An American National Standard

Designation: C562 – 91 (Reapproved 2005)

Standard Test Method for

Moisture in a Graphite Sample1
This standard is issued under the fixed designation C562; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.

1. Scope 5. Apparatus
1.1 This test method provides a practical determination for 5.1 Alumina Ceramic or Platinum Crucible or Dish, suit-
the percentage of moisture in a graphite sample. able for holding sample (subsequently called sample holder).
1.2 This standard does not purport to address all of the 5.2 Analytical Balance, capable of weighing to 60.0002 g.
safety concerns, if any, associated with its use. It is the 5.3 Drying Oven, air convection type, capable of being
responsibility of the user of this standard to establish appro- controlled to 110 6 2°C (2306 4°F).
priate safety and health practices and determine the applica- 5.4 Desiccator, charged with indicating desiccant.
bility of regulatory limitations prior to use.
6. Sampling
2. Referenced Documents 6.1 Samples may be solid or particulate. Solid bodies may
2.1 ASTM Standards:2 be sampled by removing one or more solid pieces from the
C561 Test Method for Ash in a Graphite Sample body by, for example, sawing, turning, milling, or fracturing.
Particulate samples may be generated from solid bodies by
3. Significance and Use drilling, using a carbide drill to minimize contamination, or by
3.1 This test method is feasible only for the volatile mois- other crushing and grinding methods.
ture present on the graphite due to adsorption from the
atmosphere and is not intended to give representative moisture 7. Procedure
data for graphite that has been exposed to liquid water 7.1 Tare a dried sample holder using an analytical balance.
contamination. Weigh a 25 to 50-g sample into the tared sample holder and
reweigh both. (Perform all weighings to a precision of
4. Interferences 60.002 g.)
4.1 Final weights (and therefore percent moisture values) 7.2 Place the sample holder containing the sample in a
may be influenced by the following: drying oven maintained at 110 6 2°C (230 6 4°F) for 2 h.
4.1.1 Type and condition of desiccant. Remove from the oven and immediately place in the desicca-
4.1.2 Ambient relative humidity at the time of the test. tor. When the sample has reached room temperature, remove
4.1.3 Timing and procedure for moving samples from des- from the desiccator and weigh immediately.
iccator to the balance. 7.3 Repeat the procedure prescribed in 7.2 until a constant
4.1.4 Adsorptivity of the graphite sample relative to the weight of 60.002 g is achieved.
adsorptivity of the desiccant used. 7.4 The dried sample may be reserved for ash determina-
4.1.5 Residency time in the desiccator. tion. (See Test Method C561.)
8. Calculation
1
This test method is under the jurisdiction of ASTM Committee D02 on
Petroleum Products and Lubricants and is the direct responsibility of Subcommittee 8.1 Calculate the percentage of moisture as follows:
D02.F0 on Manufactured Carbon and Graphite Products. Moisture, % 5 [~ B 2 C!/~B 2 A!# 3 100
Current edition approved June 1, 2005. Published August 2005. Originally
approved in 1965. Last previous edition approved in 2000 as C562–91(2000). DOI: where:
10.1520/C0562-91R05.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
A = weight of sample holder,
contact ASTM Customer Service at [email protected]. For Annual Book of ASTM B = weight of sample holder and sample, and
Standards volume information, refer to the standard’s Document Summary page on C = weight of sample holder and dried sample.
the ASTM website.

Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.

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 C562 – 91 (2005)
9. Report the round robin to minimize variations among samples pro-
9.1 The report shall include the following information: vided to participating laboratories.
9.1.1 Proper identification of the sample, and 10.2 On this sample the mean, standard deviation between
9.1.2 Results obtained from at least two moisture determi- laboratories and standard deviation within laboratories were,
nations, and their average. respectively:
Mean 0.0155
10. Precision and Bias 3 Between laboratories 0.0143
Within laboratories 0.0037
10.1 The precision of this test method was determined
during a round-robin test among four laboratories testing 10.3 No bias was noted during the round-robin test; how-
samples split from a common sample which was ground to pass ever, the method is empirical and there is no suitable reference
a No. 60 (250 µm) sieve. This sampling method was used for material that can be used to determine the bias of this test
method.

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11. Keywords
Supporting data have been filed at ASTM International Headquarters and may
be obtained by requesting Research Report C05-1008. 11.1 carbon; graphite; moisture

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