kg
Service life of the lamps ca. 1,000 hours of operation or Embedding aids
ca. 20,000 switching operations The polystyrene embedding aids provide a simple and cost-
Order no.: Technomat Pressure Pot
The Technotray Power provides a homogeneously Housing colour white/grey effective way to align and position the materials of a variety
Dimensions of housing L x W x H: 270 x 240 x 170 mm 66081898 Technomat Pressure Pot 1 pc.
illuminated sample chamber with space for up to of different forms precisely.
Weight approx. 3 kg Bar widths of 1, 2 and 3 mm allow for a wide range of
9 samples, auto-start and timer.
Order no.: Technotray POWER
Vacuum Set impregnation device application, e.g. for sheet metal cuttings, printed circuit
Handy device for embedding or superficial boards, securing irregularly shaped parts
66060914 Technotray POWER 230 V unit, 1 pc.
Technotray POWER – Light polymerization unit (especially for longitudinal cutting).
6 fluorescent tubes, power cable impregnation of porous samples
Equipped with high-quality aluminium reflectors and internal 66066474 Glass pane for Technotray POWER 1 pc.
dimensions of: W x D x H: 170 x 160 x 120 mm, the unit has 66015894 Lamp, 9 watts for Technotray POWER 1 pc.
a spacious and homogeneously illuminated polymerization 66096373 LED strip for Technotray POWER 1 pc. Order no.: Accessories, embedding
chamber that can accommodate up to 9 embedding forms
66021107 Dosing spoon for powder components 2 pcs.
(embedding form Ø 30 mm).
66021102 Mixing cup (rim-full volume = 200 ml) 10 pcs.
Light output 66021106 Wooden spatula 10 pcs.
The arrangement of the light sources guarantees reliable 66044445 Wooden spatula 100 pcs.
polymerization with light-curing Technovit resins. 66064604 Cover LAM protective film 100 pcs.
With a maximum of 6 blue light lamps or LED strips of 9 64713126 PE embedding form Ø 15 mm, H 23 mm 3 pcs.
watts each, the Technotray POWER is a powerful light po- 64708955 PE embedding form Ø 25 mm, H 23 mm 3 pcs.
lymerization unit that ensures fast, intensive and homogene- 64708956 PE embedding form Ø 30 mm, H 23 mm 3 pcs.
ous polymerization. 64708957 PE embedding form Ø 40 mm, H 23 mm 3 pcs.
polymerization temperature 64713127 PE embedding form Ø 50 mm, H 23 mm 3 pcs.
Ø 40 mm form fully poured without sample:
66095878 PE embedding form approx. 98 x 48 x 22 mm 1 pcs.
Order no.: Vacuum Set
66015844 Silicone embedding form 100 x 50 x 22 mm 1 pcs.
max. 120 °C 66076025 Vacuum Set Universal impregnator (100 mm pot) 1 pcs.
Ø 40 mm form cast in layers (2 mm):
64708952 Embedding aid narrow, 1 mm 1 pcs.
66080208 Vacuum Set Universal impregnator (140 mm pot) 1 pcs.
64708953 Embedding aid medium, 2 mm 1 pcs.
Irradiation 5 min: 70–90 °C
Six LED strips / fluorescent tubes ensure homogeneous illumination of 64708954 Embedding aid wide, 3 mm 1 pcs.
the sample compartment.
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EMBEDDING HOT EMBEDDING RESINS HOT EMBEDDING RESINS EMBEDDING
EMBEDDING
Curing takes place at: Curing takes place at: Curing takes place at:
Temperature 160–180 °C Temperature 160–180 °C Temperature 90–180 °C Special program for sensitive samples
Pressure 80–90 bar Pressure 80–90 bar Pressure 50–60 bar – transparent embedding at moderate
Time 10–15 min. Time 10–15 min. Time 10–15 min. temperatures:
Order no.: Technotherm 2000 Order no.: Technotherm 3000 Order no.: Technotherm 4000
kulzer-technik.de/TT4000_embed-
66003628 Technotherm 2000 1000 g 66003630 Technotherm 3000 1000 g 66009411 Technotherm 4000 1300 g
ding_parameters
66003629 Technotherm 2000 10000 g 66003631 Technotherm 3000 10000 g 66040390 Technotherm 4000 10000 g
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IMPRESSION
EMBEDDING
TAKING INDIRECT surface inspection IMPRESSION
EMBEDDING TAKING
Each impression like the original For dimensionally stable impressions Colour yellow or black
Designated use Impressions for
surface inspection
Components Powder / liquid
Mixing ratio 2:1
Analysis of Processing width [min] 2
scratch marks Curing time at 22 °C [min] 9–12
on a key
Precision impressions are used in the
Peak temperature during 110
most diverse areas and application curing in the block [°C] 30 g = 101
situations. Ball indentation hardness [N/mm²] 110 MPa
The designated purpose is to make Hardness (Shore D) [MPa] --
Temperature resistance [°C] 130
impressions, the reproduction of which Solubility swellable only
calls for a high degree of precision. Density = spec. weight [g/cm³] 1.18
Impact strength KJ/m²] 7.1
Flexural strength [N/mm²] 96
the 200x Application The flexibility in mixing the components ensures both the Compressive strength [N/mm²] 110
magnification
Surface impressions are important methods for pouring of a form and the impression in hard-to-reach Water absorption [% by vol] 0.43
documenting roughness, cracks or geometries with places, verticals as well as working overhead. Linear shrinkage [%] 1.9
high precision. To obtain a high-quality result, tools The 2-component resin consists of a powder and a liquid Volume shrinkage[%] 5.7
are necessary that can be used with high precision to component. Depending on the requirements, the material Refractive index M = 1.419
reproduce the surface to be evaluated. Monomer / polymer --
can be mixed in a ratio of 1:1 to 3:1 (powder/liquid).
Depending on the requirement or working method, the Storage temperature: [°C] 25
The standard mixing ratio of 2:1 can be poured for approx.
