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OptiFlash User Manual Abel

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0% found this document useful (0 votes)
2K views196 pages

OptiFlash User Manual Abel

Uploaded by

Kwabena Abrantie
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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OptiFlash®

Abel Flash Point Analyzers

USER MANUAL

/i

Contents OptiFlash® Abel - User Manual


Date September 28, 2016
Revision V1.0B
Revision History
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Revision Date Description


V1.0A July 16, 2015 First release
V1.0B September 28, 2016 Technical data (3.7) and List of alarm messages (9.2)
adapted, safety instructions added (5.3)
OptiFlash®

Copyright
Copyright © 2015, by Petroleum Analyzer Company, L.P.
All rights reserved.

All text, graphics, design, and other works contained herein are the copyrighted
works of Petroleum Analyzer Company, L.P. (hereinafter referred to as PAC).
Any redistribution or reproduction of any materials contained herein is strictly
prohibited without the express written permission of the copyright holder.
The PAC trademark, the PAC service mark, PAC’s logo trademark, PAC division’s
trademarks, PAC product’s trademarks, and PAC’s distinctive colour trademark as
used on its instruments and in these materials, are trademarks or service marks or
registered trademarks or registered service marks of PAC in the U.S. and other
countries and are its sole and exclusive property.
MS Windows, MS Windows XP, and MS Windows Professional are registered
trademarks of Microsoft Corp.
Other trademarks contained within these materials are the property of their
respective owners.

Information
The information contained within these materials is subject to change without
notice. PAC makes no warranties or guarantees, either expressed or implied in
these materials, including the warranty merchantability or fitness for a particular
purpose. At any time, PAC may modify these materials, its instruments or its
programs without notice and subsequent versions of these materials may contain
different information.
These materials could contain technical inaccuracies and/or typographical errors.
PAC does not assume responsibility for the accuracy of any translation of these
materials.

This manual contains confidential and proprietary information. The information


contained within these materials is the property of PAC. This manual and all
information disclosed herein shall not be used to manufacture, construct, or
fabricate the goods disclosed herein; shall not be exploited or sold; shall not be
copied or otherwise reproduced in whole or in part and shall not be revealed or
disclosed to others or in any manner made public without the express written
permission of PAC.

About PAC
PAC is an international manufacturing and service organization with a portfolio that
spans petroleum, petrochemical, biofuels, environmental, food and beverage,
pharmaceutical and industrial analysis solutions.
PAC provides advanced scientific apparatus and testing equipment for laboratory
process, on-line and field use from small to the largest enterprise businesses. PAC
offers analytical solutions for a wide variety of applications, including:
chromatographic systems and detectors, elemental, laboratory, and on-line
process instruments, software applications, and spectroscopy.
Many automatic analyzers bearing the PAC brand are recognized for increasing
test precision, boosting laboratory efficiency and reducing costs.

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Table of contents
1 General information
1.1 Policy statement .................................................................................................................... 10
1.2 Standard limited warranty of PAC ......................................................................................... 10
1.2.1 Limited warranty ....................................................................................................... 10
1.2.2 Limitations on PAC liability ....................................................................................... 14
1.2.3 Compliance .............................................................................................................. 15
1.3 Software license .................................................................................................................... 16
1.3.1 Grant of license ........................................................................................................ 16
1.3.2 Description of other rights and limitations ................................................................ 17
1.3.3 Upgrades.................................................................................................................. 18
1.3.4 Copyright .................................................................................................................. 18
1.3.5 Dual-media software ................................................................................................ 18
1.3.6 U.S. Government restricted rights ............................................................................ 18
1.4 Assumptions .......................................................................................................................... 19
1.4.1 Good Laboratory Practice ........................................................................................ 19
1.4.2 The standards of laboratory safety........................................................................... 19
1.4.3 Electronic device ...................................................................................................... 19
1.5 Return policy.......................................................................................................................... 20
1.5.1 Returned product warranty determination ................................................................ 20
1.5.2 On-site repair............................................................................................................ 20
1.5.3 Inspection ................................................................................................................. 20
1.5.4 Information ............................................................................................................... 21
1.6 Disposal................................................................................................................................. 22
1.7 Documentation ...................................................................................................................... 22
1.7.1 Document validity ..................................................................................................... 22
1.7.2 Document storage .................................................................................................... 23
1.7.3 Language ................................................................................................................. 23
1.7.4 Typographical and authoring conventions................................................................ 23

2 Safety
2.1 Certifications.......................................................................................................................... 26
2.2 Warning pictograms............................................................................................................... 27
2.3 Caution pictograms................................................................................................................ 28
2.4 Note pictograms .................................................................................................................... 29
2.5 Tip pictograms ....................................................................................................................... 29
2.6 Environmental protection....................................................................................................... 29

3 Introduction
3.1 Intended use.......................................................................................................................... 32
3.2 Intended audience ................................................................................................................. 32
3.3 Applicable standard test methods ......................................................................................... 32
3.4 Introduction to OptiFlash® Flash Point Analyzers ................................................................. 32
3.5 List of abbreviations............................................................................................................... 34
3.6 Rating plate ........................................................................................................................... 34
3.7 Technical specifications......................................................................................................... 35

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4 Description
4.1 Views of the OptiFlash® ........................................................................................................ 38
4.1.1 Front view................................................................................................................. 38
4.1.2 Rear view ................................................................................................................. 39
4.1.3 Connection ports/Interfaces ..................................................................................... 40
4.2 Test equipment ...................................................................................................................... 41
4.2.1 Test cup – Abel ........................................................................................................ 41
4.2.2 Test cup-cover insert – Abel..................................................................................... 42
4.2.3 Parts of the test cup-cover insert and test accessories ............................................ 43
4.2.4 Self-positioning automatic lift arm ............................................................................ 45
4.3 Features ................................................................................................................................ 46
4.3.1 Cooling features ....................................................................................................... 46
4.3.2 Fire detection features.............................................................................................. 46
4.3.3 Alarms/Warnings ...................................................................................................... 46
4.4 Optional accessories ............................................................................................................. 47
4.4.1 Optional external data management software: IRIS® .............................................. 47
4.4.2 Optional external printer ........................................................................................... 47
4.4.3 Optional bar code reader.......................................................................................... 48
4.4.4 Optional calibrator (probe simulator) for the temperature measuring system .......... 48
4.4.5 Optional pressure gage for the ambient pressure sensor ........................................ 48
4.4.6 Optional connection cables ...................................................................................... 48
4.4.7 More optional tools for calibration and adjustment ................................................... 48
4.5 Access levels ......................................................................................................................... 49
4.6 The Man Machine Interface (MMI)......................................................................................... 51
4.6.1 Touchscreen............................................................................................................. 51
4.6.2 Precautions for the touchscreen............................................................................... 51
4.6.3 The main screen....................................................................................................... 52
4.6.4 The virtual keyboard and keypad ............................................................................. 54
4.6.5 Structure of the main screen .................................................................................... 55
4.6.6 The menu structure .................................................................................................. 57

5 Installation
5.1 Care in unpacking.................................................................................................................. 60
5.2 Installation requirements........................................................................................................ 60
5.3 Installation location ................................................................................................................ 60
5.4 Connecting to the mains ........................................................................................................ 61
5.5 Installing the accessories holder............................................................................................ 61
5.6 Installing the igniter................................................................................................................ 62
5.6.1 Electric igniter ........................................................................................................... 62
5.6.2 Gas igniter (option)................................................................................................... 62
5.7 Installing the accessories....................................................................................................... 64
5.8 Connecting/disconnecting the test equipment with/from the lift arm...................................... 65
5.9 Connecting to a PC................................................................................................................ 66
5.9.1 Optional external PC control .................................................................................... 66
5.10 Optional external alarm output connector.............................................................................. 66

6 Operation
6.1 Preparation ............................................................................................................................ 68
6.1.1 Safety ....................................................................................................................... 68
6.1.2 Preparing the OptiFlash®......................................................................................... 69

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6.2 Sampling................................................................................................................................ 70
6.2.1 Pre-cooling ............................................................................................................... 70
6.2.2 Sample handling....................................................................................................... 70
6.2.3 Fill in the sample ...................................................................................................... 71
6.3 Perform measurements ......................................................................................................... 72
6.3.1 Entering test parameters .......................................................................................... 72
6.3.2 Starting a test ........................................................................................................... 74
6.3.3 Stopping a running test ............................................................................................ 78
6.3.4 Automatic flash point determination ......................................................................... 79
6.3.5 Measurement completed.......................................................................................... 80
6.3.6 Removing the test cup.............................................................................................. 80
6.3.7 Displaying and printing of test results....................................................................... 81
6.3.8 Cleaning the test equipment..................................................................................... 81

7 Database Management
7.1 The Results main menu......................................................................................................... 84
7.1.1 Displaying, printing and saving of results ................................................................. 84
7.1.2 Print button ............................................................................................................... 87
7.1.3 Validate button ......................................................................................................... 87
7.1.4 Chart button.............................................................................................................. 87
7.1.5 USB button ............................................................................................................... 88
7.1.6 Delete button ............................................................................................................ 88
7.2 The Advanced main menu..................................................................................................... 89
7.3 The Standard database ......................................................................................................... 90
7.3.1 View parameter details of test methods ................................................................... 91
7.3.2 Add new custom test methods ................................................................................. 95
7.4 The Products database ......................................................................................................... 97
7.4.1 View parameter details of the products .................................................................... 98
7.4.2 Add new custom products ...................................................................................... 104
7.5 The Operators database...................................................................................................... 106
7.6 The Quality database .......................................................................................................... 108
7.6.1 Quality Control........................................................................................................ 109
7.6.2 Atmospheric Pressure ............................................................................................ 112
7.6.3 Sample probe ......................................................................................................... 116
7.6.4 Extinguisher (only High End and Standard Model) ................................................ 118
7.6.5 Sample probe circuit............................................................................................... 120
7.6.6 Arm adjustment ...................................................................................................... 126
7.6.7 Adjustment of the touchscreen............................................................................... 129
7.7 The Instrument Setup database .......................................................................................... 131
7.7.1 Instrument Parameters........................................................................................... 132
7.7.2 Date & Time ........................................................................................................... 145
7.7.3 Firmware updates and Backup / Restore ............................................................... 146
7.7.4 Reset ...................................................................................................................... 150
7.8 The Measures Diagnostic database .................................................................................... 152
7.9 The Information database.................................................................................................... 159
7.9.1 Event log ................................................................................................................ 160
7.9.2 About ...................................................................................................................... 162
7.9.3 Counters................................................................................................................. 167
7.9.4 Contacts ................................................................................................................. 168

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8 Maintenance
8.1 Routine maintenance........................................................................................................... 170
8.2 Maintenance intervals.......................................................................................................... 170
8.3 Cleaning the test equipment ................................................................................................ 170
8.4 Calibration of the igniter....................................................................................................... 172
8.4.1 Calibration of an electric igniter .............................................................................. 173
8.4.2 Calibration of a gas igniter...................................................................................... 174
8.5 Optional available parts and accessories ............................................................................ 175

9 Troubleshooting
9.1 Dealing with alarm and warning messages ......................................................................... 178
9.2 List of alarm messages........................................................................................................ 179
9.3 List of warning messages .................................................................................................... 186

10 Appendix
10.1 LIMS specification for results............................................................................................... 190
10.2 Printout specifications for results ......................................................................................... 192

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General information OptiFlash®

1 General information

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OptiFlash® General information

1.1 Policy statement


The instructions given herein cover generally the description, installation,
operation, and/or maintenance of subject equipment. PAC reserves the
right to make engineering refinements that may not be reflected in this
manual. Should any questions arise which may not be answered
specifically by these instructions, they should be directed to PAC for
further detailed information and technical assistance.
Your satisfaction and safety are important to PAC, and a complete
understanding of this equipment is necessary to attain these objectives.
As the eventual user of this apparatus, it is your responsibility to
understand its proper function and operational characteristics.
This manual should be read thoroughly and all users should be given
adequate training before attempting to place this instrument in service.
Awareness of the stated cautions and warnings, and compliance with
recommended operating and maintenance parameters are important for
safe and satisfactory operation.

This apparatus should be used only for its intended operation; alterations
will void the warranty.

1.2 Standard limited warranty of PAC


This Standard Limited Warranty applies to products manufactured and
sold by Petroleum Analyzer Company, L.P., Walter Herzog GmbH,
Instrumentation Scientifique De Laboratoire SAS, A.C. Analytical Controls
B.V., and A.C. Analytical Controls Asia Pacific Pte Ltd. (hereafter each or
any of them referred to as "PAC").

1.2.1 Limited warranty

1.2.1.1 Warranty

For each product sold, PAC offers to the original owner ("Buyer") a limited
warranty against failure to conform to the product specifications or any
defects in material and workmanship for a period of
i twelve (12) months from the date of installation of the product or
ii eighteen (18) months from date of invoice,

whichever is less (the "Initial Warranty"). If a failure to conform to


specifications or a defect in materials or workmanship is discovered within
the Initial Warranty period, Buyer must promptly notify PAC in writing,
which notification, in any event must be received no later than 14 months
from the date of installation of the product. Within a reasonable time after
such notification, PAC will correct any failure to conform to specifications
or any defect in materials or workmanship, or in lieu of such repair, and at
its sole option, shall replace the product, F.O.B. PAC's city of shipment or
refund the purchase price, less a reasonable reduction in such purchase
price as determined by PAC. In no event shall PAC be liable for
consequential or special damages, or for transportation, installation,

10 UM Abel_V1.0B_EN
General information OptiFlash®

adjustment or other expenses, which may arise in connection with such


products or warranty claim. Products and parts sold by authorized PAC
Distributors are covered by the Distributor's terms and conditions.

