Design Basis of the Distillation Column.

Physical properties of the solvents

Sr. Name of M. W. B. P. Spec. Heat Latent Heat Vapour Density Vapor Density Liquid Density
No. Solvent °C Kcal / kg Kcal /kg atm. Press.,kg/m3 kg/ m3 (60mmHg) kg/ m3
1 Toluene 92 110 0.25 98 2.93 0.29 860
2 MeCl2 85 38 0.288 79 3.33 0.27 1336
3 IPA 60 82 0.73 157 2.06 0.19 789
4 Acetone 58 56 0.52 125 2.15 0.18 792
5 Water 18 100 1 550 0.59 0.06 1000
6 Cyclohexane 84 80.7 0.55 85.6 2.89 0.27 778
7 Methanol 32 64.7 0.59 260 1.15 0.10 792
8 Ethyl Acetate 88 77 0.457 102 3.06 0.28 898
9 DMF 73.09 152.8 0.5 105 2.09 0.23 945
10 Ethanol 46.07 78.29 0.68 204.26 1.60 0.15 789
11 Acetonitrile 41 81.6 0.541 183 1.41 0.13 786.6
12 EA+Acetonitrile+wate 81.6 68.8 0.483 126 2.91 0.26 893
13 TEA 101 88.8 0.525 81 3.40 0.32 730
14 Chloroform 119.38 61.2 0.234 79 4.35 0.38 1480
15 MEK 72.11 79.64 0.53 113 2.49 0.23 800

Total Vapor Load of the column for desired capacity 1000

Considering solvent with minimum vapor Density I.e. Methanol
In order to get better efficiency velocity should be 0.8

Column Diameter based on Toluene 388.58

Column Diameter based on MDC 364.29
Column Diameter based on IPA 463.25
Column Diameter based on Acetone 453.58
Column Diameter based on Water 866.94
Column Diameter based on Cyclohexane 390.80
Column Diameter based on Methanol 618.68
Column Diameter based on Ethyl Acetate 379.81
Column Diameter based on DMF 459.67
Column Diameter based on Ethanol 525.89
Column Diameter based on Acetonitrile 560.08
Column Diameter based on EA+ Acetnl+water 389.78
Column Diameter based on TEA 360.45
Column Diameter based on Chloroform 318.65
Column Diameter based on MEK 421.15
 Viscocity
Cp.

0.35
0.75
0.26
1

Kg/hr

m/s

mm
mm
mm
mm
mm
mm
mm
mm
mm
mm
mm
mm
mm
mm
mm
 Design basis for Reboiler for Column

1 Evaporation rate of Methanol kg/hr 1000

2 Latent Heat of Methanol Kcal/ kg 260
3 Heat Load of Evaporation Kcal / Hr 260000
4 Inlet Temperature of Methanol to Reboiler °C 64
5 Outlet Temperature of Methanol from Reboiler °C 65
6 Inlet Temperature of Steam to Reboiler °C 132 T1 67
7 Outet Temperature of Steam from Reboiler °C 110 T2 46
8 LMTD across the Reboiler °C 55.84
9 Overall Heat Transfer Coefficient Assumed Kcal / hr °C m2 400
10 Heat Transfer Area Required m2 11.64
11 Based on 15 % Extra Final HTA selected is 13.4

12 Evaporation rate of Toluene kg/hr 400

13 Latent Heat of Toluene Kcal/ kg 100
14 Heat Load of Evaporation Kcal / Hr 40000
15 Inlet Temperature of Toluene to Reboiler °C 108 T1 24
16 Outlet Temperature of Toluene from Reboiler °C 110 T2 10
17 Inlet Temperature of Steam to Reboiler °C 132
18 Outet Temperature of Steam from Reboiler °C 120
19 LMTD across the Reboiler °C 15.99
20 Overall Heat Transfer Coefficient Assumed Kcal / hr °C m2 400
21 Heat Transfer Area Required m2 6.25
22 Based on 15 % Extra Final HTA selected is 6.9

23 Length of Reboiler Tube m 1.5

24 Outside Diameter of the tube m 0.025
25 Internal Diameter of the tube 0.0194
26 No. of Tubes required 112
27 No of Passes on tube side 1.00
28 Vapor flowrate on tube side m3/ sec. 0.241
29 Total cross sectional area on tube side m2 0.033
30 Vapor Velocity on tube side m/sec 7.28

31 Flowrate of the steam required to Reboiler Kg/ Hr. 472.73

32 Vapor Density of Steam At 3 kg/cm2 1.63
34 Based on 20 m/sec velocity diameter of Steam pipe mm 64.15
35 Diameter of the Steam pipe mm 67
 Design basis for Reboiler for Column

1 Evaporation rate of Methanol kg/hr 400

2 Latent Heat of Methanol Kcal/ kg 260
3 Heat Load of Evaporation Kcal / Hr 104000
4 Inlet Temperature of Methanol to Reboiler °C 64
5 Outlet Temperature of Methanol from Reboiler °C 65
6 Inlet Temperature of Steam to Reboiler °C 132 T1 67
7 Outet Temperature of Steam from Reboiler °C 110 T2 46
8 LMTD across the Reboiler °C 55.84
9 Overall Heat Transfer Coefficient Assumed Kcal / hr °C m2 400
10 Heat Transfer Area Required m2 4.66
11 Based on 15 % Extra Final HTA selected is 5.1

