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Middle Palaeolithic flint procurement in Central Mediterranean Iberia:

Implications for human mobility

Article · March 2014

DOI: 10.2218/jls.v1i1.783

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 Middle Palaeolithic flint procurement in Central
Mediterranean Iberia: Implications for human mobility
Aleix Eixea1, Clodoaldo Roldán2, Valentín Villaverde1, João Zilhão3
1. Departament de Prehistòria i Arqueologia, Universitat de Valencia. Blasco Ibáñez, 28 46010 Valencia, Spain.
Email: Eixea: [email protected]; Villaverde: [email protected]
2. Instituto de Ciencia de los Materiales, Universitat de Valencia (ICMUV). Parc Cientific. C/ Catedrático José
Beltrán, 2 46980 Paterna, Valencia, Spain. Email: [email protected]
3. Departament de Prehistòria, Història Antiga i Arqueologia. Universitat de Barcelona/ICREA, Barcelona,
Spain. Email: [email protected]

Abstract:
Different flint types from the Middle Paleolithic site of Abrigo de la Quebrada (Chelva,
Valencia) are characterized, both macro- and microscopically, and compared with types found at
other localities in the region. Although procurement predominantly concerned the immediate vicinity
of sites, our results show the presence of the same types in assemblages separated by distances of up to
120 km. The long distances involved are suggestive of a pattern of North-South mobility of human
groups along the coastline of central Mediterranean Iberia.

Keywords: x-ray fluorescence; x-ray diffraction; raw materials; Middle Paleolithic; Valencian country

1. Introduction
The information available for the Valencia region on prehistoric raw material sources and
procurement is scant. Systematic studies have been carried out over limited areas only, and
geological mapping of the distribution of the siliceous variants used is nonexistent. The
available data pertain mostly to the Alicante province, and derive, namely, from studies by:
(a) Menargues (2005), on finds from Ratlla del Bubo and Cova de les Cendres; (b) García
Carrillo (García-Carrillo et al. 1991), on finds from Tossal de la Roca; (c) Faus (2008-2009),
on the outcrops of siliceous raw materials in the Comtat and Marina Alta areas; (d) Schmich
& Wilkens (2006), on the precise characterization by PIXE analysis (Proton Induced X-ray
Emission) of outcrops related to the Polop Alto sites; and (e) Molina et al. (2010) on the
Abric del Pastor (Alcoi, Alicante). As far as the Valencia province is concerned, research has
been limited to isolated classification of finds from the sites of Parpalló (Tiffagom 2006) and
Cova Negra (Moriel 1985) deposited in museum collections (Figure 1).
This lack of information is particularly problematic in the case of the region’s Middle
Paleolithic, and limits attempts at establishing a framework for the discussion of patterns of
human mobility during this period. Recently, however, analysis of the raw materials used at

Journal of Lithic Studies (2014) vol.1, nr. 1, p. xx-xx doi:10.2218/jls.v1i1.783

Published by the School of History, Classics and Archaeology, University of Edinburgh

ISSN: 2055-0472. URL: http://journals.ed.ac.uk/lithicstudies/

This work is licensed under a Creative Commons Attribution 2.5 UK: Scotland License.
A. Eixea et al. 2

Abrigo de la Quebrada (Eixea et al. 2011), located in an area so far unstudied, allowed some
interesting insights. Here, using both macro- and microscopic analyses, we compare the types
of raw material used at Quebrada with those used at other Valencian sites.

Figure 1. Map of sites referred to in the text.

2. The Abrigo de la Quebrada

The Abrigo de la Quebrada (Quebrada rock-shelter; henceforth, Quebrada) is located
near Chelva (Los Serranos), some 65 km northwest of the city of Valencia. The area’s main
geographic features are the Tuéjar-Chelva and Turia rivers and the rather steep mountains of
the Javalambre and Sierra de Utiel massifs of the Iberian Range that they drain (Figure 2).
The site is located on the left bank of the Barranco de Ahillas ravine. Defined on the
basis of the present day position of the overhang and the extent of the horizontal platform it
protects, the rock-shelter is 38 m-long and between 2 and 9 m-deep. The floor surface is
rather flat, with a slight dip from North to South. As it is oriented to the North-West and is
inset in a very narrow and steep ravine, the site receives little direct sunlight.