During the Initial Warranty period, PAC offers a limited warranty on each
part or product repaired or replaced by a PAC service person for a period
ending the later of
a the remaining term of the Initial Warranty of the product or
b ninety (90) days from the date of repair or replacement,

whichever is longer. After expiration of the Initial Warranty period, PAC


offers a ninety (90) day limited warranty on each part or product repaired
or replaced by a PAC service person. PAC further warrants that the
products and parts it sells will conform to PAC's written specifications
therefor. The foregoing limited warranties cover parts and labor only and
PAC does not warrant and will not reimburse the Buyer for any other costs
relating repairing or replacing the product at issue. The foregoing limited
warranties apply only to the repair or replacement of defective parts and/
or products and such determination will be in the sole discretion of PAC.
The limited warranties of this Section 1.2.1.1. Warranty are further subject
to those warranty exclusions set forth in Section 1.2.1.3. Limited warranty
exclusions.

1.2.1.2 Aftermarket
The use of third party parts in the operation or maintenance of the product
or repairs or servicing by unauthorized service personnel immediately
voids all further warranty obligations of PAC. PAC genuine consumables
are sold on an as-is basis and have no warranty beyond being shipped in
good working order.

1.2.1.3 Limited warranty exclusions


Other than the warranties set forth in Section 1.2.1.1. Warranty, PAC
disclaims any and all express or implied warranties, including but not
limited to the warranty of merchantability, fitness for a particular purpose
and non-infringement of the intellectual property of others. Provided,
however, this Intellectual Property Warranty shall apply to the product only
so long as Buyer
i does not modify the product, combine the product with other elements
or use the product in a practice or a process, and such modification,
combination or practice of which the product forms a part is the subject
of such claim or allegation of infringement and
ii uses the product under ordinary conditions and for their intended
purposes.

PAC makes no warranty, express or implied, as to the design, sale,


installation or use of its products. PAC's warranties will not be enlarged by,
nor will any obligation or liability of PAC arise due to PAC providing
technical advice, facilities or service in connection with any product. PAC

UM Abel_V1.0B_EN 11
OptiFlash® General information

disclaims any and all other warranties and representations and PAC
provides no warranty on the oral representations made by its personnel
while they are undertaking Services for Buyer.

There is no warranty by PAC with respect to any product’s:


i uninterrupted or error-free operation;
ii actual performance, other than the product's capability to meet PAC's
specifications therefor;
iii removal or installation from a worksite or process;
iv electronic components or associated accessories (including without
limitation circuit boards and integrated circuits);
v maintenance (including without limitation gasket and seal
replacements, adjustments, minor repairs and other inspection
requirements, preventative or otherwise);
vi use under inappropriate conditions or not in accordance with
operating instructions; or
vii use in connection with the operation of a nuclear facility.

There is no warranty for products determined to be, in PAC’s sole


discretion, damaged or impaired as a result of:
A misuse, neglect or accident;
B improper application, installation, storage or use;
C improper or inadequate maintenance or calibration;
D operation outside of the published environmental specification;
E improper site preparation or maintenance;
F unauthorized repairs or replacements;
G modifications negligently or otherwise improperly made or performed
by persons other than PAC;
H Buyer-supplied software or supplies;
I use in conjunction with or interfacing with unapproved accessory
equipment;
J use of ABC-style or dry powder fire suppression agents; or
K leaked sample materials.

To the extent a PAC product is used in connection with the operation of a


nuclear power facility, Buyer agrees to indemnify and hold PAC harmless
from any and all actions, claims, suits, damages and expenses arising
from such use. PAC provides no warranty on the oral representations
made by its personnel while they are attempting to assist Buyer in the
operation of a product. This Standard Limited Warranty does not apply to
items consumed by the products during their ordinary use, including but
not limited to fuses, batteries, paper, septa, fittings, screws, fuses,
pyrolysis, dryer or scrubber tubes, sample boats, furnaces or lamps.

12 UM Abel_V1.0B_EN
General information OptiFlash®

This warranty is valid only if genuine PAC parts, consumables and


standards are used in PAC products.

1.2.1.4 Resale products


Resale products are goods (that are sold with PAC's products) which are
not manufactured by PAC and which are supplied as an accommodation
to Buyer. PAC MAKES NO WARRANTY FOR RESALE PRODUCTS,
EITHER EXPRESS OR IMPLIED, INCLUDING WARRANTIES OF
MERCHANTABILITY AND FITNESS FOR A PARTICULAR PURPOSE.
THE SOLE WARRANTY SHALL BE THAT OF THE RESALE PRODUCT
MANUFACTURER.
Buyer agrees that PAC has no liability for resale products beyond the
services within PAC's direct control necessary to reasonably discharge the
above stated responsibility and that PAC shall not be liable for delays
caused by resale product manufacturer. PAC does not warrant products it
does not manufacture except to the extent the warranty of the
manufacturer of the product at issue passes through or is otherwise
assigned to PAC. Buyer further agrees that Buyer's SOLE AND
EXCLUSIVE REMEDY for PAC's breach of the stated responsibility shall
be limited to the difference between the resale product manufacturer's
price to PAC and PAC's price to Buyer for resale products.

1.2.1.5 Expenses on non-warranty work


All repairs or replacements by PAC after the expiration of any applicable
limited warranty period will be performed in accordance with PAC’s
standard rate for parts and labour. Further, if upon PAC’s inspection and
review, PAC determines the condition of the product for which a warranty
claim is submitted is not caused by a defect in PAC’s material and
workmanship, but is the result of some other condition, including but not
limited to damage caused by any of the events or conditions set forth in
Section 1.2.1.3. Limited warranty exclusions, Buyer shall be liable for all
expenses incurred by PAC to conduct the inspection and review of the
product.

1.2.1.6 Exclusive remedy


The limited warranty contained herein constitutes Buyer's exclusive
remedy with respect to products sold by PAC and PAC's liability shall be
exclusively limited to the written limited warranty specified herein. No
employee, representative or agent of PAC is authorized to either expressly
or impliedly modify, extend, alter or change any of the limited warranties
expressed herein to Buyer.

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OptiFlash® General information

1.2.1.7 Procedure and costs


All limited warranty claims must be made in writing promptly following
discovery of any failure to conform to specifications or any defect in
materials or workmanship. Buyer must hold products for inspection by
PAC. If requested by PAC, Buyer must send the product to PAC for
inspection. Any such returns by Buyer will be at Buyer’s expense and
Buyer will remain liable for any loss of or damage to the product during
such product’s transportation to PAC. No products will be sent to PAC for
inspection unless PAC has authorized Buyer to do so.

1.2.1.8 Terms and conditions


PAC’s General Terms and Conditions are incorporated herein by
reference and Buyer accordingly agrees to be bound by the terms thereof.

1.2.2 Limitations on PAC liability

1.2.2.1 General
Buyer agrees that in no case shall PAC be liable for any special, incidental,
consequential, or punitive damages based upon any legal theory whether
or not such damages are foreseeable. Such damages include, but are not
limited to, loss of profits, loss of savings or revenue, loss of use of the
product or any associated equipment, cost of capital, cost of any substitute
equipment, facilities or services, downtime, the claims of third parties
including customers, injury to property and, unless precluded under
applicable state law, bodily and personal injury. PAC's total liability for any
and all losses and damages arising out of any and all causes whatsoever
including, without limitation, defects in the product(s), services, software,
or documentation supplied or breach of this agreement, shall in no event
exceed the purchase price of the applicable product(s). Buyer agrees
these limitations on PAC’s liability are reasonable and reflected in the
amounts charged by PAC for its products.

1.2.2.2 Buyer Data


If any data supplied by Buyer, whether in the form of Buyer specifications
or pursuant to any purchase order or other documentation, proves to be
inaccurate, any warranties or other related obligations of PAC relying
thereon will be void.

14 UM Abel_V1.0B_EN
General information OptiFlash®

1.2.2.3 Force majeure


This Standard Limited Warranty does not cover and PAC shall not be liable
for either direct or consequential damage caused, either directly or
indirectly, as a result of:
i any act of God, including but not limited to natural disaster, such as
floods, earthquakes, or tornadoes;
ii damages resulting from or under the conditions of labor disputes,
strikes or riots, insurrection, civil commotion or war;
iii damages or improper operation due to intermittent power line voltage,
frequency, electrical spikes or surges, unusual shock or electrical
damage;
iv accident, fire or water damage, neglect, corrosive atmosphere or
causes other than ordinary use;
v failure of supplies or transportation, or governmental action; or
vi any other causes beyond Seller's reasonable control.

1.2.2.4 Limitation on warranty claims


Prior to any obligation of PAC to perform any limited warranty service as
set forth herein, Buyer must have:
i paid all invoices to PAC in full, whether or not they are specifically
related to the product at issue; and
ii notified PAC of the limited warranty claim within sixty (60) days from
the date Buyer knew or had reason to know of the defect.

1.2.3 Compliance

1.2.3.1 General
These Warranty Terms are subject to change without notice. PAC also
retains the right to modify these warranty terms in order to comply with
policy or laws governing warranty issues in states or countries having
specific remedies differing or additional to those described within this
document.

1.2.3.2 Severability
If any one or more of the provisions or subjects contained in the
Agreement shall for any reason be held invalid, illegal, or unenforceable,
it shall not affect the validity and enforceability of any other provisions or
subjects.

UM Abel_V1.0B_EN 15
OptiFlash® General information

1.3 Software license


This End-User License Agreement (“EULA”) is a legal agreement between
you (either an individual or a single entity) and the manufacturer (“PC
Manufacturer”) of the computer system (“COMPUTER”) with which you
acquired or installed the Sulfacert software product(s) identified above
(“SOFTWARE PRODUCT” or “SOFTWARE”).
If the SOFTWARE PRODUCT is not installed into a new computer system,
you may not use or copy the SOFTWARE PRODUCT. The SOFTWARE
PRODUCT includes computer software, the associated hardware and
media, any printed materials, and any “on-line” or electric documentation.
By installing, copying, or otherwise using the SOFTWARE PRODUCT, you
agree to be bound by the terms of this EULA.
If you do not agree to the terms of this EULA, PC Manufacturer and PAC
are unwilling to license the SOFTWARE PRODUCT to you. In such event,
you may not use or copy the SOFTWARE PRODUCT and you In such
event, you may not use or copy the SOFTWARE PRODUCT, and you
should promptly contact your local PAC representatives for return of the
unused product(s) for a refund.

The SOFTWARE PRODUCT is protected by copyright laws and


international copyright treaties, as well as other intellectual property laws
and treaties. The SOFTWARE PRODUCT is licensed, not sold.

1.3.1 Grant of license

This EULA grants you the following rights:


• Software
You may install and use one copy of the SOFTWARE PRODUCT on
the COMPUTER. A license for the SOFTWARE PRODUCT may not
be shared or used concurrently on different computers.
• Back-up Utility
If PC Manufacturer has not included a back-up copy of the
SOFTWARE PRODUCT with the COMPUTER, you may use the
back-up utility, if included with the SOFTWARE PRODUCT, to make a
single back-up copy of the SOFTWARE PRODUCT. You may use the
back-up copy solely for archival purposes. After the single back-up
copy is made, the backup utility will be permanently disabled.

16 UM Abel_V1.0B_EN
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1.3.2 Description of other rights and limitations


• Limitations on Reverse Engineering, Decompilation and Disassembly
You may not reverse engineer, decompile, or disassemble the
SOFTWARE PRODUCT, except and only to the extent that such
activity is expressly permitted by applicable law notwithstanding this
limitation.
• Separation of Components
The SOFTWARE PRODUCT is licensed as a single product. Its
component parts may not be separated for use on more than one
computer.
• Single COMPUTER
The SOFTWARE PRODUCT is licensed with the COMPUTER as a
single integrated product. The SOFTWARE PRODUCT may only be
used with the COMPUTER.
• Rental
You may not rent or release the SOFTWARE PRODUCT.
• Software Transfer
You may permanently transfer all of your rights under this EULA only
as part of a sale or transfer of the COMPUTER, provided you retain
no copies, you transfer all of the SOFTWARE PRODUCT (including
all component parts, the media and printed materials, any upgrades,
this EULA and, if applicable, the Certificate(s) of Authenticity), and the
recipient agrees to the terms of this EULA. If the SOFTWARE
PRODUCT is an upgrade, any transfer must include all prior versions
of the SOFTWARE PRODUCT.
• Termination
Without prejudice to any other rights, PAC may terminate this EULA if
you fail to comply with the terms and conditions of this EULA. In such
event, you must destroy all copies of the SOFTWARE PRODUCT and
all of its component parts.

UM Abel_V1.0B_EN 17
OptiFlash® General information

1.3.3 Upgrades
If the SOFTWARE PRODUCT is an upgrade of a component of a package
of software programs which you licensed as a single product, the
SOFTWARE PRODUCT may be used and transferred only as part of that
single product package and may not be separated for use on more than
one computer.

