Eihp 12B (DF)
Eihp 12B (DF)
Prepared by:
UN ECE WP.29 GRPE Informal Group “Hydrogen/Fuel Cell Vehicles” based on proposals
originally developed by the Partners of the European Integrated Hydrogen Project – Phase II
(EIHP2).
Notes:
1. For editing purposes the following colour codes have been adopted:
i) Green highlighting identifies reference to standards, etc.
ii) Yellow highlighting identifies references to other parts of this document.
2. A number of key words or phrases have been defined and are indicated in the text by
Capitalised Italic Font. As these definitions are crucial to the correct interpretation of
this document it is strongly recommended that they remain highlighted in the final
Regulation.
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CONTENTS
REGULATION
Page No.
1 Scope
2 Definitions, container types, pressure classifications and service
conditions
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ANNEXES
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1 SCOPE
1.1 Compressed gaseous hydrogen systems for motor vehicles in which the hydrogen is
stored in its gaseous phase under pressure and essentially at ambient temperature,
including the complete Hydrogen System, i.e. excluding the Propulsion System
(internal combustion engine or fuel cell system) or any auxiliary power unit.
2.1 DEFINITIONS
For the purpose of this Regulation and the accompanying Annexes the following
definitions shall apply and are indicated in the text by capitalised italic words, e.g.
Valve:
2.1.1 "Approval Of A Vehicle Type": Approval of a type of vehicle with regard to its
Hydrogen System installed as original equipment.
2.1.2 "Automatic Valve": A valve that is not operated manually. A Non-return Valve
is not an Automatic Valve.
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2.1.11 "Container": Any vessel used for the storage of compressed gaseous
hydrogen within the temperature limits specified in this Regulation, excluding
any other Hydrogen Components which may be attached to or fitted inside the
Container.
2.1.13 “Duty Cycle”: One start up and shut down cycle of the Hydrogen Conversion
System(s).
2.1.15 "Excess Flow System": A system that shuts off the flow without manual
intervention in the event of a line rupture or similar severe leakage.
2.1.16 “Filling Cycle”: A pressure increase of more than 25% of the Working
Pressure of the Container due to an external source of hydrogen.
2.1.18 “First Pressure Regulator”: The Pressure Regulator having the Container
pressure as its inlet pressure.
2.1.20 "Flexible Fuel Line": A flexible tubing or hose of any length through which
hydrogen flows.
2.1.21 "Fuel Supply Line": The line that supplies the Hydrogen Conversion System(s)
with hydrogen.
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2.1.22 “Fully Wrap”: Over-wrap with the filaments wound around the Liner both in the
circumferential and longitudinal directions of the Container.
2.1.25 "Hydrogen Conversion System": Any system designed for the conversion of
hydrogen into electrical, mechanical or thermal energy, and includes, for
example, the Propulsion System(s) or auxiliary power unit(s).
2.1.26 “Hydrogen Filter”: A filter used to separate oil, water and dirt from hydrogen.
2.1.29 “Leak Test Gas”: Hydrogen, helium or an inert gas mixture containing at least
5% hydrogen or 10% helium or a demonstrated detectable amount of helium
or hydrogen gas.
2.1.30 “Liner”: A Container that is used as a gas tight, inner shell, on which
reinforcing fibres are filament wound to reach the necessary strength. Liners
may be designed to share the load with the reinforcement, or not to carry any
part of the load.
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3 3
2.1.35 “Nm “ or “Ncm “ (normal cubic metre or centimetre): A volume of dry gas that
3 3
occupies a volume of 1 m or 1 cm at a temperature of 273.15 K (0 °C) and
an absolute pressure of 101.325 kPa (1 atm).
2.1.37 "Non-return Valve": A valve that allows hydrogen to flow in only one direction.
2.1.42 “Pressure Relief Valve”: A reclosing pressure activated device that prevents a
Hydrogen Component from bursting due to excessive pressure.
2.1.43 "Propulsion System": The internal combustion engine or fuel cell system used
to propel the vehicle
2.1.44 "Range of Control": Refers to an output variable and defines the range over
which the system is likely to exercise control.
2.1.45 "Receptacle": A device fitted in the vehicle used to permit refilling of the
Container(s), i.e. a filling unit.
2.1.48 "Rigid Fuel Line": Tubing that has not been designed to flex in normal
operation and through which hydrogen flows.
2.1.49 ”Safety Concept": Measures designed into the system to ensure safe
operation even in the event of a failure or random faults.
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2.1.52 “Service Life”: The life in years during which the Containers may safely be
used in accordance with the service conditions.
2.1.54 "Transmission Links": The means used for interconnecting distributed Units for
the purpose of conveying signals, operating data or an energy supply. This
equipment is generally electrical but can be mechanical, pneumatic or
hydraulic.
2.1.55 "Units": The smallest divisions of system components that will be considered,
as these combinations of components will be treated as single entities for
purposes of identification, analysis or replacement.
2.1.56 “Usage Monitoring And Control System”: A system that counts the Filling
Cycles and prevents further use of the vehicle when a predetermined number
of Filling Cycles is exceeded.
2.1.57 "Vehicle Type": A vehicle fitted with Specific Components for the use of
hydrogen that does not differ with respect to the following conditions:
i) The Manufacturer(s),
ii) The installation of the Hydrogen Components,
iii) Type(s) of Specific Components.
A Container shall be classified into the following types according to the type of
construction:
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Unless indicated otherwise the following service conditions shall apply throughout this
Regulation and its Annexes:
The MAWP(s) shall be equal to or shall exceed the set pressure of the
overpressure protection specified in Paragraph 14.1.18 of this Regulation.
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2.4.5 Temperatures
2.4.6.1 General
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2.4.7.1 General
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Part I
PART I
SPECIFIC COMPONENTS OF
MOTOR VEHICLES USING COMPRESSED GASEOUS HYDROGEN
3.2 The application for type approval shall be accompanied by the following documents in
triplicate:
3.3 At the request of the Technical Service responsible for conducting approval tests, two
samples of the Specific Component shall be provided unless otherwise stated in this
Regulation.
3.4 The Competent Authority shall verify the existence of satisfactory arrangements for
ensuring effective control of conformity of production before type approval is granted.
4 MARKINGS
4.1 The samples of the Specific Component submitted for approval shall bear the trade
name or mark of the Manufacturer and the type; and in addition for Flexible Fuel
Lines the manufacturing month and year. The marking shall be legible and indelible.
4.2 All Specific Components shall have a space large enough to accommodate the
approval mark. This space shall be shown on the drawings referred to in Paragraph
3.2 ii) of this Regulation.
5 APPROVAL
5.1 If the Specific Component samples submitted for approval meet the relevant
requirements of Paragraph 6 of this Regulation, approval of the type of Specific
Component shall be granted.
5.2 An Approval number shall be assigned to each type of Specific Component type
approved. Its first two digits shall indicate the series of amendments to this
Regulation incorporating the most recent major technical amendments made at the
time of granting the approval (00 for the Regulation in its original form). The same
Contracting Party shall not assign the allocated code to another type of Specific
Component.
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5.4 In addition to the markings prescribed in Paragraph 4.1 of this Regulation and for
Containers in Annex 7 to this Regulation, there shall be affixed conspicuously in the
space referred to in Paragraph 4.2 of this Regulation, to all Specific Components
conforming to a type approved under this Regulation, an international approval mark
consisting of:
i) A circle surrounding the letter "E“ followed by the distinguishing number of the
country that has granted approval (see Note *1 below).
ii) The number of this Regulation, followed by the letter "R", a dash and the
approval number to the right of the circle prescribed in i) above. This approval
number consists of the Specific Component type approval number that appears
on the certificate completed for this type (see Paragraph 5.2 of this Regulation
and Annex 4 to this Regulation) preceded by 2 figures indicating the sequence of
the latest series of amendments to this Regulation.
5.6 Annex 3 to this Regulation gives an example of the arrangement of the aforesaid
approval mark.
__________________________________________________________________________
Note *1:
1 for Germany, 2 for France, 3 for Italy, 4 for Netherlands, 5 for Sweden, 6 for Belgium, 7 for
Hungary, 8 for the Czech Republic, 9 for Spain, 10 for Yugoslavia, 11 for the United
Kingdom, 12 for Austria, 13 for Luxembourg, 14 for Switzerland, 15 (vacant), 16 for Norway,
17 for Finland, 18 for Denmark, 19 for Romania, 20 for Poland, 21 for Portugal, 22 for the
Russian Federation, 23 for Greece, 24 Ireland, 25 for Croatia, 26 for Slovenia, 27 for
Slovakia, 28 for Belarus, 29 for Estonia, 30 (vacant), 31 for Bosnia and Herzegovina, 32-36
(vacant), 37 for Turkey,38-39 (vacant) and 40 for the former Yugoslav Republic of
Macedonia, 43 Japan.
Subsequent numbers shall be assigned to other countries in the chronological order in which
they ratify or accede to the Agreement concerning the Adoption of Uniform Technical
Prescriptions for Wheeled Vehicles, Equipment and Parts which can be Fitted or be Used on
Wheeled Vehicles and the Conditions for Reciprocal Recognition of Approvals Granted on
the Basis of these Prescriptions, and the numbers thus assigned shall be communicated by
the Secretary-General of the United Nations to the Contracting Parties to the Agreement.
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6.1.1 The Hydrogen Components shall function in a correct and safe way as
specified in this Regulation. They shall remain functional under the
mechanical, thermal and chemical service conditions specified in Paragraph
2.4 of this Regulation, and shall also reliably withstand these conditions
without leaking or visibly deforming.
6.1.2 The materials of components which are in contact with hydrogen shall be
compatible with hydrogen and expected additives and production
contaminants.
6.1.3 Material compatibility with the service conditions defined in Paragraph 2.4 of
this Regulation shall be demonstrated either by the material tests in Annexes
7 and 8 to this Regulation, or by a previously approved test certificate.
6.1.4 All Hydrogen Components that are designed for uni-directional flow shall have
the flow direction clearly indicated.
6.1.5 Specific Components shall be type approved in accordance with the relevant
electromagnetic compatibility requirements of ECE Regulation No 10, 02
series of amendments, or equivalent.
6.1.9 Unless indicated otherwise, the requirements of this Regulation and its
Annexes shall take precedence over any standards referred to herein.
6.1.10 The documentation and test reports shall be sufficiently detailed to enable an
independent third party test facility to reproduce the appropriate type approval
tests and test results.
6.2.2 The shape of a Container is free provided that it fulfils all the appropriate
provisions laid down in Annex 7 to this Regulation.