2-component resin Technovit 3040, Technovit Provil Shelf life [years] 3
2 minutes and then is malleable for approx. 30 seconds.
silicones, or light-curing resins of the Technovit 2200 Lin. TCE 110 x 10-6
The curing time is 9–12 minutes from the start of mixing.
series are used. Modulus of elasticity [MPa] 2000–2300
Properties and application EN ISO 604: 2003
a 200x
magnification of
Prepared for all problems Impression accuracy 1 μm
if the sample is too large or heavy for laboratory Order no.: Technovit 3040
the impression dimensionally stable and easily removable
with Technovit examination 64708806 Technovit 3040 powder yellow 1000 g
variable mixing ratio possible
Provil if the sample has to be examined non-destructively
Stabilization for mechanical processing 64708807 Technovit 3040 powder yellow 2 x 1000 g
if the point to be examined is difficult for measuring
Impressions can be evaluated with probes or non-contact 64708808 Technovit 3040 powder yellow 10000 g
instruments to access measuring methods 64708813 Technovit 3040 Powder black 1000 g
for documentation of wear
64708814 Technovit 3040 Powder black 2 x 1000 g
for measuring initial samples and prototypes From practice 64708815 Technovit 3040 Powder black 10000 g
to ensure dimensional accuracy, keep the impression
for the documentation of crack propagation 66022678 Technovit Universal Liquid 500 ml
surfaces as small as possible (for larger volumes, work in 66022679 Technovit Universal Liquid 5000 ml
Properties and application multiple layers)
Detection of Wear measurements
the modelling of a handle facilitates the removal of the
microcracks
ambulatory metallography
during ambula- impression from the original
tory micrography Impression taking for restorations and mineralogy
Impressions should have a minimum thickness of
Reconstruction in case of damage
5 mm in order to avoid slight distortion during removal.
Forensic investigations
Impressions of undercuts cannot be taken!
Optimization of process technologies
To take impressions on verticals or overhead, we
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IMPRESSION
EMBEDDING
TAKING IMPRESSION SILICONES IMPRESSION SILICONES IMPRESSION
EMBEDDING TAKING
Technovit® Provil® Putty Technical specifications Technovit® Provil® Light Technical specifications
The addition-curing silicones consist of a base and catalyst Technovit Provil Light is a free-flowing silicone and therefore
component and are malleable by hand in a ratio of 1:1. ideally suited for moulding difficult geometric shapes. The
The compound is applied to the relevant area to take an application system consisting of a dispensing gun, double
impression. After 4.5–5 minutes, the silicone is cured and cartridge and mixing cannulas ensures a constant mixing
can be removed or demoulded. The two products differ ratio and thus a reliable and faultless application.
mainly in consistency and final hardness (see technical
With the mixing gun, the silicone is pressed evenly from
specifications). A typical application is impression taking
both chambers of the double cartridge through the mixing
for measuring in form and tool making. No special prior
cannula. Hence, Technovit Provil Light is applied directly to
knowledge of the application is required.
the object in the form of a bead without bubbles. Additional
Properties and application mixing cannula attachments can be used to fill small cavities
when impressions of larger areas have to be taken (boreholes or similar).
in places that are difficult to access or also for working
Properties and application
overhead highest impression accuracy – therefore, for example,
for stabilizing impressions with the flexible Technovit
etched microstructures can be visualized (max. 500:1)
Provil Light
faultless work due to the easiest application
Perfect results with the combination of Technovit Technovit Provil Light creates exact 3D replicas of the
Exact 3D replicas
The advantages are used, for example, to measure and 2
document wear marks in hard-to-reach places and
geometries on tools and machine parts – without having to
Order no.: Technovit Provil Putty and Putty Soft purchase cost-intensive devices. Order no.: Technovit Provil Light
66004371 Technovit Provil Putty 450 ml base, 450 ml cat. 66009333 Technovit Provil Light 2 x 50 ml
66004372 Technovit Provil Putty Soft 450 ml base, 450 ml cat. 66009334 Mixing cannulas 48 pcs.
66009335 Mixing cannula attachments 96 pcs.
66009337 Mixing gun 1 pc.
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IMPRESSION
EMBEDDING
TAKING IMPRESSION SILICONES IMPRESSION SILICONES IMPRESSION
EMBEDDING TAKING
easy to remove
cost-efficient process
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IMPRESSION
EMBEDDING
TAKING LIGHT-CURING PRECISION IMPRESSION TAKING LIGHT-CURING PRECISION IMPRESSION TAKING IMPRESSION
EMBEDDING TAKING
1 – Apply Technovit 2210 on the clean surface. 1 – Grind, polish, etch, apply Technovit 2220, spread thinly on a film,
2 – Polymerize with Technovit Blue LED for 40 seconds. cover and polymerize.
The Technovit 2200 series represents a product line of 3 – Remove the hardened impression from the surface. 2 – Carefully remove cured Technovit 2220.
light-curing materials for quality assurance measures and Ready for tactile measurement. 3.– To secure the sample, apply Technovit 2200 to the slide, position
the impression, (CAUTION: Place the reverse side on the slide)
material tests that go beyond the classic procedures. press this "sandwich" as plane-parallel as possible with a second slide
and cure with blue light.
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IMPRESSION
EMBEDDING
TAKING LIGHT-CURING PRECISION IMPRESSION TAKING RESISTANCES TECHNOVIT
EMBEDDINGSYSTEMS
Why are material samples embedded? When is embedding under pressure useful? Heat of reaction – influence temperature Why hot embedding
The polymerization of cold embedding resins under pressure behaviour Hot embedding is an alternative to cold embedding. Here,
The main reason is the easier handling for the later sample
preparation – the samples are brought into a standardised is always advantageous if the sample is to be bubble-free. It Cold embedding resins cure by starting the polymerization. with the aid of an embedding press, the 1-component
size to be able to process them automatically later. is a must-have for transparent resin samples, otherwise the This begins as soon as the various components are mixed embedding resins are melted under pressure and heat and
embedding appears milky and no target preparation is together. This results in an exothermic reaction that releases thus formed into a homogeneous test sample.
But embedding also provides better handling for manual
possible. MMA/PMMA-based embedding systems are heat. The benefits
processing for a hardness test.
particularly suitable for use with the Technomat. Mixing ratios can be changed slightly as required thus 1-component resin – no mixing errors
Another aspect is the stabilization of the material samples by
When does embedding under vacuum changing temperature and time curves. preset programs of the press for routine samples
additional infiltration with the embedding resin. flat sample surface
make sense? The higher the volume of the powder/liquid mixture, the
What is the optimal embedding? When embedding porous samples, samples with blind holes higher the temperature generated by the polymerization
good edge definition
This depends on the objective of the embedding or sample or undercuts, it is highly recommended to infiltrate the process. What general conditions have to be met?
preparation. A simple flat sample is often sufficient for a embedding resin into the sample with vacuum support. Higher temperatures, both ambient and that of the product, The material sample must be resistant to pressure and heat.
simple hardness measurement. It is important that the However, only cold embedding resins with a sufficiently long accelerate, lower temperatures slow down the curing. For The selection of the embedding resin should be based on
workpiece to be tested is optimally held in the embedding pot time (at least 4 min.) are suitable for this purpose. This embedding larger samples or casting larger areas, it is the objective of the sample preparation. For recurring
resin and that measurements at different points do not lead starts with the light-curing embedding resins and polyether/ necessary to work in several layers. This is the only way to samples, it is useful to work your way up to the correct
to loosening of the workpiece. MMA-based filled embedding resins up to the epoxy resins. prevent excessive heating and keep shrinkage low. temperature/pressure/time program.