1.3.4 Copyright
All title and copyrights in and to the SOFTWARE PRODUCT (including but
not limited to any images, photographs, animations, video, audio, music,
text and “applets,” incorporated into the SOFTWARE PRODUCT), the
accompanying printed materials, and any copies of the SOFTWARE
PRODUCT, are owned by PAC or its suppliers. The SOFTWARE
PRODUCT is protected by copyright laws and international treaty
provisions. You may not copy the printed materials accompanying the
SOFTWARE PRODUCT.

1.3.5 Dual-media software


You may receive the SOFTWARE PRODUCT in more than one medium.
Regardless of the type or size of medium you receive, you may only use
one medium that is appropriate for your single computer. You may not use
or install the other medium on another computer. You may not loan, rent,
lease, or otherwise transfer the other medium to another user, except as
part of the permanent transfer (as provided above) of the SOFTWARE
PRODUCT.

1.3.6 U.S. Government restricted rights


The SOFTWARE PRODUCT and documentation are provided with
RESTRICTED RIGHTS. Use, duplication, or disclosure by the
Government is subject to restrictions as set forth in subparagraph (c)(1)(ii)
of the Rights in Technical Data and Computer Software clause at DFARS
252.227-7013 or subparagraphs (c)(1) and (2) of the Commercial
Computer Software-Restricted Rights at 48 CFR 52.22719, as applicable.
Manufacturer is PAC, L.P., 8824 Fallbrook Drive Houston, TX 77064, USA.
For the limited warranties and special provisions pertaining to your
particular jurisdiction, please refer to the software product printed
materials.

18 UM Abel_V1.0B_EN
General information OptiFlash®

1.4 Assumptions

1.4.1 Good Laboratory Practice


Refer to Good Laboratory Practice or GLP as a system of management
controls for laboratories and research organizations to ensure the
consistency and reliability of results - as outlined in the Organisation for
Economic Co-operation and Development (OECD) Principles of GLP and
national regulations.
GLP applies to non-clinical studies conducted for the assessment of the
safety of chemicals to man, animals and the environment. The
internationally accepted definition reads:
• Good Laboratory Practice (GLP) embodies a set of principles that
provides a framework within which laboratory studies are planned,
performed, monitored, recorded, reported and archived. These
studies are undertaken to generate data by which the hazards and
risks to users, consumers and third parties, including the environment,
can be assessed for pharmaceuticals (only preclinical studies),
agrochemicals, cosmetics, food additives, feed additives and
contaminants, novel foods, biocides, detergents, etc.
• GLP helps assure regulatory authorities that the data submitted are a
true reflection of the results obtained during the study and can
therefore be relied upon when making risk/safety assessments.

1.4.2 The standards of laboratory safety


Refer to the standards of laboratory safety, wearing appropriate gloves,
glasses and clothing to handle materials safely.

1.4.3 Electronic device


Refer to the standards of manipulating an electronically / electrical device
and electrical current safely.

UM Abel_V1.0B_EN 19
OptiFlash® General information

1.5 Return policy


No product may be returned, whether in warranty or out of warranty,
without first obtaining approval from PAC. No replacements will be
provided nor repairs be made for products returned without such approval.
A return authorization number must accompany any returned product. The
buyer will pay for the expense of returning the instrument to PAC for
service. The status of any product returned later than 30 days after the
issuance of a return authorization number will be subject to review.
Products may not be returned that are contaminated by radioactive
materials, infectious agents, or other materials constituting health hazards
to PAC's employees.

1.5.1 Returned product warranty determination


After PAC’s examination, warranty or out-of-warranty status will be
determined. If a warranted defect exists, the product will be repaired at no
charge and shipped pre-paid back to the buyer. Warranty repairs do not
extend the original warranty period.
If an out-of-warranty defect exists, the buyer shall be notified of the repair
cost. At such time, the buyer must issue a valid purchase order to cover
the cost of the repair and freight, or authorize the products to be shipped
back as is, at the buyer’s expense. Failure to obtain a purchase order
number approval within fifteen days of notification will result in the
products being returned as is, at the buyer’s expense.

1.5.2 On-site repair


If a PAC product cannot be made functional by telephone assistance or by
installing replacement parts, and cannot be returned to PAC for repair, the
following policy applies.
PAC will provide an on-site field service representative in a reasonable
amount of time, provided that the customer issues a valid purchase order
to PAC covering all transportation, subsistence, and prevailing labour
costs, including travel time, necessary to complete the repair. For warranty
field repairs, the customer will not be charged for the cost of
transportation, labour, or materials. If service is rendered at times other
than normal work periods, then special service rates may apply.

1.5.3 Inspection
This system was thoroughly inspected and carefully packed before
leaving our factory. Responsibility for its safe delivery was assumed by the
carrier upon acceptance of the shipment. Claims for loss or damage
sustained in transit must be made upon the carrier by the recipient as
follows.

20 UM Abel_V1.0B_EN
General information OptiFlash®

1.5.3.1 Visible loss or damage


Note any external evidence of loss or damage on the freight bill or express
receipt, and have it signed by the carrier’s agent. Failure to adequately
describe such external evidence of loss or damage may result in the
carrier’s refusing to honour your damage claim. The form required to file
such a claim will be supplied by the carrier.

1.5.3.2 Concealed loss or damage


Concealed loss or damage means loss or damage, which becomes
apparent when the merchandise is unpacked and inspected. Should
concealed loss or damage occur, make a written request for inspection by
the carrier’s agent within 15 days of the delivery date, then file a claim with
the carrier since the damage is the carrier’s responsibility.
By following these instructions carefully, we guarantee our full support of
your claim to be compensated for loss from shipping damage.

NOTE
DO NOT - for any reason - return the instrument without first obtaining
authorization.

1.5.4 Information
In any correspondence to PAC, please supply the data from the
nameplate, including catalogue number and serial number.
/i

Catalog number:
Serial number:
Purchase date:

UM Abel_V1.0B_EN 21
OptiFlash® General information

1.6 Disposal
Correct disposal of Waste Electrical and Electronic
Equipment in the end-of life
Applicable in the European Union and other European
countries with separate collection systems.

This product is designed for exclusive professional use by


commercial companies. This marking shown on the product or its
literature, indicates that it should not be disposed with other household
wastes at the end of its working life.
To prevent possible harm to the environment or human health from
uncontrolled waste disposal, please separate this from other types of
wastes and recycle it responsibly to promote the sustainable reuse of
material resources.
Business users should contact the producer or the importer and check the
terms and conditions of the purchase contract. If you have a separate
agreement with your producer or your importer on the end-of-life disposal
in a way that you will care for disposal by your own, would you please
ensure an environmentally sound disposal according to the legal
regulations for electric and electronic waste equipment in your country.
This product should not be mixed with other commercial wastes for
disposal.

The above WEEE-symbol is the official marking for equipment under the
WEEE-scope. In some EC-Member states "pure B2B equipment" is not
necessarily marked with the waste bin-symbol. To provide a homogenous
EC-wide procedure, PAC however uses the marking in all EC-Member
states.

1.7 Documentation

1.7.1 Document validity


This manual has been prepared with great care, in compliance with the
relevant regulations, and based on PAC’s experience and latest
knowledge.
The information in this document is therefore valid and correct at the
moment of release of this version. (The version number is indicated on the
front page of this manual). However, changes and improvements may be
made to this document at any time and without prior notice.
This document is only complete in conjunction with all other system-
related documents.

22 UM Abel_V1.0B_EN
General information OptiFlash®

This User Manual describes the following models of the Flash Point
Analyzer series:
/i

Abel Flash Point Analyzers Built in Fire Electric Gas


Liquid Extinguisher Igniter Igniter
Cooling
104010 High End Model Electric Igniter X X X
104011 High End Model Gas Igniter X X X
104012 Standard Model Electric Igniter X X
104013 Standard Model Gas Igniter X X
104014 Basic Model Electric Igniter X
104015 Basic Model Gas Igniter X

NOTE
If functions described in this user manual are not applicable for all of the
Flash Point Analyzer models listed above, then the respective sections
or paragraphs are marked with "only High End Model" or "only High End
and Standard Model", etc.

1.7.2 Document storage


This document is part of the apparatus that is described in it, and must be
kept in a safe place near the apparatus.
This document must be accessible at all times.

1.7.3 Language
The source language of this manual is English.
As a translation may be inaccurate or imprecise, the original source text
will be legally binding and shall prevail in the case of any difference
between the source text and any translation.

1.7.4 Typographical and authoring conventions


• Hardware buttons that can be pushed, software buttons that can be
clicked in the Man Machine Interface (MMI) of software applications,
menu commands that can be selected, and data that can be entered
via a keyboard, are indicated in the font as shown in the following
example:
Click OK.
• Combined menu selections in the MMI are indicated by the ‘>’ symbol,
e.g.
Select File > Save As.
• File names and texts in the MMI are indicated in the font as shown
here:
The menu Temperature of the Weather screen appears.

UM Abel_V1.0B_EN 23
OptiFlash® General information

• E-mail and internet addresses are indicated as in the following


example:
[email protected].
• Lists and enumerations without prescribed order are always preceded
by bullets (like this list).
• Steps in a procedure, which must be performed in consecutive order,
are always numbered.
• Abbreviations are defined upon their first use in a document (except
in a title).
• Throughout this manual, PAC L.P. and its subsidiaries are referred to
as ‘PAC’.
• Throughout this manual, PAC automatic laboratory equipment (or
device, unit, or apparatus) is referred to as the ‘instrument’.
• Throughout this manual, the complete analysis system is referred to
as ‘the system’.

24 UM Abel_V1.0B_EN
Safety OptiFlash®

2 Safety

UM Abel_V1.0B_EN 25
OptiFlash® Safety

2.1 Certifications
The system and its components have been designed with safety in mind.
The design applies to the use, the conditions and the instructions
described in the documentation.

The system meets the requirements of the European Directives


concerning health, hygiene and safety. The standards applied are listed in
the “CE Declaration of Conformity”.

For a copy of the corresponding declarations, please consult the Service


Organization of PAC (see back page).

If the user makes changes or modifications that are not expressly


approved by PAC, PAC reserves the right to void the user’s authority to
operate the equipment.

During performance or routine maintenance, the system operator may be


exposed to potentially dangerous chemicals, temperatures, electrical
voltages and/or other hazards. In order to reduce the personal risk
involved, the following guidelines are established. These requirements are
within accepted standards for general analytical laboratory operation.

WARNING
• Failure to follow the instructions and procedures contained in this
manual could result in death or serious injury.
• The instructions and procedures must be performed by qualified and
trained personnel only.
• Do not perform installation or maintenance operations or procedures
outside the scope of this manual.

Please refer to the corresponding Material Safety Data Sheet (MSDS) for
each PAC-supplied product and also reference the corresponding MSDS
that is vendor-supplied for each sample and standard utilized with the
product for the established safety requirements and government safety
and disposal standards.

26 UM Abel_V1.0B_EN
Safety OptiFlash®

2.2 Warning pictograms


A warning pictogram denotes a dangerous situation that, if not avoided,
will result in serious injury or death. The following warning pictograms can
be found in the manuals and on the apparatus.

WARNING
General warning

WARNING
Danger of high voltages: shock hazard, electrocution hazard

WARNING
Fire hazard

WARNING
Hot surfaces present: burn hazard

WARNING
Cold surfaces present: freeze hazard

WARNING
Danger to jam hands or feet

WARNING
Pinch danger

WARNING
Wedge present

UM Abel_V1.0B_EN 27
OptiFlash® Safety

WARNING
Sharp edges present

WARNING
Dangerous fluids and gases

/i

WARNING
Harmful substances

2.3 Caution pictograms


A caution pictogram denotes a situation that, may result in injury or
damage. The following caution pictograms can be found in the manuals
and on the apparatus.

CAUTION
General caution

CAUTION
Recycling

CAUTION
Wear a gas mask!

CAUTION
Wear protective gloves!

CAUTION
Wear safety glasses!

28 UM Abel_V1.0B_EN
Safety OptiFlash®

2.4 Note pictograms


A note pictogram denotes a recommendation that, if not followed, may
result in minor damage. The following note pictogram can be found in the
manuals.

NOTE
General note

2.5 Tip pictograms


A tip pictogram denotes a recommendation that can help in understanding
how to operate or service the apparatus. The following tip pictograms can
be found in the manuals.

TIP
General tip

TIP
Read the Service Manual

2.6 Environmental protection


Please observe all local regulations and recommendations for the
disposal, recycling or environmentally friendly processing of parts and
materials that have been used or replaced during installation, operation,
and maintenance tasks.

UM Abel_V1.0B_EN 29
OptiFlash® Safety

30 UM Abel_V1.0B_EN
Introduction OptiFlash®

3 Introduction

UM Abel_V1.0B_EN 31
OptiFlash® Introduction

3.1 Intended use


The OptiFlash® flash point analyzer, described in this document, has been
designed and is intended for the empirical determination of the flash point
of combustible liquids in accordance with standardized test procedures
and standards.

Any other use or modification of the apparatus, without written agreement


from PAC, will be regarded as non-compliant: PAC will not be liable for any
possible resulting damage or injury and the warranty will be voided.
The apparatus may only be operated and serviced by trained, qualified
and authorized persons.
The operator must refrain from any operation that can affect the safety of
the system and persons. The operator is always required to ensure that
the apparatus is in proper condition when it is operating.