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6.2.3.5 Flexible Fuel Lines shall not be used as integral interconnecting fuel
lines in a Container Assembly.
6.3.2 Unless otherwise stated in this Regulation, the parts of a Removable Storage
System Connector mounted on the Removable Storage System and on the
vehicle shall be treated as separate components.
Rigid Fuel Lines upstream of the First Pressure Regulator shall be bent through 180
degrees at the minimum bending radius specified by the Manufacturer and shall then
be hydraulically pressure tested to 3 times Nominal Working Pressure without
rupturing. Rigid Fuel Lines, downstream of the First Pressure Regulator shall be bent
through 180 degrees at the minimum bending radius specified by the Manufacturer
and shall then be hydraulically pressure tested to 3 times MAWP without rupturing.
7.3 The competent authority issuing the extension of approval shall assign a series
number to each communication form (specified in Paragraph 5.3 of this Regulation)
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issued for such an extension, and shall inform the other Parties to the Agreement
with a form conforming to the model in Annex 4 to this Regulation.
8 CONFORMITY OF PRODUCTION
The conformity of production procedures shall comply with those set out in the
Agreement, Appendix 2 (E/ECE/324-E/ECE/TRANS/505/Rev.2) and with the
following requirements:
i) A Hydrogen Component type approved according to this Regulation shall be
manufactured so as to conform to the type approved by meeting the
requirements specified in Paragraph 6 of this Regulation.
ii) The approval authority that has granted type approval may at any time verify the
conformity control methods applied in each production facility. The normal
frequency of these verifications shall be once every two years.
9.1 The approval granted in respect of a Specific Component in accordance with this
Regulation may be withdrawn if the requirements laid down in Paragraph 8 of this
Regulation are not complied with.
9.2 If a Contracting Party to the Agreement that applies this Regulation withdraws an
approval it has previously granted, it shall immediately notify the other Contracting
Parties applying this Regulation by means of a communication form conforming to
the model in Annex 4 to this Regulation.
If the holder of the approval for a Specific Component type approved in accordance
with this Regulation, permanently ceases to manufacture the component, he shall
immediately inform the authority which granted the approval. Upon receiving the
relevant communication, that authority shall inform the other Parties to the
Agreement applying this Regulation of that communication, by means of a
communication form conforming to the model in Annex 4 to this Regulation.
The Parties to the Agreement applying this Regulation shall communicate to the
United Nations Secretariat the names and addresses of the Technical Services
responsible for conducting approval tests and of the Administrative Departments
which grant approval and to which forms certifying approval or extension or refusal or
withdrawal of approval issued in other countries, are to be sent.
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PART II
VEHICLES WITH REGARD TO THE INSTALLATION OF SPECIFIC COMPONENTS FOR
THE USE OF COMPRESSED GASEOUS HYDROGEN
12.1 The application for Approval Of A Vehicle Type with regard to the installation of
Specific Components for the use of compressed gaseous hydrogen shall be
submitted by the vehicle manufacturer or by his duly accredited representative.
12.2 The application shall be accompanied by a description of the vehicle comprising all
the relevant particulars referred to in Annex 2 to this Regulation in triplicate.
12.3 A vehicle, representative of the Vehicle Type to be type approved, shall be submitted
to the Technical Service conducting the approval tests.
12.4 The competent authority shall verify the existence of satisfactory arrangements for
ensuring effective control of conformity of production before type approval is granted.
13 APPROVAL
13.1 If the vehicle submitted for type approval pursuant to this Regulation is fitted with
Specific Components in accordance with Part I of this Regulation and meets the
requirements of Part II of this Regulation, approval of that Vehicle Type shall be
granted.
13.2 An approval number shall be assigned to each Vehicle Type approved. Its first two
digits shall indicate the series of amendments to this Regulation incorporating the
most recent major technical amendments made at the time of granting the approval
(00 for the Regulation in its original form). The same Contracting Party shall not
assign the approval number to another Vehicle Type.
13.4 There shall be affixed to every Vehicle Type approved under this Regulation,
conspicuously and in a readily accessible space specified on the approval form
referred to in Paragraph 13.3 of this Regulation, an international approval mark
consisting of:
i) A circle surrounding the letter "E“ followed by the distinguishing number of the
country that has granted approval (see Note *1 below).
ii) The number of this Regulation, followed by the letter "R", a dash and the
approval number to the right of the circle prescribed in Paragraph i) above. This
approval number consists of the Vehicle Type approval number that appears on
the certificate completed for this type (see Paragraphs 13.2 and 13.3 of this
Regulation and Annex 6 to this Regulation).
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13.5 If the vehicle conforms to a Vehicle Type approved under one or more other
Regulations annexed to the Agreement in the country which has granted approval
under this Regulation, the symbol prescribed in Paragraph 13.4 i) of this Regulation
need not to be repeated. In such a case, the Regulation and approval numbers and
the additional symbols of all the Regulations under which approval has been granted
in the country that has granted approval under this Regulation shall be placed in
vertical columns to the right of the symbol prescribed in Paragraph 13.4 i) of this
Regulation.
13.6 The type approval mark shall be clearly legible and be indelible.
13.7 The type approval mark shall be placed close to or on the statutory plate of the
vehicle.
13.8 Annex 5 to this Regulation gives examples of the arrangement of the type approval
mark referred to above.
_______________________________________________________________________
Note *1:
1 for Germany, 2 for France, 3 for Italy, 4 for Netherlands, 5 for Sweden, 6 for Belgium, 7 for
Hungary, 8 for the Czech Republic, 9 for Spain, 10 for Yugoslavia, 11 for the United
Kingdom, 12 for Austria, 13 for Luxembourg, 14 for Switzerland, 15 (vacant), 16 for Norway,
17 for Finland, 18 for Denmark, 19 for Romania, 20 for Poland, 21 for Portugal, 22 for the
Russian Federation, 23 for Greece, 24 Ireland, 25 for Croatia, 26 for Slovenia, 27 for
Slovakia, 28 for Belarus, 29 for Estonia, 30 (vacant), 31 for Bosnia and Herzegovina, 32-36
(vacant), 37 for Turkey,38-39 (vacant) and 40 for the former Yugoslav Republic of
Macedonia, 43 Japan.
Subsequent numbers shall be assigned to other countries in the chronological order in which
they ratify or accede to the Agreement concerning the Adoption of Uniform Technical
Prescriptions for Wheeled Vehicles, Equipment and Parts which can be Fitted or be Used on
Wheeled Vehicles and the Conditions for Reciprocal Recognition of Approvals Granted on
the Basis of these Prescriptions, and the numbers thus assigned shall be communicated by
the Secretary-General of the United Nations to the Contracting Parties to the Agreement.
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14.1 GENERAL
14.1.1 The Hydrogen System of a vehicle shall function in a safe and proper
manner. It shall reliably withstand the chemical, electrical, mechanical and
thermal service conditions specified in Paragraph 2.4 of this Regulation
without leaking or visibly deforming. The number of Hydrogen
Components, connections and the length of lines shall be kept to the
minimum compatible with safety and the correct functioning of the
Hydrogen System.
14.1.3 The materials used in the Hydrogen System shall be compatible with
gaseous hydrogen and expected additives and production contaminants,
and expected temperatures and pressures.
14.1.4 The temperature range shall be in accordance with Paragraph 2.4.5 of this
Regulation.
14.1.6 The Hydrogen System shall be installed such that it is protected against
damage so far as is reasonably practical, such as damage due to moving
vehicle components, impacts, grit or due to the loading or unloading of the
vehicle or the shifting of loads. This Paragraph also applies to Pressure
Relief Device vents.
14.1.7 No component of the Hydrogen System shall be located near the exhaust
of an internal combustion engine or other heat source, unless such
components are adequately shielded against heat.
14.1.8 The ventilating or heating system for a passenger compartment and places
where leakage or accumulation of hydrogen is possible shall be kept apart
so that hydrogen is not drawn into the vehicle.
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14.1.11 In the event of hydrogen leakage or venting, hydrogen shall not be allowed
to accumulate in enclosed or semi-enclosed spaces.
14.1.12 Hydrogen Components that could leak hydrogen and that are mounted
within the passenger or luggage compartment or other non-ventilated
compartment shall be enclosed by a gas tight housing in accordance with
Paragraph 14.10 of this Regulation or by an equivalent solution.
14.1.13 The location of the Container or Container Assembly shall take into
account possible sources of corrosion, e.g. due to road de-icing salt,
leakage of acid batteries.
14.1.15 All Pressure Relief Devices, other safety components and vent lines shall
be protected against unauthorised interference so far as is reasonably
practicable.
14.1.17 Automatic Valves shall fail to the safest mode of operation for the particular
application, i.e. fail-safe.
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14.2.5 The provision of Paragraph 14.2.4 shall not apply if the vehicle is approved
according to ECE R 94 and ECE R 95, nonetheless, no uncontrolled
release of hydrogen is permitted.
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14.3.4 A single interface for the flow of hydrogen shall be provided between the
Removable Storage System and the part of the Hydrogen System
permanently installed in the vehicle. The Nominal Working Pressure of the
Hydrogen System at the interface shall be less than or equal to 3.0 MPa.
14.3.5 When the Removable Storage System is installed in the vehicle the
connection with the part of the Hydrogen System permanently installed in
the vehicle shall be made without the use of tools and shall be capable of
fulfilling the requirements of Paragraphs 14.1.10 and 14.2.4 of this
Regulation.
14.3.6 At the time of disconnection of the Removable Storage System, the volume
of hydrogen released shall not exceed 200Ncm3 and shall not be released
near a possible ignition source. The build up of hydrogen due to successive
disconnections shall be prevented.
14.3.7 The part of the Removable Storage System Connector permanently fitted
to the vehicle shall be of a unique design for the applicable vehicle type
and shall not be compatible with standard refilling nozzles for either
hydrogen or other gaseous fuels.
14.3.11 Use of the Hydrogen System shall be prevented if a partial or total failure of
the Removable Storage System Connector or electrical connectors
between the Removable Storage System and the vehicle occurs, that may
affect the safety of the Hydrogen System.
14.3.12 The installation and removal operations for the Removable Storage System
shall be illustrated on a label attached to the vehicle close to the mounting
point of the Removable Storage System. The label shall also state the
Nominal Working Pressure of the Container(s) or Container Assembly and
the Removable Storage System Connector.
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14.3.13 A label shall be attached to the Removable Storage System stating the
Nominal Working Pressure of the Container(s) or Container Assembly and
the Removable Storage System Connector.
14.3.14 The vehicle type approval mark specified in Paragraph 13.4 of this
Regulation shall be reproduced on the Removable Storage System.