12 Evaporation rate of Toluene kg/hr 400

13 Latent Heat of Toluene Kcal/ kg 100
14 Heat Load of Evaporation Kcal / Hr 40000
15 Inlet Temperature of Toluene to Reboiler °C 108 T1 24
16 Outlet Temperature of Toluene from Reboiler °C 110 T2 10
17 Inlet Temperature of Steam to Reboiler °C 132
18 Outet Temperature of Steam from Reboiler °C 120
19 LMTD across the Reboiler °C 15.99
20 Overall Heat Transfer Coefficient Assumed Kcal / hr °C m2 400
21 Heat Transfer Area Required m2 6.25
22 Based on 15 % Extra Final HTA selected is 6.9

23 Length of Reboiler Tube m 1.5

24 Outside Diameter of the tube m 0.025
25 Internal Diameter of the tube 0.0194
26 No. of Tubes required 43
27 No of Passes on tube side 1.00
28 Vapor flowrate on tube side m3/ sec. 0.096
29 Total cross sectional area on tube side m2 0.013
30 Vapor Velocity on tube side m/sec 7.61

31 Flowrate of the steam required to Reboiler Kg/ Hr. 189.09

32 Vapor Density of Steam At 3 kg/cm2 1.63
34 Based on 20 m/sec velocity diameter of Steam pipe mm 40.57
35 Diameter of the Steam pipe mm 43
 Design basis for Condenser for RE-3101

Evaporation Capacity of the Reactor

1 Capacity of the Reactor 4 KL
2 HTA of the Reactor 5.5 m2
3 Boiling point of the solvent 65 °C
4 Utility Inlet temperature 132
5 Utility Outlet temperature 110 t1 67
6 Overall Heat Transfer Coefficient 300 t2 45
7 LMTD across the reactor 55.27 °C
8 Heat Load of Evaporation 91199.13 Kcal
9 Rate of Evaporation of Methanol 350.8 Kg/hr

Based on Methanol Condensation

1 Evaporation rate of Methanol kg/hr 350.8
2 Latent Heat of Methanol Kcal/ kg 260
3 Subcooling down to Temperature °C 60
4 Heat Load of Condensation Kcal / Hr 92171.8
5 Inlet Temperature of Methanol to Condenser °C 64.7
6 Outlet Temperature of Methanol from Condenser °C 60
7 Inlet Temperature of Cooling Water to Condenser °C 31 T1 28.7
8 Outet Temperature of Cooling Water from Condenser °C 36 T2 29
9 LMTD across the Condenser °C 28.85
10 Overall Heat Transfer Coefficient Assumed Kcal / hr °C m2 350
11 Heat Transfer Area Required m2 9.13
12 Based on 15 % Extra Final HTA selected is 10.50

Tubeside Design
25 Length of Condenser Tube m 3
26 Outside Diameter of the tube m 0.0190
27 Internal Diameter of the tube 0.0154
28 No. of Tubes required 58
29 No of Passes on tube side 4.00
30 Cooling water flowrate required on tube side m3/ Hr. 18.43
31 Total cross sectional area on tube side m2 0.0109
32 Cross Sectional area on tube side per pass m2 0.0027
33 Cooling Water Velocity on tube side m/sec 1.88
34 Based on 2 m/s velocity diameter of cooling nozzles m 0.06
35 Standard size of the Nozzle taken m 0.060

Shell Side Design

36 Flowrate of the vapors on the shell side m3/ Sec. 0.0844
37 Inside Diameter of the Shell m 0.30
38 No. of Baffles on Shell Side 14.00
39 Baffles Spacing based on 3 m Length m 0.21
40 Tube Pitch m 0.025
41 Flow Area on Shell Side m2 0.016097
42 Flowrate of the vapors on Shell Side m3/sec 0.084369
43 Velocity of the vapors on shell side m/sec 5.24
44 Based on 5 m/s velocity diameter on vapor inlet nozzle m 0.146566
45 Based on the standard size diameter of the nozzle m 0.16
 Design basis for Condenser for RE-3102

Evaporation Capacity of the Reactor

1 Capacity of the Reactor 5 KL
2 HTA of the Reactor 5 m2
3 Boiling point of the solvent 35 °C
4 Utility Inlet temperature 80
5 Utility Outlet temperature 75 T1 45
6 Overall Heat Transfer Coefficient 250 T2 40
7 LMTD across the reactor 42.45 °C
8 Heat Load of Evaporation 53063.67 Kcal
9 Rate of Evaporation of Toluene 541.5 Kg/hr

Based on Toluene Condensation

1 Evaporation rate of Toluene kg/hr 541.5
2 Latent Heat of Toluene Kcal/ kg 98
3 Subcooling down to Temperature °C 50
4 Heat Load of Condensation Kcal / Hr 111801.5
5 Inlet Temperature of Toluene to Condenser °C 85
6 Outlet Temperature of Toluene from Condenser °C 80
7 Inlet Temperature of Cooling Water to Condenser °C 32 T1 47
8 Outet Temperature of Cooling Water from Condenser °C 38 T2 18
9 LMTD across the Condenser °C 30.22
10 Overall Heat Transfer Coefficient Assumed Kcal / hr °C m2 250
11 Heat Transfer Area Required m2 14.80
12 Based on 15 % Extra Final HTA selected is 17

