Materials Lab PDF
Materials Lab PDF
Sanith Vaddepalli
510362324
1. Introduction
AIM - The objective of the experiment is to;
• To Conduct a 3-point bending test on the provided glass specimen and interpret the obtained
results
• To determine the mechanical properties (Flexure modulus and strength) of the given specimen
• To Understand the concepts of fracture mechanics and calculate Stress intensity factor, and
fracture toughness)
• To interpret and apply the concept of Weibull analysis to the fracture analysis.
Background
A 3 point test is performed to determine the modulus of elasticity in bending, stress-strain response and
flexure stress-strain of the provided specimen. The specimen is kept under two simply supported joints in
a Universal testing machine. The load is applied at the center of the specimen until a fracture occurs and
the corresponding load-displacement data is recorded.
Source -https://upload.wikimedia.org/wikipedia/commons/thumb/e/e9/Beam_bending.svg/500px-
Beam_bending.svg.png
Source -
https://upload.wikimedia.org/wikip
edia/commons/thumb/e/e2/Beam_s
tress.svg/500px-
Beam_stress.svg.png
As depicted in fig 1 the maximum tensile strength is applied at the center of the specimen. The upper half
of the specimen undergoes compression and the lower half undergoes tension. In general, brittle materials
display higher strength in compression than in tension as the crack propagates faster in tension. i.e tensile
strength of ceramic is about one-tenth of their compressive force [1].
The stress experienced by the specimen can be calculated by the thickness, bending moment and moment
of inertia. The results of tensile stress obtained by the test are not an accurate depiction as the failure
occurs around the griping of the specimen
• Flexural strength - “Flexural strength, also known as modulus of rupture, or bend strength,
or transverse rupture strength is a material property, defined as the stress in a material just
before it yields in a flexure test.” [2]
• Flexure modulus - the modulus defines the slope of the stress deflection curve
i. Flexural strength -
Moment,
From eq 1 & 2
𝑏ℎ3
𝐼=
12
If the applied force is considered as p and it is plotted on a graph against wo (displacement ). We obtain straight
line and the gradient of the line is given by
Hence,
3. Procedure
i. Apparatus
ii. Steps -
1. The thickness and width of the specimen are measured using a vernier caliper at three different
points and the average of the value is tabulated in the datasheet.
3. The bending test is performed in an Instron Universal Test Machine with Instron Application
Software where the load cell is 1 kN the load cell is calibrated to a load rate of 1mm/min and a
data logging rate of 20ms.
4. The specimen is placed symmetrically between two supports such that an anvil is positioned at the
mid-span of the specimen. Now, the anvil is lowered just above the specimen and the reading is
set to zero. A small compression preload of 0.1 -1 N is applied then the load reading is set to zero.
5. Click the start button to begin the test. The force and displacement of the specimen are recorded
till the specimen fails. At the end of the test, the date is saved to a predefined location.
6. The required mechanical properties (fracture load, flexural strength, fracture modulus ) and values
are calculated from the obtained load vs displacement graph.
4. Results
Specimen No
Type Geometry
• Length = 60 mm
• Width = 25.2 mm
• Thickness =1.07 mm
• I = 2.5 mm4
Load VS Displacement
35
30
25
FORCE (N)
20
15
10
5
0
0.0 0.1 0.2 0.3 0.3 0.4 0.5 0.6 0.7
DISPLACEMENT (MM)
Second sample is used calculations of material properties
𝑃𝐿 29.21 𝑥 60
𝑀𝑚𝑎𝑥 = = 438.15 Nmm
𝐴 4
1.07
𝑀𝑚𝑎𝑥 × 𝑐 438.15 × 2
𝜎𝑓𝑏 = = = 92.73 𝑀𝑃𝑎
𝐼 2.527746
𝐿3 𝑑𝑃 603
𝐸= × = × 42.04 = 73.65 𝐺𝑃𝑎
4𝑤𝑡 3 𝑑v 4 × 25.16 × 1.073
𝜎 𝑚
−( )
𝑃𝑠 ( 𝑉0 ) = 𝑒 𝜎0
Y= mx+ C = 9.5-41
𝑚 = 𝑠𝑙𝑜𝑝𝑒 = 9.5
−𝑚 ln 𝜎0 = −41
𝜎0 = 72.4 𝑀𝑝𝑎
5. Discussion
As the test was performed on a brittle specimen the data Cleary depicts the effect of cracks and
imperfections on the strength of a material. From the data it can be observed that control group could with
stand a maximum load of 29.21 N before failure, whereas test specimen with a surface crack could withstand
a load of 18N. Even though the 3 test specimen, have similar specification such as thickness length width
they display different strengths this is due to the surface cracks and defects
Fracture toughness of materials depicts the resistance of brittle materials to failure or crack propagation an d
it is quantified by the equation K=Yσ√(π×a) From this equation it can be seen that fracture toughness is
directly proportional to the crack size which means lower load could also cause failure if the crack size is
larger. In other words, with an increase in crack size, the concentration factor also increases leading to
failures at lower loads.
Failure in any materials occurs due to the breakage of atomic bonds. Ductile material displays significant
plastic formation as these bonds are broken whereas brittle material does not display any plastic deformation
the crack propagates instantly leading to catastrophic failures. Any imperfections due to surface defects
become regions of stress concentration.
• Specimen gripping - The specimen could have been placed at the exact same spot during each test.
Minute variation in placement can affect the facture load of the specimen
• Material impurities- surface impurities such during manufacturing can cause stress concentration
leading to cracks or non-uniform arrangement
• Geometry - small variation in geometric properties can provide different mechanical properties of
flexural stress and modulus.
• Treatment - Surface cracks on some specimens may have been larger to others as the treatment is
done manually.
6. Conclusion
The bent test is a very efficient method to determine the maximum load a material can withstand as the
deformation is directly proportional to the applied load. From the obtained load VS displacement curve, we
can observe that crack propagation in a brittle martial happens without any plastic deformation. The
deformation is directly promotional to the applied load. The presence of surface defects significantly effect
the load-bearing capacity of brittle material. The presence of crack lead to the formation of stress
concentration near that region and failure takes place even at lower loads.
The Weibull analysis performed indicates that the survival probability of a specimen is higher it is
subjected to lower stress i.e. for stress 20MPa the survival probability is 97% and 2% for a stress of 90
MPA
References