3.2 Intended audience


This document is intended for customer personnel that installs, sets up,
calibrates and operates the instrument in order to perform analyses, does
preventive maintenance on the instrument and maintains its internal
database.

The content of this document must be read, understood and observed in


all points and by each person responsible for preparation, transport,
storage, installation, operation and maintenance of the instrument, before
starting to work with and on the instrument.

3.3 Applicable standard test methods


/i

Standard method Remark


EN ISO 13736 International standard test method
IP 170 International standard test method

3.4 Introduction to OptiFlash® Flash Point


Analyzers
Flash point The flash point determination is an empirical method. It is therefore
determination important to comply with the standard specifications as accurately as
possible, both in respect of the equipment and of procedures. The flash
point of a material is used in transport and safety provisions to define
"flammable" and "combustible" substances. The flash point is one of
several material properties referred to in the determination of the overall
fire risk of a material.

To determine the flash point, the test cup is filled up to a particular marking
with the sample. The sample is heated at a constant rate of heating whilst
being continuously stirred.
A small gas flame or electric igniter is immersed in the cup at regular
intervals, during which stirring is interrupted.

32 UM Abel_V1.0B_EN
Introduction OptiFlash®

The flash point is defined as the lowest temperature of the liquid at which
the vapour above the sample ignites as a result of the introduction of the
flame.

The test procedures are standardized and laid down in the above-
mentioned standards (see 3.3 Applicable standard test methods).
The measurement period is from approx. 30 to 60 minutes, depending on
the flash point of the material. With manual measurement, high
requirements are set of the laboratory technician carrying out the
measurement, both in respect of the handling of the sample (avoidance of
loss of volatile substances, precise observation of the flash point) and of
the subsequent cleaning of the equipment.

When using this test equipment the operator's only task is to place the test
cup in the heating block, fill it with the sample and remove the test cup
once measurement is complete. It is necessary to pay attention to the
standards while preparing the sample.

The OptiFlash® OptiFlash® automatic flash point analyzers are designed to simplify the
Flash Point testing of hydrocarbon and other chemical samples using the Abel or other
Analyzer series closed cup test methods.

OptiFlash® analyzers are well known by their proven reliability, superior


design and quality. The OptiFlash® series has been designed to save
time, money and bench space. The OptiFlash® automatically determines
the flash point in strict compliance with the appropriate test method. In
addition to standard test methods, the OptiFlash® may be programmed
with user-defined test methods.

To increase test productivity on products with an elevated flash point, there


is a capability to start with fast heating rate. The instrument automatically
switches to the standard heating rate at appropriate temperature to ensure
accurate result. When the flash point is detected, the results are
automatically corrected for standard barometric pressure and displayed
on a bright, easy-to-read OptiFlash® graphics readout and can also be
output automatically on an optional printer or computer system.

UM Abel_V1.0B_EN 33
OptiFlash® Introduction

3.5 List of abbreviations


/i

°C Degrees Celsius
°F Degrees Fahrenheit
AN Application Note
CAN bus Control Area Network
exp. FP expected Flash Point
FP Flash Point
hPa hecto Pascal (1 hPa = 1 mbar)
ID Identity - Identification
K Degrees Kelvin
kPa kilo Pascal (1 kPa = 10 mbar)
LCD Liquid Crystal Display
LED Light Emitting Diode
LIMS Lab Information Management System
mA milliamps
mmHG millimeters of mercury column
MMI Man Machine Interface
P/N Part Number
PAC Petroleum Analyzer Company, L.P.
QC Quality Control
Temp. Temperature
TFT Thin Film Transistor

3.6 Rating plate


The rating plate is located on the rear of the OptiFlash® housing.

34 UM Abel_V1.0B_EN
Introduction OptiFlash®

3.7 Technical specifications


/i

Operating voltage range 100 - 240 VAC ±10% (automatic switching)


Operating voltage frequency 50/60 Hz
range
Max. power consumption 500 W
Stand-by power consumption ≤1W
Fuses T 10A (2x)
Maximum dimensions 250mm x 510 mm x 560 mm
(width x depth x height)
Weight approx. 25 kg (55 lbs)
Operating temperature range +10 °C to +35 °C (+50 °F to +95 °F)
Max. relative humidity max. 80% rel. at +35 °C (+95 °F)
(non condensing)
Storage temperature range -25 °C up to +70 °C (-13 °F to +158 °F)
Gas connection / gas pressure Propane or butane / 5 kPa (50 mBar)
(only for instruments with gas
ignition option)
Temperature range for flash point -35 °C to +120 °C (-31 °F to 248 °F)
determination
User interface (MMI) 7-inch color TFT touchscreen
Communication interfaces • 2x USB A (1x at the rear, 1x at the front of the
instrument):
Connection of an optional external printer,
external keyboard, mouse or memory device
(USB key) and for data transfer and firmware
update
• RS-232 serial port: connection to LIMS with
user-customizable communication protocol
(CTS, ENQ, ACK, XON, XOFF)
• RJ45: Ethernet connection for networking with
IRIS®, data transfer and firmware update
Fire extinguisher gas pressure Fire extinguisher gas: N2 (inlet at the rear of the
specification instrument)
Gas pressure at inlet:
• min. 2000 hPa (2 Bars)
• max. 8000 hPa (8 Bars)
External alarm output Potential-free changeover contact load capacity
max. 250 V / 5 A
Temperature rates 0.2 to 3 °C/min
user selectable (fast temp rate (ambient to 100 °C) 6 °C/min ± 2 °C)
Stirrer speed 30 rpm (± 5 rpm) - EN ISO 13736
user adjustable within 0 to 300 rpm
Block cooling speed, empty cup
- air cooled: ≤ 300s (25 °C to 10 °C)
- liquid cooled: ≤ 20min (25 °C to -20 °C)

UM Abel_V1.0B_EN 35
OptiFlash® Introduction

36 UM Abel_V1.0B_EN
Description OptiFlash®

4 Description

UM Abel_V1.0B_EN 37
OptiFlash® Description

4.1 Views of the OptiFlash®

4.1.1 Front view

OptiFlash® – Front view

A ON/Standby button with indicator light (green = ON, red = Standby)


B USB port, type A, for connection of an external printer, USB key, mouse or an external
keyboard
C Gas control valve (only instruments with gas ignition option)
D Gas igniter connection (only instruments with gas ignition option)
E Automatic lift arm for the test equipment
F Automatic shutter/opener device link for the igniter shutter plate
G Fire extinguisher system (only High End and Standard Model)
H Test cup with handle
I Test module
J Test cup-cover insert with mountings for the test accessories
K Fire detection sensor (UV-Sensor, only High End and Standard Model)
L Quick coupling to connect the test cup-cover insert to the lift arm and stirrer drive shaft
M Accessories holder (park position) for the electric igniter, flash point detection sensor
and sample temperature probe
N Connector for the electric igniter (grey)
O Connector for the flash point detection sensor (blue)
P Connector for the sample temperature probe (green)
Q MMI (Man Machine Interface) touchscreen

38 UM Abel_V1.0B_EN
Description OptiFlash®

4.1.2 Rear view

OptiFlash® – Rear view

A Fire extinguisher gas source inlet connector (only High End and Standard Model)
B Mains switch
C Power supply mains socket
D Inlet connection for external liquid cooling devices (only High End Model)
E Outlet connection for external liquid cooling devices (only High End Model)
F Gas connection (only instruments with gas ignition option)
G External alarm output connector (option)
H RS232 connector for Debug and LIMS communication
I RJ45 Ethernet connector for connection to the network
J USB port, type A, for connection of an external printer, USB key, mouse or
an external keyboard

UM Abel_V1.0B_EN 39
OptiFlash® Description

4.1.3 Connection ports/Interfaces


The following connection ports/interfaces are available:

At the front of the • USB port, type A: connection of either


OptiFlash®
- an optional external printer
- or an USB memory stick for software updating and data transfer
(results, products, etc.)
- or an external mouse
- or an external keyboard
• Connector for the electric igniter
• Connector for the flash point detection sensor
• Connector for the sample temperature probe
• Gas igniter connection (only instruments with gas ignition option)

At the rear of the • USB port, type A: connection of either


OptiFlash®
- an optional external printer
- or an USB memory stick for software updating and data transfer
(results, products, etc.)
- or a external mouse
- or an external keyboard
• RS232 connector for Debug and LIMS communication
• RJ45 Ethernet connector: connection to the IRIS® network on a
Server PC via a router
• Power supply mains socket
• Fire extinguisher gas source inlet connection (only High End and
Standard Model)
• Gas source inlet connection for a gas igniter (only instruments with
gas ignition option)
• In and Outlet connection for external liquid cooling devices (only High
End Model)
• External alarm output (option)

40 UM Abel_V1.0B_EN
Description OptiFlash®

4.2 Test equipment

4.2.1 Test cup – Abel

A B

Abel test cup

A Test cup with handle


B Sample filling gauge

Test cup – sample At the inner side of the test cup is a rod bent upwards and terminating in
filling gauge a point (B). The point indicates the filling level of the sample. When filling
in a sample into the test cup, make sure
• that the filling level is aligned with the point
• that no sample gets onto the test cups inner surface above the
marking

Otherwise, precise flash point measurement results cannot be ensured.

UM Abel_V1.0B_EN 41
OptiFlash® Description

4.2.2 Test cup-cover insert – Abel

NOTE
• The OptiFlash® can be operated with either an electric igniter or, as
an option, with a gas igniter.
• When using a gas igniter, an electric igniter must also be installed as
a fallback.

Test cup-cover The figure below shows the test cup-cover insert of the OptiFlash® and the
insert with electric arrangement of test accessories with electric ignition.
igniter

D E

C F

B G

K
A

Abel test cup-cover insert and test accessories with electric igniter

A Test cup-cover insert


B Flash point detection sensor
C Shutter plate linkage
D Sample temperature probe
E Stirrer drive coupling
F Test equipment quick coupling
(connection of test equipment with the automatic lift arm)
G Electric igniter
H Shutter plate
J Stirrer shaft
K Stirrer

42 UM Abel_V1.0B_EN
Description OptiFlash®

Test cup-cover The figure below shows the test cup-cover insert of the OptiFlash® and the
insert with gas arrangement of test accessories with a gas ignition option.
igniter option

C E

D M

B J

G K

Abel test cup-cover insert and test accessories with gas igniter option

A Test cup-cover insert


B Flash point detection sensor
C Shutter plate linkage
D Sample temperature probe
E Stirrer drive coupling
F Test equipment quick coupling (connection of test equipment with the automatic lift
arm)
G Electric igniter as a fallback
H Shutter plate
J Stirrer shaft
K Stirrer
L Gas igniter
M Bead as reference mark for size of gas igniter flame

4.2.3 Parts of the test cup-cover insert and test accessories


The test cup-cover insert consists of several parts and is equipped with
supports for the test accessories.

Sample The sample temperature probe is a Pt100 IEC751 Class-A platinum probe
temperature probe with a built-in memory chip including probe correction values. This means
the OptiFlash® automatically recognizes the probe and imports data at
plug-in to its connector on the front of the OptiFlash®. There is no need to
manually enter probe correction values and probe ID. Up to 10 calibration
points can be memorized (2 calibration points as standard).

Flash point The automatic flash point detection sensor consists of a stainless steel
detection sensor jacket with a thermocouple at the lower end to detect temperature
differences.

UM Abel_V1.0B_EN 43
OptiFlash® Description

Shutter plate The test cup-cover insert has a shutter plate which opens a window to
allow the igniter to dip into the sample. The instrument's shutter device
connects with the linkage on the shutter plate while a test is initiated.
During the test, the shutter device opens and shuts the igniter window
periodically. This is carried out fully automatically and controlled by the
internal software of the OptiFlash®, according to the test method
requirements for the currently running test.

Bead as reference Upon the cover there is a bead mounted. The bead is a reference mark to
mark for flame decipt the size of the gas igniter flame (3.6 mm to 4.1 mm), as required by
size adjustment the standard.

Electric igniter The OptiFlash® can be operated with either an electric igniter or an
optional gas igniter.

Gas igniter OptiFlash® instruments with gas igniter option provide a connection for
external gas sources at the rear side of the housing as well as a
connection for the gas igniter itself at the front side of the housing.
To operate the gas igniter, the use of propane/butane gas is
recommended.
When using a gas igniter, an electric igniter must additionally be installed.
This is because the control of the OptiFlash® detects if the gas flame
extinguishes during a test. In that case the electric igniter will immediately
be actuated to reignite the flame.
If a fire extinguisher is installed (only High End and Standard Model), the
UV sensor on the right hand side is the gas flame detector.
Without a fire extinguisher option (Basic Model) the gas flame detection is
enabled by a change in resistance of the electric igniter.

Stirrer The stirrer is driven by the stirrer drive which is located in the automatic lift
arm of the OptiFlash®. The stirrer shaft works as the link for both, stirrer
and drive. As soon as the test cup-cover insert is connected to the
automatic lift arm, the stirrer is also connected with the stirrer drive and
ready for a test.