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A. Eixea et al. 3

Figure 2. The geological setting of Quebrada, according to sheet 666, 27-26 (Chelva) of the 1:50.000 Geological
Map of Spain (IGME 1972). J23-32 (Jurassic Malm Upper Kimmeridgian), J1-32 (Jurassic Malm Lower
Kimmeridgian) and O (Ordovician).

In geological terms, the area belongs to the Iberian Range (Cordillera Ibérica) geological
unit, which belongs to the Upper Jurassic complex (Kimmeridgian) and features the
deposition of pisolitic and oolitic limestone in a neritic to coastal, 30 to 40 m deep water. The
fact that this section is generally micritic and only occasionally, on the upper part, sparitic,
indicates a mid-energy environment where pisoid formation is explained by pressure from
algae in a carbonate-rich basin. The upper part of the Kimmeridgian reflects a higher energy
environment, given the sparitic matrix and the presence of intraclasts and oolites. In
paleogeographic terms, this Jurassic complex lies within the Iberian facies domain (dominio
de facies ibérica). More specifically, it is located at the boundary between the Iberian and the
Prebaetic facies; some authors (IGME 1972) have used the “Betiberian facies” (facies
betibéricas) expression to refer to this boundary.
The Abrigo de la Quebrada stratigraphy features a total of eight units distributed over a
thickness of some 3 m. The base of the sequence has not yet been reached. Level 1 is a
disturbed unit resulting from use of the rock-shelter as a sheep pen in recent times. Below,
levels 2 through 5, 7 and 8 show evidence of human occupation. Level 6, almost 1 m-thick, is
sterile. All the occupations feature Middle Paleolithic stone tool assemblages. The richest are
those in levels 3, 4 and 5. The following AMS dates on charcoal have been obtained: for level
3, 40,500 ± 530 BP (Beta-244003), on a sample of Pinus nigra recovered in spit 5 of square
B5; for level 4, 43,930 ± 750 BP (Beta-244002) on an ABA-treated sample of Pinus cf.
pinaster from a combustion feature in spit 6 of square A4, and >50.8 ka BP (OxA-24855) on
a ABOx-ed sample of Pinus cf. nigra (Villaverde et al. 2008; Eixea et al. 2011-2012).

3. Methods
Our main objective was to provide a petrographic context for the Quebrada artifacts. In
order to allow a provenience study of the highest possible resolution, they were compared to a
reference collection of geological raw materials located in the immediate vicinity, assembled
on the basis of a systematic survey. This survey covered an area of some 400 km² around the
site, although potential sources up to 60 km away were also visited. We followed the habitual
protocol: analysis of geological maps, assessment of toponymic information, and questioning

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A. Eixea et al. 4

of local informants. We also ran a few 2-3 km-long transects where raw material and encasing
rock formations were systematically recorded, photographed and collected. The located
outcrops feature the raw material variants making up the archaeological assemblages for the
most part. Even though also found farther away, all such variants, namely the Domeño-type
flint (see below), could be documented at <10 km from the site. In the near future we plan to
refine this “local,” umbrella classification on the basis of detailed mineralogical, petrological
and hydrological analyses aiming at a better understanding of lithological heterogeneity
within and between sources.
Macroscopic analysis (Masson 1979, 1981) was carried out with a binocular microscope
under 20x or 40x magnification and used Munsell and Pantone tables. Color, texture,
impurities and cortex features were recorded.
In addition, we obtained chemical data for 46 Quebrada-related samples, of which 41
were archaeological finds and five were from the regional outcrops located during the survey
work. Comparative data for the assessment of the provenience of the site’s allochthonous
flints were obtained through the analysis of an additional set of nine samples. Six were
artefact samples from sites located in the southern part of the study area — Middle Paleolithic
Cova Negra (Xátiva, Valencia) and Upper Paleolithic Cova de les Cendres (Moraira,
Alicante) (Villaverde 1984; Villaverde et al. 2010). The other three samples were from
natural flint outcrops — Serreta-type (Alicante) (Molina et al. 2010) and Mora de Rubielos
(Teruel) — located to both the North and the South of the study region and that are known to
have been widely used throughout the Paleolithic of Valencia. (See Table 1.)