For examinations in the edge region, it is particularly The correct handling of cold It is necessary to let the previous layer cool down completely
important to generate gap-free embeddings. Well-adhering Sample size and position
embedding resins between the working steps. (heat acts as a catalyst, too fast
embedding resin supports and protects sensitive coatings curing leads to bubble formation) As with cold mounting resins, the sample size in relation to
from damage as well as edge rounding, which would, for Always mix multicomponent resins homogeneously; correct the cylinder must also be taken into account when hot
mixing is the basis for optimum embedding. Avoid beating Use small embedding forms if possible to keep the polymeri-
example, make coating thickness measurements more embedding; here, a sufficient distance to the edge of
when mixing, as this will trap air in the dough-like resin that zation temperature low.
difficult. approx. 3–5 mm is recommended (especially for geometri-
may not be able to escape and thus lead to the formation of cally complicated sample forms) and sufficient embedding
Ideally, the grinding behaviour of the embedding resin is bubbles. Basic information on samples and
resin over the sample.
adapted to that of the sample so that it is much easier to embedding
achieve and evaluate plane grinding surfaces. Hard and To avoid air inclusions in the lower part of the sample, it is
helpful to first cast a "mirror" and only then orientate the Samples must always be clean and free of grease; contami- Can the sample be positioned before
high-strength samples are therefore best cast with mineral- the embedding process?
sample in the embedding form. This is particularly useful nation of the samples can lead to interference during
filled embedding resins.
when embedding, for example, spot welds of sheet metal or embedding. Technovit 2210 can also be used here to keep the samples
Why cold embedding? similar. If several workpieces are to be cast in an embedding form, in the desired position during hot embedding. The sample is
Cold embedding is a simple and cost-effective method to arrange the samples so that the distances between the secured on the stamp of the press and the paste is cured for
Always completely pour embedding resin onto the sample to
produce materialographic samples. The expenditure on individual parts and the edge of the embedding form are as 60 seconds with the Technovit Blue LED.
ensure that the sample is securely fixed during preparation.
technical aids is rather small. Many embedding systems equal as possible. Spacing between individual workpieces Hot embedding of temperature-sensitive
offer a variable mixing ratio, which makes the process easy. that is too narrow can prevent the penetration of embedding samples
Especially if the samples are not "simple" there are advan- resins and thus produce air pockets.
tages of temperature behaviour, pressure and infiltration Hot embedding is often ruled out for material samples that
Always align samples centrally in the embedding form so are pressure-resistant but temperature-sensitive. We have
possibilities. Fast embedding is possible for large sample
that the sample is surrounded by sufficient embedding resin worked out a special temperature program for Technotherm
volumes or in-process controls.
(edge distance approx. 3-5 mm). 4000 – see:
The benefits kulzer-technik.de/TT4000_Einbettparameter
After demoulding, allow the sample to cool at room tempera-
inexpensive systems without investment
ture. No "quenching" in cold water or a refrigerator compart-
variable in time, temperature and mixing behaviour Avoidance of adhesion of the hot
ment. Different expansion coefficients of resin and work-
fast processes embedding resin
piece can thus lead to increased gap formation or cracks.
flexible in the choice of sample dimensions
In this case, it is recommended to brush the stamp and the
wide range of resins for all materialographic issues
press cylinder of the press with Solilub. This serves as a
release agent and prevents the hot embedding resin from
sticking in the press.
38 kulzer-technik.com 39
EMBEDDING
CUTTING Machines and MATERIAL CUTTING
CUTLAM 3.1
40 kulzer-technik.com 41
CUTTING CUT-OFF WHEELS CUT-OFF WHEELS CUTTING
Developed for very high requirements, these cut-off wheels The new Excellence cut-off wheels enable faster cuts without
provide the user with precise cutting, also thanks to the heating. They can be used at higher turning speeds and
properties of the binder and the quality of the abrasives. make excellent quality cuts without damaging the structure
The cut-off wheels can be used in all commercially available of the material. The manufacturing quality guarantees
cutting machines of all manufacturers and produce very limited wear and freedom from vibration during cutting. With
fine, precise separating cuts that reduce all subsequent the three available models, Excellence H1, H2 and H4, any
processing steps to a minimum. type of metallic material can be cut. To help you choose the
Precision cut-off wheels Excellence high performance cut- Adapter rings
right wheel, the table below gives recommendations for use
Available in 4 variants depending off wheels For cut-off wheels for fitting
depending on the material to be cut – the optimum cut-off on their hardness and used Available in 3 variants the inner diameter on different drive
wheels for in-process quality control. abrasives shafts
The universal cut-off wheels, which can be used on all White (SiC) White H4 Adapter ring PVC*
commercially available cut-off machines, reduce the time
66064594 125 x 12.7 x 0.45 mm 66076099 250 x 32 x 1.5 mm 66070154 22.1–12.7 mm
required for the subsequent cutting process due to their very
66064595 150 x 12.7 x 0.45 mm 66076100 300 x 32 x 2.0 mm 66064596 25.4–12.7 mm
good cutting properties. Due to the efficient cutting and the Quantity per delivery unit: 5 pieces 66076101 350 x 32 x 2.5 mm 66064597 25.4–22.1 mm
low wear, these cut-off wheels are very cost-effective. 66076102 400 x 32 x 3.0 mm 66064598 32.0–25.4 mm
66058082 203 x 25.4 x 1.0 mm
Quantity per delivery unit: 10 pieces Quantity per delivery unit: 5 pieces
66058083 230 x 22 x 1.2 mm
66058084 250 x 32 x 1.5 mm Green H1 Adapter-Ring Metal**
66058085 305 x 32 x 1.5 mm
66076091 250 x 32 x 1.5 mm 66070155 22.1–12.7 mm
Quantity per delivery unit: 10 pieces
66076092 300 x 32 x 2.0 mm 66064599 25.4–12.7 mm
Precision cut-off
wheel 'black', 66076093 350 x 32 x 2.5 mm 66064600 25.4–22.1 mm
Red (AI203)
diamond 66076094 400 x 32 x 3.0 mm 66064601 32.0–25.4 mm
66058070 125 x 12.7 x 0.45 mm
not recommended Quantity per delivery unit: 10 pieces Quantity per delivery unit: 10 pieces
66058071 150 x 12.7 x 0.45 mm
possible
Quantity per delivery unit: 5 pieces Yellow H2 *For all wheels with a metal-
The right precision cut-off wheel Application area
reinforced inner hole
66058072 203 x 25.4 x 1.0 mm 66076095 250 x 32 x 1.5 mm ** For all wheels without
66058073 230 x 22 x 1.2 mm 66076096 300 x 32 x 2.0 mm metal reinforcement in the inner
White (SiC) 66076097 350 x 32 x 2.5 mm hole
soft and tough 66058074 250 x 32 x 1.5 mm
Non-ferrous metals 66058075 305 x 32 x 1.5 mm 66076098 400 x 32 x 3.0 mm
soft and medium-hard fer- Red (AI203) Quantity per delivery unit: 10 pieces
Quantity per delivery unit: 10 pieces
rous metals
Blue (AI203) Blue (AI203)
hard and very hard ferrous
metals 66058076 125 x 12.7 x 0.45 mm
Black (diamond) 66058077 150 x 12.7 x 0.45 mm
very hard ferrous metals
hard metals, ceramics Quantity per delivery unit: 5 pieces
42 kulzer-technik.com 43
GRINDING / POLISHING MATERIALOGRAPHY GRINDING / POLISHING
A decisive factor to be able to make state- The use of new materials has undergone rapid development
in recent years. Ever-thinner coatings and extreme differenc-
ments in materialography is the precise
es in hardness within a sample require particularly individual
surface preparation. preparation methods.