Based on Toluene Condensation

13 Evaporation rate of Toluene kg/hr 541.5
14 Latent Heat of Toluene Kcal/ kg 98
15 Subcooling down to Temperature 30
16 Heat Load of Condensation Kcal / Hr 53740.5
17 Inlet Temperature of Toluene to Condenser °C 35
18 Outlet Temperature of Toluene from Condenser °C 30
19 Inlet Temperature of Chilling Water to Condenser °C 11 T1 19
20 Outet Temperature of Chilling Water from Condenser °C 16 T2 19
21 LMTD across the Condenser °C 16
22 Overall Heat Transfer Coefficient Assumed Kcal / hr °C m2 300
23 Heat Transfer Area Required m2 11.20
24 Based on 20 % Extra Final HTA selected is 13.55
Tubeside Design
25 Length of Condenser Tube m 3
26 Outside Diameter of the tube m 0.0190 0.0036 0.364
27 Internal Diameter of the tube 0.0154
28 No. of Tubes required 95
29 No of Passes on tube side 4.00
30 Cooling water flowrate required on tube side m3/ Hr. 22.36
31 Total cross sectional area on tube side m2 0.0177
32 Cross Sectional area on tube side per pass m2 0.0044
33 Cooling Water Velocity on tube side m/sec 1.41
34 Based on 2 m/s velocity diameter of cooling nozzles m 0.06
35 Standard size of the Nozzle taken m 0.066

Shell Side Design

36 Flowrate of the vapors on the shell side m3/ Sec. 0.5148
37 Inside Diameter of the Shell m 0.30
38 No. of Baffles on Shell Side 9.00
39 Baffles Spacing based on 3 m Length m 0.33
40 Tube Pitch m 0.025
41 Flow Area on Shell Side m2 0.025039
42 Flowrate of the vapors on Shell Side m3/sec 0.514839
43 Velocity of the vapors on shell side m/sec 20.56
44 Based on 15 m/s velocity diameter on vapor inlet nozzle m 0.209034
45 Based on the standard size diameter of the nozzle m 0.23
1.82 mm thick
 Design basis for Condenser for RE-3103

Evaporation Capacity of the Reactor

1 Capacity of the Reactor 5 KL
2 HTA of the Reactor 6 m2
3 Boiling point of the solvent 38 °C
4 Utility Inlet temperature 75
5 Utility Outlet temperature 70 T1 37
6 Overall Heat Transfer Coefficient 250 T2 32
7 LMTD across the reactor 34.44 °C
8 Heat Load of Evaporation 51659.29 Kcal
9 Rate of Evaporation of Toluene 527.1 Kg/hr

Based on Toluene Condensation

1 Evaporation rate of Toluene kg/hr 527.1
2 Latent Heat of Toluene Kcal/ kg 98
3 Subcooling down to Temperature °C 35
4 Heat Load of Condensation Kcal / Hr 51791.08
5 Inlet Temperature of Toluene to Condenser °C 36
6 Outlet Temperature of Toluene from Condenser °C 35
7 Inlet Temperature of Cooling Water to Condenser °C 12 T1 20
8 Outet Temperature of Cooling Water from Condenser °C 16 T2 23
9 LMTD across the Condenser °C 21.47
10 Overall Heat Transfer Coefficient Assumed Kcal / hr °C m2 250
11 Heat Transfer Area Required m2 9.65
12 Based on 15 % Extra Final HTA selected is 11

Tubeside Design
25 Length of Condenser Tube m 3
26 Outside Diameter of the tube m 0.0190
27 Internal Diameter of the tube 0.0154
28 No. of Tubes required 62
29 No of Passes on tube side 4.00
30 Cooling water flowrate required on tube side m3/ Hr. 10.36
31 Total cross sectional area on tube side m2 0.0115
32 Cross Sectional area on tube side per pass m2 0.0029
33 Cooling Water Velocity on tube side m/sec 1.00
34 Based on 2 m/s velocity diameter of cooling nozzles m 0.04
35 Standard size of the Nozzle taken m 0.045

Shell Side Design

36 Flowrate of the vapors on the shell side m3/ Sec. 0.5012
37 Inside Diameter of the Shell m 0.30
38 No. of Baffles on Shell Side 9.00
39 Baffles Spacing based on 3 m Length m 0.33
40 Tube Pitch m 0.025
41 Flow Area on Shell Side m2 0.025039
42 Flowrate of the vapors on Shell Side m3/sec 0.501213
43 Velocity of the vapors on shell side m/sec 20.02
44 Based on 21 m/s velocity diameter on vapor inlet nozzle m 0.174312
45 Based on the standard size diameter of the nozzle m 0.19
 Design basis for Condenser for RE-3104

Evaporation Capacity of the Reactor

1 Capacity of the Reactor 4 KL
2 HTA of the Reactor 5.5 m2
3 Boiling point of the solvent 38 °C
4 Utility Inlet temperature 80
5 Utility Outlet temperature 75 T1 42
6 Overall Heat Transfer Coefficient 250 T2 37
7 LMTD across the reactor 39.45 °C
8 Heat Load of Evaporation 54239.9 Kcal
9 Rate of Evaporation of Toluene 553.5 Kg/hr

Based on Toluene Condensation

1 Evaporation rate of Toluene kg/hr 553.5
2 Latent Heat of Toluene Kcal/ kg 98
3 Subcooling down to Temperature °C 30
4 Heat Load of Condensation Kcal / Hr 55346.84
5 Inlet Temperature of Toluene to Condenser °C 38
6 Outlet Temperature of Toluene from Condenser °C 30
7 Inlet Temperature of Cooling Water to Condenser °C 12 T1 22
8 Outet Temperature of Cooling Water from Condenser °C 16 T2 18
9 LMTD across the Condenser °C 19.93
10 Overall Heat Transfer Coefficient Assumed Kcal / hr °C m2 275
11 Heat Transfer Area Required m2 10.10
12 Based on 15 % Extra Final HTA selected is 12