Table 1. Samples analyzed in this study.

Sample type Number of
Sample type code samples Source
Allochthonous Type 1 (archaeological) A1 5 Abrigo de la Quebrada
Allochthonous Type 2 (archaeological) A2 9 Abrigo de la Quebrada
Allochthonous Type 3 (archaeological) A3 8 Abrigo de la Quebrada
Allochthonous Type 4 (archaeological) A4 5 Abrigo de la Quebrada
Geological M 5 Chelva quarries
Archaeological CN 2 Cova Negra
Archaeological CC 4 Cova de les Cendres
Geological UV1 1 Penella (Alicante)
Geological UV2 1 Beniaia (Alicante)
Geological UV3 1 Mora de Rubielos (Teruel)

All samples were analyzed in non-destructive mode by means of energy dispersive X-ray
fluorescence spectrometry (EDXRF). A selected set of artefact samples (chippage or debris)
was ground and the resulting powder was analyzed by X-ray diffraction spectrometry (XRD).
All measurements were performed at the Archaeometry Unit of the Materials Science
Institute, University of Valencia (ICMUV). In order to obtain better petrographic information,
thin sections of these samples are currently being processed. The results of their forthcoming
analysis are expected to improve the lithological information obtained so far.
EDXRF analysis was performed using a portable spectrometer equipped with a silver
transmission target X-ray tube (40 kV/50 A, maximum) and a Peltier cooled Si-PIN detector
with a resolution of 165 eV (FWHM @5.9 keV). An aluminium collimator reduces the X-ray
beam to a 3-5 mm diameter spot size. The X-ray beam impinges perpendicular to the sample
and the excited fluorescence radiation of the sample is recorded by the detector under 45º
geometry. The spectrometer was operated at 30 kV and 4 A with an acquisition time of 180
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A. Eixea et al. 5

live seconds. The minimum detection levels for the spectrometer in terms of %-weight are:
about 2-3% for Si and about 0.1% for elements with Z between Z=18 and Z=30. All
archaeological and quarry samples were left untreated except for cleaning with demineralized
water prior to analysis.
Only one EDXRF analysis was performed for each sample. Therefore, and considering
the raw materials’ heterogeneous composition, the results presented here should be considered
preliminary. Previous analyses have shown that results can vary within a single sample
depending on the measurement spot, because of heterogeneity in composition. Thus, in order
to increase the resolution and statistical power of the analysis, a larger number of
measurements per sample will be carried out in future stages of the project.
The EDXRF spectra of the analyzed samples indicate that the identified elements are Si,
P, S, Cl, Ca, Ti, Mn and Fe, with Si, K, Ca and Fe as the elements showing higher
fluorescence line intensity. The heterogeneity of the samples is high, especially in regard to
the presence of calcium; even on the same sample, the net areas of this element show, extreme
variability caused by the heterogeneous presence of calcium minerals. These observations
highlight the limitations of non-destructive EDXRF analyses in relation to e.g. sample
homogeneity, mineralogy or surface irregularity.
XRD analysis was performed using a Bruker D8-Advance diffraction system operating at
40 kV and 30 mA with a Cu anode. The intensity was measured in the range from 5º to 80º 2
at a step size of 0.02º and a counting time of 0.2 s. per step. Prior to measurement, the
samples were powered in an agate mortar.

