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CMSA 2021 IOP Publishing
Journal of Physics: Conference Series 1995 (2021) 012011 doi:10.1088/1742-6596/1995/1/012011

Mechanical Properties Test and Simulation Analysis of Glass


Coated Amorphous Filaments

Shujuan Qin, Junqing Yin*, Shan Liu, Yongdang Chen and Jinyu Gu
School of Mechanical and Electrical Engineering, Xi’an Polytechnic University, Xi’an,
China

*Corresponding author email: [email protected]

Abstract. Taking the Co68.7Fe4Ni1B13Si11Mo2.3 glass-coated amorphous microwire as the


research object, the mechanical properties of the amorphous wire were tested through biaxial
tensile experiments, and the fracture deformation process of the amorphous wire was analyzed.
Based on the experimental data, the finite element method was used The simulation software
ABAQUS numerically simulates the tensile deformation of the amorphous wire, and the
fracture relationship between the glass cladding layer and the core wire, and further reveals the
tensile deformation fracture behavior of the amorphous wire was analyzed. The experimental
results indicate that the fabricated microwires exhibit good tensile properties, and the
maximum tensile breaking strength can reach 2918MPa; the fracture of the amorphous wire is
a typical brittle fracture, and there is no obvious yield phenomenon. The tensile mechanics
simulation results of the amorphous wire are consistent with the experimental results. The glass
cladding layer breaks before the core wire, and the stress transfer effect in the amorphous wire
is good. The model fracture is consistent with the fracture morphology of the amorphous wire.
These results show that the amorphous wire exhibits good tensile properties and stress
transmission capabilities, confirming the huge application potential of amorphous wire
materials in sensor applications and functional composite materials.

1. Introduction
Amorphous wire material has attracted great interest due to its potential use in a series of scientific
research and engineering applications. It has many excellent electromagnetic properties such as giant
magnetic impedance, magnetic bistability, microwave absorption, electromagnetic interference
shielding, etc. [1-3], has been widely used in a variety of sensors and electronic devices [4-6], as well as
functional composite materials [7-8]. The microstructure and magnetic properties of these amorphous
wires can be adjusted by annealing and mechanical processing during or after the manufacturing
process [9-11], and they can also achieve giant magnetic impedance under the action of Giant magneto-
impedance (GMI) effect is significantly improved [12]. However, the potential engineering application
value of ferromagnetic amorphous wire not only depends on its excellent magnetic properties, but also
closely related to its excellent mechanical properties. Its high strength, high toughness, and high wear
resistance make it maintain during the application process. In order to understand the structural
strength integrity of other materials, we need to understand its basic mechanical properties and change
laws in practical applications, and use these laws to analyze the application of amorphous wires in
sensors, functional composite materials and other aspects in combination with their electromagnetic
properties. Therefore, mechanical research on this kind of amorphous microwires is essential to
enhance their magnetic properties and solve the problems related to their applications in sensors and
other aspects. Most of the previous research mainly focused on the tensile strength of amorphous wire

Content from this work may be used under the terms of the Creative Commons Attribution 3.0 licence. Any further distribution
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Published under licence by IOP Publishing Ltd 1
CMSA 2021 IOP Publishing
Journal of Physics: Conference Series 1995 (2021) 012011 doi:10.1088/1742-6596/1995/1/012011

[13-15]
. This is due to the small size of the amorphous wire and the rapid fracture process. It is difficult
to observe the tensile strength of the amorphous wire during the experiment. The specific fracture
process of the amorphous wire can only be analyzed simply through experimental data. The stress
transfer process when the amorphous wire is subjected to a tensile force and the fracture relationship
between the glass coating layer and the core wire have not been fully studied. In this paper, the
mechanical parameters of these CoFe-based amorphous wires during biaxial tensile deformation are
measured through biaxial tensile experiments. The deformation process is revealed on the basis of
theoretical analysis, and the tensile deformation behavior is further carried out by finite element
software. Numerical simulation reveals the stress transfer process of the amorphous wire when
subjected to tensile force, and the breaking sequence of the glass cladding layer and the core wire,
which is the application of the amorphous wire in force sensors, magnetic sensors and their functional
composite materials The research provides the theoretical basis and simulation basis.

