ICL CALIBRATION LABORATORIES, INC. ISONEC 17026 and ANSUNCSL 2640-1 accredited | 1501 Decker Avenue Sue 116 Sart F400 UG ‘Tho specialists in ASTM and laboratory thermometers & hydromet STE ee embers. ASTM API NGSLL” ASGNGWM us emetwareclabe com Setting new standards incalbraton excellence! toc: Caps, PR Tl 767 288748 CALIBRATION REPORT FOR HYDROMETER Report No. P137221 Page 1 of 2 THIS REPORT OF CALIBRATION SHALL DOCUMENT THAT THE INSTRUMENT DESCRIBED HEREIN WAS EXAMINED AND TESTED IN ICL'S ISOMEC 17025 ACCREDITED CALIBRATION LABORATORY, AGAINST NIST TRACEABLE REFERENCE STANDARDS, IN ‘ACCORDANCE WITH ICL'S ISO/EC 17025 CALIBRATION PROCEDURE REFERENCED BELOW. THIS CALIBRATION MEETS THE REQUIREMENTS OF ISOAEC 17025, ANSIINCSL 2540-1-1994, (WHICH SUPERCEDED AND REPLACED MIL-STD 486624), AND THE 180.8000 AND QS:$000 SERIES OF QUALITY STANDARDS. CUSTOMER INFORMATION: SAMPLE COMPANY STREET ADDRESS ory, stare ze ‘PURCHASE ORDER NUMBER: NOT AVAILABLE ‘SUBMITTED BY: SAMPLE CUSTOMER INSTRUMENT DESCRIPTION: ‘Serial No: XXX Inserition: CHASE Date calibrated: 06-12-2008 ‘Scale: American Petroleum Institute scale for petroleum products HYDROMETER ASTM 4H Scate ange: 29/41 API Scale divisions: .1 °API ‘Movet No: 4o004H.c (MAXIMUM SCALE ERROR PERMITTED BY ASTM E-100: +/-0.1 API RESULTS OF PHYSICAL EXAMINATION: THIS INSTRUMENT WAS EXAMINED UNDER A POLARIZED LENS AND STRAINS IN THE GLASS, IF ANY, WERE JUDGED TO BE MINIMAL AND OF NO DETRIMENT TO THE FUNCTION OF THE INSTRUMENT. THERE WAS NO LOOSE BALLAST OR OTHER MATERIAL OBSERVED WITHIN THE HYDROMETER, UNLESS OTHERWISE NOTED BELOW, A SCALE SLIPPAGE INDICATOR IS PRESENT AND CORRECTLY POSITIONED WITHIN THIS INSTRUMENT. IT WAS DETERMINED THAT THIS INSTRUMENT 1S IN GOOD WORKING ORDER AND IS THEREFORE SUITABLE FOR CALIBRATION. CALIBRATION PROCEDURE USED: ICt Procedure 02, which is based upon ASTM E-126 RESULTS OF CALIBRATION: NOTE: The indications ofthis instrument cannot be adjusted or moditied by ordinary means; accordingly, the readings given inthe table below should be considered, in effect, 19 be both “As Found’ end ‘As Left’ reedings TEST POINT READING, CORRECTION TOLERANCE © «IN TOL? ©=——UNCERTAINTY 30-00°APT —«-30.02°API = -0. 02a. 0.10¢aPr ves* 0.083 °apr 35/00°API —«35.08°API | 0: 08°APT O:10°apr vEs* 02083 °APT 40:00°API = «38136°APE © 40104°APT O:20°aPr YvES* 0:083°APr THE ABOVE READINGS WERE MADE UNDER MAGNIFICATION AND RESOLVED TO ONE TENTH OF ONE SCALE DIVISION. THE TEST POINTS LISTED IN THE ABOVE TABLE ARE THOSE SPECIFIED IN ASTM E-100 (CURRENT REVISION) THE INDICATIONS OF THIS INSTRUMENT COMPLY WITH THE ACCURACY TOLERANCE REFERENCED ABOVE, THE SCALE READING IS DETERMINED BY THE INTERSECTION OF THE HORIZONTAL PLANE, TANGENT TO THE BOTTOM OF THE MENISCUS, ON THE STEM SCALE. SEE ASTM D-1298 FOR DRAWINGS, DISCUSSION AND INSTRUCTION ON MAKING ACCURATE HYDROMETER READINGS. THE ABOVE READINGS (AND CORRECTIONS) REPRESENT THE AVERAGE OF AT LEAST THREE INDEPENDENT OBSERVATIONS (OF THE SUBJECT HYDROMETER AND AT LEAST FOUR OBSERVATIONS OF THE REFERENCE HYDROMETER. DECISION RULE: Unless otherwise instructed, ICL uses the following decision rule: f indications are perceived to reside within the tolerance limits, the indications are considered as ‘In-Tolerance’: any indications perceived to reside outside the tolerance limits are considered to be "Out ‘of Tolerance’. The measurement uncertainty isnot considered in this decioration ‘An asterik (*) alongside the "Yes" or ‘No" in the ‘IN TOLERANCE?" column in the table of corrections above should alert the user thatthe amountby which the device is either n-Tolerance or Out-ol-Tolerance is smaller than the meesurement uncertainty attributable fo thet calibration result. Our best measurement capebilties are as follows: from 0 to 92 AP +/- 0.082 API; from .620 TO 2.000 Speciic Gravity, +/. 