44 UM Abel_V1.0B_EN
Description OptiFlash®

4.2.4 Self-positioning automatic lift arm

C A

Self positioning automatic lift arm with test equipment

A Automatic lift arm


B Test equipment
C Test equipment quick coupling/uncoupling device (push button with integrated spring
mechanism)

Once the test cup is inserted in its place in the instrument, filled with a
sample and the test equipment is assembled and connected to the lift arm,
the control of the OptiFlash® brings all equipment into its intended position
fully automatically when a test is started.

UM Abel_V1.0B_EN 45
OptiFlash® Description

4.3 Features

4.3.1 Cooling features


OptiFlash® analyzers have several cooling features.

Internal cooling All Abel OptiFlash® models include internal cooling devices (Peltier
system element and fan) to cool down the heating/cooling block, test cup, cover
and sample.

Liquid cooling Abel OptiFlash® High End Models have an additional liquid cooling circuit.
system In conjunction with an external liquid circulation cooler coolant flows
around the heating/cooling block and cools down the Peltier element in
addition. Liquid cooling is recommended for samples with expected flash
points below 10 °C (50 °F).

4.3.2 Fire detection features


The OptiFlash® High End and Standard Models are equipped with fire
detection sensors and an automatic fire extinguisher system.

Fire extinguisher Built-in ultraviolet fire sensors alert you instantly to flames outside the test
system cup. The system detects a fire time of 5 seconds minimum and triggers a
visual and acoustic fire alarm. A fixed gas-based fire suppression system
will be activated, if necessary.
After a fire alarm, switch off and restart the instrument.

4.3.3 Alarms/Warnings
Alarms/Warnings are accompanied by an audio alarm buzzer. They
remain visible as long as the default persists; even if the alarm has been
acknowledged.
Alarms warn the operator in the event of a malfunction whether the Flash
Point Analyzer is in test or in idle:
• detection of a default during the test run
• component failure detection
• detection of a safety state (either absolute or fixed by the user)

WARNING
When the alarm buzzer is triggered, the operator must display the cause
and ensure that safety features are working correctly, in general.

Failure alarm detection has at least one of the following consequences:


• a test cannot be started
• a test in progress is stopped

When a test is stopped the following occurs (if a power supply cut-off has
not already occurred):

46 UM Abel_V1.0B_EN
Description OptiFlash®

• a message appears on the screen


• a test in progress is stopped
• the OptiFlash® goes into the cooling phase

When a test has been stopped due to a fire outside the test cup:
After extinguishing, the instrument must be switched off and restarted
again (see also chapter 9. Troubleshooting).

4.4 Optional accessories


For the optimum use of the OptiFlash®, a wide range of optional tools and
accessories is available.

4.4.1 Optional external data management software: IRIS®

IRIS® software The IRIS® software has been designed and is intended to provide data
management features, including the ability to:
• control and monitor PAC instruments;
• collect and archive test data;
• perform and report on test results and trends;
• provide analysis of collected result data;
• connect to external Lab Information Management Systems (LIMS).

IRIS® collects test results from your PAC instruments and stores this data
in an SQL database.
With the integrated online manager you can define your operation, tests
and instruments. You can also specify users, access privileges and test
result parameters.
The workbench, a further component of IRIS®, communicates with the
instruments: it controls the execution of tests and gathers and analyzes
real-time data.
Each PAC instrument has a PAC instrument plug-in associated with it.
Instrument plug-ins extend the functionality of the workbench by providing
features that are specific to the corresponding instrument.
IRIS® comes in two versions:
• a stand-alone version
• a Client-Server version

4.4.2 Optional external printer


An external printer, available as optional accessory, allows all printouts of
the results and the quality control database.

NOTE
The printer must support PCL5 emulation language (or above such as
PCL6 or variants such as PCL5e).

See printer documentation provided for explanations on its operation.

UM Abel_V1.0B_EN 47
OptiFlash® Description

4.4.3 Optional bar code reader

Bar code reader

Bar code reader

A bar code reader is available as an optional accessory. The bar code


reader allows entering of the sample name or number during test
configuration without spelling mistakes. When connected, the bar code
reader can be activated after selecting the sample name/number field.

4.4.4 Optional calibrator (probe simulator) for the


temperature measuring system

Probe simulator A PT100 probe simulator is available to calibrate the temperature


measuring system of the OptiFlash®.

4.4.5 Optional pressure gage for the ambient pressure


sensor

Pressure gage For the calibration of the ambient pressure sensor, a reference barometer
indicating absolute pressure values (not values corrected to sea level) is
required.
The optional available pressure gage meets the requirements for the
calibration of the instruments ambient pressure sensor.

4.4.6 Optional connection cables

Connection cables • Printer cable


• Ethernet cable
• RS 232 cable

4.4.7 More optional tools for calibration and adjustment

More tools for For the part numbers of the above mentioned optional accessories and for
calibration and more optional tools for the calibration and adjustment of the OptiFlash®,
adjustment see chapter 8.5. Optional available parts and accessories.

48 UM Abel_V1.0B_EN
Description OptiFlash®

4.5 Access levels


Password security Instrument configuration, calibration and maintenance functions can be
password protected by setting supervisor and maintenance passwords in
the instrument setup database.
Operator functions, necessary for test runs, cannot be password
protected.
If a supervisor password is set, only the supervisor has access to
important and/or sensitive operating parameters and functions of the
instrument, the access level 1. The supervisor will have to enter a special
password to access these functions.
If a maintenance password is set, only qualified technicians have access
to the units service parameters, diagnostic and calibration menus, the
access level 2. The technician will have to enter a special password to
access these functions.
When the unit is switched on, it goes to the configured start up access
level.
The system control of the OptiFlash® has a password protection with three
user levels.

Multi-level The three user access levels are:


passwords
1 Operator (Level 0, no password protection possible)
2 Supervisor (Level 1, password protection possible)
3 Maintenance (Level 2, password protection possible)

The lock symbol in the status bar of the touchscreen indicates the current
active access level.

NOTE
When the instrument is shipped, there is no password protection for the
Supervisor and Maintenance level.

NOTE
The system administrator should set-up these passwords during installa-
tion to prevent unauthorized persons from changing the settings of the
instrument. In this way, access to important operations can be restricted
to a limited number of persons.
The set-up of passwords for access levels is covered in chapter 7.7. The
Instrument Setup database >7.7.1.4. Accessibility.

When an access level is confirmed by entering the correct password, it


remains available until a lower access level is explicitly requested or
during a time set in the instrument‘s internal parameters. If the
touchscreen does not detect any contact up to the end of this time, the
access level is reset to the default level as configured in the instrument
setup database. The countdown is reset at each touchscreen contact.

UM Abel_V1.0B_EN 49
OptiFlash® Description

Example:
If the Operator level is configured as default access level at power on and
Maintenance level is currently active, the instrument will change
automatically to the Operator level after the access level reset time has
elapsed.

However it is not necessary to wait until the access level reset time has
elapsed. The access level can be reset immediately by pressing the lock
symbol in the status bar of the touchscreen. The following message
appears:

Default access level reset message

Press the Continue button to confirm the access level reset message or
press the Cancel button to cancel the action.

50 UM Abel_V1.0B_EN
Description OptiFlash®

4.6 The Man Machine Interface (MMI)

4.6.1 Touchscreen
The OptiFlash® analyzers provide a Man Machine Interface (MMI) with a
large (7-inch) high-resolution graphic color TFT touchscreen.
A number of large area function keys allow short cuts to most frequently
used functions for comfortable operation. User/machine dialogue is
carried out via a virtual keyboard, keypad and location sensitive graphic
buttons located on the touchscreen.

4.6.2 Precautions for the touchscreen


• Avoid high temperature and high humidity. Ensure that the storage
and operating temperatures, given in the Technical Specifications, are
observed (environmental requirements).
• The touchscreen shall be operated within the limits specified in the
Technical Specifications.
• Water may cause damage or discoloration. Clean any condensation
or moisture from any source immediately.
• Electricity fed to a touchscreen with moisture on its surface may
damage it. Gently wipe off any moisture or let it dry before using the
touchscreen.
• The touchscreen is rugged, but can be easily scratched if rubbed or
forcibly touched by hard or pointed objects. Handle the touchscreen
with care so as not to scratch it.
• The touchscreen can be marred by fingerprints, aqueous fluids,
starch, oil or fat. If the screen becomes discolored, gently wipe it with
a soft and clean cloth. The touchscreen material provides high
resistance to the most chemicals and organic solvents encountered in
the flash point detection environment (acetone, toluene,
trichlorethylene, alcohol or the like). Ordinary glass cleaner can be
used to clean the touchscreen or housing.

UM Abel_V1.0B_EN 51
OptiFlash® Description

4.6.3 The main screen

1. Switch the main power switch at the back of the instrument to the ON
position.
A red indicator lamp on the ON/Standby button at the front of the
OptiFlash® lights up indicating that the analyzer is powered on and in
Standby mode.
2. Push the ON/Standby button at the front of the instrument.
• The indicator lamp on the ON/Standby button changes from red to
green.
• A self diagnostic test is started.
• When the self diagnostic test is completed, the main screen
appears with the Run menu opened:

The main screen –


page 1

Page 1 of the main screen – Run menu

3. Use the arrow Down button at the left of the screen to access the
second page of the main screen.

52 UM Abel_V1.0B_EN
Description OptiFlash®

The main screen –


page 2

Page 2 of the main screen – Run menu

Initiating a test requires only the following parameters:


• the operator name
• the sample ID
• the product name
• the expected flash point temperature

These parameters can either be:


• selected in lists pre-configured by the supervisor and stored in the
internal database of the OptiFlash®
• or entered manually using the virtual keyboard and keypad

UM Abel_V1.0B_EN 53
OptiFlash® Description

4.6.4 The virtual keyboard and keypad

The virtual The keyboard appears each time a text entry field is activated on the
keyboard touchscreen to enter a new text or modify the one stored.

The virtual keyboard

The virtual keypad The virtual keypad is typical for all numerical entries. It appears each time
a numerical entry field is activated to enter a new value, or to change
settings by entering the desired numbers by pressing the 0-9 number
keys.

The virtual keypad

54 UM Abel_V1.0B_EN
Description OptiFlash®

4.6.5 Structure of the main screen

A B C

E
J

H G
Structure of the main screen

A Displaying of device type/instrument ID information and navigation bar (displaying of


the currently active menu/submenu)
B Icon bar (Displaying of status icons such as active alarms, warnings, USB device,
access level status. At the same time the icons are touch sensitive navigation buttons
for quick access to instrument settings and event log databases.)
C Time and Date (Displaying of actual time and date and quick access to time and date
setup menu)
D Displaying of the actual instrument status
E Displaying of actual measurement values
F Displaying instruction messages, test results
G Run/Stop buttons: Start test, Stop test, Remove Cup
H Main menu tabs: Run, Results, Advanced
J Test parameter fields with touch sensitive entry/selection buttons and status icons

Icons on the The icon bar on top of the main screen can display these icons:
main screen
/i

Displaying of an active alarm and quick access to alarm details available in


the event log database by pressing the icon.

Displaying of an active warning and quick access to warning details available


in the event log database by pressing the icon.

Displaying of an active USB device and quick access to the instrument setup
database “Backup/Restore” by pressing the icon.

Displaying of the current access status (Supervisor or Maintenance) and


quick access to the default access level reset screen by pressing the icon

Displaying of the current access status (Operator) and quick access to the
default access level reset screen by pressing the icon

UM Abel_V1.0B_EN 55
OptiFlash® Description

Next to the test parameter buttons the icons below can display:
/i

Reuse of the parameter value from the previous test

New parameter value selected

The parameter value must still be entered or confirmed

56 UM Abel_V1.0B_EN
Description OptiFlash®

4.6.6 The menu structure


/i

Main Databases and Submenus Access level


Menus permission
Run Operator
Results Result details Heating rate Operator
Advanced Environment Standard Supervisor
Products Supervisor
Operators Supervisor
Quality Quality control Operator
More... Quality Control Chart Operator
List Operator
Atmospheric Supervisor
Pressure
Sample probe Supervisor
1)
Extinguisher Supervisor
Sample probe Supervisor
circuit
Arm adjustment Supervisor
Touch panel Operator
Backlight Operator
Instrument Parameters Supervisor
setup
Date & Time Operator
More... Parameters Supervisor
Date & Time Operator
Backup + Restore Maintenance
Reset Maintenance
Service Measures Maintenance
Diagnostic
Information Event log Operator
About Operator
More... Event log Operator
About Operator
Counters Operator
Contacts Operator
1) only High End and Standard Model

UM Abel_V1.0B_EN 57
OptiFlash® Description

58 UM Abel_V1.0B_EN
Installation OptiFlash®

5 Installation

UM Abel_V1.0B_EN 59
OptiFlash® Installation

5.1 Care in unpacking


Carefully unpack the unit and its accessories and inspect for damage. If
equipment damage exists, keep the equipment, shipping carton and
packaging materials and file a claim with the final carrier. Usually, the
carrier will send an inspector to ascertain liability. Send a copy of the claim
to PAC or to your local sales office.

NOTE
Do not return the OptiFlash® or any part to the factory without factory
authorization.

After unpacking, verify the unit and its accessories as well as any possible
damage sustained in transit, which must immediately brought to the
attention of the carrier so that a statement of damage can be made.
The various parts of the OptiFlash® are carefully verified and tested before
shipping.
Nevertheless, it is worth verifying that the equipment received
corresponds to the packing list enclosed.
On taking delivery of the OptiFlash®, unpack all parts.