2. Mechanical Properties Test of Amorphous Filaments

2.1. Experimental Materials


The composition of Co-based amorphous wire studied in this paper is: Co68.7Fe4Ni1B13Si11Mo2.3, The
microwire has a core-shell structure with uniform thickness and a smooth surface. The total diameter
of the microwire is D=27μm, and the diameter of the metal core layer is d=22μm.

2.2. Experimental Scheme


Cut 10 wires from the same batch of amorphous wires, make tensile samples according to the
international standard ASTM D3379-75, install the cut 10 wires on the fixture as shown in Figure.1,
and place the microwires in the middle of the hollow rectangular cardboard, both ends are fixed with
tape, and then a layer of cardboard is covered on both ends and bonded with adhesive glue. In the
mechanical performance test, the samples prepared above are clamped and cut off the cardboard on
both sides, and the test is carried out according to the set loading rate. The tensile test was carried out
on the single-fiber strength machine LLY-06ED material testing machine. The maximum tensile force
is set to 200cN(I.e.1.96N, 1N=102cN), and a high-precision sensor is used to measure and analyze the
tensile process. The tensile rate is 1mm/min (I.e.16.667μm/s), and the amorphous wire is stretched to
break.

Figure 1. Schematic diagram of stretched sample

2.3. Experimental Results and Analysis


The maximum fracture strength of the 10 samples ranged from 1609 MPa to 2918 MPa, the average
maximum fracture strength was σbmax=2043MPa, and the average maximum strain was about 2.1%.
Calculate the average value of the measured data and draw the average stress-strain curve of the
amorphous filaments, as shown in Figure.2. It can be clearly seen that the fracture of amorphous
filaments is typical brittle fracture without obvious plastic strain. Samples in the elongation rate is
about 1.2% when suddenly there was a obvious stress reduce the drop zone, namely the red box circle

2
CMSA 2021 IOP Publishing
Journal of Physics: Conference Series 1995 (2021) 012011 doi:10.1088/1742-6596/1995/1/012011

part of the figure, analysis think this is because there is such a large glass of brittleness and extension
rate is small, so when the glass layer in the event of rupture, which is associated with crack in glass
layer spread rapidly, resulting in glass layer broke off and failure, After the failure of the glass coating,
the core does not fracture, and the core continues to be stressed until the second fracture occurs. The
slope of the curve during the second fracture can be approximately regarded as the elastic modulus of
the alloy core material.

Figure 2. Tensile stress-strain curve of glass-coated amorphous wire

3. Numerical Simulation

3.1. Parameter Setting and Condition Definition

3.1.1. Geometric parameter and material property setting. The structure diagram of the finite element
simulation model of amorphous wire mechanics is shown in Figure.3. It consists of two parts: a metal
core layer and a glass cladding layer. The diameter of the amorphous wire core layer is d=22μm, and
the diameter of the glass cladding layer is D=27μm. The length is L=500μm. The stress-strain data in
the parameter attribute setting of the core material adopts the amorphous wire mechanical property test
data in section 2.3, See Table 1 for details. the cladding material is SiO2, the elastic modulus is 20GPa,
and the parameter setting refers to the literature [16]. In the finite element simulation, the clamping
length of the two ends of the amorphous wire is ignored, and the stress is directly applied to the two
ends to perform the finite element simulation.

Figure 3. Schematic diagram of amorphous wire structure

3
CMSA 2021 IOP Publishing
Journal of Physics: Conference Series 1995 (2021) 012011 doi:10.1088/1742-6596/1995/1/012011

Table 1. stress-strain parameters of core material

Stress (MPa) Strain (%) Stress (MPa) Strain (%)


859.28 0.7083 1789.86 1.6667
1121.37 0.9167 1926.36 1.8333
1354.42 1.1250 2006.85 1.9583
1500.63 1.2917 2043.39 2.1000

3.1.2. Model Meshing and Load Definition. When meshing, taking into account the different fracture
characteristics of the core layer and the cladding layer, the core layer is meshed. The inner and outer
layers are scanned using the hexahedral advanced algorithm, and the unit type is set to eight. The
nodal linear hexahedral element reduces the integral (C3D8R), as shown in Figure.4. Load the
displacement load at both ends during load definition. The maximum displacement is set to 16 μm, the
load is loaded at a uniform speed, and the set tensile rate is 16.667 μm/s (I.e. 1 mm/min), which is the
same as the parameters of the tensile test. be consistent.