14.4.1 The flow of hydrogen from a Container or Container Assembly into the Fuel
Supply Line shall be secured with an Automatic Valve (idle closed). This
valve shall be mounted directly on or within either every Container or one
Container in a Container Assembly.
14.4.3 If a single line is used into the Container or Container Assembly for both
refilling and fuel supply, it shall be secured as described in Paragraph
14.4.2 of this Regulation on the refilling line at the junction between the
refilling line and the Fuel Supply Line.
14.4.4 In the event of breakage of the refilling lines or Fuel Supply Line(s), the
isolating valves referred to in Paragraphs 14.4.1 and 14.4.2 of this
Regulation shall not be separated from the Container or Container
Assembly.
14.4.6 The Automatic Valve for the Fuel Supply Line of the Propulsion System
shall be operated such that the hydrogen supply to the Propulsion System
is cut off when the Propulsion System is switched off, irrespective of the
position of the activation switch, and shall remain so until the Propulsion
System is required to operate.
14.4.7 The Automatic Valve for the Fuel Supply Line of other Hydrogen
Conversion System(s) shall be operated such that the hydrogen supply to
other Hydrogen Conversion System(s) is cut off when the respective
Hydrogen Conversion System is switched off, irrespective of the position of
the activation switch, and shall remain so until the Hydrogen Conversion
System is required to operate.
14.5.1 A Pressure Relief Device shall be directly installed into the opening of a
Container or at least one Container in a Container Assembly, or into an
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14.5.2 It shall not be possible to isolate the Pressure Relief Device from the
Container protected by the Pressure Relief Device, by the normal operation
or failure of another component.
14.5.3 The vent of a Pressure Relief Device shall not discharge into a wheel arch,
nor shall it be aimed at a heat source such as the exhaust or at other
Containers or Container Assemblies if fitted. Additionally it shall discharge
such that hydrogen cannot enter the inside of the vehicle.
14.5.4 The internal dimensions of the vent shall not impede the function of the
Pressure Relief Device.
14.5.5 The vent of the Pressure Relief Device shall be protected against
blockage, e.g. by dirt, ice, and ingress of water etc., so far as is reasonably
practicable.
14.5.6 The outlet of the Pressure Relief Device shall be orientated such that if the
vent becomes detached from the Pressure Relief Device, the resulting gas
flow does not impinge directly on other Containers or Container Assemblies
unless they are protected.
14.6.1 A Pressure Relief Valve shall be installed in such a manner that it shall
discharge the hydrogen into an atmospheric outlet that vents to the outside
of the vehicle.
14.6.2 It shall not be possible to isolate the Pressure Relief Valve from the
Hydrogen Components or section of the Hydrogen System that it protects,
by the normal operation or failure of another component.
14.6.3 The vent of a Pressure Relief Valve shall not discharge into a wheel arch,
nor shall it be aimed at a heat source such as the exhaust or at any
Container or Container Assembly. Additionally it shall discharge such that
hydrogen cannot enter the inside of the vehicle.
14.6.4 The vent of the Pressure Relief Valve shall be protected against blockage,
e.g. by dirt, ice, and ingress of water etc., so far as is reasonably
practicable.
14.7.1 Rigid Fuel Lines shall be secured such that they shall not be subjected to
critical vibration or other stresses.
14.7.2 Flexible Fuel Lines shall be secured such that they shall not be subjected
to torsional stresses and abrasion is avoided.
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14.7.3 Rigid Fuel Lines and Flexible Fuel Lines shall be designed to reasonably
minimise stresses in the lines during removal or installation of adjoining
Hydrogen Components.
14.7.4 At fixing points, Rigid Fuel Lines and Flexible Fuel Lines shall be fitted in
such a way that galvanic and crevice corrosion are prevented.
14.7.5 Rigid Fuel Lines and Flexible Fuel Lines shall be routed to reasonably
minimise exposure to accidental damage whether inside the vehicle, e.g.
due to placing or movement of luggage or other loads, or outside the
vehicle, e.g. due to rough ground or vehicle jacks etc.
14.7.6 At passages through the vehicle body or other Hydrogen Components, the
fuel lines shall be fitted with grommets or other protective material.
14.7.8 Class 0 metallic Rigid Fuel Lines shall be seamless and shall elongate by
at least 14% before rupture.
14.8.1 The materials used in Fittings shall be chosen in such a way that galvanic
and crevice corrosion are prevented.
14.8.3 Any joints shall be made in locations where access is possible for
inspection and also for leak testing.
14.9.1 The Receptacle shall be secured against maladjustment and rotation. The
Receptacle shall also be protected from unauthorised interference, and the
ingress of dirt and water so far as is reasonably practicable, e.g. a locked
hatch. It shall be safe against reasonably foreseeable handling errors.
14.9.2 The Receptacle shall be installed such that access for refilling shall not be
required in the passenger, luggage, or in any other unventilated
compartment.
14.9.3 The Receptacle shall not be mounted within the external energy absorbing
elements, e.g. bumper.
14.9.4 The Nominal Working Pressure of the Receptacle shall be equal to the
Nominal Working Pressure of the Class 0 Hydrogen Components upstream
of and including the First Pressure Regulator.
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Part II
14.9.6 A label shall be provided close to the Receptacle, for example, inside a
refilling hatch, showing the following information:
H2 GAS
“xx” MPa
where “xx” = Nominal Working Pressure of the Container(s).
14.10.2 The ventilation opening of the gas tight housing shall be at the highest
point of the housing when installed in the vehicle. It shall not ventilate into a
wheel arch, nor shall it be aimed at a heat source such as the exhaust.
Additionally it shall vent such that hydrogen cannot enter the inside of the
vehicle.
14.10.3 The electrical connections and components in the gas tight housing shall
be constructed such that no sparks are generated.
14.10.4 During testing the vent line shall be hermetically sealed and the gas tight
housing shall then meet the leakage requirements of Paragraph 14.1.10 of
this Regulation at an over pressure of 0.01 MPa and without any
permanent deformations.
14.10.5 Any connecting system shall be secured by clamps, or other means, to the
gas tight housing or sleeve and the lead-through to ensure that a joint is
formed meeting the leakage requirements of Paragraph 14.10.4 of this
Regulation.
14.11.2 The metallic components of the Hydrogen System shall have electrical
continuity with the vehicle’s earth, e.g. chassis.
14.11.3 During the refilling process the Hydrogen System shall have the means to
provide electrical continuity with the refilling facilities before hydrogen
transfer is permitted.
14.11.4 Power supply connections shall not permit the ingress of hydrogen where
hydrogen leaks are possible.
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Revision 12b, 12.10.03
Part II
14.14.2 The label shall be installed on the front and rear of the vehicle and one to
the side of each set of doors.
15.1 Every modification of the Vehicle Type or of its installation of Specific Components
for the use of hydrogen shall be notified to the Administrative Department that
granted approval of the Vehicle Type. The Administrative Department may then
either:
i) Consider that the modifications made are unlikely to have an appreciably
adverse effect, and that the vehicle still complies with the requirements of this
Regulation;
or
ii) Require a further report from the Technical Service responsible for carrying out
the tests.
15.3 The competent authority issuing the extension of approval shall assign a series
number to each communication form (specified in Paragraph 13.3 of this Regulation)
issued for such an extension.
16 CONFORMITY OF PRODUCTION
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Revision 12b, 12.10.03
Part II
The conformity of production procedures shall comply with those set out in the
Agreement, Appendix 2 (E/ECE/324- E/ECE/TRANS/505/rev.2) and with the following
requirements:
i) A Vehicle Type, type approved according to this Regulation shall be
manufactured so as to conform to the type approved by meeting the
requirements specified in Paragraph 14 of this Regulation.
ii) The approval authority that has granted type approval may at any time verify the
conformity control methods applied in each production facility. The normal
frequency of these verifications shall be once every two years.
17.1 The type approval granted in respect of a Vehicle Type in accordance with this
Regulation may be withdrawn if the requirements laid down in Paragraph 16 of this
Regulation are not complied with.
17.2 If a Contracting Party to the Agreement that applies this Regulation withdraws an
approval it has previously granted, it shall immediately notify the other Contracting
Parties applying this Regulation by means of a communication form conforming to
the model in Annex 6 to this Regulation.
The Parties to the Agreement applying this Regulation shall communicate to the
United Nations Secretariat the names and addresses of the Technical Services
responsible for conducting approval tests and of the Administrative Departments
which grant approval and to which forms certifying approval or extension or refusal or
withdrawal of approval issued in other countries, are to be sent.
29 CGH2R-12b.doc
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Revision 12b, 12.10.03
Annex 1
Annex 1
1 Automatic Valve:
1.1 Make:
1.2 Type:
1.5 Material(s):
2 Non-return Valve:
2.1 Make:
2.2 Type:
2.5 Material(s):
4 Fittings:
4.1 Make:
4.2 Type:
4.5 Material(s):
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Revision 12b, 12.10.03
Annex 1
*1
5 Flexible Fuel Lines: yes/no
5.1 Make:
5.2 Type:
5.5 Material(s):
6.1 Make:
6.2 Type:
6.5 Material(s):
7.1 Make:
7.2 Type:
7.5 Material(s):
8.1 Make:
8.2 Type:
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Revision 12b, 12.10.03
Annex 1
8.5 Material(s):
9.1 Make:
9.2 Type:
9.5 Material(s):
10.1. Make:
10.2 Type:
10.3 Drawings:
11.1 Make:
11.2 Type:
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Revision 12b, 12.10.03
Annex 1
11.6 Material:
2
11.7 Set (trigger) temperature: *
12.1 Make:
12.2 Type:
12.5 Material:
13 Receptacle:
13.1 Make:
13.2 Type:
13.5 Material:
14.1 Make:
14.2 Type:
14.5 Material:
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Revision 12b, 12.10.03
Annex 1
Notes:
*1 - Strike out what does not apply.
2
* - Specify the tolerance.