5.2 Installation requirements


The OptiFlash® is designed for laboratory conditions. Prior to installing the
instrument, check that the requirements mentioned in chapter 3.7.
Technical specifications are met.

5.3 Installation location


• Install the unit on a level, flat and stable laboratory workbench.
• Make sure that the installation location is completely free from air
drafts and vibrations.
• In order to be able to determine the flash point visually (with the naked
eye), it should be possible to darken the room.
• Provide enough space so that the OptiFlash® can be operated
conveniently and with access to the rear connectors.
/i

WARNING
If the Instrument is used for tests of harmful or unknown substances,
harmful fumes and gases in hazardous concentrations and quantities
may form. Risk of damage to health through inhalation!
• For tests with harmful or unknown substances, only operate the
instrument inside a closed laboratory fume cupboard.
• If for tests of such substances the operation of the instrument inside
a closed laboratory fume cupboard is not possible, the operator and
other persons nearby must wear respiratory masks with appropriate
filters.

60 UM Abel_V1.0B_EN
Installation OptiFlash®

5.4 Connecting to the mains


The mains adaptor of the OptiFlash® has an operating voltage detection
device with automatic switching.
1. Make sure that the main voltage and frequency at the installation
location are within the ranges as specified on the rating plate of the
OptiFlash® and in chapter 3.7. Technical specifications of this user
manual.
2. Connect the mains plug of the instrument to a properly installed
grounded socket.

5.5 Installing the accessories holder


The accessories holder is used for accommodating the test accessories
such as the electric igniter, sample temperature probe, flash point
detection sensor and test cup cover insert.

Accessories holder
1. Put the accessories holder (A) with the keyholes onto the bolts and
push the holder fully downwards.
2. Slide the electric igniter (B), sample temperature probe (C) and flash
point detection sensor (D) into their appropriate park positions at the
holder (A) as shown in the figure above.

UM Abel_V1.0B_EN 61
OptiFlash® Installation

5.6 Installing the igniter


NOTE
• The OptiFlash® can be operated with either an electric igniter or, as
an option, with a gas igniter.
• When using a gas igniter, an electric igniter must also be installed as
a fallback.

5.6.1 Electric igniter

Installing the
electric igniter

C
B

Installing the electric igniter


A Electric igniter
B Electric igniter support
C Electric igniter connection (grey)

1. Insert the electric igniter (A) until the end stop into its support (B) on
the test cup-cover insert and fix it with the knurled head screw.
2. Connect the plug of the electric igniter to the respective connector (C)
at the front side of the instrument.

5.6.2 Gas igniter (option)


When using a gas igniter, an electric igniter must additionally be installed.
This is because the control of the OptiFlash® detects if the gas flame
extinguishes during a test. In that case, the electric igniter will immediately
be actuated to reignite the flame.

62 UM Abel_V1.0B_EN
Installation OptiFlash®

Installing a gas
igniter (option) E

C D

Installing of a gas igniter

A Gas igniter
B Electric igniter (as a fallback)
C Connector for the electric igniter
D Gas igniter connection
E Gas control valve
F Bead as reference mar for flame size adjustment

WARNING
Risk of fire due to a gas leakage!
The maximum gas pressure at the gas igniter connector of the Opti-
Flash® must not exceed 5 kPa.
Install a pressure reducer if the gas pressure at the connector is higher
than 5 kPa.

NOTE
The manufacturer recommends the use of propane/butane to operate
the gas igniter.

1. Install the gas igniter (A) to its support on the test cup-cover insert.
2. Connect the gas igniter hose to the gas igniter connector (D) on the
front side of the instrument.
3. Install the electric igniter (B) to its support on the test cup-cover insert.
4. Connect the plug of the electric igniter to the respective connector (C)
on the front side of the instrument.
5. Connect the gas supply source (e. g. gas bottle) to the gas connection
at the back of the instrument (see 4.1.2. Rear view).

UM Abel_V1.0B_EN 63
OptiFlash® Installation

5.7 Installing the accessories

A
C

Installing the accessories

A Sample temperature probe


B Flash point detection sensor (thermocouple)
C Connector for the flash point detection sensor (blue)
D Connector for the sample temperature probe (green)

Flash point 1. Install the flash point detection sensor (B) to its support on the test
detection sensor cup-cover insert and fix it with the knurled head screw.
2. Connect the plug to the blue connector (C) at the front of the
instrument.

Sample 1. Install the sample temperature probe (A) to its support on the test cup-
temperature probe cover insert and fix it with the knurled head screw.
2. Connect the plug to the green connector (D) at the front of the
instrument.

64 UM Abel_V1.0B_EN
Installation OptiFlash®

5.8 Connecting/disconnecting the test equipment


with/from the lift arm
Quick coupling of
test equipment
B C

Connecting the test equipment with the lift arm

A Test cup-cover insert with installed accessories


B Mounting receptacle
C Stirrer drive receptacle
D Stirrer shaft linkage

1. To connect the test equipment with the lift arm insert the test cup-cover
insert (A) and Stirrer shaft linkage (D) into the mounting receptacle (B)
and strirrer drive receptacle (C).

Quick uncoupling
of test equipment E
B C
1

A 2

Disconnecting the test equipment from the lift arm (only High End Model)

A Test cup-cover insert with installed accessories


B Mounting receptacle
C Stirrer drive receptacle
D Stirrer shaft linkage
E Quick uncoupling device (push button with integrated spring mechanism)

1. To disconnect the test equipment from the lift arm push the quick
uncoupling device (E).

UM Abel_V1.0B_EN 65
OptiFlash® Installation

2. Remove the test cup-cover insert (A) and Stirrer shaft linkage (D) from
their receptacles (B/C).
3. Release the quick uncoupling device (E).

5.9 Connecting to a PC

5.9.1 Optional external PC control


The OptiFlash® can be connected to the IRIS® network on a Server PC
via a router through the RJ45 Ethernet connector, which is located at the
rear of the instrument. The connection to the router is plug and play. The
OptiFlash® is automatically detected. Connection of the PC to the LIMS
can be done either by RS232 or Ethernet connection. For details about
communication formats refer to chapter 10.1. LIMS specification for
results.

5.10 Optional external alarm output connector


If you have an alarm system available in your laboratory, you can connect
the instrument to it with the aid of the optional external alarm output
connector. The connector is located at the rear of the OptiFlash® and
labelled with "EXT. ALARM".
The potential-free changeover contact of the alarm relay is switched and
controlled by the instrument’s software.
Based on the software control, the following options can be tapped from
the external alarm output connector:
• fire alarm
• end of test
• cooling down (e. g. to activate an exhaust ventilation system, while the
instrument cools)
• unit ready (or unit disabled)

Optional external alarm output connector

66 UM Abel_V1.0B_EN
Operation OptiFlash®

6 Operation

UM Abel_V1.0B_EN 67
OptiFlash® Operation

6.1 Preparation

6.1.1 Safety
This instrument has been carefully designed, manufactured and
inspected for quality. It has been equipped with a number of safety
features.
However, the use of this instrument may involve the handling of solvents,
chemicals, and other potentially dangerous flammable, toxic, etc.
materials.
Always exercise caution when handling these materials while operating
the instrument.
• read the manual
• wear proper protective clothing
• perform all suggested service procedures
• handle with care to prevent accidents

WARNING
The sample materials can be dangerous. Risk of poisoning, irritation or
burns!
• Wear proper protective clothing when handling solvents, chemicals,
and other potentially dangerous flammable, toxic, etc. materials.
• Handle all solvents, chemicals and other potentially dangerous
materials with care.
• The operator needs to have training about potential hazards, before
operating the system.

Wear safety glasses when handling dangerous materials.

Wear protective gloves when handling dangerous materials.

Use only PAC products and accessories with the OptiFlash®.


Defects or damage that result from the use of non-PAC branded or
certified products, accessories, software or other peripheral equipment
are excluded from warranty.

68 UM Abel_V1.0B_EN
Operation OptiFlash®

6.1.2 Preparing the OptiFlash®

WARNING
A damaged electric igniter may cause a risk of fire!
• If using an electric igniter, always check it for mechanical or other
damage, prior to starting the test. A damaged igniter may mean that
the ignition process is not carried out properly and consequently,
that the flash point is not determined correctly or determined at all.
• The fact that no flash point is determined may lead the operator to
assume, that the flash point of the sample is higher than the actual
value and therefore to choose a higher expected flash point. This
could result in the self-ignition of the sample – risk of fire!

WARNING
The test cup and test cup-cover insert may be hot. Risk of burns!
Take care when removing hot parts.

NOTE
The temperature of the heater block, test cup and sample must not be
higher than specified in the standards.

1. Check the igniter for signs of mechanical or other damage prior to


starting the test.
2. Insert the test cup into the heating block.

B B
A

Test cup lock and unlock positions

A Unlocking area
B Locking area
C Sample filling gauge

UM Abel_V1.0B_EN 69
OptiFlash® Operation

3. Lock the test cup by turning the handle to the left or right from the
unlocking area (A) to the locking area (B).
4. Connect the test cup-cover insert with the mounting receptacle of the
lift arm.
See chapter 5.8. Connecting/disconnecting the test equipment with/
from the lift arm
5. Check that the accessories (igniter, flash point sensor and sample
temperature probe) are connected to the respective connector
sockets.

6.2 Sampling

6.2.1 Pre-cooling
The standard of the applicable test method may require to cool down test
equipment and sample prior to starting a test.
The required temperatures can be found in the standard.

External sample Adjust the external cooling system (e, g. a refrigerator), if required.
pre-cooling Follow the procedure as described in the standard to cool down test
equipment and sample.

Internal sample The OptiFlash® includes internal cooling devices to cool down the heating/
pre-cooling cooling block, test cup, cover and also the sample.
The internal sample pre-cooling function can be enabled or disabled
individually for each custom product in the product database, see 7.4.1.
View parameter details of the products and 7.4.2. Add new custom
products.
(Remark: Internal sample pre-cooling does not comply with the standard.)
High End Models can additionally be connected to an external liquid
circulation cooler. If a liquid cooler is connected or not must be configured
in the instrument setup database, see 7.7.1. Instrument Parameters /
7.7.1.9. Device settings.

6.2.2 Sample handling

1. Prepare the sample according to the standard of the applicable test


method.
2. After sampling, close the sample container immediately with a tight
fitting closure.

70 UM Abel_V1.0B_EN
Operation OptiFlash®

6.2.3 Fill in the sample


The sequence, when the sample has to be filled into the test cup and
placed in the instrument depends on the conditions at test start. See also
6.3.2. Starting a test.

Pre-cooling not If no pre-cooling is required, or if the internal sample pre-cooling function


required or is used, fill in the sample into the test cup and insert the cup in its position
internal sample prior to start a test.
pre-cooling is used
After pressing the Start test button,
- the test will either be started directly (if no pre-cooling is required)
- or the instrument cools down the test equipment and sample
according to the settings in the products database.
(Remark: Internal sample pre-cooling does not comply with the standard.)
See also 6.3.2.1. Starting a test if pre-cooling is not required or internal
sample pre-cooling is used.

External sample If external sample cooling is performed (e.g. in a refrigerator), fill in the pre-
cooling cooled sample after the block has been pre-cooled.
After pressing the Precool button, the instrument cools down the test
equipment to the predefined settings in the products database.
As soon as the predefined block temperature has been reached, the
Operator is prompted to lift up the arm and fill in the sample.
See also 6.3.2.2. Starting a test if sample cooling is done externally (e.g.
in a refrigerator).

UM Abel_V1.0B_EN 71
OptiFlash® Operation

6.3 Perform measurements

6.3.1 Entering test parameters


After the OptiFlash® has been switched on, the menu tab Run opens and
the Run/Start test screen appears:

Entering test
parameters

The first page of the Run / Start test screen

1. Press the corresponding field on the touchscreen and enter the


required test parameters:
• Operator identification
• Sample ID
• Product name
• expected FP (Flash Point) temperature
• Pretest: On or Off

According to the instrument‘s setup, the test parameters can be entered


in different ways:
• either by selecting standard or customized predefined parameters
from the pre-stored list. The unit has implemented:
- a products database for up to 200 products
- an operator database for up to 40 operator identifications
• or reusing the parameters from the previous test
• or manual entering by the operator for each test using the virtual
keyboard or keypad
• or manual entering using an external keyboard and mouse if
connected

72 UM Abel_V1.0B_EN
Operation OptiFlash®

The icons below indicate whether all test parameters are entirely filled in:
/i

Reuse of the parameter value from the previous test

New parameter value selected

The parameter value must still be entered or confirmed

NOTE
• Confirming the expected FP (Flash Point) is mandatory.
• After a product change it is mandatory to confirm the expected FP
again.
• For an expected FP below 10 °C (50 °F) it is recommended to use
an external liquid cooling device. If the instrument does not recog-
nize a liquid cooling device, a warning message appears stating that
liquid cooling is recommended.

NOTE
Manually entered or changed test parameters are only valid for the sub-
sequent measurement. Permanent changes to the parameters must be
made in the products database. Regarding permanent changes of test
parameters see chapter 7.4. The Products database

Pretest For safety reasons, a pretest is recommended when tests are carried out
on samples for which the expected flash point is unknown.