Figure 4. Finite element model of amorphous wire

3.1.3. Boundary Conditions and Definition of Contact Relationship. The boundary conditions,
coordinate definitions and axis constraints are shown in Figure.4. Both ends of the amorphous wire are
fully constrained by the X and Y axes, and are only allowed to move in the Z direction to apply
displacement loads. Because the contact between the cladding layer and the core layer is more
complicated, in this study, the interface effect of the interaction between the inner and outer layers of
the amorphous wire is not considered for the time being. It is assumed that the inner and outer layers
of the amorphous wire are in hard contact. The surface-to-surface contact type is adopted. Considering
the strength between the interfaces, the contact coefficient is set to be larger.

3.2. Finite Element Simulation Examples and Analysis


When loading, the tensile stress is transferred from the two ends of the amorphous wire to the middle
of the amorphous wire. At this time, the glass coating layer of the amorphous wire and the core wire
are subjected to the same tensile force. When the tensile stress reaches 1324MPa, the coating layer has
already occurred. Fracture, as shown in Figure 5(a), at this time the core layer has not yet been
significantly broken. Before the glass coating layer is broken, the core wire has been subjected to a
considerable load. As the displacement load increases, the coating layer is completely broken. When
the glass coating layer is broken, the load continues to act on the core wire. When the stress reaches
1647MPa, the core layer begins to crack initially. With the increase of displacement load, when the
stress reaches the limit close to the average maximum tensile strength σbmax of the amorphous wire, the
core layer is completely broken, and finally the amorphous wire breaks and separates. As shown in
Figure 5(b). The fracture morphology of the amorphous wire after tensile fracture is shown in Figure
5(c). According to the simulation results, it can be seen that the fracture morphology of the amorphous

4
CMSA 2021 IOP Publishing
Journal of Physics: Conference Series 1995 (2021) 012011 doi:10.1088/1742-6596/1995/1/012011

wire is not completely flat. This result is consistent with the literature [17-19] The fracture morphology
of the amorphous wire in] basically coincides, indicating that the established simulation model has a
certain validity.

(a) Fracture sign of glass coating (b) Cross-section diagram of core fracture
process

(c) Fracture morphology characteristics


Figure 5. Mechanical simulation results of amorphous filaments

4. Results and Discussion


The tensile deformation fracture behavior of glass-coated Co68.7Fe4Ni1B13Si11Mo2.3 amorphous
microwires was systematically studied and analyzed by experimental research and numerical
simulation. The conclusions are as follows:
(1) The experimental results show that the tensile fracture behavior of the amorphous wire is elastic
deformation, almost no plastic strain, its maximum fracture strength is distributed between 1609MPa
and 2918MPa, and the average fracture strength is 2043MPa, showing good mechanical properties.
(2) A simulation model of the tensile mechanics of amorphous wire was established, and the specific
fracture deformation behavior and stress transmission process of the amorphous wire under biaxial
tension were simulated. It was found that the glass coating layer of the amorphous wire was earlier
than the core wire. The fracture is consistent with the experimental results, and the stress transfer
effect in the amorphous wire is good.
Good mechanical properties and stress transfer ability are necessary conditions for the application of
amorphous wire to sensors and functional composite materials. The conclusions obtained in this article
have not only confirmed the huge application potential of amorphous wire in sensor applications and
functional composite materials, but also It provides a theoretical basis and simulation basis for the

5
CMSA 2021 IOP Publishing
Journal of Physics: Conference Series 1995 (2021) 012011 doi:10.1088/1742-6596/1995/1/012011

research and development of the application of amorphous wire and its functional composite materials
in mechanics.

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