Tubeside Design
25 Length of Condenser Tube m 3
26 Outside Diameter of the tube m 0.0190
27 Internal Diameter of the tube 0.0154
28 No. of Tubes required 65
29 No of Passes on tube side 4.00
30 Cooling water flowrate required on tube side m3/ Hr. 11.07
31 Total cross sectional area on tube side m2 0.0121
32 Cross Sectional area on tube side per pass m2 0.0030
33 Cooling Water Velocity on tube side m/sec 1.02
34 Based on 2 m/s velocity diameter of cooling nozzles m 0.04
35 Standard size of the Nozzle taken m 0.046

Shell Side Design

36 Flowrate of the vapors on the shell side m3/ Sec. 0.5263
37 Inside Diameter of the Shell m 0.30
38 No. of Baffles on Shell Side 9.00
39 Baffles Spacing based on 3 m Length m 0.33
40 Tube Pitch m 0.025
41 Flow Area on Shell Side m2 0.025039
42 Flowrate of the vapors on Shell Side m3/sec 0.526251
43 Velocity of the vapors on shell side m/sec 21.02
44 Based on 5 m/s velocity diameter on vapor inlet nozzle m 0.183024
45 Based on the standard size diameter of the nozzle m 0.20
 Design basis for Condenser for RE-3106

Evaporation Capacity of the Reactor

1 Capacity of the Reactor 2 KL
2 HTA of the Reactor 3.5 m2
3 Boiling point of the solvent 35 °C
4 Utility Inlet temperature 80
5 Utility Outlet temperature 75 T1 45
6 Overall Heat Transfer Coefficient 250 T2 40
7 LMTD across the reactor 42.45 °C
8 Heat Load of Evaporation 37144.57 Kcal
9 Rate of Evaporation of Ethyl Acetate 364.2 Kg/hr

Based on Ethyl Acetate Condensation

1 Evaporation rate of Ethyl Acetate kg/hr 364.2
2 Latent Heat of Ethyl Acetate Kcal/ kg 102
3 Subcooling down to Temperature °C 30
4 Heat Load of Condensation Kcal / Hr 38143.1
5 Inlet Temperature of Ethyl Acetate to Condenser °C 36
6 Outlet Temperature of Ethyl Acetate from Condenser °C 30
7 Inlet Temperature of Cooling Water to Condenser °C 11 T1 20
8 Outet Temperature of Cooling Water from Condenser °C 16 T2 19
9 LMTD across the Condenser °C 19.50
10 Overall Heat Transfer Coefficient Assumed Kcal / hr °C m2 250
11 Heat Transfer Area Required m2 7.83
12 Based on 15 % Extra Final HTA selected is 9

Tubeside Design
25 Length of Condenser Tube m 3
26 Outside Diameter of the tube m 0.0190
27 Internal Diameter of the tube 0.0154
28 No. of Tubes required 50
29 No of Passes on tube side 4.00
30 Cooling water flowrate required on tube side m3/ Hr. 7.63
31 Total cross sectional area on tube side m2 0.0093
32 Cross Sectional area on tube side per pass m2 0.0023
33 Cooling Water Velocity on tube side m/sec 0.91
34 Based on 2 m/s velocity diameter of cooling nozzles m 0.04
35 Standard size of the Nozzle taken m 0.039

Shell Side Design

36 Flowrate of the vapors on the shell side m3/ Sec. 0.3620
37 Inside Diameter of the Shell m 0.30
38 No. of Baffles on Shell Side 9.00
39 Baffles Spacing based on 3 m Length m 0.33
40 Tube Pitch m 0.025
41 Flow Area on Shell Side m2 0.025039
42 Flowrate of the vapors on Shell Side m3/sec 0.361993
43 Velocity of the vapors on shell side m/sec 14.46
44 Based on 3 m/s velocity diameter on vapor inlet nozzle m 0.17528
45 Based on the standard size diameter of the nozzle m 0.19
 Design basis for Condenser for RE-3107

Evaporation Capacity of the Reactor

1 Capacity of the Reactor 4 KL
2 HTA of the Reactor 5.5 m2
3 Boiling point of the solvent 35 °C
4 Utility Inlet temperature 75
5 Utility Outlet temperature 70 T1 40
6 Overall Heat Transfer Coefficient 250 T2 35
7 LMTD across the reactor 37.44 °C
8 Heat Load of Evaporation 51486.02 Kcal
9 Rate of Evaporation of Cyclohexane 601.5 Kg/hr

Based on Cyclohexane Condensation

1 Evaporation rate of Cyclohexane kg/hr 601.5
2 Latent Heat of Cyclohexane Kcal/ kg 85
3 Subcooling down to Temperature °C 34
4 Heat Load of Condensation Kcal / Hr 51786.76
5 Inlet Temperature of Cyclohexane to Condenser °C 36
6 Outlet Temperature of Cyclohexane from Condenser °C 35
7 Inlet Temperature of Cooling Water to Condenser °C 12 T1 19
8 Outet Temperature of Cooling Water from Condenser °C 17 T2 22
9 LMTD across the Condenser °C 20.46
10 Overall Heat Transfer Coefficient Assumed Kcal / hr °C m2 275
11 Heat Transfer Area Required m2 9.20
12 Based on 15 % Extra Final HTA selected is 11