NOTE
The pretest button on the Run/Start test screen is only visible if the pre-
test question parameter in the products database is activated for the
selected product. When deactivated, the pretest button is not displayed
on the Run/Start test screen and the expected FP button is then
extended over the entire width. See chapter 7.4. The Products database.

Provided that the pretest question parameter is activated, pretest can be


selected by pressing the Pretest button. The field changes from Off to On.
If Pretest is selected, an igniter dip-in cycle is activated for a certain
interval of temperature increase as from the start of a test. The dip in cycle
depends on the settings of the parameters “Test interval 1“ and “Test
Interval 2“ in the Products database.

NOTE
Measurements with pretest setting may only be considered as succes-
sive approximations to unknown flash points.

UM Abel_V1.0B_EN 73
OptiFlash® Operation

The Run / Start test screen has a second page to enter additional optional
test parameters, if required.

2. Use the arrow Down button on the left side of the screen to access the
second page of the Run / Start test screen

The second page of the Run / Start test screen

3. Press again the corresponding field on the touchscreen and enter


optional test parameters if required, e. g.:
• Sample description
• Note

6.3.2 Starting a test


After all test parameters are completely filled in, the instrument is ready.
Depending on the test start conditions one of the below buttons appears:

The green Start test button appears on the Run / Start test screen if the
following test start conditions are met:
• Pre-cooling is not required for the selected product
• or internal sample pre-cooling is enabled for the selected product.
When pressing the Start test button, the internal cooling device cools
down block and sample to the required temperature prior to starting a
test.

The blue Precooling button appears on the Run / Start test screen if the
following test start condition is met:
• External sample cooling is performed, e.g. in a refrigerator (internal
sample pre-cooling is disabled for the selected product).
When pressing the Precooling button, the internal cooling device cools
down block and test cup first. After the required temperature has been
reached, the operator is prompted to lift up the arm and fill in the pre-
cooled sample. After confirmation, the test will be started.

74 UM Abel_V1.0B_EN
Operation OptiFlash®

6.3.2.1 Starting a test if pre-cooling is not required or internal


sample pre-cooling is used

Preconditions If pre-cooling is not required or internal sample pre-cooling is enabled for


the selected product, the following preconditions are required:
• All test parameters are completely filled in
• The instrument is ready
• The green Start test button appears on the screen

Pre-cooling not
required or
internal sample
pre-cooling is used

The Run / Start test screen

1. Fill the sample into the test cup.


- Make sure that the quantity of sample is in accordance with the
standard.
- Make sure that no sample gets onto the test cup's inner surface
above the final liquid level.

2. Insert the test cup (with sample) in its position and connect the test
cup-cover insert including all accessories to the lift arm.
3. Press the Start test button.
- The lift arm lowers, positions the test cup-cover insert and closes
the test cup automatically.
- The Start test button changes to Stop test.
- If required, the OptiFlash® goes into the pre-cooling cycle to cool
down block and sample.
- After the correct temperature is reached, the test will be started.

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OptiFlash® Operation

The Run / Stop test screen – pre-cooling cycle

6.3.2.2 Starting a test if sample cooling is done externally (e.g. in a


refrigerator)

Preconditions Prior to starting a test with external sample cooling the following precondi-
tions are required:
• All test parameters are completely filled in
• The instrument is ready
• The blue Precooling button appears on the screen.

External sample
cooling

The Run / Start test screen with Precooling button

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Operation OptiFlash®

1. Insert the empty test cup (without sample) in its position and connect
the test cup-cover insert including all accessories to the lift arm.

NOTE
It is not absolutely mandatory to insert the test cup and install the test
cup-cover insert at this step of the procedure. If desired, test cup and test
cup-cover insert can also be pre-cooled externally, e.g. in a refrigerator.
In this case, insert the pre-cooled test cup with sample and install the
test cup-cover insert at step 4 of the following procedure.

2. Press the Precooling button.


- The lift arm lowers, positions the test cup-cover insert into the test
cup and closes the test cup automatically.
- The Start test button changes to Stop test.
- A message is displayed, stating that the OptiFlash® cools down
the block.
- As soon as the predefined temperature has been reached, the
screen displays further instructions.

A message indicates that the predefined block temperature has been


reached

3. Press OK to lift up the arm or abort the test by pressing Cancel.


If OK has been pressed:
- the lift arm goes up and opens the test cup.
- a message appears prompting the operator to fill in the sample
into the test cup and confirm the test start.

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OptiFlash® Operation

4. Fill the pre-cooled sample into the test cup.


- Make sure that the quantity of sample is in accordance with the
standard.
- Make sure that no sample gets onto the test cup's inner surface
above the final liquid level.
5. Confirm the message and start the test by pressing the OK button or
abort the test by pressing the Cancel button. If OK has been pressed:
- the lift arm lowers again, positions the test cup-cover insert into
the test cup and closes the test cup automatically.
- the test will be started

6.3.3 Stopping a running test

Stopping a test A running test can be stopped at any time by pressing the Stop test button.
A message screen comes up and asks if you really want to stop the test:
• to stop the test, confirm by pressing the Yes button
• or continue with the test by pressing the Cancel button.

The Run / Stop test screen – alarm message when stopping a test

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Operation OptiFlash®

6.3.4 Automatic flash point determination

Test in progress Once a test has been started by pressing the Start test button, the system
initiates the measurement process and carries out flash point determina-
tion automatically:
• an instrument self diagnostic is performed
• the zero point of the shutter device is adjusted
• the sample is heated up and being stirred
• the MMI touchscreen informs continuously about the actual status of
the test in progress

The Run / Stop test screen with actual test status information

Actual test status During a test is running, the Run screen provides actual test status
information information in realtime, such as:
• the actual instrument status (Igniter test, Start precooling, Heating,
Cooling down, Ready)
• the progress of the test on the bar indicator
• the actual temperature of the block (TBlock)
• the current air-pressure
• and the actual sample temperature (TSample)

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OptiFlash® Operation

6.3.5 Measurement completed

Test completed After the test has been completed,


• the test result (determined flash point) is displayed below the field
Flash point:
• the test result is automatically stored in the Results database
• the OptiFlash® goes into the cooling cycle, if the heating block or
sample temperature is above the cooling temperature set in the
products database.
If the heating block or sample temperature is at or below the set
cooling temperature, a yellow Remove Cup button is displayed,
indicating to remove the test cup and finish the test.

Remove Cup

The Run / Remove Cup screen

6.3.6 Removing the test cup

WARNING
The test cup, test cup-cover insert and the sample may be hot. Risk of
burns!
Take care when removing the hot test cup with the hot sample.

1. Press the Remove Cup button. The Remove Cup button changes to
Start test, indicating that the OptiFlash® is ready for a new test.
- The lift arm goes up and opens the test cup.

2. Unlock the test cup by turning the handle from the locking area (closed
lock pictogram) to the unlocking area (open lock pictogram).
3. Remove the test cup with the sample from the block.

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Operation OptiFlash®

4. Place the test cup with the sample in a suitable heat resistant storage
container.
5. For the disposal of the sample observe all local regulations.

6.3.7 Displaying and printing of test results


Displaying results At the end of a test, the test results including all test parameters are stored
automatically in the Results database.
The internal memory of the OptiFlash® can store up to 500 test results,
that can be displayed at any time.
To display and print the test results, refer to 7.1. The Results main menu.
1. To access the Results database, press the Results menu tab at the
bottom of the Run screen.

6.3.8 Cleaning the test equipment

Cleaning The test equipment must be cleaned thoroughly after the end of a test or,
at the latest, before running a new test. For detailed instructions refer to
chapter 8.3. Cleaning the test equipment.

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Database Management OptiFlash®

7 Database Management

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OptiFlash® Database Management

7.1 The Results main menu


Required access and permissions:

Required access • Level 0 (Operator):


Reading, printing, validating and transmitting of test results
• Level 1/2 (Supervisor/Maintenance):
Deleting of test results

7.1.1 Displaying, printing and saving of results


The Results database of the OptiFlash® can store up to 500 test results.
At the end of a test, the test result, including all test parameters, is stored
automatically.
These test results can be displayed at any time. The last result of the list
is the last test result stored. When the memory is full, the OptiFlash®
automatically deletes the first result stored (the oldest).

Displaying of 1. Press the Results menu tab at the bottom of the Run screen.
results The Results main menu opens.

Screen of the Results main menu


/i

Buttons on the Results main menu screen


Details Displaying the details of the selected result
Print Printing the details of the selected result
Validate Validating the selected result and sending it to the LIMS
Up/Down arrow Up/Down arrow buttons to scroll through the results pages

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The left side of the Results main screen displays:


• date and time of the results at the end of the tests
• Sample ID to identify the test results

The right side of the Results main screen displays:


• the corrected flash point for the selected result
• the expected flash point for the selected result

2. Use the Up/Down arrow buttons of the screen to scroll through the
stored results.
3. To view the details of a certain result, touch it or select it with the arrow
buttons and then press the Details button.

The Results details menu page 1

The left side of the first screen displays the test parameters of the result.
• Operator: operator initials
• SampleID: sample identification
• Sample des: sample description (if entried)
• Product: product identification
• Method No.: measurement method/standard
• Pretest: pretest On or Off
• Expected FP: the expected flash point
• Ignition type: type of igniter, electric or gas

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OptiFlash® Database Management

The right side of the first screen displays the measurement results.
• Flash point: the corrected flash point (air pressure corrected)
• Status: status of the result
• Performed: the date and time of the result at the end of the test
• Ending: End of test condition, e. g.:
- Stop on flash point, if the test was completed
- or Stop by operator, if the test was stopped manually
- or Stop on Alarm (followed by the relevant alarm message), if the
test was stopped due to an alarm
• The corresponding air pressure measured

4. Use the Up/Down arrow buttons on the right side of the screen to see
more details of test parameters and measurement results, such as:
• Instrument name
• Max. temperature
• Warning: events which occurred during the test and could
influence the result
• Uncorrected FP: the measured flash point
• Note: additional notes (if entried)
• Correlation
• File: file name

The Results details menu page 2

5. To exit the Results main menu details screen press the Exit button.

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7.1.2 Print button

Printing of results The complete result values, including all test parameters displayed, can
be sent to a connected printer. (For details about printout formats refer to
chapter 10.2. Printout specifications for results)
1. Press the Print button to print out the result displayed.

7.1.3 Validate button


After validating of a test result, it can be sent to the LIMS. (For details
about communication formats refer to chapter 10.1. LIMS specification for
results)

Validating results 1. Press the Validate button to validate a test result and send it to the
and sending it to LIMS.
the LIMS
7.1.4 Chart button

Displaying of the The heating rate, as a function of time, is stored as a part of the test result
heating rate chart and can be displayed on a chart.
1. Press the Chart button to display the heating rate curve.

Chart of the heating rate as a function of time

2. To exit the chart and return to the Result details pages press the Exit
button.

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OptiFlash® Database Management

7.1.5 USB button

Saving of results The USB button enables to save the (complete) results database to an
to an USB device USB device.
1. Connect an USB device to one of the USB connectors at the front or
the rear of the instrument.
2. Press the USB button to save the results database to the USB device.

7.1.6 Delete button

Deleting of results With Supervisor/Maintenance access level, the Delete button enables to
delete a selected result.
1. Press the Delete button to remove the result selected from the results
database.

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7.2 The Advanced main menu


The Advanced main menu is the gateway to the internal databases of the
OptiFlash®.
1. Press the main menu tab Advanced at the bottom line of the Run
screen.
The Advanced main menu opens.

The Advanced main menu screen

The Advanced main menu is divided into groups of databases as below:


• Environment:
with databases that contain the conditions for accurate measurements
according to the standards
• Quality:
with quality related parameters and calibration setting databases
• Instrument Setup:
with databases for the configuration and setup of the instrument
• Service:
with diagnostic functions for the maintenance of the instrument and
troubleshooting procedures
• Information:
with various types of information regarding the instrument and event
logs that have occurred during measurements

For details regarding the structure of menus and databases refer to


chapter 4.6.6. The menu structure.

2. For access to the databases, press the respective menu button.

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OptiFlash® Database Management

7.3 The Standard database


Required access and permissions:
• Level 0 (Operator): reading and printing of standard parameters
• Level 1 (Supervisor): level 0 + creation, adding and deleting of custom
test methods

The standard main menu allows accessing a database, stored in the


OptiFlash®, in which the pre-set standard test methods are stored. The
standard test methods include settings and limit values used by products
to monitor the flash point test.
Standard factory set test methods comply with international standard test
methods and cannot be changed.
However, with a level 1-access authorization (Supervisor), these standard
test methods can be displayed and copied as a basis for the creation of
new custom test methods, which can additionally be stored in the standard
database.
The Standard database allows storage of up to 50 standard and custom
test methods in total.
1. Press Advanced > Environment/Standard to enter the database.
The Standard database opens.

The Standard
database

The main screen of the Standard database


/i

Buttons on the Standard database main screen


Details Displaying the parameters of the selected test method
Add Add a new custom test method to the database
Delete (option) Delete a custom test method from the database (the delete button is
only visible when a custom test method is selected)
Up/Down arrow Up/Down arrow buttons to scroll through the list of test methods
Exit Exit the standard database

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2. Select a test method from the list on the left side of the screen by
pressing on the required method.