0.00075 Specific Gravity ielatve density); equivalent values in othorscetes. These uncertainties have been calculated utiizing the methods elaborated IANIST Technical Note 1297 end the ANSI NCSL document Z-540.2 entitled ‘Guide to the Expression of Uncertainty in Measurement’, Commonly refered 10 2s the “GUM. A coverage factor of 2 sigma ik=2] has boen applied f0 the standard uncertainty in order to express the expanded uncertainty at spproximataly 2 98% confidence level THE UNCERTAINTIES PRESENTED ABOVE IN THE ‘RESULTS’ TABLE MAY BE LARGER THAN QUA SYSTEM UNCERTAINTIES, AS THe RESOLUTION OF THIS INSTRUMENT, ESTIMATED TO BE 0.01°API, HAS BEEN FACTORED INTO THE CALCULATION. THE EXPANDED UNCERTAINTIES (K'= 2) REPORTED HERE DO NOT CONTAIN ESTIMATES FOR (1) ANY EFFECTS THAT MAY BE INTRODUCED BY TRANSPORTATION OF THE INSTRUMENT BETWEEN ICL AND THE USER'S LABORATORY, (2) DRIFT OF THE INSTRUMENT. (2) HYSTERESIS OF THE INSTRUMENT, OR (4) ANY MEASUREMENT UNCERTAINTIES INTRODUCED BY THE USER, FOR FURTHER DISCUSSION OF ACCURACIES ATTAINABLE WITH HYDROMETERS SEE ASTM E-100, E-126 AND D-1298. LABORATORY ENVIRONMENTAL CONDITIONS: TEMPERATURE: 23°C +/+ 2°C RELATIVE HUMIDITY: BETWEEN 40% AND 60% [ALL TEMPERATURES GIVEN IN THIS REPORT ARE THOSE DEFINED BY THE INTERNATIONAL TEMPERATURE SCALE OF 1990 (TS-90) THIS CALIBRATION WAS PERFORMED BY: CINDY MARKEY THE CALIBRATION PERFORMED AND DOCUMENTED BY THIS REPORT OF TESTIS A FULL SCALE CALIBRATION AND NO LIMITATIONS OF USE ARE IMPOSED ON THs INSTRUMENT. TRACEABILITY INFORMATION ‘This calration is traceable to NIST through an unbroken chain of comparisons. The reference standard is used to calibrate the transfer TTandard, which in turn is used fo calrate the chent’s instrument. Each step in the chain is ful documented, and measurement luncertainty at each step has been cateuleted. ‘The NIST primary reference hydrometers) and transfer standard hydrometers(s) utilzed in the performance ofthis calibration are ted below. "Trenstor standard hydrometers are calibrated annually against the NIST reference hydrometers. Test Point _NISTReference hyrometerts) Transter Standard = MTE#—-Manufacturor ‘Next Due 30.00%apr 909457 & 347873, Ame 410 32633 0/02/06 35.o0rapz 909457 & 347873 ‘nora air 32633 10/02/06 40 lo0xpE 909457 & 347873, ‘neTM 4 32633, 0/02/05 ICL CALIBRATION LABORATORIES, INC. “J, JEFF KELLY, TECHNICAL DIRECTOR. DEBORAH MM. WEBER, A.S.C.P. ACCREDITED TECHNOLOGIST ‘BRUCE MARKEY, V.P. TECHNICAL SERVICES ‘This document prepared by LORI PARR and reviewed by KAREN ALLEBORN DATE CALIBRATED: 06-12-2006 _RECALIBRATION DATE SPECIFIED BY CLIENT: June 12, 2007 [MIST GMP-11 (Mar 03), ‘Good Measurement Practice for Assignment and Adjustment of Calibration intervals for Standords’ states that, “Temperatura standords are dynamic with use. Shock, contamination and other factors cen cause drift from accepted values”. Thbie 4 of GMP=11 recommends recalibration of liquid:hglass thermometers, standard thermistors and PRTs at 12 month intervals. Tutti gas tormometers used for Temperature Critcel Perameters” should be recaliorted at 6 month intervols. MIST GMP-11 i ‘Svniable Yor download in Adobe pat format on our website at wwew.fllabs.com Follow the link for ‘Downloads’ The API ‘Menual of Petroleum Measurement Standards’, Chapter 7, June, 2001, specifies» 12 month recalibration interval for Iiquic-nsglass thermometers (see section 8.3) and for portable elecironic thermometers (PETsI. See section 8.2 The user should be eware thet any number of factors may cause ths instrument to dit out of calibration before the specitiod calibration Intervet has expired. ‘This Report of Test may not be reproduced except in full without the express written permission of ICL Calibration Laboratories, Inc. This report apples only to the item calibrated. Report No. P137221 Page 2of 2