Tubeside Design
25 Length of Condenser Tube m 3
26 Outside Diameter of the tube m 0.0190
27 Internal Diameter of the tube 0.0154
28 No. of Tubes required 59
29 No of Passes on tube side 4.00
30 Cooling water flowrate required on tube side m3/ Hr. 10.36
31 Total cross sectional area on tube side m2 0.0110
32 Cross Sectional area on tube side per pass m2 0.0027
33 Cooling Water Velocity on tube side m/sec 1.05
34 Based on 2 m/s velocity diameter of cooling nozzles m 0.04
35 Standard size of the Nozzle taken m 0.045

Shell Side Design

36 Flowrate of the vapors on the shell side m3/ Sec. 0.6264
37 Inside Diameter of the Shell m 0.30
38 No. of Baffles on Shell Side 9.00
39 Baffles Spacing based on 3 m Length m 0.33
40 Tube Pitch m 0.025
41 Flow Area on Shell Side m2 0.025039
42 Flowrate of the vapors on Shell Side m3/sec 0.62636
43 Velocity of the vapors on shell side m/sec 25.02
44 Based on 3 m/s velocity diameter on vapor inlet nozzle m 0.199675
45 Based on the standard size diameter of the nozzle m 0.22
 Design basis for Condenser for RE-3108

Evaporation Capacity of the Reactor

1 Capacity of the Reactor 3 KL
2 HTA of the Reactor 4.5 m2
3 Boiling point of the solvent 35 °C
4 Utility Inlet temperature 80
5 Utility Outlet temperature 75 t1 45
6 Overall Heat Transfer Coefficient 250 t2 40
7 LMTD across the reactor 42.45 °C
8 Heat Load of Evaporation 47757.3 Kcal
9 Rate of Evaporation of Cyclohexane 557.9 Kg/hr

Based on Cyclohexane Condensation

1 Evaporation rate of Cyclohexane kg/hr 557.9
2 Latent Heat of Cyclohexane Kcal/ kg 85.6
3 Subcooling down to Temperature °C 32
4 Heat Load of Condensation Kcal / Hr 48371.01
5 Inlet Temperature of Cyclohexane to Condenser °C 34
6 Outlet Temperature of Cyclohexane from Condenser °C 32
7 Inlet Temperature of Cooling Water to Condenser °C 11 T1 18
8 Outet Temperature of Cooling Water from Condenser °C 16 T2 21
9 LMTD across the Condenser °C 19.46
10 Overall Heat Transfer Coefficient Assumed Kcal / hr °C m2 250
11 Heat Transfer Area Required m2 9.94
12 Based on 15 % Extra Final HTA selected is 11.43

Tubeside Design
25 Length of Condenser Tube m 3
26 Outside Diameter of the tube m 0.0190
27 Internal Diameter of the tube 0.0154
28 No. of Tubes required 64
29 No of Passes on tube side 4.00
30 Cooling water flowrate required on tube side m3/ Hr. 9.67
31 Total cross sectional area on tube side m2 0.0119
32 Cross Sectional area on tube side per pass m2 0.0030
33 Cooling Water Velocity on tube side m/sec 0.91
34 Based on 2 m/s velocity diameter of cooling nozzles m 0.04
35 Standard size of the Nozzle taken m 0.043

Shell Side Design

36 Flowrate of the vapors on the shell side m3/ Sec. 0.5810
37 Inside Diameter of the Shell m 0.30
38 No. of Baffles on Shell Side 9.00
39 Baffles Spacing based on 3 m Length m 0.33
40 Tube Pitch m 0.025
41 Flow Area on Shell Side m2 0.025039
42 Flowrate of the vapors on Shell Side m3/sec 0.580998
43 Velocity of the vapors on shell side m/sec 23.20
44 Based on 20 m/s velocity diameter on vapor inlet nozzle m 0.192309
45 Based on the standard size diameter of the nozzle m 0.21
 Design basis for Condenser for RE-3109

Evaporation Capacity of the Reactor

1 Capacity of the Reactor 1.5 KL
2 HTA of the Reactor 2.8 m2
3 Boiling point of the solvent 35 °C
4 Utility Inlet temperature 80
5 Utility Outlet temperature 75 t1 45
6 Overall Heat Transfer Coefficient 250 t2 40
7 LMTD across the reactor 42.45 °C
8 Heat Load of Evaporation 29715.65 Kcal
9 Rate of Evaporation of Methanol 114.3 Kg/hr

Based on Methanol Condensation

1 Evaporation rate of Methanol kg/hr 114.3
2 Latent Heat of Methanol Kcal/ kg 260
3 Subcooling down to Temperature °C 30
4 Heat Load of Condensation Kcal / Hr 29985.38
5 Inlet Temperature of Methanol to Condenser °C 34
6 Outlet Temperature of Methanol from Condenser °C 30
7 Inlet Temperature of Cooling Water to Condenser °C 11 T1 18
8 Outet Temperature of Cooling Water from Condenser °C 16 T2 19
9 LMTD across the Condenser °C 18.50
10 Overall Heat Transfer Coefficient Assumed Kcal / hr °C m2 250
11 Heat Transfer Area Required m2 6.48
12 Based on 15 % Extra Final HTA selected is 7.46