Only through optimal sample preparation Kulzer offers you a mature, clearly structured product range
for materialography with solutions for all sample preparations
can the actual microstructural state of a
in high quality.
material be reliably determined.
The result is: minimization of preparation steps and low
material consumption – an economical system for first-class
grinding qualities.
You will find Kulzer Technik to be a reliable partner when
it comes to materialography. We offer you free, individual
advice on-site and work with you to develop preparation
methods for new tasks. Convince yourself of the quality of
our products in your laboratory.
Profit from efficient working techniques through
perfectly coordinated products.
P500 30.2 (± 1.5) -- 30 µm -- long service life, thus optimum cost-benefit factor
44 kulzer-technik.com 45
GRINDING SIC PAPERS DIAMOND GRINDING DISKS GRINDING
The extremely stable SiC abrasive paper ensures very SiC wet abrasive paper SiC wet abrasive paper Technodisc Diamond The nickel-bonded Technodisc Diamond Grinding Disks
good, even material removal – the reliable classic in non self-adhesive self-adhesive Grinding Disk, self-adhesive have a very good grip and are characterised by a high
Quantity per delivery unit: Quantity per delivery unit: Quantity per delivery unit: 1 pieces
materialography, especially for softer materials. material removal rate. They are available in grain sizes
100 sheets 100 sheets
Technodisc 250 μm, 125 μm, 75 μm, 40 μm and 20 μm.
Technodisc SiC paper P80 Technodisc SiC paper P80 Diamond Grinding Disk 10 μm The Technodisc system is complemented by the two,
66061031 Ø 200 mm 66061021 Ø 200 mm 64708640 Ø 200 mm very fine Technodisc 30 and 10 μm with a synthetic resin
66061032 Ø 230 mm 66061021 Ø 230 mm 64708660 Ø 250 mm bond. The excellent efficiency is the result of a long tool life
P80
(detailed 66061033 Ø 250 mm 66061023 Ø 250 mm 64708670 Ø 300 mm as well as the good and fast material removal rate of the
picture) 66061034 Ø 300 mm 66061024 Ø 300 mm Technodisc.
Technodisc
Technodisc SiC paper P120 Technodisc SiC paper P120 Diamond Grinding Disk N 20 μm Technodisc Diamond Grinding Disks can also be combined
66058025 Ø 200 mm 66058046 Ø 200 mm 64708639 Ø 200 mm with other grinding systems without any problems.
66061038 Ø 230 mm 66061035 Ø 230 mm 64708659 Ø 250 mm
For example, the Technodisc 125 μm as a pre-grinding step
66058032 Ø 250 mm 66058053 Ø 250 mm 64708669 Ø 300 mm
for carbide is a good preparer for the subsequent CAMEO
66058039 Ø 300 mm 66058060 Ø 300 mm
Technodisc DISK SILVER with BioDiamant Liquid green. However, it
Technodisc SiC paper P240 Technodisc SiC paper P240 Diamond Grinding Disk 30 μm can just as well be used for cold-embedded, medium-hard
P320
66058026 Ø 200 mm 66058047 Ø 200 mm 64708638 Ø 200 mm steels with poor cut-off as preparation for the subsequent
(detailed
picture) 66061040 Ø 230 mm 66061039 Ø 230 mm 64708658 Ø 250 mm CAMEO DISK PLATINIUM. The nickel bond enables good
66058033 Ø 250 mm 66058054 Ø 250 mm 64708668 Ø 300 mm pre-grinding – both for embedding resin as well as steel.
66058040 Ø 300 mm 66058061 Ø 300 mm Water or the "Booster Liquid" is used as the lubricant.
Technodisc
Technodisc SiC paper P320 Technodisc SiC paper P320 Diamond Grinding Disk 40 μm Alternative lubricants can also be used for water-sensitive
66058027 Ø 200 mm 66058048 Ø 200 mm 64708637 Ø 200 mm samples.
