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    Experiment No. 6: Preparation and Standardization of Silver Nitrate Solution (Agno)

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    Banana Q
    This document provides instructions for preparing and standardizing a silver nitrate solution. It involves weighing silver nitrate crystals, dissolving them in water to make a 1 L stock solution. To standardize it, an aliquot of the solution is diluted and treated with hydrochloric acid to precipitate silver chloride. The precipitate is collected, weighed, and used to calculate the molarity and normality of the original silver nitrate solution. The objectives are to prepare a standardized silver nitrate solution to use for subsequent quantitative analysis experiments.

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    Experiment No. 6: Preparation and Standardization of Silver Nitrate Solution (Agno)

    Uploaded by

    Banana Q
    774 views3 pages
    This document provides instructions for preparing and standardizing a silver nitrate solution. It involves weighing silver nitrate crystals, dissolving them in water to make a 1 L stock solution. To standardize it, an aliquot of the solution is diluted and treated with hydrochloric acid to precipitate silver chloride. The precipitate is collected, weighed, and used to calculate the molarity and normality of the original silver nitrate solution. The objectives are to prepare a standardized silver nitrate solution to use for subsequent quantitative analysis experiments.

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    This document provides instructions for preparing and standardizing a silver nitrate solution. It involves weighing silver nitrate crystals, dissolving them in water to make a 1 L stock solution. To standardize it, an aliquot of the solution is diluted and treated with hydrochloric acid to precipitate silver chloride. The precipitate is collected, weighed, and used to calculate the molarity and normality of the original silver nitrate solution. The objectives are to prepare a standardized silver nitrate solution to use for subsequent quantitative analysis experiments.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    774 views3 pages

    Experiment No. 6: Preparation and Standardization of Silver Nitrate Solution (Agno)

    Uploaded by

    Banana Q
    This document provides instructions for preparing and standardizing a silver nitrate solution. It involves weighing silver nitrate crystals, dissolving them in water to make a 1 L stock solution. To standardize it, an aliquot of the solution is diluted and treated with hydrochloric acid to precipitate silver chloride. The precipitate is collected, weighed, and used to calculate the molarity and normality of the original silver nitrate solution. The objectives are to prepare a standardized silver nitrate solution to use for subsequent quantitative analysis experiments.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    of 3

    University of Perpetual Help System

    Dr. Jose G. Tamayo Medical University


    System - JONELTA
    College of Pharmacy

    Group No.: Date:


    Group member/Assigned task: 3.
    1. 4.
    2. 5.

    Experiment No. 6:

    PREPARATION AND STANDARDIZATION OF


    SILVER NITRATE SOLUTION
    (AgNO3)

    Materials required:
    Silver nitrate crystals
    Distilled water
    Diluted hydrochloric acid solution
    Nitric acid

    Preparation of silver nitrate solution


    1. Weigh accurately 17.5 g of silver nitrate crystals
    2. Dissolve the crystals in a sufficient amount of distilled water to make one (1) L solution
    3. Pour the solution into a 1 L amber stock bottle
    4. Label properly

    Standardization of silver nitrate solution


    1. Measure accurately 40 mL of silver nitrate solution, and then dilute the solution with 100
    mL of distilled water. Heat the solution.
    2. Add slowly with continuous stirring, standard hydrochloric acid solution until it has
    produce there is a complete precipitation of sodium chloride.
    3. Boil the mixture for 5 minutes.
    4. Allow it to stand in the dark until the supernatant liquid is clear and all the precipitate has
    settled at the bottom
    5. Transfer the precipitate into a tared crucible
    6. Wash the precipitate with small portions of distilled water, then acidified slightly with nitric
    acid
    7. Dry the precipitate at 110°C to constant weight. Determine the weight of silver chloride.
    8. Calculate the molarity and normality of silver nitrate solution

    1|P a g e

    This study source was downloaded by 100000864622566 from CourseHero.com on 03-28-2023 03:53:14 GMT -05:00

    https://www.coursehero.com/file/85961680/Midterm-Experiment-No-6-PREPARATION-AND-STANDARDIZATION-OF-SILVER-NITRATE-SOLUTIONpdf/
    OBJECTIVES: To prepare and standardize silver nitrate solution.

    METHOD OF ANALYSIS: Precipitation

    EQUATION/S INVOLVED:
    AgNO3 + H2O AgOH + HNO3
    AgOH + HCl AgCl + H2O

    USP standard: 99.8% -100.5%

    DATA:

    Weight of weighing bottle + silver nitrate 23.5 g 22.25 g


    Weight of weighing bottle 22.75 g 22.75 g
    Weight of silver nitrate ? g ? g
    Weight of crucible + precipitate 31.45 g 30.55 g
    Weight of crucible 29.5 g 29.5 g
    Weight of precipitate ? g ? g
    Calculated Molarity of standard Silver nitrate solution ? M ? M
    Calculated Normality of standard Silver nitrate solution ? N ? N

    CALCULATIONS:

    Meq/mL or N = wt of AgCl x AgNO3 / AgCl


    mL x 0.16987

    2|P a g e

    This study source was downloaded by 100000864622566 from CourseHero.com on 03-28-2023 03:53:14 GMT -05:00

    https://www.coursehero.com/file/85961680/Midterm-Experiment-No-6-PREPARATION-AND-STANDARDIZATION-OF-SILVER-NITRATE-SOLUTIONpdf/
    Answer the following:

    Name of Sample

    Other Name/s

    Molecular Weight

    Factor

    Standard solution

    Indicator

    End Point

    Chemical Reaction

    Involved

    Reason for special step

    CONCLUSION:

    3|P a g e

    This study source was downloaded by 100000864622566 from CourseHero.com on 03-28-2023 03:53:14 GMT -05:00

    https://www.coursehero.com/file/85961680/Midterm-Experiment-No-6-PREPARATION-AND-STANDARDIZATION-OF-SILVER-NITRATE-SOLUTIONpdf/
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