Tubeside Design
25 Length of Condenser Tube m 3
26 Outside Diameter of the tube m 0.0190
27 Internal Diameter of the tube 0.0154
28 No. of Tubes required 42
29 No of Passes on tube side 4.00
30 Cooling water flowrate required on tube side m3/ Hr. 6.00
31 Total cross sectional area on tube side m2 0.0077
32 Cross Sectional area on tube side per pass m2 0.0019
33 Cooling Water Velocity on tube side m/sec 0.86
34 Based on 2 m/s velocity diameter of cooling nozzles m 0.03
35 Standard size of the Nozzle taken m 0.034

Shell Side Design

36 Flowrate of the vapors on the shell side m3/ Sec. 0.1190
37 Inside Diameter of the Shell m 0.3000
38 No. of Baffles on Shell Side 9.0000
39 Baffles Spacing based on 3 m Length m 0.3333
40 Tube Pitch m 0.0254
41 Flow Area on Shell Side m2 0.0250
42 Flowrate of the vapors on Shell Side m3/sec 0.3124
43 Velocity of the vapors on shell side m/sec 12.4775
44 Based on 20 m/s velocity diameter on vapor inlet nozzle m 0.1410
45 Based on the standard size diameter of the nozzle m 0.1551
 Design basis for Condenser for RE-3111

Evaporation Capacity of the Reactor

1 Capacity of the Reactor 3 KL
2 HTA of the Reactor 4.5 m2
3 Boiling point of the solvent 80 °C
4 Utility Inlet temperature 132
5 Utility Outlet temperature 90 T1 52
6 Overall Heat Transfer Coefficient 250 T2 10
7 LMTD across the reactor 25.48 °C
8 Heat Load of Evaporation 28659.66 Kcal
9 Rate of Evaporation of Toluene 292.4 Kg/hr

Based on Toluene Condensation

1 Evaporation rate of Toluene kg/hr 292.4
2 Latent Heat of Toluene Kcal/ kg 98
3 Subcooling down to Temperature °C 34
4 Heat Load of Condensation Kcal / Hr 32841.63
5 Inlet Temperature of Toluene to Condenser °C 60
6 Outlet Temperature of Toluene from Condenser °C 55
7 Inlet Temperature of Cooling Water to Condenser °C 30 T1 25
8 Outet Temperature of Cooling Water from Condenser °C 35 T2 4
9 LMTD across the Condenser °C 11.46
10 Overall Heat Transfer Coefficient Assumed Kcal / hr °C m2 275
11 Heat Transfer Area Required m2 10.42
12 Based on 15 % Extra Final HTA selected is 12

Tubeside Design
25 Length of Condenser Tube m 3
26 Outside Diameter of the tube m 0.0190
27 Internal Diameter of the tube 0.0154
28 No. of Tubes required 67
29 No of Passes on tube side 4.00
30 Cooling water flowrate required on tube side m3/ Hr. 6.57
31 Total cross sectional area on tube side m2 0.0124
32 Cross Sectional area on tube side per pass m2 0.0031
33 Cooling Water Velocity on tube side m/sec 0.59
34 Based on 2 m/s velocity diameter of cooling nozzles m 0.03
35 Standard size of the Nozzle taken m 0.036

Shell Side Design

36 Flowrate of the vapors on the shell side m3/ Sec. 0.3045
37 Inside Diameter of the Shell m 0.30
38 No. of Baffles on Shell Side 9.00
39 Baffles Spacing based on 3 m Length m 0.33
40 Tube Pitch m 0.025
41 Flow Area on Shell Side m2 0.025039
42 Flowrate of the vapors on Shell Side m3/sec 0.304546
43 Velocity of the vapors on shell side m/sec 12.16
44 Based on 3 m/s velocity diameter on vapor inlet nozzle m 0.139232
45 Based on the standard size diameter of the nozzle m 0.15
 Design basis for Condenser of RE-3112

Based on Water Condensation

1 Evaporation rate of Water kg/hr 400
2 Latent Heat of Water Kcal/ kg 540
3 SubCooling down to Temperature °C 62
4 Heat Load of Condensation Kcal / Hr 224360
5 Inlet Temperature of Water to Condenser °C 100 T1 64
6 Outlet Temperature of Water from Condenser °C 99 T2 67
7 Inlet Temperature of Cooling Water to Condenser °C 32
8 Outet Temperature of Cooling Water from Condenser °C 36
9 LMTD across the Condenser °C 65.5
10 Overall Heat Transfer Coefficient Assumed Kcal / hr °C m2 250
11 Heat Transfer Area Required m2 13.70
12 Based on 15 % Extra Final HTA selected is 15
13 Vapor Density of Water at working Pressure 0.59 Kg/cm3

Tubeside Design
25 Length of Condenser Tube m 3
26 Outside Diameter of the tube m 0.0190
27 Internal Diameter of the tube 0.0154
28 No. of Tubes required 84
29 No of Passes on tube side 2.00
30 Cooling water flowrate required on tube side m3/ Hr. 44.87
31 Total cross sectional area on tube side m2 0.0156
32 Cross Sectional area on tube side per pass m2 0.0078
33 Cooling Water Velocity on tube side m/sec 1.59
34 Based on 2 m/s velocity diameter of Cooling nozzles m 0.09
35 Standard size of the Nozzle taken m 0.092

Shell Side Design

36 Flowrate of the vapors on the shell side m3/ Sec. 0.1889
37 Inside Diameter of the Shell m 0.35
38 No. of Baffles on Shell Side 9
39 Baffles Spacing based on 3 m Length m 0.30
40 Tube Pitch m 0.025
41 Flow Area on Shell Side m2 0.026291
42 Flowrate of the vapors on Shell Side m3/sec 0.1889
43 Velocity of the vapors on shell side m/sec 7.19
44 Based on 10 m/s velocity diameter on vapor inlet nozzle m 0.155
45 Based on the standard size diameter of the nozzle m 0.16
 Design basis for Condenser of C-3101