4. Results
4.1. Macroscopically defined flint types
Four different lithological types have so far been identified among the Quebrada raw
materials: flint, limestone, quartzite and quartz. Flint is the most abundant raw material in all
levels, followed in smaller percentages by limestone and quartzite; quartz is sporadic (Table
2).

Table 2. Raw materials used in levels 2, 3 and 4 of Quebrada.

Flint Limestone Quartzite Quart
Level II 75.20% 12.80% 12% 0
Level III 70.10% 15.10% 14.30% 0.50%
Level IV 55.25% 20.49% 24.20% 0.06%

The local flint type (from 5 to 8 km around the site) is the most abundant. Its stratotype is
located on the slopes of the Turia River, close to the ruined village of Domeño. We have
called it “Domeño-type flint” (sílex tipo Domeño) (Villaverde et al. 2008) (Figure 3). The
coordinates of the type section on the geological map (sheet no. 27-26 (666), Chelva) are lat.
39.805622º and long. -1011372º (Gómez & Fernández 2004). This flint occurs in formations
belonging to the Middle Jurassic (Dogger) of the Iberian Range, embedded within blocks of
microcrystalline limestone; despite the common geological origin, it presents considerable
variability in internal color. It is fine-grained and shiny, and of good knapping quality. The
surface is smooth, without inclusions, opaque, with a microcrystalline texture. The base color
is grey, with shades of dark green distributed smoothly and homogenously. The external
appearance is semi-coarse, with brown and orangey tones. It also occurs as 15-20 cm irregular
nodules incrusted in limestone blocks, featuring different morphologies (longish, globular,
etc.) and a rather thin cortex.

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A. Eixea et al. 6

Figure 3. The locally available Domeño-type flint and its variants.

Going into more detail, this flint is characterized by the presence of mosaics of detrital
macroquartz and of a large number of inclusions, with sub-types and variants being found
together in a single outcrop. The non-siliceous components include iron oxides (hematite),
dispersed or grouped, and other relict minerals, as well as calcium carbonate formed prior to
silicification. The presence of triaxon sponge spicules and microforaminifera indicates a
marine formation environment. A process of phased silicification is documented: at first
fibrous quartz is generated, and then macroquartz grains are formed.
Our survey identified a series of outcrops in the vicinity of the site (Eixea et al. 2011),
namely, El Collado de las Granzas, Corrales de Silla and El Mozul (Figure 4). Both
morphologies (nodules and beds), indistinctly combined, are present in these outcrops, all of
which are in primary position: on one hand, we have 25 to 30 cm-thick, >30 m-long incrusted
subhorizontal strata exposed along the slopes; on the other, we have nodules with a semi-
coarse cortex indicative of little rounding that remain incrusted in the encasing calcareous
rock but can also be found loose on the ground. These outcrops are easily accessible,
detached nodules can be found a few meters away from the primary outcrop, and the material
is altogether plentiful. The abundance of material of good quality for knapping in outcrops
located in the vicinity of the site indicates that the Quebrada flints were mostly procured from
such sources.
Regarding the allochthonous flints, four groups have been defined so far (Figure 5). For
the moment, their differentiation relies entirely on macroscopic observation (Masson 1979,
1981). Type 1 is a whitish chert with brownish and yellowish tones. The study of its cortex
indicates continental formation in an evaporitic sedimentary basin, probably of Tertiary age.
This chert is fine-grained and translucent. Among the inclusions, some — acicular

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A. Eixea et al. 7

pseudomorphs (gypsum crystals), iron oxide cryptograins and some anhydritic components —
indicate chert formation environments with high salinity levels. Two variants can be
discriminated within this type: one featuring more reddish colors, due to the fact that hematite
or iron oxide grains are more abundant; and another, featuring a mudstone texture, relicts of
the original carbonate, and macroquartz particles, which give it a brownish color. The source
of both variants remains unknown.

Figure 4. Procurement territories for the Domeño-type flint and other Quebrada raw materials.