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Revision 12b, 12.10.03
Annex 2
Annex 2
0.1 Make:
0.2 Type(s):
1 Description Of The Hydrogen System Used For The propulsion Of The Vehicle *1
1.4.1 Make(s):
1.4.2 Type(s):
1.5.1 Make(s):
1.5.2 Type(s):
1.6.1 Make(s):
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Revision 12b, 12.10.03
Annex 2
1.6.2 Type(s):
1.7.1 Make(s):
1.7.2 Type(s):
1.8 Fittings:
1.8.1 Make(s):
1.8.2 Type(s):
1.9.1 Make(s):
1.9.2 Type(s):
1.10.1 Make(s):
1.10.2 Type(s):
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Revision 12b, 12.10.03
Annex 2
1.11.1 Make(s):
1.11.2 Type(s):
1.12.1 Make(s):
1.12.2 Type(s):
1.13.1 Make(s):
1.13.2 Type(s):
1.14.1 Make(s):
1.14.2 Type(s):
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Revision 12b, 12.10.03
Annex 2
1.15.1 Make(s):
1.15.2 Type(s):
2
1.15.3 Normal maximum operating temperature: * °C
(in accordance with Paragraph 2.4.5 of this Regulation)
1.16.1 Make(s):
1.16.2 Type(s):
1.17 Receptacle:
1.17.1 Make(s):
1.17.2 Type(s):
1.18.1 Make(s):
1.18.2 Type(s):
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Revision 12b, 12.10.03
Annex 2
2 Description Of The Hydrogen System(s) Used For Purposes Other Than The
Propulsion Of The Vehicle *1
2.3 Manufacturer's system code(s) (as marked on the system, or other means of
identification):
1
2.4 Automatic Valve(s): yes/ same component as used in Propulsion System *
2.4.1 Make(s):
2.4.2 Type(s):
2.5.1 Make(s):
2.5.2 Type(s):
2.6.1 Make(s):
2.6.2 Type(s):
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Revision 12b, 12.10.03
Annex 2
2.7.1 Make(s):
2.7.2 Type(s):
2.8.1 Make(s):
2.8.2 Type(s):
2.9.1 Make(s):
2.9.2 Type(s):
2.10.1 Make(s):
2.10.2 Type(s):
2.11.1 Make(s):
2.11.2 Type(s):
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Revision 12b, 12.10.03
Annex 2
2.12.1 Make(s):
2.12.2 Type(s):
2.13.1 Make(s):
2.13.2 Type(s):
2.14.1 Make(s):
2.14.2 Type(s):
2.15 Pressure Relief Device: yes/ same component as used in Propulsion System
*1
2.15.1 Make(s):
2.15.2 Type(s):
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Revision 12b, 12.10.03
Annex 2
2
2.15.3 Normal maximum operating temperature: * °C
(in accordance with Paragraph 2.4.5 of this Regulation)
2.16.1 Make(s):
2.16.2 Type(s):
2.17.1 Make(s):
2.17.2 Type(s):
2.18.1 Make(s):
2.18.2 Type(s):
3 Further documentation:
42 CGH2R-12b.doc
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Draft ECE Compressed Gaseous Hydrogen Regulation
Revision 12b, 12.10.03
Annex 2
3.2 System layout including electrical connections, and other external system
inputs or outputs, etc.
Notes:
43 CGH2R-12b.doc
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Revision 12b, 12.10.03
Annex 3
Annex 3
a
a
2
E1 a
3
xx R-002439
Where: a ≥ 4 mm
The above approval mark affixed to the Hydrogen Component shows that this component
has been type approved in Germany (E1), pursuant to the Regulation No. xx under approval
number 002439. The first two digits of the approval number indicate that the approval was
granted in accordance with the requirements of Regulation No. xx in its original form.
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Revision 12b, 12.10.03
Annex 4
Annex 4
*1
E ...
2
Concerning: APPROVAL GRANTED *
APPROVAL EXTENDED *2
APPROVAL REFUSED *2
APPROVAL WITHDRAWN *2
PRODUCTION DEFINITELY DISCONTINUED *2
of a Specific Component pursuant to Regulation No. xx
Approval No.: ................................... Extension No.: ................…………
1. Specific Component considered:
Automatic Valve *2
Non-return Valve *2
Container *2
Fittings *2
Flexible Fuel Line *2
Heat exchanger *2
Hydrogen Filter
Hydrogen Sensor
Manual Valve *2
Pressure sensor *2
Temperature sensor *2
Flow sensor *2
Pressure or hydrogen remaining indicator
Pressure Regulator *2
Pressure Relief Device *2
Pressure Relief Valve *2
Receptacle *2
Removable Storage System Connector *2
45 CGH2R-12b.doc
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Revision 12b, 12.10.03
Annex 4
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Revision 12b, 12.10.03
Annex 5
Annex 5
Model A
(See Paragraph 13.4 of this Regulation)
a
a
2
E1 a
3
xx R-002439
Where: a ≥ 8 mm
The above approval mark affixed to a vehicle shows that the vehicle has, with regard to the
installation of a Hydrogen System for the use of compressed gaseous hydrogen, has been
type approved in Germany (E1), pursuant to the Regulation No. xx under approval number
002439. The first two digits of the approval number indicate that the approval was granted in
accordance with the requirements of Regulation No. xx in its original form.
Model B
(See Paragraph 13.4 of this Regulation)
a
a
2
E1 a
3
xx 002439
83 021628
Where: a ≥ 8 mm
The above approval mark affixed to a vehicle shows that the vehicle has been type approved
in Germany (E1), pursuant to the Regulation Nos. xx and 83. The approval numbers indicate
that, at the dates when the respective approvals were given, Regulation No. xx was in its
original form and Regulation No. 83 included the 02 series of amendments
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Revision 12b, 12.10.03
Annex 6
Annex 6
*1
E ...
2
Concerning: APPROVAL GRANTED *
APPROVAL EXTENDED *2
APPROVAL REFUSED *2
APPROVAL WITHDRAWN *2
2
PRODUCTION DEFINITELY DISCONTINUED *
of a Vehicle Type with regard to the installation of a Hydrogen System pursuant to
Regulation No. xx
Approval No.: ................................………... Extension No.: ...............……………….….
1. Trade name or mark of vehicle: . . . . . . . . . . . . . . . . . . . . . . . . . . . .
2. Vehicle Type: . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
3. Vehicle category: . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
4. Vehicle manufacturer’s name and address: . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
5. If applicable, name and address of vehicle manufacturer’s representative: . . . . . .
. . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
6. Description of the vehicle with regard to the installation of Hydrogen System (add
drawing if appropriate): . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
7. Hydrogen System
7.1 Trade name or mark of components and their approval numbers:
7.1.1 Container or Container Assembly: . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . .
7.1.2 Other components: . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . .
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Revision 12b, 12.10.03
Annex 6
Drawings, diagrams and scheme plans regarding the components and the installation of the
Hydrogen System considered to be of importance for the purpose of this Regulation:
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Where applicable drawings of the various equipment and their position in the vehicle:
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
____________
Notes:
*1 Distinguishing number of the country that has granted/extended/refused/withdrawn
approval (see approval provisions in the Regulation).
2
* Strike out what does not apply
49 CGH2R-12b.doc
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Revision 12b, 12.10.03
Annex 7
Annex 7
Contents Page
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Revision 12b, 12.10.03
Annex 7
Annex 7: Part A
A1 REFERENCES
The following standards contain provisions that, through reference in this text,
constitute provisions of this Annex. Where standards other than ISO standards are
referenced they may be replaced by equivalent national standards.
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Revision 12b, 12.10.03
Annex 7
A2 GENERAL REQUIREMENTS
A2.1 GENERAL
The service conditions do not include external loads that may arise from vehicle
collisions, or integration of the Container into the vehicle, etc. Containers need not be
designed for continuous exposure to mechanical or chemical attack, e.g. leakage
from cargo that may be carried on vehicles or severe abrasion damage from road
conditions.
The Container, Pressure Relief Device(s) and any added insulation or protective
material shall collectively protect the Container from rupture when exposed to fire.
The arrangement of the fire protection system shall be specified.
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Revision 12b, 12.10.03
Annex 7
Openings with tapered or straight threads may be used in all Container Types.
Threads shall comply with a recognised international or national standard. Threads
shall be clean cut, even, without surface discontinuities, and to gauge.
Any coatings applied to Containers shall be such that the application process does
not adversely affect the mechanical properties of the Container. The coating shall
facilitate subsequent in-service inspection and the Manufacturer shall provide
guidance on coating treatment during such inspection to ensure the continued
integrity of the Container.
A3 APPROVAL REQUIREMENTS
A3.1 GENERAL
Document Annex 7
Reference
Statement Of Service A3.2
Container Drawings A3.3
Material Specifications and Test Data A3.4
Container Specifications and Test Data A3.5
Manufacturing Data A3.6
Stress Analysis A3.7
The Manufacturer's statement of service and all necessary information to ensure the
proper handling, use and in-service inspection of the Container shall be supplied to
the purchaser of the Container.
The statement of service shall include the information given in Table 7A.2 as a
minimum.
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Revision 12b, 12.10.03
Annex 7
A detailed description of all principal material properties and tolerances used in the
Container design shall be provided according to Table 7A.3. The material
specifications shall be verified by appropriate material tests and the results from
these tests shall be provided according to Table 7A.3.
If more samples than required are tested, all results shall be documented.
The Container design specifications for each test that is required shall be provided
according to Table 7A.4. The design specifications shall be verified by appropriate
Container tests and the results from these tests shall be provided according to Table
7A.4.
All results shall be documented if more Containers or Liners than required are tested.
54 CGH2R-12b.doc
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Revision 12b, 12.10.03
Annex 7
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Revision 12b, 12.10.03
Annex 7
Applicable to Material
Material Specification
Aluminium Alloy
Plastic Liner
Details
Coating
Resin
Fibre
Steel
Material Manufacturer
Type of Material
Material Identification
Heat Treatment Definition
Chemical Composition
Cold- or Cryoforming Procedure
1 1
Welding Procedure Definition * *
Specified
Technical Service:
Inspector’s signature:
Place, Date:
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Revision 12b, 12.10.03
Annex 7
Notes:
1
* –
For Containers with welded Liners only.
2
* –
i) For steel Containers or Liners refer to Paragraph 10.2 of ISO 9809-1 or
Paragraph 10.2 of ISO 9809-2 as appropriate,
ii) For stainless steel Containers or Liners refer to Paragraph 7.1.2.1 of EN
1964-3,
iii) For welded stainless steel Liners refer to Paragraph 8.4 of EN 13322-2.
iv) For aluminium alloy Containers or Liners refer to Paragraph 10.2 of ISO 7866,
v) For welded aluminium alloy Liners refer to Paragraphs 7.2.3 and 7.2.4 of EN
12862,
vi) For non-metallic Liners refer to Paragraph B1 of this Annex.
3
* –
i) For steel Containers or Liners refer to Paragraph 10.4 of ISO 9809-1 or
Paragraph 10.4 of ISO 9809-2 as appropriate,
ii) For stainless steel Containers or Liners refer to Paragraph 7.1.2.4 of EN
1964-3,
iii) For welded stainless steel Liners refer to Paragraph 8.6 of EN 13322-2.
