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1. The document describes a pipette calibration experiment conducted by an analytical laboratory. 2. The procedure involved weighing an empty beaker, adding measured volumes of tap water using a 10 mL pipette, and weighing the beaker with water to calculate volumes and check for accuracy. 3. The results showed the measured volumes were close to the expected volumes, with less than 1% error, indicating the pipette was properly calibrated.

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7 views7 pages

Ex

1. The document describes a pipette calibration experiment conducted by an analytical laboratory. 2. The procedure involved weighing an empty beaker, adding measured volumes of tap water using a 10 mL pipette, and weighing the beaker with water to calculate volumes and check for accuracy. 3. The results showed the measured volumes were close to the expected volumes, with less than 1% error, indicating the pipette was properly calibrated.

Uploaded by

bayarali1993
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as DOCX, PDF, TXT or read online on Scribd
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Analytical laboratory

Name of experiment: Pipette Calibration

Department: oil

Group: D

Chemicals and Supplies


Chemicals Supplies
Tap water in room temperature Beaker 10 ml
Pipette 10 ml
Scale

Procedure:
1. Rinse the given pipette and beaker with small amount of tap water.
2. Weight the empty beaker and record the mass.
3. Use the empty clean and dry beaker and then use the pipet to add a volume of
water (ml), students can take the variables shown table below, and record the
mass of the water in the scale.

9.9700 mL 10.0360 mL 9.9650 mL 10.0150 mL 10.0200 mL

4. Measure the temperature of the water at room conditions and record it.
5. notes the density of water at room temperature from table (Density of Liquid
Water From 0°C to 100°C).
6. Repeat step-3 for all students group to fined mass and volume measurements.
7. Complete all calculations.
8. Complete all information at table below.
9. sketch graphic data between densities and volumes that calibrated and
calculated.
Analytical laboratory

(Calibration Table)

Solution Volume Beaker Beaker mass Water Density Volume Temp.


No. ml mass + water mass mass g/ml water °c
g g g ml
1 3 42.489 45.460 2.971 0.998 2.976 18
2 4 50.899 54.889 3.991 0.998 3.997 18
3 5 48.908 53.894 4.986 0.998 4.995 18
4 2 48.896 50.817 1.104 0.998 1.106 18
5

Calculations:

Volume = 3 ml
beaker mass = 42.489 g
beaker mass+water mass = 45.460 g
water mass = 2.971 g
density = 0.998 g/ml at temp 18 °c

water volume = mass /density

= 2.971/0.998
= 2.976 ml
Analytical laboratory

Discussion:

We cleaned and dried a beaker and


a pipette
Then an empty beaker weight
Then we added 3 ml of distilled
water, then weighed it again, and
calculated the weight of the water
and its density at room
temperature.
It showed us through this
experiment that the percentage of
error is small, it is 0.024
It was a successful experiment .
Analytical laboratory
Analytical laboratory

sketch graphic data between densities and volumes that calibrated and
calculated.

v
6

v
3

0
0 1 2 3 4 5 6
Analytical laboratory

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