Type 2 is fine-grained, with a smooth surface and microcrystalline structure, and is also
of good knapping quality. Its color is light brown with small dark speckles. Internally, spicule
sections, inertites and the presence of microforaminifera indicate a marine formation
environment, probably of Cretaceous age. As with Type 1, variants can be discriminated, in
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A. Eixea et al. 8

this case on the basis of a lower or higher degree of silicification. An interesting point is that
some flints show remains of whitish patinas as well as of a fine, smooth cortex; these features
suggest that the sources correspond to tabular siliceous formations that remain to be located.

Figure 5. Allochthonous flints from Quebrada.

Type 3 is mainly characterized by its blackish color. It is also fine-grained, with a smooth
surface and microcrystalline structure, and good for knapping. The presence of intraclasts of
biogenic origin, along with algae remains and sea urchin spicules, suggests a marine origin for
this type.
Type 4 remains incompletely characterized, but doesn’t fit into any of the former. Its
recognition as a separate group is corroborated by the microscopic analyses (see below).

4.2. Chemical and mineralogical analyses

Principal Component Analysis (PCA) was used as a clustering data reduction technique
from the normalized net areas of the major elements identified by EDXRF (Si, K, Ca and Fe).

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A. Eixea et al. 9

PCA uses the principal components method of extraction, analyzing the correlation matrix of
rotated factors. Based on these data, diagrams showing the principal components were drawn
for comparison between the local, internally variable flint samples, and the allochthonous
flints (Figures 6 and 7).

Figure 6. Principal components 1 and 2 derived from PCA analysis of the Domeño flint and its outcrops (XRF
data).

Principal component 2 (PC2) is highly correlated (positive correlation) with Fe and to a

lesser extent with K, while PC1 has a positive correlation with Ca and negative correlation
with Si. The Quebrada samples macroscopically catalogued as local (labelled D) cluster
separately in this projection (PC2>0 in Figure 6), except for: (a) the D20 sample, which
clusters with two allochthonous types, Type 2 (labelled A2) and Type 3 (labelled A3), and
whose EDXRF spectrum presents a low intensity of the fluorescence peak of iron (PC2<0);
and (b) the D16 and D18 outliers, which, in contrast, have EDXRF spectra with intense iron
fluorescence lines. The Quebrada samples of Type 2 and Type 3 present similarities (PC1<0
and PC2<0 in Figure 6) but do not cluster together; two of them project away from those
quadrants — A2-17, which is close to the Quebrada local flints, and A2-19, which features a
high intensity of the calcium fluorescence line. The Type 4 samples (labelled A4) form a
separate group with values of PC1>0 and PC2<0 (Figure 6). Finally, the Type 1 samples
(labelled A1) appear close to Type 2 and Type 3 (in two cases) or to Type 4 (in three cases);
the A1-5 outlier presents very intense calcium fluorescence lines. Among the geologically
local samples (labelled M), M7, M9 and M10 present similarities and cluster with the
Domeño-type archaeological samples, while M6 and M8 are closer to Type 4 and to Type 2
or 3, respectively.
The macroscopic assessment and the microscopic analyses confirm the homogeneity of
the Domeño-type flint. As illustrated by Figure 6, artefact samples in this raw material are
quite distinct from those made on allochthonous flints while being closely related to samples
from this type taken from the local outcrops. This confirms our working hypothesis that this

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A. Eixea et al. 10

type of flint is of local origin and was procured within a radius of between 5 and 8 km from
the site. The outlier situation of samples D-16, D-18 and D-20 may be due to analytical issues
associated with surface alterations or sampling error.

Figure 7. Principal components 1 and 2 derived from PCA of the allochthonous flints (XRF data).