66061042 Ø 230 mm 66061041 Ø 230 mm 64708657 Ø 250 mm
66058034 Ø 250 mm 66058055 Ø 250 mm 64708667 Ø 300 mm
66058041 Ø 300 mm 66058062 Ø 300 mm Comparison of grain size for SiC papers / diamond
P1200 Technodisc
(detailed grinding disks
Technodisc SiC paper P400 Technodisc SiC paper P400 Diamond Grinding Disk 75 μm
picture)
66058028 Ø 200 mm 66058049 Ø 200 mm 64708635 Ø 200 mm
Magnification
66061044 Ø 230 mm 66061043 Ø 230 mm 64708655 Ø 250 mm
Technodisc 250 µm
66058035 Ø 250 mm 66058056 Ø 250 mm 64708665 Ø 300 mm
66058042 Ø 300 mm 66058063 Ø 300 mm
Technodisc
Technodisc SiC paper P600 Technodisc SiC paper P600 Diamond Grinding Disk 125 μm
66058029 Ø 200 mm 66058050 Ø 200 mm 64708633 Ø 200 mm
P4000 66061046 Ø 230 mm 66061045 Ø 230 mm 64708653 Ø 250 mm
(detailed 66058036 Ø 250 mm 66058057 Ø 250 mm 64708663 Ø 300 mm
picture) 66058043 Ø 300 mm 66058064 Ø 300 mm
Technodisc
Technodisc SiC paper P1200 Technodisc SiC paper P1200 Diamond Grinding Disk 250 μm
66058030 Ø 200 mm 66058051 Ø 200 mm 64708632 Ø 200 mm
See also Booster Liquid – Increased per-
66061048 Ø 230 mm 66061047 Ø 230 mm 64708652 Ø 250 mm formance and durability due to the correct
66058037 Ø 250 mm 66058058 Ø 250 mm 64708662 Ø 300 mm lubricant (page 47).
66058044 Ø 300 mm 66058065 Ø 300 mm
Technodisc SiC-Papier P2500 Technodisc SiC-Papier P2500 Matching metal blanks to Cut-out surfaces, Technodisc
66058031 Ø 200 mm 66058052 Ø 200 mm stick-on the disks Diamond Grinding Disks
66061050 Ø 230 mm 66061049 Ø 230 mm Quantity per delivery unit: 1 piece
66058038 Ø 250 mm 66058059 Ø 250 mm
Metal blanks
66058045 Ø 300 mm 66058066 Ø 300 mm
Specifications 66078656 Ø 200 mm
Technodisc SiC paper P4000 Technodisc SiC paper P4000 66078659 Ø 250 mm
Carrier Latex/paper, tear-resistant, waterproof, flexible
Abrasives Silicon carbide 66067822 Ø 200 mm 66069201 Ø 200 mm 66078660 Ø 300 mm
Binding Synthetic resin 66067823 Ø 230 mm 66070156 Ø 230 mm
66067824 Ø 250 mm 66069202 Ø 250 mm Magnification
Dispersion Closed Technodisc 125 µm
66067825 Ø 300 mm 66069203 Ø 300 mm
Design self-adhesive or non-adhesive
46 kulzer-technik.com 47
GRINDING CAMEO DISK PLATINIUM CAMEO DISK PLATINIUM GRINDING
The PLATINIUM Diamond Grinding Disks are an alternative Automatic preparation Cleaning
to SiC paper for grinding medium-hard to hard materials To achieve flatness of the samples and uniform wear of the The CAMEO DISK PLATINIUM is regularly honed with the
such as steel, hard metal, ceramics and various material disk, the sample holder is placed in such a way that the enclosed whetstone under running water at 150 rpm directly
composites. samples reach to the centre and protrude a few millimetres in the machine and thus reconditioned.
beyond the working disk at the outer diameter. When using
TYPE 0 larger working disks, change the sample holder position CAMEO DISK PLATINIUM
corresponds to Quantity per delivery unit: 1 piece
from time to time in order to maintain the flatness of the disk
CAMEO DISK PLATINIUM Material Removal Rate grain size 60–80
Adaptation: Metal backing for magnet systems
and to make optimum use of the abrasive.
Material removal [gr]
0,6
PLATINIUM TYPE 0 PLATINIUM TYPE 3
Manual preparation
0,5 Re-conditioning
The CAMEO DISK PLATINIUM is also excellently suited 66050031 Ø 200 mm 66012985 Ø 200 mm
with whetstone
0,4
for manual sample preparation. Here, the samples are 66050032 Ø 250 mm 66012988 Ø 250 mm
0,3 moved from the edge to the centre and back again during 66050033 Ø 300 mm 66012991 Ø 300 mm
TYPE 1
0,2
corresponds to the preparation process in order to achieve uniform loading PLATINIUM TYPE 1 PLATINIUM TYPE 4
0,1 grain size120–180 on the disk. Despite the different surface, they feel when 66012983 Ø 200 mm 66018162 Ø 200 mm
0 sanded like a well ground SiC paper – permanently. 66012986 Ø 250 mm 66018164 Ø 250 mm
1’ 5’ 10’ 15’ 25’ 30’
10 (For higher material removal rates, work with the Booster 66012989 Ø 300 mm 66018165 Ø 300 mm
Processing time [min]
n] Liquid. The lubricant is specially adapted to the Platinium and
CAMEO PLATINIUM 1 SiC-Paper DISK other manufacturer keeps the gaps clean and guarantees uniformly high material PLATINIUM TYPE 2
P 320
removal.) 66012984 Ø 200 mm
TYPE 2
corresponds to 66012987 Ø 250 mm
grain size 220–320 Contact surface
66012990 Ø 300 mm
The homogeneous diamond distribution of the CAMEO
The secret of the material removal rate – the DISK PLATINIUM ensures constant material removal rates
patented CAMEO DISK cell structure. throughout the life of the disk. The special honeycomb
structure guarantees optimum lubrication of the samples
during the grinding process. The individual cells hold the
The CAMEO DISK PLATINIUM diamond grinding disks TYPE 3
corresponds to
lubricant, or water, on the surface and thus counteract the Booster Liquid
can be used in all common automatic and semi-automatic grain size 600 centrifugal force of the grinding disk. The excellent cutting
grinding and polishing machines. However, due to the The Booster Liquid is
action of the CAMEO honeycomb structure enables a high
narrow grid of the diamond-tipped bars, the CAMEO a specially developed
material removal rate at low pressure. This protects the
DISK PLATINIUM is also excellently suited for manual lubricant for use on the
sample, disk and machine.
preparation. CAMEO DISK PLATINIUM
during grinding. This
CAMEO DISK PLATINIUM is very easy to use. Water or the TYPE 4 Booster Liquid maintains
"Booster Liquid" is used as a lubricant. Alternative lubricants corresponds to
grain size 1200 the optimum grip of the
can also be used for water-sensitive samples. diamond grinding disks over the entire service life and at the
The edge definition is significantly better than with same time buffers sensitive samples.
Rotation Specimen
preparation using SiC paper, which is related to both the Ready to use, this lubricant ensures constant conductivity
DISK
abrasive itself (diamond) and the flat, stable carrier. and avoids the use of a grindstone.