*4 –
i) For welded stainless steel Liners refer to Paragraph 8.5 of EN 13322-2,
ii) For welded aluminium alloy Liners refer to Paragraphs 7.2.5, 7.2.6 and 7.2.7
of EN 12862.
*5 –
For welded stainless steel Liners refer to Paragraph 8.7 of EN 13322-2.
*6 –
i) For aluminium alloy Containers or Liners refer to Annex A of ISO 7866,
ii) For welded aluminium alloy Liners refer to Annex A of EN 12862.
*7 –
i) For aluminium alloy Containers or Liners refer to Annex B of ISO 7866, but
excluding the second paragraph of Clause B.2,
ii) For welded aluminium alloy Liners refer to Annex B of EN 12862, but
excluding Paragraph B.2.2.
*8 –
i) This test is not required for:
a) Steels that conform to Paragraphs 6.3 and 7.2.2 of ISO 9809-1,
b) Aluminium alloys that conform to Paragraph 6.1 of ISO 7866,
ii) For other metallic Containers or Liners hydrogen compatibility of the material,
including welds, shall be demonstrated in accordance with ISO 11114-1,
ISO/DIS 11114-4 or Paragraph B7 of this Annex as appropriate,
iii) For non-metallic materials hydrogen compatibility shall be
demonstrated.
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Revision 12b, 12.10.03
Annex 7
Applicable To
Specified
Test and Annex 7 Reference Container Type Test Value
Design Value
1 2 3 4
B9 Burst Test
B10 Ambient Temperature Pressure
Cycling Test
B11 LBB Performance Test
B12 Bonfire Test
B13 Penetration Test
B14 Chemical Exposure Test
B15 Composite Flaw Tolerance Test
B16 Accelerated Stress Rupture Test
B17 Extreme Temperature Pressure
Cycling Test
B18 Impact Damage Test
B19 Leak Test
B20 Permeation Test
B21 Boss Torque Test
B22 Hydrogen Gas Cycling Test
Container Identification:
Manufacturer:
Name, position and signature:
Place, Date:
Technical Service:
Inspector’s signature:
Place, Date:
A stress analysis shall be carried out. A table summarising the calculated stresses
shall be provided for information purposes only.
A3.8.1 General
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Annex 7
A3.8.2 Steel
A3.8.2.1 Steels for Containers and Liners shall conform to the material
requirements of Paragraphs 6.1 to 6.4 of ISO 9809-1or
Paragraphs 6.1 to 6.3 of ISO 9809-2 as appropriate.
A3.8.3.1 Aluminium alloys for Containers and Liners shall conform to the
material requirements of Paragraphs 6.1 and 6.2 of ISO 7866.
A3.8.5 Fibres
The Container Manufacturer shall keep on file for the intended life of the
Container design the published specifications for composite materials
including principal test results, i.e. tensile test, the material Manufacturer’s
recommendations for storage, conditions and shelf life.
The Container Manufacturer shall keep on file, for the intended life of each
batch of Containers, the fibre Manufacturer’s certification that each shipment
conforms to the Manufacturer’s specifications for the product.
A3.8.6 Resins
The minimum Burst Pressure ratios, i.e. the minimum actual Burst Pressure of the
Container divided by its Nominal Working Pressure, shall not be less than the values
given in Table 7A.5.
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Revision 12b, 12.10.03
Annex 7
Container Type
Construction Type 1 Type 2 Type 3 Type 4
All metal 2.25
Glass 2.75 3.65 3.65
1
(2.50* ) (3.50*1)
Over-wrap
A forming process shall not be used to close the ends of aluminium alloy Containers.
The base ends of steel Containers that have been closed by forming, shall be
inspected using NDE or equivalent techniques. Metal shall not be added in the
process of closure at the end. Each Container shall be examined before end forming
operations for thickness and surface finish.
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Revision 12b, 12.10.03
Annex 7
After end forming, Containers shall be heat treated to the hardness range specified
for the design. Localised heat treatment is not permitted.
When a neck ring, foot ring or attachments for support are provided, it shall be of
material compatible with that of the Container and shall be securely attached by a
method other than welding, brazing or soldering.
The maximum curing time and temperature for Containers with aluminium
alloy Liners shall be below the time and temperature that adversely affect the
properties of the metal.
For Type 4 Containers the curing temperature for thermosetting resins shall
be at least 10 °C below the softening temperature of the plastic Liner.
A4.2.3 Auto-frettage
Auto-frettage, if used, shall be carried out before the hydraulic test. The Auto-
frettage Pressure shall be within the limits established by the Manufacturer.
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Welding of stainless steel Liners shall conform to Paragraphs 6.1, 6.2 and 6.4
of EN 13322-2. Welding of aluminium alloy Liners shall conform to
Paragraphs 4.1.2 and 6.1 of EN 12862.
A5.1.1 General
The Manufacturer shall conduct batch testing on Finished Containers that are
representative of normal production. The Finished Containers to be tested
shall be randomly selected from each Batch. A Batch shall not exceed 200
Finished Containers plus those Finished Containers to be used in destructive
tests, or one shift of successive production, whichever is greater.
With reference to Table 7A.6, the following batch tests are required:
i) One Finished Container shall be subjected to the ambient temperature
pressure cycle test at the frequency given in Paragraph A5.1.2 of this
Annex,
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If more Containers than required are subjected to the tests, all results shall be
documented.
All Containers represented by a batch test that fail to meet the specified
requirements shall follow the procedures specified in Paragraph A5.2 of this
Annex.
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Applicable To Specified
Test
Test and Annex Reference Container Type Design
Value
1 2 3 4 Value
*1 Tensile Test *5 *5 *5
*2 Charpy Impact Test *5 *5
3 5
* Bend Test *
4 5
* Macroscopic Examination *
5
B2 Softening/Melting Temp. Test *
B6 Coating Batch Test
B9 Burst Test
B10 Ambient Temperature Pressure *6
Cycle Test
B19 Leak Test *6
B21 Boss Torque Test *6
Notes:
1
* –
i) For steel Containers or Liners refer to Paragraph 10.2 of ISO 9809-1 or
Paragraph 10.2 of ISO 9809-2 as appropriate,
ii) For stainless steel Containers or Liners refer to Paragraph 7.1.2.1 of EN 1964
-3,
iii) For welded stainless steel Liners refer to Paragraph 8.4 of EN 13322-2.
iv) For aluminium alloy Containers or Liners refer to Paragraph 10.2 of ISO 7866,
v) For welded aluminium alloy Liners refer to Paragraphs 7.2.3 and 7.2.4 of
EN12862,
vi) For non-metallic Liners refer to Paragraph B1 of this Annex.
*2 –
i) For steel Containers or Liners refer to Paragraph 10.4 of ISO 9809-1 or
Paragraph 10.4 of ISO 9809-2 as appropriate,
ii) For stainless steel Containers or Liners refer to Paragraph 7.1.2.4 of EN
1964-3,
iii) For welded stainless steel Liners refer to Paragraph 8.6 of EN 13322-2.
*3 –
i) For welded stainless steel Liners refer to Paragraph 8.5 of EN 13322-2,
ii) For welded aluminium alloy Liners refer to Paragraphs 7.2.5, 7.2.6 and 7.2.7
of EN 12862.
*4 –
For welded stainless steel Liners refer to Paragraph 8.7 of EN 13322-2.
*5 –
Test on Liner material.
*6 –
The following test sequence shall be used for Container Type 4: Boss Torque Test
(B21), followed by an Ambient Temperature Pressure Cycling Test (B10), followed
by a Leak Test (B19).
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In the event of failure to meet the test requirements, retesting or reheat treatment and
retesting shall be carried out as follows:
i) If there is evidence of a fault in carrying out a test, or an error of
measurement, a further test shall be performed. If the result of this test is
satisfactory, the first test shall be ignored,
ii) If the test has been carried out in a satisfactory manner, the cause of the test
failure shall be identified.
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If the failure is considered to be due to the heat treatment applied, the Manufacturer
may subject all the Containers of that Batch to a further heat treatment.
If the failure is not due to the heat treatment applied, all the identified defective
Containers shall be rejected or repaired by an approved method. The non-rejected
Containers shall then be considered as a new Batch.
In both cases all the relevant prototype or batch tests needed to prove the
acceptability of the new Batch shall be repeated. If one or more tests prove even
partially unsatisfactory, all Containers of the Batch shall be rejected.
Production examination and tests shall be carried out on all Containers during
manufacture and after completion, as follows:
i) Verification that the principal dimensions and mass of the Finished Container and
of any Liner and Over-wrap are within design tolerances,
ii) Verification of compliance with principal manufacturing parameters, in
accordance with Paragraph A3.6 of this Annex, including examination of any
specified surface finish with special attention to deep drawn surfaces and folds or
laps in the neck or shoulder of forged or spun end enclosures or openings,
iii) For metallic Containers and Liners, NDE in accordance with Annex B of ISO
9809 or Annex C of EN 1964-3 or Annex B of EN 13322-2 as appropriate, or a
demonstrated equivalent method capable of detecting the maximum defect size
allowed, to verify that the maximum defect size does not exceed the size
specified in the design as determined below.
The design of Type 1, 2 and 3 Containers shall identify the maximum allowable
defect size at any location in the metal Container or Liner that will not grow to a
critical size within either the specified retest period or Service Life if no retest is
specified. The critical defect size is defined as the limiting through-wall
(Container or Liner) thickness defect that would allow stored gas to be
discharged without rupturing the Container. Defect sizes for the rejection criteria
for ultrasonic scanning or equivalent, shall be smaller than the maximum
allowable defect sizes. For Type 2 and 3 Containers, it shall be assumed that
there is no damage to non-metallic materials due to any time-dependent
mechanisms. The allowable defect size for NDE shall be determined by an
appropriate method.
iv) Hardness test for metallic Containers and Liners in accordance with Paragraph
B8 of this Annex and fulfil the requirements therein,
v) Hydraulic test, in accordance with Paragraph B23 of this Annex and fulfil the
requirements therein,
vi) Leak test for Type 4 Containers, in accordance with Paragraph B19 of this Annex
and fulfil the requirements therein,
vii) Verification of markings, in accordance with Paragraph A4.3 of this Annex.
A summary of the required production examination and tests for each Container is
provided in Table 7A.7.
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Applicable To
Production Examination And Tests
Container Type
& Annex 7 Reference
1 2 3 4
Principal Design Dimensions
A3.6 Principal Manufacturing
Parameters
NDE *1 *1
B8 Hardness Test *1 *1
B19 Leak Test
B23 Hydraulic Test
A4.3 Markings
Note:
*1 - Test on metallic Liner
A7 MODIFICATIONS
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Type Of Test
Table 7A.8:
pressure Cycling
Permeation B20
Impact Damage
Ambient Temp.