The separateness of the allochthonous types and their classification into different groups
are also clearly supported by the analyses (Figure 7). Based on macroscopic criteria that have
yet to be corroborated, we have assigned to these types flints from other sites of the Valencian
Paleolithic located at considerable distances from Quebrada. Although such results are
preliminary, they suggest that Type 1 is present in the Middle Paleolithic of Cova de la
Petxina (100 km) and Rambla de los Morenos (30 km), and in the Upper Paleolithic of Cova
del Parpalló (100 km). As to Type 2, we have identified it in (a) the Middle and Lower
Paleolithic of San Luís (40 km), Rambla de los Morenos (30 km), Barranco de Carcalín (40
km), Las Fuentes (70 km), Cova de la Petxina (100 km), Cova del Bolomor (100 km) and
Cova Negra (100 km), (b) the Upper Paleolithic of Cova de les Malladetes (100 km), Volcán
del Faro (90 km) and Abric de la Senda Vedada (80 km), and (c) the Epipaleolithic of Cueva
de la Cocina (50 km); this type may also be represented in the Middle Paleolithic of Abric del
Pastor and the natural flint outcrops from La Serreta, in the Alcoi area (Molina et al. 2010),
indicating that it circulated widely. Type 3 has been documented at Cova del Parpalló (100
km), Cova de les Malladetes (100 km), Cova de les Cendres (150 km), Balma de la Roureda
(90 km) and Sant Joan de Nepomucè (100 km). For Type 4, no secure identification of its
presence at other sites can be made with current data.
Twenty-one samples were analyzed by XRD: seven of Domeño-type, two of
allochthonous Type 1, four of allochthonous Type 2, four of allochthonous Type 3 and four
archaeological samples from Cova de les Cendres. They show quartz and calcite as the main
crystalline phases with occasional presence of pyrolusite, moganite, silicates and oxides.
Comparison is made difficult due to the dominance of quartz in all of them. However, we
noted that the size of quartz crystals, estimated by means of the equation of Scherrer (based

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A. Eixea et al. 11

on the resolution of the quartz diffraction patterns around the peak at 2 68º), is larger among
the local Domeño-type samples than among those catalogued as allochthonous. This supports
the separateness of the Domeño type indicated by the XRF analysis.

5. Conclusions
Our study is still in an initial stage and the results obtained so far are preliminary and in
need of corroboration and augmentation by additional analysis and field work. Yet, it is
already possible to derive from them a suggestion of significant levels of mobility across
extended territories, including the transit areas and natural corridors of the Valencian region
(Aura et al. 1993) that connect interior and coast via the Turia, Plana de Utiel and Magro
corridors. These rivers all converge to the large Valencia plain, allowing for movement
towards the North (Quebrada) as much as to the South, namely to the site clusters of Gandia
and Xàtiva (Cova Negra, Cova Foradada, Cova del Gat and Cova de la Petxina) or Alcoi
(Cova Beneito, Abric del Pastor and El Salt) (See Figure 1).
At present, we favor the explanation that the spatial distribution pattern observed reflects
the circulation of individual groups across subsistence territories of rather large size.
Alternatively, it could reflect the circulation of raw materials through long distance exchange
networks. Additional work is ongoing or in preparation with the aim of testing these
alternatives. The planned work includes extended survey to locate as yet unknown sources
and the analysis of more samples from a wider range of sites from different parts of the region
and from different periods of its Prehistory.

Acknowledgements
Research for the present paper has been supported by the following projects: “El final del
Paleolítico medio y el Paleolítico superior en la región central del Mediterráneo ibérico” (FFI
2008-01200/FISO), “La conducta de los neandertales: una aproximación a partir del registro
arqueológico del Abrigo de la Quebrada (Chelva, Valencia)” (HAR 2008-04273-E/HIST),
"Paleolítico medio final y Paleolítico superior inicial en la región central mediterránea
(Valencia y Murcia)" (HAR2011-24878) and “Mas allá de la Historia: los inicios del
poblamiento paleolítico valenciano” (PROMETEOII/2013/016). Finally, the authors would
like to thank Jorgelina Carballo for her help in carrying out the EDXRF analyses.

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