Based on Methanol Condensation

1 Evaporation rate of Methanol kg/hr 400
2 Latent Heat of Methanol Kcal/ kg 260
3 SubCooling down to Temperature °C 63
4 Heat Load of Condensation Kcal / Hr 104220
5 Inlet Temperature of Methanol to Condenser °C 64 T1 28
6 Outlet Temperature of Methanol from Condenser °C 63 T2 31
7 Inlet Temperature of Cooling Water to Condenser °C 32
8 Outet Temperature of Cooling Water from Condenser °C 36
9 LMTD across the Condenser °C 29.5
10 Overall Heat Transfer Coefficient Assumed Kcal / hr °C m2 250
11 Heat Transfer Area Required m2 14.14
12 Based on 15 % Extra Final HTA selected is 16
13 Vapor Density of Methanol at working Pressure 1.15 Kg/cm3

Tubeside Design
25 Length of Condenser Tube m 3
26 Outside Diameter of the tube m 0.0190
27 Internal Diameter of the tube 0.0154
28 No. of Tubes required 87
29 No of Passes on tube side 4.00
30 Cooling water flowrate required on tube side m3/ Hr. 20.84
31 Total cross sectional area on tube side m2 0.0161
32 Cross Sectional area on tube side per pass m2 0.0040
33 Cooling Water Velocity on tube side m/sec 1.43
34 Based on 2 m/s velocity diameter of Cooling nozzles m 0.06
35 Standard size of the Nozzle taken m 0.063

Shell Side Design

36 Flowrate of the vapors on the shell side m3/ Sec. 0.0962
37 Inside Diameter of the Shell m 0.35
38 No. of Baffles on Shell Side 9
39 Baffles Spacing based on 3 m Length m 0.30
40 Tube Pitch m 0.024
41 Flow Area on Shell Side m2 0.021
42 Flowrate of the vapors on Shell Side m3/sec 0.0962
43 Velocity of the vapors on shell side m/sec 4.58
44 Based on 10 m/s velocity diameter on vapor inlet nozzle m 0.111
45 Based on the standard size diameter of the nozzle m 0.12
 Design basis for Condenser of C-3102

Based on Cyclohexane Condensation

1 Evaporation rate of Cyclohexane kg/hr 700
2 Latent Heat of Cyclohexane Kcal/ kg 85
3 SubCooling down to Temperature °C 80
4 Heat Load of Condensation Kcal / Hr 59885
5 Inlet Temperature of Cyclohexane to Condenser °C 81 T1 45
6 Outlet Temperature of Cyclohexane from Condenser °C 80 T2 48
7 Inlet Temperature of Cooling Water to Condenser °C 32
8 Outet Temperature of Cooling Water from Condenser °C 36
9 LMTD across the Condenser °C 46.5
10 Overall Heat Transfer Coefficient Assumed Kcal / hr °C m2 250
11 Heat Transfer Area Required m2 5.15
12 Based on 15 % Extra Final HTA selected is 10
13 Vapor Density of Cyclohexane at working Pressure 2.89 Kg/cm3

Tubeside Design
25 Length of Condenser Tube m 3
26 Outside Diameter of the tube m 0.0190
27 Internal Diameter of the tube 0.0154
28 No. of Tubes required 56
29 No of Passes on tube side 4.00
30 Cooling water flowrate required on tube side m3/ Hr. 11.98
31 Total cross sectional area on tube side m2 0.0104
32 Cross Sectional area on tube side per pass m2 0.0026
33 Cooling Water Velocity on tube side m/sec 1.28
34 Based on 2 m/s velocity diameter of Cooling nozzles m 0.05
35 Standard size of the Nozzle taken m 0.047

Shell Side Design

36 Flowrate of the vapors on the shell side m3/ Sec. 0.0672
37 Inside Diameter of the Shell m 0.35
38 No. of Baffles on Shell Side 9
39 Baffles Spacing based on 3 m Length m 0.30
40 Tube Pitch m 0.025
41 Flow Area on Shell Side m2 0.026291
42 Flowrate of the vapors on Shell Side m3/sec 0.0672
43 Velocity of the vapors on shell side m/sec 2.56
44 Based on 10 m/s velocity diameter on vapor inlet nozzle m 0.092
45 Based on the standard size diameter of the nozzle m 0.10
 Design basis for Condenser of C-3103

Based on Toluene Condensation

1 Evaporation rate of Toluene kg/hr 700
2 Latent Heat of Toluene Kcal/ kg 105
3 SubCooling down to Temperature °C 108
4 Heat Load of Condensation Kcal / Hr 74270
5 Inlet Temperature of Toluene to Condenser °C 110 T1 74
6 Outlet Temperature of Toluene from Condenser °C 108 T2 76
7 Inlet Temperature of Cooling Water to Condenser °C 32
8 Outet Temperature of Cooling Water from Condenser °C 36
9 LMTD across the Condenser °C 75.0
10 Overall Heat Transfer Coefficient Assumed Kcal / hr °C m2 250
11 Heat Transfer Area Required m2 3.96
12 Based on 15 % Extra Final HTA selected is 10
13 Vapor Density of Toluene at working Pressure 2.89 Kg/cm3