Even non-embedded samples and large welds can be Application advantages of Booster Liquid
processed without problems after a good cut. After 2 to a CAMEO DISK PLATINIUM at a glance improved performance of the diamond grinding disks
maximum of 3 grinding steps, the samples are optimally excellent edge definition – even with non-embedded keeps efficiency constant over time
prepared for the subsequent polishing. samples reduces the consumption of water
Suspension Contact Area
In addition to the long service life, the excellent grinding easy handling, easy to clean universally applicable, can be used for all types of material
quality is the big plus. This means that preparation with reproducible results Ready for use
CAMEO DISK PLATINIUM provides excellent value for for manual and automatic grinding
48 kulzer-technik.com 49
GRINDING CAMEO DISK SILVER & GOLD CAMEO DISK SILVER & GOLD GRINDING
The CAMEO DISK SILVER and CAMEO DISK GOLD lap- CAMEO DISK SILVER Automatic preparation
ping disks with a gentle, constant material removal rate. The To achieve precise flatness of the samples and uniform wear
Fine grinding of medium-hard to very hard materials (> 200
BioDiamant Liquids serve as abrasives. The CAMEO Disk of the CAMEO DISK, the sample holder is placed in such a
HV) in combination with diamond liquids from 12–6 μm.
replaces work steps for which abrasive papers with grain way that the samples reach to the centre and protrude a few
sizes 240–4000 are used as an alternative for medium-hard millimetres beyond the working disk at the outer diameter.
CAMEO DISK GOLD
to hard materials. When using larger working disks, it is advisable to change
Fine grinding of hard, brittle materials, for example ceramics, the sample holder position from time to time to maintain the
material composites, soft materials and non-ferrous materi- flatness of the disk and to make optimum use of the
CAMEO DISK Comparison to SiC Paper als, in combination with diamond
CAMEO DISK PLATINIUMliquids fromRemoval
Material 12-3 μm.
Rate abrasive.
0,5 0,5 Re-conditioning CAMEO DISK SILVER & GOLD are excellent for manual
with whetstone
0,4 CAMEO 0,4 DISK Advantages sample preparation. To achieve uniform loading of the disks,
easy handling
0,3 the samples are guided from the edge to the centre during
0,3
very good material removal rate
0,2
the preparation process.
0,2
grinding step jumps, for example, from the 120 grind-
0,1 Cleaning
0,1 ing stone on the CAMEO DISK SILVER with Suspension
0 The CAMEO DISK SILVER & GOLD are easily cleaned with
0 green are1’possible.5’ 10’ 15’ 25’ 30’
a soft brush under running water after use and can then be
1 2 3 4 5 6 7 8 9 10
economical – with a single disk, CAMEO Processing time [min]
time [min] replaces the used further with any diamond grain size.
whole range of PLATINIUM
CAMEO SiC papers1 from grainDISK
SiC-Paper sizeother
240–4000 –
manufacturer
CAMEO DISK silver P 1200 P 600 P 400 P 320
with ideal edge definition
the patented surface profile creates a highly constant
CAMEO DISK SILVER & GOLD are lapping disks with suspension on the disk, the CAMEO DISK is optimally
a highly constant material removal rate and excel- lubricated, and the cutting edges of the diamond grains EMBEDDING RESIN
lent edge definition. are utilised in the best possible way. They significantly
reduce the need for diamond suspension compared to
lapping systems from other suppliers. SPECIMEN
compatible with all grinding and polishing systems!
The patented, close-meshed honeycomb pattern of the
time-saving preparation with optimal surface flatness of all
CAMEO DISK optimizes the operation of the sprayed Diamond
BioDiamant Liquids. The diamond suspension remains samples Liquid
efficient: Different grain sizes of diamond suspensions 1 2
on the disk and is thus optimally utilized. The CAMEO
process guarantees optimum flatness and gentle material can be used on just one CAMEO lapping disk.. The disk
removal for all types of samples with minimum material adapts to the requirements. CAMEO DISK SILVER & GOLD
50 kulzer-technik.com 51
POLISHING POLISHING CLOTHS POLISHING CLOTHS POLISHING
Various cloths are available in the TOUCH- A polishing cloth is a complex combination of different TOUCHLAM 2TT1 TOUCHLAM 2TS8
material layers, each of which has a specific function. The Hard cloth made of woven synthetic taffeta fibres for good With its flat surface and soft natural fibre thread, the orange
LAM system. These differ in material and overall structure determines the cloth quality and is essential material removal rates and flatness. The field of application polishing cloth 2TS8 provides a precise fine polish with very
type of fabric, flocking or fibre, density and for the polishing result and durability. The cloth is selected is mainly pre-polishing. Works out deformations quickly and good edge definition when using BioDiamant Liquids 1–6
thickness. The cloths are finely graduated according to the type of samples and/or polishing step. easily – especially with tough materials such as titanium. For µm. For multi-stage polishing with the 1 μm suspension, it
so that the polishing steps can be individu- In combination with the right polishing agents, even difficult combination with BioDiamant Liquids 6–12 µm. is the perfect complement to the 2TS1 Polishing Cloth with
sample surfaces can be polished artefact-free in a very short BioDiamantLiquids, 6 µm or 3 µm..
ally matched to the preparation. TOUCHLAM 2TS1
time. Too many polishing steps and long polishing times,
especially on soft cloths, significantly reduce the flatness of Satin-woven, waterproof, natural fibre cloth for a high TOUCHLAM 3TL1
a sample. material removal rate and excellent edge definition. For Robust all-round wool cloth for soft to hard routine samples.
polishing almost all materials especially for thin layers Particularly suitable for polishing soft to hard non-embedded
The active surface of the polishing cloth is the first selection of different hardness in combination with BioDiamant samples. For combination with BioDiamant Liquids 1–6
Too many polishing steps and long polishing times criterion; the other parameters result from the layer Liquids 1–6 µm. µm.
significantly reduce the flatness of a sample. Therefore, structure. The insulating layer prevents the cloth from being
it is particularly important to carefully match the cloths soaked so that the surface does not separate from the TOUCHLAM 2TS4 TOUCHLAM 3FV1
adhesive. This is the basis for a long service life. Satin woven natural fibre cloth for high flatness and edge Flocked, medium-hard synthetic fibre cloth. For the
used to the polishing steps.
The adhesive layer guarantees optimum adhesion within definition on samples with different hardness or coated final polishing of hard embedded samples as a universal
the composite. It influences the hardness and the polishing materials. For combination with BioDiamant Liquids 1–6 polishing wheel with 3 µm in the hardening shop as well as
behaviour of the cloth by its consistency. µm. for the fine polishing of medium-hard to hard samples. For
combination with BioDiamant Liquids 1–6 µm.