Rupture – B16
as applicable
Approval Testing Of
Compatibility
Performance
Table 7A.3
Cycling B22
Penetration
Acc. Stress
Note * to
Tolerance
Hydrogen
Hydrogen
Exposure
Chemical
Materials
B1 – B8,
Bonfire
Modifications
Burst
8
Test
LBB
B10
B11
B12
B13
B14
B15
B18
B9
Fibre Manufacturer 2, 3, 4 2, 3, 4 2, 3, 4 2, 3, 4 3, 4
Metallic Container Or Liner Material 1, 2, 3 1, 2, 3 1, 2, 3 1, 2, 3 1, 2 1, 2, 3 1, 2, 3 1, 2, 3 2, 3 2, 3 3
Plastic Liner Material 4 4 4 4 4
Fibre Material 2, 3, 4 4 2, 3, 4 2, 3, 4 2, 3, 4 2, 3, 4 2, 3, 4 2, 3, 4 2, 3, 4 2, 3, 4 3, 4
Resin Material 4 2, 3, 4 2, 3, 4 2, 3, 4 2, 3, 4 3, 4
Diameter Change ≤20% 1, 2, 3, 4 1, 2, 3, 4
Diameter Change >20% 1, 2, 3, 4 1, 2, 3, 4 1, 2, 3, 4 1, 2, 3, 4 2, 3, 4 3, 4
Length Change ≤ 50% 1, 2, 3, 4 -
Length Change> 50% 1, 2, 3, 4 1, 2, 3, 4 1, 2, 3, 4 3, 4
Nominal Working Pressure Change 1, 2, 3, 4 1, 2, 3, 4
1
≤20% *
Nominal Working Pressure Change 1, 2, 3, 4 1, 2, 3, 4 1, 2, 3, 4 1, 2, 3, 4 1, 2, 3, 4
1
>20% *
Dome Shape 1, 2, 3, 4 1, 2, 3, 4 4
Opening Size 1, 2, 3, 4 1, 2, 3, 4
Coating Change 2, 3, 4 2, 3, 4
2
End Boss Design 4*
3
Change In Manufacturing Process* 1, 2, 3, 4 1, 2, 3, 4
Fire Protection System 1, 2, 3, 4
Notes: For example: 2,3 indicates that a test is required for Type 2 and 3 Containers only
1
* - Only when thickness change is proportional to diameter or pressure change
2
* - A hydrogen cycle test is not required if the stresses in the neck are equal to the original or reduced by the design change (e.g. reducing the diameter of
internal threads, or changing the boss length), the liner to boss interface is not affected, and the original materials are used for boss, liner, and seals.
3
* – Any deviation from the parameters specified in Paragraph A3.6 of this Annex is considered to be a change in manufacturing process.
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Annex 7: Part B
B1 TENSILE TEST
B1.1 Sampling
B1.2 Procedure
B1.3 Requirements
B1.4 Results
The tensile yield strength and ultimate elongation of plastic Liner materials shall be
presented in a test summary, e.g. Table 7A.3 of this Annex.
B2.1 Sampling
B2.2 Procedure
B2.3 Requirement
B2.4 Results
The softening temperature shall be presented in a test summary, e.g. Table 7A.3 of
this Annex.
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B3.1 Sampling
B3.2 Procedure
B3.3 Requirements
B3.4 Results
Final results from the test shall be documented by a test report and presented in a
test summary, e.g. Table 7A.3 of this Annex. The glass transition temperature to be
presented shall be the minimum measured value.
B4.1 Sampling
B4.2 Procedure
B4.3 Requirement
After boiling in water for 24 hours the minimum shear strength of the composite shall
be 13.8 MPa.
B4.4 Results
The minimum resin shear strength shall be presented in a test summary, e.g. Table
7A.3 of this Annex.
B5 COATING TEST
B5.1 Sampling
The test applies to all Container Types where exterior environmental protective
coating is used, e.g. organic coating/paint.
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B5.3 Results
Final results from the test shall be presented in a test summary, e.g. Table 7A.3 of
this Annex.
B6.1 Sampling
The test applies to all Container Types where exterior environmental protective
coating is used, e.g. organic coating/paint.
Batch testing - Number of Containers/samples to be tested per Batch: In
accordance with Paragraph A5.1 of this Annex.
B6.3 Results
Final results from the test shall be presented in a test summary, e.g. Table 7A.3 of
this Annex.
The Manufacturer shall keep the coating thickness and adhesion strength values on
file throughout the Service Life of the Container.
B7.1 Sampling
The test applies to Type 1, 2 and 3 Containers in accordance with Note *8 to Table
7A.3 of this Annex.
B7.2 Procedure
At ambient temperature use hydrogen to pressure cycle for 3.0 times the number of
Filling Cycles in accordance with Paragraph 2.4.6 of this Regulation, either:
i) The Container between 2.0 MPa and 1.25 times the Nominal Working
Pressure,
or
ii) The Liner between the pressure levels that will provide an equivalent Liner wall
stress as would be present at 2.0 MPa and 1.25 times the Nominal Working
Pressure for the Container.
B7.3 Requirement
The Containers or Liners shall not fail before reaching 3.0 times the number of Filling
Cycles in accordance with Paragraph 2.4.6 of this Regulation.
B7.4 Results
Final results from the test shall be documented by a test report and presented in a
test summary, e.g. Table 7A.3 of this Annex.
The Manufacturer shall keep the results on file throughout the Service Life of the
Container.
B8 HARDNESS TEST
B8.1 Sampling
The test applies to all Containers and Liners of Type 1, 2 and 3 Containers.
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The test shall be carried out after the final heat treatment.
B8.2 Procedure
A hardness test shall be carried out on the parallel wall at the centre and at one of
the domed ends of each Container or Liner in accordance with ISO 6506-1.
B8.3 Requirement
The hardness value shall be in the range specified for the design.
B8.4 Results
The hardness value shall be presented in a test summary, e.g. Table 7A.3 of this
Annex.
The Manufacturer shall keep the results on file throughout the Service Life of the
Container.
B9 BURST TEST
B9.1 Sampling
B9.2 Procedure
The Container shall be hydraulically burst tested at ambient temperature using the
following procedure:
The rate of pressurisation shall be 1.4 MPa/s for pressures higher than 80% of the
Nominal Working Pressure times the Burst Pressure ratio stated in Paragraph A3.9 of
this Annex. If the rate exceeds 0.35 MPa/s at pressures higher than 80% of the
Nominal Working Pressure times the Burst Pressure ratio, then either the Container
shall be placed in series between the pressure source and the pressure
measurement device, or the time at pressure above the Nominal Working Pressure
times the Burst Pressure ratio shall exceed 5 seconds.
B9.3 Requirement
The Burst Pressure of the Container shall exceed the Nominal Working Pressure
times the Burst Pressure ratio stated in Paragraph A3.9 of this Annex.
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The Burst Pressure of the Liner shall exceed 1.25 times the Nominal Working
Pressure.
B9.4 Results
The Burst Pressure shall be presented in a test summary, e.g. Table 7A.4 of this
Annex.
The Manufacturer shall keep the Burst Pressure value on file throughout the Service
Life of the Container.
B10.1 Sampling
B10.2 Procedure
For type approval, Containers shall be cycled until failure occurs or up to 9 times the
number of Filling Cycles.
For batch testing, Containers shall be destroyed either by continuing the cycling until
failure occurs or in accordance with the burst testing procedure of Paragraph B9.2 of
this Annex. For batch testing of Type 4 Containers, the test sequence given in Note *6
to Table 7A.6 to this Annex shall be followed before destroying the Container.
B10.3 Requirement
The Containers shall not fail before reaching 3.0 times the number of Filling Cycles in
accordance with Paragraph 2.4.6 of this Regulation. For type approval, the
Containers shall either reach 9.0 times the number of Filling Cycles without failure, in
which case the LBB test in Paragraph B19 of this Annex is not required, or they shall
fail by leakage and not by rupture.
B10.4 Results
The number of cycles to failure, along with the location and description of the failure
initiation shall be documented and presented in a test summary, e.g. Table 7A.4 of
this Annex.
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The Manufacturer shall keep the results on file throughout the Service Life of the
Container.
B11.1 Sampling
The test applies to all Container Types. The test is not required if the Container
design is already proven to exceed 9.0 times the number of Filling Cycles in
accordance with Paragraph 2.4.6 of this Regulation, when tested in accordance with
Paragraph B10 of this Annex.
Type approval testing - Number of Finished Containers to be tested: 3
B11.2 Procedure
B11.3 Requirement
The Containers tested shall either fail by leakage or shall exceed 3.0 times the
number of Filling Cycles in accordance with Paragraph 2.4.6 of this Regulation
without failure.
B11.4 Results
The number of cycles to failure, along with the location and description of the failure
initiation, shall be presented in a test summary, e.g. Table 7A.4 of this Annex.
B12.1 Sampling
B12.2 Procedure
iii) If the Container is > 1.65 m and it is fitted with a Pressure Relief Device at only
one end, the fire source shall commence at the opposite end,
iv) If the Container is > 1.65 m and it is fitted with Pressure Relief Devices at more
than one location along its length, the centre of the fire source shall be centred
midway between those Pressure Relief Devices that are separated by the
greatest horizontal distance,
v) If the Container is > 1.65 m and it is additionally protected by thermal insulation,
2 fire tests shall be performed at Nominal Working Pressure. The Container shall
be positioned centrically above the fire source in one test, while the fire shall
commence at one of the Container ends in the other,
vi) Metallic shielding shall be used to prevent direct flame impingement on Container
valves, Fittings, or Pressure Relief Devices. The metallic shielding shall not be in
direct contact with the Pressure Relief Devices. Any failure during the test of a
valve, Fitting or tubing that is not part of the intended protection system for the
design shall invalidate the result,
vii) Surface temperatures shall be monitored by at least three thermocouples located
along the bottom of the Container and spaced not more than 0.75 m apart.
Metallic shielding shall be used to prevent direct flame impingement on the
thermocouples. Alternatively, thermocouples may be inserted into blocks of metal
measuring less than 25 mm x 25 mm x 25 mm,
viii) The fire source shall provide direct flame impingement on the Container surface
across its entire diameter immediately following ignition,
ix) Thermocouple temperatures and the Container pressure shall be recorded at
intervals of 10 seconds during the test,
x) Within 5 minutes of ignition and for the remaining duration of the test the
temperature of at least one thermocouple shall indicate at least 590 °C,
B12.3 Requirement
The Container shall only vent through the Pressure Relief Device(s) and shall not
rupture.