Tubeside Design
25 Length of Condenser Tube m 3
26 Outside Diameter of the tube m 0.0190
27 Internal Diameter of the tube 0.0154
28 No. of Tubes required 56
29 No of Passes on tube side 4.00
30 Cooling water flowrate required on tube side m3/ Hr. 14.85
31 Total cross sectional area on tube side m2 0.0104
32 Cross Sectional area on tube side per pass m2 0.0026
33 Cooling Water Velocity on tube side m/sec 1.59
34 Based on 2 m/s velocity diameter of Cooling nozzles m 0.05
35 Standard size of the Nozzle taken m 0.053

Shell Side Design

36 Flowrate of the vapors on the shell side m3/ Sec. 0.0672
37 Inside Diameter of the Shell m 0.35
38 No. of Baffles on Shell Side 9
39 Baffles Spacing based on 3 m Length m 0.30
40 Tube Pitch m 0.025
41 Flow Area on Shell Side m2 0.026291
42 Flowrate of the vapors on Shell Side m3/sec 0.0672
43 Velocity of the vapors on shell side m/sec 2.56
44 Based on 10 m/s velocity diameter on vapor inlet nozzle m 0.092
45 Based on the standard size diameter of the nozzle m 0.10
 Design basis for Condenser of C-3103

Based on Toluene Condensation

1 Evaporation rate of Toluene kg/hr 100
2 Latent Heat of Toluene Kcal/ kg 105
3 SubCooling down to Temperature °C 33
4 Heat Load of Condensation Kcal / Hr 10885
5 Inlet Temperature of Toluene to Condenser °C 40 T1 25
6 Outlet Temperature of Toluene from Condenser °C 33 T2 23
7 Inlet Temperature of Cooling Water to Condenser °C 10
8 Outet Temperature of Cooling Water from Condenser °C 15
9 LMTD across the Condenser °C 24.0
10 Overall Heat Transfer Coefficient Assumed Kcal / hr °C m2 250
11 Heat Transfer Area Required m2 1.82
12 Based on 15 % Extra Final HTA selected is 1.96
13 Vapor Density of Toluene at working Pressure 0.27 Kg/cm3

Tubeside Design
25 Length of Condenser Tube m 2
26 Outside Diameter of the tube m 0.0190
27 Internal Diameter of the tube 0.0154
28 No. of Tubes required 16
29 No of Passes on tube side 4.00
30 Cooling water flowrate required on tube side m3/ Hr. 3.63
31 Total cross sectional area on tube side m2 0.0031
32 Cross Sectional area on tube side per pass m2 0.0008
33 Cooling Water Velocity on tube side m/sec 1.32
34 Based on 2 m/s velocity diameter of Cooling nozzles m 0.03
35 Standard size of the Nozzle taken m 0.026

Shell Side Design

36 Flowrate of the vapors on the shell side m3/ Sec. 0.1041
37 Inside Diameter of the Shell m 0.35
38 No. of Baffles on Shell Side 9
39 Baffles Spacing based on 3 m Length m 0.20
40 Tube Pitch m 0.025
41 Flow Area on Shell Side m2 0.017528
42 Flowrate of the vapors on Shell Side m3/sec 0.1041
43 Velocity of the vapors on shell side m/sec 5.94
44 Based on 10 m/s velocity diameter on vapor inlet nozzle m 0.115
45 Based on the standard size diameter of the nozzle m 0.12
 Design basis for Condenser of C-3103

Based on Toluene Condensation

1 Evaporation rate of Toluene kg/hr 90
2 Latent Heat of Toluene Kcal/ kg 105
3 SubCooling down to Temperature °C 30
4 Heat Load of Condensation Kcal / Hr 9846
5 Inlet Temperature of Toluene to Condenser °C 38 T1 47
6 Outlet Temperature of Toluene from Condenser °C 30 T2 42
7 Inlet Temperature of Cooling Water to Condenser °C -12
8 Outet Temperature of Cooling Water from Condenser °C -9
9 LMTD across the Condenser °C 44.5
10 Overall Heat Transfer Coefficient Assumed Kcal / hr °C m2 250
11 Heat Transfer Area Required m2 0.89
12 Based on 15 % Extra Final HTA selected is 1
13 Vapor Density of Toluene at working Pressure 0.27 Kg/cm3

Tubeside Design
25 Length of Condenser Tube m 1.5
26 Outside Diameter of the tube m 0.0190
27 Internal Diameter of the tube 0.0154
28 No. of Tubes required 12
29 No of Passes on tube side 4.00
30 Cooling water flowrate required on tube side m3/ Hr. 3.28
31 Total cross sectional area on tube side m2 0.0022
32 Cross Sectional area on tube side per pass m2 0.0006
33 Cooling Water Velocity on tube side m/sec 1.65
34 Based on 2 m/s velocity diameter of Cooling nozzles m 0.02
35 Standard size of the Nozzle taken m 0.025

Shell Side Design

36 Flowrate of the vapors on the shell side m3/ Sec. 0.0937
37 Inside Diameter of the Shell m 0.35
38 No. of Baffles on Shell Side 9
39 Baffles Spacing based on 3 m Length m 0.15
40 Tube Pitch m 0.025
41 Flow Area on Shell Side m2 0.013146
42 Flowrate of the vapors on Shell Side m3/sec 0.0937
43 Velocity of the vapors on shell side m/sec 7.13
44 Based on 10 m/s velocity diameter on vapor inlet nozzle m 0.109
45 Based on the standard size diameter of the nozzle m 0.11