An important aspect is also the carrier. It is the foundation TOUCHLAM 2TS5
and thus responsible for the stiffness, flatness and elasticity Flexible, medium-hard natural fibre cloth consisting of a TOUCHLAM 4FV1
2TS1 of the polishing cloth. salmon-coloured satin fabric. The combination of soft thread Flocked, medium-hard synthetic fibre cloth. For final
Designs and flat surface provides fine polishing results with good polishing of hard embedded samples. Can also be used very
Depending on the design, all cloths can be easily placed on edge definition. Suitable for the preparation of almost the well as a universal polishing cloth for undemanding samples.
various changing systems and also removed again – wrinkle- entire range of materials in combination with BioDiamant For combination with BioDiamant Liquids 1–3 µm. Can
2TS4 free, without leaving any residue and without taking a lot of Liquids 1–6 µm. be used just as well as with oxide polish (Al²O³) or SiO² for
time. finishing.
with self-adhesive back TOUCHLAM 4MP1
with flexible metallic carrier for direct adaptation to The chemically resistant cloth made of microporous PU
3FV1 magnet systems foam can be used with all oxide polishing agents and shows
with flat, smooth, stable plastic back for adaptation to the
no edge rounding even with longer polishing times of difficult
XLAM adhesive system preparations. Etching polishes are also possible.
4FV1
52 kulzer-technik.com 53
POLISHING POLISHING CLOTHS POLISHING AGENT POLISHING
TOUCHLAM 2TT1 The BioDiamantLiquids are diamond All input materials of the BioDiamant
SA MG XLAM
abrasives that meet our high quality products comply with European standards
Ø 200 mm 66055540 66055543 66055549
Ø 250 mm 66055541 66055545 66055550
requirements, both in the high quality of 1999/45/EC and 2000/59/EC. In this way,
Ø 300 mm 66055542 66055546 66055551 the diamond grain, the grain size we have achieved our goal of offering users
TOUCHLAM 2TS1 distribution, but also regarding health and high-performance products that do not pose
SA MG XLAM environmental compatibility. any environmental or health risks.
Ø 200 mm 66055554 66055561 66055566
Ø 250 mm 66055556 66055562 66055567
Ø 300 mm 66055557 66055563 66055568
TOUCHLAM 3FV1
Metallographic grinding and polishing machines
SA MG XLAM
Ø 200 mm 66055602 66055605 66055608
Ø 250 mm 66055603 66055606 66055609
Ø 300 mm 66055604 66055607 66055610
TOUCHLAM 4FV1
SA MG XLAM
Ø 200 mm 66055612 66055616 66055620
Quantity per delivery unit: Ø 250 mm 66055613 66055617 66055621
5 pcs. special varieties and Ø 300 mm 66055614 66055618 66055622
diameter on request! SMARTLAM 2.0 MASTERLAM 3.0
TOUCHLAM 4MP1
SA = self-adhesive
MG = magnetic SA MG XLAM
XLAM = adapter system Ø 200 mm 66055623 66055626 66055629 Kulzer offers a wide range of machines for the use of our and polishing machine MASTERLAM with central and
Ø 250 mm 66055624 66055627 66055630 grinding disks and polishing cloths. From the manual or individual sample pressure, all requirements for modern
Ø 300 mm 66055625 66055628 66055631 semi-automatic SMARTLAM to the automatic grinding sample preparation are covered here.
54 kulzer-technik.com 55
POLISHING POLISHING AGENT POLISHING AGENT POLISHING
100
Percentage [%]
BIODIAMANT yellow
80 Competitors
(6 µm)
product (6 µm)
60
Competitors
40 product (6 µm)
20
0
0 2 4 6 8 10 12
Diamond grain-size [µm]
Kulzer "All-in-One" diamond suspensions are used without We remain true to the claim of perfect sample preparation. Final Liquid
BIODIAMANT stands for uniform grain distribution any additional lubricant, which results in a consistent, But NEODia Liquids can do more: Optimum polishing Final polishing solution made of colloidal silicon dioxide.
reproducible quality at all times and a significant savings results due to good material removal behaviour are Abrasive: Silica (SiO2) pH 9 with a grain size of 50 nm.
100
High efficiency with flocked polishing cloths (TouchLam
Percentage [%]
80
(6 µm) Competitors system, the
20 special types MM 140 as an unpigmented (Volatile Organic Compounds) refers to the group of volatile The extremely fine open particles guarantee an excellent
100
product (6 µm) polish. Easy to use and very well suited for the final polish
[%]
4 Liquids
6 can be8 optimally
10 applied
80 Competitors
(6 µm) Competitors 2 12 NEODia benefits
product (6 µm) sizes (Superfinish 1 = 0.25 μm and Superfinish 2 =
Uniform
40 grain distribution & optimum
productdosage
(6 µm) with automatic dosing equipment as wellDiamond as withgrain-size
the manual[µm] VOC-free, non-toxic, harmless to health
60
uniform material removalEmbedding resin
Competitors pump bottle. narrow tolerances of the grain sizes
0.05 μm).