B12.4 Results
The results shall be presented in a test summary, e.g. Table 7A.4 of this Annex, and
shall include the following data for each Container as a minimum:
i) The elapsed time from ignition of the fire to the start of venting through the
Pressure Relief Device(s),
ii) The maximum pressure and time of evacuation until a pressure 1.0 MPa is
reached.
B13.1 Sampling
B13.2 Procedure
The Container, complete with protective coating, shall be tested in the following
sequence:
i) Pressurise with compressed gas to Nominal Working Pressure ± 1.0 MPa,
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ii) Penetrate at least one sidewall of the Container by an armour piercing bullet
with a diameter of 7.62 mm or greater. The projectile shall impact the sidewall
at an approximate angle of 45°.
B13.3 Requirement
B13.4 Results
The approximate size of the entrance and exit openings and their locations shall be
presented in a test summary, e.g. Table 7A.4 of this Annex.
B14.1 Sampling
B14.2 Procedure
v) Pressure cycle between 2MPa and 1.25 times Nominal Working Pressure
for the number of Filling Cycles calculated in accordance with Paragraph 2.4.6
of this Regulation, at a maximum pressurisation rate of 2.75 MPa/s,
vi) Pressurise to 1.25 times Nominal Working Pressure and hold at that pressure
for a minimum of 24 hours until the elapsed exposure time (pressure cycling
and pressure hold) to the environmental fluids equals at least 48 hours,
vii) Burst Test in accordance with Paragraph B9.2 of this Annex.
B14.3 Requirement
The Container shall achieve a Burst Pressure of 1.8 times Nominal Working
Pressure.
B14.4 Results
The Burst Pressure shall be presented in a test summary, e.g. Table 7A.4 of this
Annex.
B15.1 Sampling
B15.2 Procedure
The Container, complete with protective coating, shall be tested in the following
sequence:
i) Flaws in the longitudinal direction shall be cut into the Over-wrap. The flaws
shall be greater than the visual inspection limits as specified by the
Manufacturer, and at least the following flaws shall be cut in the longitudinal
direction into the Container sidewall:
a) 25mm long by 1.25mm deep,
b) 200mm long by 0.75mm deep.
ii) Pressure cycle the flawed Container between 2.0 MPa and 1.25 times
Nominal Working Pressure at ambient temperature for 3.0 times the number of
Filling Cycles in accordance with Paragraph 2.4.6 of this Regulation.
B15.3 Requirement
The Container shall not leak or rupture within 0.6 times the number of Filling Cycles
in accordance with Paragraph 2.4.6 of this Regulation, but may fail by leakage during
the remaining test cycles.
B15.4 Results
The number of cycles to failure, along with the location and description of the failure
initiation shall be presented in a test summary, e.g. Table 7A.4 of this Annex.
B16.1 Sampling
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B16.2 Procedure
The Container, free of any protective coating, shall be tested in the following
sequence:
i) Pressurise to 1.25 times Nominal Working Pressure for 1000 hours at 85 °C,
ii) Burst Test in accordance with Paragraph B9.2 of this Annex.
B16.3 Requirement
The Container shall achieve a Burst Pressure of 0.85 times the Nominal Working
Pressure times the Burst Pressure ratio given in Paragraph A3.9 of this Annex.
B16.4 Results
The Burst Pressure shall be presented in a test summary, e.g. Table 7A.4 of this
Annex.
B17.1 Sampling
B17.2 Procedure
The Containers, with the composite wrapping free of any protective coating, shall be
hydrostatically cycle tested in the following sequence:
i) Condition for 48 hours with a temperature 85 °C and a relative humidity
95%,
ii) Pressure cycle between 2.0 MPa and 1.25 times Nominal Working
Pressure at a temperature 85 °C and a relative humidity 95%, for 1.5 times
the number of Filling Cycles calculated in accordance with Paragraph 2.4.6 of
this Regulation,
iii) Stabilise at ambient conditions,
iv) Condition the Container and test fluid to a temperature -40 °C as measured
on the Container surface and in the fluid,
v) Pressure cycle between 2.0 MPa and Nominal Working Pressure at -40
°C, for 1.5 times the number of Filling Cycles calculated in accordance with
Paragraph 2.4.6 of this Regulation,
vi) Leak Test*1 in accordance with Paragraph B19 of this Annex,
vii) Burst Test in accordance with Paragraph B9.2 of this Annex.
B17.3 Requirement
The Containers shall be cycle tested without showing evidence of rupture, leakage, or
fibre unravelling.
The Containers shall not burst at less than 85% of the Nominal Working Pressure
times the Burst Pressure ratio given in Paragraph A3.9 of this Annex.
B17.4 Results
The Burst Pressure shall be presented in a test summary, e.g. Table 7A.4 of this
Annex.
B18.1 Sampling
B18.2 Procedure
The surface onto which the Container is dropped shall be a smooth, horizontal
concrete pad or similar rigid floor.
B18.3 Requirements
The Container shall not leak or rupture within 0.6 times the number of Filling cycles
calculated in accordance with Paragraph 2.4.6 of this Regulation, but may fail by
leakage during the remaining test cycles.
B18.4 Results
The number of cycles to failure, along with the location and description of the failure
initiation shall be presented in a test summary, e.g. Table 7A.4 of this Annex.
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B19.1 Sampling
B19.2 Procedure
For batch testing, follow the test sequence given in Note *6 to Table 7A.6 to this
Annex.
B19.3 Requirement
Any leakage detected through cracks, pores, unbonds or similar defects shall cause
the Container to be rejected. Permeation through the wall in accordance with
Paragraph B20 of this Annex is not considered to be leakage.
B19.4 Results
The total leakage value shall be presented in a test summary, e.g. Table 7A.4 of this
Annex. The leakage rate is applicable to tests carried out with 100% hydrogen only.
Leakage rates for other gases or gas mixtures shall be converted to an equivalent
leakage rate to that for 100% hydrogen.
The Manufacturer shall keep the total leakage value on file throughout the Service
Life of the Container.
B20.1 Sampling
B20.2 Procedure
B20.3 Requirement
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3
The steady state permeation rate shall be less than 1.0 Ncm per hour of hydrogen
per litre internal volume of the Container.
B20.4 Results
The steady state permeation rate shall be presented in a test summary, e.g. Table
7A.4 of this Annex.
B21.1 Sampling
B21.2 Procedure
B21.3 Requirement
For type approval, the Container shall meet the leak and burst test requirements.
For batch testing, the Container shall meet the leak test requirements.
B21.4 Results
The applied torque, leakage and Burst Pressure shall be presented in a test
summary, e.g. Table 7A.4 of this Annex. The leakage rate is applicable to tests
carried out with 100% hydrogen only. Leakage rates for other gases or gas mixtures
shall be converted to an equivalent leakage rate to that for 100% hydrogen.
The Manufacturer shall keep the results on file throughout the Service Life of the
Container.
B22.1 Sampling
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B22.2 Procedure
B22.3 Requirement
The Liner and Liner/end boss interface shall be free of any deterioration, such as
fatigue cracking or electrostatic discharge.
B22.4 Results
The total leakage value shall be presented in a test summary, e.g. Table 7A.4 of this
Annex.
B23.1 Sampling
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10%. Elastic expansion is defined as the total expansion less the permanent
expansion (see iii above).
v) Any Container that does not meet the defined expansion limit shall be rejected,
but may still be used for batch test purposes.
B23.3 Results
The results shall be presented in a test summary, e.g. Table 7A.4 of this Annex.
The Manufacturer shall keep the results on file throughout the Service Life of the
Container.
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Annex 8
Annex 8
Contents Page
A1 References
A2 General Requirements
A3 Approval Requirements
B2 Ageing Test
B5 Endurance Test
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Annex 8: Part A
A1 REFERENCES
The following standards contain provisions that, through reference in this text,
constitute provisions of this Annex. Where standards other than ISO standards are
referenced they may be replaced by equivalent national standards.
ISO 6957: 1988 Copper Alloys - Ammonia Test For Stress Corrosion
Resistance
ISO 7866:1999 Gas Cylinders - Refillable Seamless Aluminium Alloy
Gas Cylinders - Design, Construction And Testing
ISO 9227: 1990 Corrosion Tests In Artificial Atmospheres - Salt Spray
Tests
ISO 9809-1:1999 Gas Cylinders - Refillable Seamless Steel Gas Cylinders
- Design, Construction And Testing - Part 1: Quenched
And Tempered Steel Cylinders With Tensile Strength
Less Than 1100 Mpa
ISO 11114-1: 1997 Transportable Gas Cylinders – Compatibility Of Cylinder
And Valve Materials With Gas Contents – Part 1:
Metallic Materials
ISO/DIS 11114-4: 2002 Transportable Gas Cylinders – Compatibility Of
Cylinders And Valve Materials With Gas Contents – Part
4: Test Methods For Selecting Metallic Materials
Resistant To Hydrogen Embrittlement
ISO/WD 17268: 2001 Gaseous Hydrogen – Land Vehicle Filling Connectors
A2 GENERAL REQUIREMENTS
A2.1 Unless otherwise stated in this Annex all tests shall be performed at 20°C ± 5°C.
A2.2 Explosive gas mixtures shall be prevented from developing during the test
procedures described in this Annex.
A2.3 The test period for leakage and pressure tests shall be not less than 3 minutes.
A2.4 Unless otherwise stated the applied test pressure is to be measured at the inlet of the
component under test.
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A2.5 If a component is exposed to the pressure due to refilling operations, then Filling
Cycles shall be used. If a component is exposed to pressure due to the operation of
the vehicle, i.e. switching of the vehicle activation switch, then Duty Cycles shall be
used.
A3 APPROVAL REQUIREMENTS
A3.1.1 In addition to the requirements given below, the Manufacturer shall complete
all documents referred to in Part B of this Annex and submit them to the
Competent Authority when applying for type approval.
A3.1.2 The Specific Components shall be subjected to the applicable test procedures
laid down in Table 8A.1 of this Annex. The tests shall be conducted on
Specific Components that are representative of normal production and
complete with identification marks.
A3.2.1 Approval for a Flexible Fuel Line shall be given for one of any length with a
minimum bending radius specified by the Manufacturer and when assembled
with a specific type of Fitting.
A3.2.2 Any reinforcing interlayer of a Flexible Fuel Line shall be protected against
corrosion either by a cover or by using a corrosion resistant material for the
reinforcement(s), e.g. stainless steel. If a cover is used the formation of
bubbles between layers shall be prevented.
A3.2.3 Flexible Fuel Lines shall have an electrical resistance of less than 1 mega-
ohm per meter.
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Material Tests Corrosion Endurance Test Hydraulic Internal Leakage External Leakage
Resistance Test Pressure Cycle Test Test
B5 Test
B1, B2 & B3 B4 B6 B7 B8
Automatic Valves
Fittings
Heat Exchangers
Hydrogen Filters
Manual Valves
Non-Return Valves
Pressure Regulators
Receptacles
Table 8A.1: Applicable Test Procedures For Specific Components Other Than Containers
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Annex 8: Part B
MATERIAL TESTS
B1.1 Sampling
The test applies to the materials used in a Specific Component where the material is
in contact with hydrogen except:
i) Aluminium alloys that conform to Paragraphs 6.1 and 6.2 of ISO 7866,
ii) Steels that conform to Paragraph 6.3 and 7.2.2 of ISO 9809-1.
Number of material samples to be tested: 3
i) For metallic materials other than those stated above hydrogen compatibility
shall be demonstrated in accordance with ISO11114-1 or ISO/DIS 11114-4.
ii) Non-metallic materials
Hydrogen compatibility shall be demonstrated.
B1.3 Results
B2 AGEING TEST
B2.1 Sampling
The test shall be undertaken in accordance with ASTM D572. The sample shall be
exposed to oxygen at the maximum material temperature in accordance with
Paragraph 2.4.5.1 of this Regulation at 2.0 MPa for a period of 96 hours. Either the
tensile strength and elongation or the microhardness shall comply with the
specifications given by the Manufacturer. No visible cracking of the test samples is
allowed.
B2.3 Results
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B3.1 Sampling
B3.3 Results
B4.1 Sampling
Test i) Metallic components shall be submitted to a 144 hour salt spray test in
accordance with ISO 9227 with all connections closed and shall meet the
requirements therein.
Test ii) A copper alloy component shall also be submitted to 24 hours immersion in
ammonia in accordance with ISO 6957 with all connections closed and shall
meet the requirements therein.
B4.3 Results
B5 ENDURANCE TEST
B5.1 Sampling
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B5.2.2 Fittings
The length of the flexible part of the Flexible Fuel Line with its Fittings
attached, to be used in the following test shall be calculated as follows:
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L = 4.142R + 3.57D
where:
L = Length of the flexible part of the Flexible Fuel Line
R = Minimum bending radius specified by the Manufacturer
D= Outside diameter of the Flexible Fuel Line
The Flexible Fuel Line shall be bent in the manner depicted in Figure 8B.1 of
this Annex and attached to a fixture in that position by the Fittings with which it
is to be approved. One end of the Flexible Fuel Line shall be attached to a
reciprocating manifold and the other end shall be attached to a stationary
manifold connected to a hydraulic supply. The Flexible Fuel Line shall be
pressurised quickly by means of a quick opening solenoid valve, such that
one cycle consists of holding the pressure at 1.25 times the Nominal Working
Pressure for 10 ± 1 seconds (except for Flexible Fuel Lines with a required
material temperature of 1200C where the hold pressure shall be 1.37 times
Nominal Working Pressure) and then reducing it to less than 0.1 times the
Nominal Working Pressure for 5 ± 0.5 seconds. The total number of test
cycles shall be equal to 2.0 times the number of Filling Cycles or Duty Cycles
as appropriate to the use of the Flexible Fuel Line in accordance with
Paragraph 2.4.6 or 2.4.7 of this Regulation as appropriate. 50% of the test
cycles shall be performed at the minimum and the remaining 50% at the
maximum material temperature in accordance with Paragraph 2.4.5.1 of this
Regulation.
A = 1.75R + D
The Flexible Fuel Line shall not show any visible signs of damage.
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i) Creep Test
Pressure Relief Devices shall be hydrostatically pressurised to 1.25
times Nominal Working Pressure and held for 500 hours at a
temperature (TL) calculated from the following equation:
TL = T (0.057) (0.34 log(T/Tf))
where
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TL = Test temperature, ºC
Tf = Activation temperature of the Pressure Relief Device, ºC
T= 82ºC
Log is base 10
Pressure Relief Devices shall not show signs of creep and shall fulfil
the requirements of the Internal Leakage Test (Paragraph B7 of this
Annex) after being subjected to the above test.
Pressurise the Pressure Relief Valve for 25 cycles. A test cycle consists of
pressurising the Pressure Relief Valve to the activation pressure causing the
Pressure Relief Valve to open and vent. Once the Pressure Relief Valve is
venting the inlet pressure shall be reduced causing the Pressure Relief Valve
to re-seat. The cycle time shall be a period of 10 ± 2 s. For the final cycle the
activation pressure shall be reported and shall correspond to the activation
pressure specified by the Manufacturer within a range of ±5%.
B5.2.7 Receptacles
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the Removable Storage System Connector mounted on the vehicle and on the Removable
Storage System are separated and also when connected together.
B5.3 Results
B6.1 Sampling
Pressure Relief Devices shall be subjected to 1.5 times the number of Filling
Cycles calculated in accordance with Paragraph 2.4.6 of this Regulation at
both the minimum and maximum material temperatures in accordance with
Paragraph 2.4.5.1 of this Regulation.
The pressure shall periodically change from 2 MPa to 1.25 times Nominal
Working Pressure at a rate not exceeding 4 cycles per minute, except when
tested at the minimum material temperature when the maximum test pressure
shall be Nominal Working Pressure.
If fusible metal is used in a Pressure Relief Device it shall show no visible sign
of extrusion.
The pressure shall periodically change from 2.0 MPa to 1.25 times Nominal
Working Pressure for components upstream of the First Pressure Regulator,
or from 0.1 times MAWP to MAWP for components downstream of the First
Pressure Regulator, at a rate not exceeding 4 cycles per minute.
Subsequently the Component shall fulfil the requirements of the Internal and
External Leakage Tests (Paragraphs B7 and B8 of this Regulation).
B6.3 Results
B7.1 Sampling
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B7.2 Procedure
The Specific Components shall be tested using Leak Test Gas and shall be
pressurised at the inlet of the component when it is in its characteristic closed
position and with the corresponding outlet port open.
The component shall be observed for leakage with its outlet port open. The leakage
can be determined by a flowmeter installed on the inlet side of the component or by
another test method, which has been demonstrated to be equivalent.
B7.3 Requirements
When pressurised the Specific Component shall stay bubble free for three minutes or
shall not leak internally at a rate exceeding 10 Ncm3 per hour. The permitted leakage
rate is applicable to tests with 100% hydrogen only. Permitted leakage rates for other
gases or gas mixtures shall be converted to an equivalent leakage rate to that for
100% hydrogen.
B7.4 Results
B8.1 Sampling
B8.2 Procedure
The Specific Components shall be tested using Leak Test Gas at the following
conditions:
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i) At 20°C ± 5°C and at 0.02 times Nominal Working Pressure and at Nominal
Working Pressure.
ii) At the minimum required material temperature, in accordance with Paragraph
2.4.5.1 of this Regulation, after 2 hours conditioning to this temperature and at
0.02 times Nominal Working Pressure and at Nominal Working Pressure.
iii) At the maximum required material temperature, in accordance with Paragraph
2.4.5.1 of this Regulation, after 2 hours conditioning to this temperature and at
0.02 times Nominal Working Pressure and 1.25 times Nominal Working
Pressure, except for components with a required material temperature of
1200C where the higher test pressure shall be 1.37 times Nominal Working
Pressure.
For heat exchangers this test shall only be undertaken on the hydrogen circuit.
B8.3 Requirements
Throughout the test the Specific Component shall be free from leakage through stem
or body seals or other joints, and shall not show evidence of porosity in casting,
demonstrated by a surface active agent without formation of bubbles for 3 minutes or
3
measured with a combined leakage and permeation rate less than 10 Ncm per hour
3
(for Flexible Fuel Lines only 10 Ncm per hour per meter) or it shall be tested by
using a demonstrated equivalent test method. The permitted leakage rate is
applicable to tests with 100% hydrogen only. Permitted leakage rates for other gases
or gas mixtures shall be converted to an equivalent leakage rate to that for 100%
hydrogen.
B8.4 Results
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Revision 12b, 12.10.03
Annex 9
Annex 9
1 GENERAL
This Annex defines the special requirements for documentation, verification and test
with respect to the safety aspects of Complex Electronic Vehicle Control Systems as
far as this Regulation is concerned.
2 DOCUMENTATION
2.1 Requirements
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A list shall be provided, collating all the Units of “The System” and
mentioning the other vehicle systems that are needed to achieve the
control function in question. An outline schematic showing these Units
in combination, shall be provided with both the equipment distribution
and the interconnections clearly identified.
The function of each Unit of “The System” shall be outlined and the
signals linking it with other Units or with other vehicle systems shall be
shown. This may be provided by a labelled block diagram or other
schematic, or by a description aided by such a diagram.
2.3.3 Interconnections
2.4.1 The vehicle manufacturer shall provide a statement that affirms that
the strategy chosen to achieve “The System” objectives will not, under
non-fault conditions prejudice the safe operation of systems which are
subject to the prescriptions of this Regulation.
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For each of the chosen provisions, the driver shall be warned for
example by warning signals or message displays. When the system is
not deactivated by the driver, e.g. by turning the vehicle activation
switch to “off”, or by switching off that particular function if a special
switch is provided for that purpose, the warning shall be present as
long as the fault condition persists.
2.4.5 The documentation shall itemise the parameters being monitored and
shall set out, for each fault condition of the type defined in Paragraph
2.4.3 of this Annex, the warning signal to be given to the driver or to
service/technical inspection personnel.
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3.1 The functional operation of “The System”, as laid out in the documents
required in Paragraph 2 of this Annex shall be tested as follows:
3.2 The warning signal specified in Paragraph 2.4.3 of this Annex may, in general,
be satisfied by one optical signal per complex vehicle system unless any other
Regulation applicable to the same equipment specifically requires multiple
signals.
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Annex 10
Annex 10
H2
GAS
The colour and dimensions of the sticker shall fulfil the following requirements:
Colours:
Background: Green
Border: White
Letters: White
Either the borders and letters or the background shall be retro-reflective.
Colorimetric and photometric properties shall comply with the requirements
of clause 11 of ISO 3864-1:2002 (Graphical symbols – Safety colours and
safety signs – Part 1: Design principles for safety signs in workplaces and
public areas).
Dimensions:
Border width: 5 mm
Sticker width: 125 mm (across flat sides)
Sticker height: 125 mm (across flat sides)
Font size:
Font height: 25 mm
Font thickness: 5 mm
The words shall be in upper case characters, centralised to suit the dimensions.
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