20
40
short product (6 µm) times
preparation polycrystalline diamonds provide the best cutting edges
BioDiamant Benefits
0lower deformation depth Specimen Delivery units NEODia Liquids
more efficient than conventional diamond suspensions homogeneous micrograph due to high concentration of
20 0 2 4 6 8 10 12
uniform deformation
Diamond grain-size [µm] harmless to health poly-crystalline diamonds and finely graded grain sizes 66077903 BioDiamant NEODia F POLY, blue 1 µm 400 ml
0contact to the working disk
narrow tolerances of the grain sizes biodegradable liquid, compostable bottle 66077904 BioDiamant NEODia F POLY, green 3 μm 400 ml
0 2 4
adequate lubrication/cooling
6 8 10 12 Embedding resin
high diamond concentrations excellent cost-effectiveness 66077905 BioDiamant NEODia F POLY, yellow 6 μm 400 ml
Diamond grain-size [µm]
optimum lubricating effect of the water-based suitable for the NEODIA suspensions:
carrier fluid
Specimen 66077906 BioDiamant NEODia F POLY, red 9 µm 400 ml
economical in use 66079385 BioDiamant NEODia F POLY, grey 14 µm 400 ml
Lubricant Fluid MM 702 and MM 704
optimal
BIODIAMANT steht fürfor processingKornverteilung
gleichmäßige in automatic machines or manually 66077907 BioDiamant NEODia F POLY, blue 1 µm 2500 ml
Avoid application errors Embedding resin
Water-based lubricants for combination with the NEODia
All-in-One
suspensions.. The formula provides the best lubrication 66077908 BioDiamant NEODia F POLY, green 3 μm 2500 ml
Korngrößenverteilung von Diamantstaub
Specimen and cooling during preparation. The sample can be easily 66077909 BioDiamant NEODia F POLY, yellow 6 μm 2500 ml
Poor dosage Embedding resin
Aquaplaning effect
Adapter systems
The efficient way
1 1 1 1 1 1 1
2 2 2 2 2 2 2
3 3 3 3 3 3 3
1. SiC paper without adhesive 1. SiC paper without adhesive 1. SiC paper self-adhesive, 1. SiC paper self-adhesive, 1. SiC paper self-adhesive, 1. SiC paper self-adhesive, 1. Grinding or polishing disk
backing backing Grinding or polishing disk Grinding or polishing disk Grinding or polishing disk Grinding or polishing disk metal-backed
2. FIXLAM 2. FIXLAM-M adhesive-backed adhesive-backed with smooth back with smooth back 2. MS-Disk
3. FAS / FAS-M Disk 3. MS-Disk 2. FAS Disk 2. FAS-M Disk 2. XLAM 2. XLAM-M 3. support disk
or carrier disk or magnetic 3. support disk 3. MS disk or magnetic 3. FAS / FAS-M Disk 3. MS disk or magnetic (non-magnetic)
(non-magnetic) support disk (non-magnetic) support disk or carrier disk support disk
(non-magnetic)
58 kulzer-technik.com 59
GRINDING/POLISHING ACCESSORIES SAMPLE PREPARATION
Manual sample holder Ceramic ring (manual Manual sample holder With the grinding and polishing products from Kulzer,
sample An important tool for target preparation. The risk of over- surfaces are removed very gently without deformation or
holder view from below) artefacts.
grinding and the microscopic control effort are extremely
minimized. The manual sample holder is designed for An optimally prepared sample reproduces the true
polished sections as well as thin sections (holder or insert microstructure unaltered. Inhomogeneous structures are
H). The vernier setting makes it possible to achieve a uniformly well represented, brittle edge layers are proc-
defined material removal (distance between 2 graduation essed without breakouts and soft microstructural compo-
marks of the scale = 0.02 mm). The locking ring prevents nents are not eroded or smeared. Only optimally prepared
the preset dimension from being altered during the grinding samples ensure the exact evaluation of the microstruc-
process. The very hard ceramic ring prevents over-grinding tures.
Insert M Insert H and ensures reliable material removal to the desired level.
Grinding III CAMEO DISK PLATINIUM 3 Water 1–3 min work step Grinding/polishing cloth Grinding/polishing agent Time
Polish I 2TS1 BioDiamant Liquid yellow 3 min Grinding I CAMEO DISK PLATINIUM 2 Water 1 min
Insert
Polish II 4FV1 BioDiamant Liquid red 1 min Grinding II CAMEO DISK PLATINIUM 4 Water 2 min
Specimen locking screw Polish I 2TS1 BioDiamant Liquid yellow 3–5 min
Alternative
BOX LAM 300 Polish II 4FV1 BioDiamant Liquid MM 140 1–2 min
The BOX LAM 300 storage system for disks and cloths up work step Grinding/polishing cloth Grinding/polishing agent Time
to Ø 300 mm. 10 push trays with a special surface provide Grinding I CAMEO DISK PLATINIUM 1 or Water until flat
Specimen 2, depending on the quality of
space for disks as well as samples, among other things,
the cut
which can be placed in foam pads (accessories).
Grinding II CAMEO DISK SILVER BioDiamant Liquid blue 3 min
or green
Polish I 2TS1 BioDiamant Liquid yellow 1–3 min
BOX LAM 300
Polish II 4FV1 BioDiamant Liquid red 1 min
BOX LAM
66056022 BOX LAM 300 storage system 1 pc.
60 kulzer-technik.com 61
SAMPLE PREPARATION
EMBEDDING SAMPLE PREPARATION
From practice
The result counts
Sample material: Sprayed layer on steel Sample material: Aluminium and alloys Sample material: Glass body soldered in steel sleeve embedded in: Sample material: Sandwich metal steel, bronze, aluminium, unetched
embedded in: hot embedding resin Technotherm 2000 or cold embedded in: cold embedding resin Technovit 4071, Technovit cold embedding resin 4071 or Technovit EPOX embedded in: Cold embedding resin Technovit 4002 IQ
embedding resin Technovit 4002 IQ 4002 IQ, Technovit 4006 SE or light-curing embedding resin Technovit
work step Grinding/polishing cloth Grinding/polishing agent Time work step Grinding/polishing cloth Grinding/polishing agent Time
2000 LC
work step Grinding/polishing cloth Grinding/polishing agent Time
Grinding I Diamond grinding disk 20 µm Water until flat Grinding I SiC paper 180 grain size
work step Grinding/polishing cloth Grinding/polishing agent Time or CAMEO DISK PLATINIUM 2
Grinding I CAMEO DISK PLATINIUM 1 Water until flat Grinding II SiC paper 1200 grain size
Grinding II CAMEO DISK PLATINIUM 2 Water 1–2 min Grinding I SiC paper 180 grain size Water until flat Grinding II CAMEO DISK GOLD BioDiamant Liquid green 3 min
Polish I 2TS1 BioDiamant Liquid yellow 3 min
Grinding III CAMEO DISK PLATINIUM 3 Water 1 min Grinding II SiC paper 320 grain size Water 1 min Polish I 2TS1 BioDiamant Liquid yellow 3 min
Polish II 2TS5 BioDiamant Liquid MM 140 4 min
Grinding IV CAMEO DISK PLATINIUM 4 Water 1 min Grinding III SiC paper 600 grain size Water 1 min Polish II 2TS4 BioDiamant Liquid MM 140 2 min
Polish III 4FV1 BioDiamant Liquid red 1 min
Polish I 2TS1 BioDiamant Liquid yellow 3–5 min Grinding IV SiC paper 1200 grain size Water 1 min Polish III 4FV1 BioDiamant Final Liquid 1 min
62 kulzer-technik.com 63
KULZER Technik – reliable and up-to-date, Kulzer GmbH
Leipziger Straße 2
highest level of quality. 63450 Hanau, Germany
PDF Catalog Materialography 2022-12