The main screen of the Standard database offers two possibilities to


proceed with test methods selected in the list:
- use the Details button to view the details of the selected test
method, see 7.3.1. View parameter details of test methods
- or use the Add button to create a new custom test method by
copying the selected one as a basis and modify and store it as a
new method, see 7.3.2. Add new custom test methods

7.3.1 View parameter details of test methods


1. Press the Details button to access the first page with standard
parameters.

Standard database
-first parameter
page

The first parameter page of the Standard database


/i

Parameters on the first page


Name Denomination of the standard, e.g. EN, ISO, IP, etc. and denomi-
nations of customer defined test methods
Temp. unit Temperature unit: °C / °F
Start Test min. Minimum sample temperature below the expected flash point, at
which the test will be started.
Start Test max. Maximum sample temperature below the expected flash point, at
which the test will be started
End of Test min. Minimum sample temperature above the expected flash point, at
which the test will be ended.

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Parameters on the first page


End of Test max. Maximum sample temperature above the expected flash point, at
which the test will be ended
Stirrer speed min. Minimum stirrer speed
Stirrer speed max. Maximum stirrer speed

2. Press the arrow Down button to access the second page with
standard parameters.

Standard database
-second parameter
page

The second parameter page of the Standard database


/i

Parameters on the second page


Switch heat rate min. The temperature to switch over from Heating Rate 1 min. to
Heating Rate 2 min. is calculated from the expected flash point
temperature value minus the value specified for Switch heat rate
min.
Switch heat rate max. The temperature to switch over from Heating Rate 1 max. to
Heating Rate 2 max. is calculated from the expected flash point
temperature value minus the value specified for Switch heat rate
max.
Heating Rate 1 min. Temperature increase per minute for Heating Rate 1 min. until
the calculated switch over temperature specified in Switch heat
rate min. is reached.
Heating Rate 1 max. Temperature increase per minute for Heating Rate 1 max. until
the calculated switch over temperature specified in Switch heat
rate max. is reached.

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Parameters on the second page


Heating Rate 2 min. Temperature increase per minute for Heating Rate 2 min. as from
the calculated switch over temperature specified in Switch heat
rate min.
Heating Rate 2 max. Temperature increase per minute for Heating Rate 2 max. as
from the calculated switch over temperature specified in Switch
heat rate max.

3. Press the arrow Down button to access the third page of standard
parameters.

Standard database
- third parameter
page

The third parameter page of the Standard database


/i

Parameters on the third page


Switch test interval The first igniter dipping takes place as soon as the sample tem-
min. perature specified in the start test settings has been reached.
If the expected flash point is lower than or equal to the temper-
ature specified for Switch test interval min., then the periodic
dipping of the igniter will take place according to the values as
defined for Test interval 1 min., otherwise according to the val-
ues specified in Test interval 2 min.
Switch test interval The first igniter dipping takes place as soon as the sample tem-
max. perature specified in the start test settings has been reached.
If the expected flash point is lower than or equal to the temper-
ature specified for Switch test interval max., then the periodic
dipping of the igniter will take place according to the values as
defined for Test interval 1 max., otherwise according to the val-
ues specified in Test interval 2 max.
Test interval 1 min. The Test interval 1 min. value specifies the minimum selectable
value for the frequency of igniter dipping. Every time the sam-
ple temperature increases by the value specified for Test inter-
val 1 min., the igniter dips into the test cup.

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Parameters on the third page


Test interval 1 max. The Test interval 1 max. value specifies the maximum selecta-
ble value for the frequency of igniter dipping. Every time the
sample temperature increases by the value specified for Test
interval 1 max., the igniter dips into the test cup.
Test interval 2 min. The Test interval 2 min. value specifies the minimum selectable
value for the frequency of igniter dipping. Every time the sam-
ple temperature increases by the value specified for Test inter-
val 2 min., the igniter dips into the test cup.
Test interval 2 max. The Test interval 2 max. value specifies the maximum selecta-
ble value for the frequency of igniter dipping. Every time the
sample temperature increases by the value specified for Test
interval 2 max., the igniter dips into the test cup.

4. Press the arrow Down button to access the fourth page of standard
parameters.

Standard database
- fourth parameter
page

The fourth parameter page of the Standard database


/i

Parameters on the fourth page


Safety test interval start The Safety test interval start min. temperature value specifies
min. the limit for the Safety test interval min.
Safety test interval start The Safety test interval start max. temperature value specifies
max. the limit for the Safety test interval max.
Safety test interval min. The Safety test interval min. value specifies the frequency of
igniter dipping. Every time the sample temperature increases
by the value specified for the Safety test interval min., the
igniter dips into the test cup.
Safety test interval max. The Safety test interval max. value specifies the frequency of
igniter dipping. Every time the sample temperature increases
by the value of the Safety test interval max., the igniter dips
into the test cup.

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5. In order to print the parameters of the actual standard, including the


values, press the Print button.
6. Press the arrow Up button to return to the previous page or press the
Exit button to return to the main screen of the Standard database.

7.3.2 Add new custom test methods


1. On the left side of the Standard database main screen, select the test
method (standard or custom) that you want to use as the basis for a
new test method.
2. Press the Add button on the main screen of the Standard database to
access the first page with standard parameters of the selected test
method.

Create a new test


method

The first parameter page of the Standard database with the possibility to
modify parameters and save them as a new custom test method.
/i

Buttons on the Parameter pages of the Standard database


Cancel Cancel the action and go back to the previous page
Save Save changes made in the parameter field
Print Print parameters
Up/Down arrow Up/Down arrow buttons to scroll through the list of test methods

3. Press the name field to assign a new name to the test method to be
added. The virtual keyboard or keypad opens.
4. Enter the name of the new test method using the virtual keyboard or
keypad.
5. Confirm the entry by pressing the Enter button on the virtual keyboard
or keypad.
6. Press further parameter fields to be modified.

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7. Enter the values to be modified using the virtual keyboard or keypad.


8. Confirm the entries by pressing the Enter button on the virtual
keyboard or keypad.
9. Use the arrow Down button to scroll to the next parameter page of the
Standard database.
10. To modify further parameters repeat steps 6 to 9 above.

CAUTION
Make sure to entry a new name for the new custom method. Otherwise
saving will overwrite the previous custom method which was used as the
basis for the new one.
If you try to save a standard test method without renaming it, a message
appears, stating that it is not possible to overwrite a standard test
method.

11. When all modifications have been made, press the Save button to
store the new custom test method to the Standard database
or
quit without saving by pressing the Cancel button.

NOTE
The parameter pages of the standard database are quite similar in the
Details and Add mode. Only the buttons at the lower center of the screen
are different:
• Exit button in Details mode
• Cancel and Save button in Add mode

For the complete overview of all parameter pages refer to 7.3.1. View
parameter details of test methods.

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7.4 The Products database


Required access and permissions:
• Level 0 (Operator): reading and printing of product parameters
• Level 1 (Supervisor): Level 0 + creation, adding and deleting of
custom and routine products

The Products menu allows access to a database, in which up to 200 pre-


set products can be stored. A product consists of a series of parameters
and limit values that will act as a guideline for the flash point test,
complying with the standard test method and the group set-up.
Factory set products comply with international standard test methods and
cannot be changed.
However, with a level 1-access authorization (Supervisor), these products
can be displayed and copied as a basis for the creation of new custom
products, which can additionally be stored in the products database.

NOTE
Products are specified on the basis of test methods (standard or custom
methods). The product parameters of custom products can therefore
only be adapted within the limit values of the test method. The limit val-
ues of the test methods are specified in the standard database.

1. Press Advanced > Environment/Products to enter the database.


The Products database opens.

The Products
database

The main screen of the Products database


/i

Buttons on the Products database main screen


Details Displaying the parameters of the selected product
Add Add a new product to the database

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Buttons on the Products database main screen


Up/Down arrow Up/Down arrow buttons to scroll through the list of products
Exit Exit the products database

2. Select a product from the list on the left side of the screen by pressing
on the required product.

The main screen of the Products database offers two possibilities to


proceed further with products selected in the list:
- use the Details button to view the details of the selected product, see
7.4.1. View parameter details of the products
- or use the Add button to create a new custom product by copying the
selected one as a basis and modify and store it as a new product, see
7.4.2. Add new custom products

7.4.1 View parameter details of the products


1. Press the Details button to access the first page with product
parameters.

Products database
- first parameter
page

The first parameter page of the Products database


/i

Parameters on the first page


Name Name of the product (up to 20 characters)
Standard Name Denomination of the standard, e.g. EN, ISO, etc.
Temp. unit Temperature unit: °C / °F (The selection of the temperature unit is
only valid for the product parameters of the selected product. All other
temperature unit settings will remain as specified in the instrument
setup.)

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Parameters on the first page


Expected FP Expected flash point temperature
Product type Routine product, QC (Quality control) product
If QC product is selected, all test results which are based on this pro-
duct will - in addition to the results database - automatically be stored
in the quality control database. This allows analysis of deviations and
statistical quality evaluations of test results.
Min. spec. Minimum specification limit for the quality control
Max. spec. Maximum specification limit for the quality control

2. Press the arrow Down button to access the second page with product
parameters.

Products database
- second
parameter page

The second parameter page of the Products database


/i

Parameters on the second page


Switch heat rate temp The temperature to switch over from Heating Rate 1 to Heat-
ing Rate 2 is calculated from the expected flash point temper-
ature value minus the value specified for Switch heat rate
temp.
Heating Rate 1 Temperature increase per minute for Heating Rate 1 until the
calculated switch over temperature specified in Switch heat
rate temp is reached.
Heating Rate 2 Temperature increase per minute for Heating Rate 2 as from
the calculated switch over temperature specified in Switch
heat rate temp.

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Parameters on the second page


Switch test interval temp The first igniter dipping takes place as soon as the sample
temperature specified in the start test settings has been
reached.
If the expected flash point is lower than or equal to the tem-
perature specified for Switch test interval temp, then the peri-
odic dipping of the igniter will take place according to the
values as defined for Test interval 1, otherwise according to
the values specified in Test interval 2.
Test Interval 1 The Test interval 1 value specifies the value for the frequency
of igniter dipping. Every time the sample temperature
increases by the value specified for Test interval 1, the igniter
dips into the test cup.
Test Interval 2 The Test interval 2 value specifies the value for the frequency
of igniter dipping. Every time the sample temperature
increases by the value specified for Test interval 2, the igniter
dips into the test cup.

3. Press the arrow Down button to access the third page of product
parameters.

Products database
- third parameter
page

The third parameter page of the Products database

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/i

Parameters on the third page


Start test Sample temperature below the expected flash point at which the
test will be started:
Example: Start test temperature = 9 °C or 16 °F
- expected flash point 32 °C (90 °F), start test temperature at
23 °C (74 °F)
End of test This setting is there for safety reasons. To prevent overheating of
the sample if the flash point is not determined, the heater cuts out
as soon as the temperature exceeds the expected flash point plus
the end of test value, e.g. 8 °C or 14 °F.
Example: End of test temperature = 8 °C or 14 °F
- expected flash point 32 °C (90 °F), cut out at 40 °C (104 °F)
Safety test interval For safety reasons, the safety test interval is activated if the
start expected flash point temperature is equal or above the value
specified in this field.
Example:
Safety test interval start value = 50 °C (122 °F)
Safety test interval value = 5 °C (9 °F)
As of 50 °C (122 °F) sample temperature the igniter will dip-in at
every 5 °C (9 °F) temperature increase.
Safety test interval Igniter dip-in interval which is activated when the sample temper-
ature reaches the value specified in Safety test interval start.
Example: With a safety test interval value of 5 °C (9 °F), the
igniter dips in at every 5 °C (9 °F) temperature increase.
Safety stop at For safety reasons, the test stops as soon as the sample temper-
sample temp. ature reaches the set value, e.g. 130.0 °C (266 °F).
Cooling temperature Heating block and sample cool-down temperature at the end of a
test.
Pretest question Pretest On or Off
On: Pretest button is displayed on the Run/Start test screen
Off: Pretest button is not displayed on the Run/Start test screen
and expected FP button is then extended over the entire width
Stirrer speed The stirrer speed is predefined by the standard method: e. g:
EN ISO 13736: 30 rpm.
For customized products the stirrer speed can be set in a range
between 0 to 300 rpm.

4. Press the arrow Down button to access the fourth page of the
Products database.

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Products database
- fourth parameter
page

The fourth parameter page of the Products database


/i

Parameters on the fourth page


Result offset The corrected flash point result will be shifted by the value set in
this field.
Lims report Data format to be sent to the LIMS:
- Short: Reduced set of results data and parameters
- Full: Extended set of results data and parameters
Note: If a result is created (test performed) - a type of LIMS format
is recorded. In case the product LIMS format is changed from
short to full (or vice versa) afterwards, the LIMS report printout of
already existing results in the database will also change. For
details about communication formats refer to chapter 10.1. LIMS
specification for results.
Print report Data format to be sent to a printer:
- Short: Reduced set of results data and parameters
- Long: Extended set of results data and parameters
- Full: Complete set of result data, parameters and product
parameters in addition
For details about printout formats refer to chapter 10.2. Printout
specifications for results
Internal sample Pre-cooling of the sample internal or external:
pre-cooling - On: If pre-cooling of the sample is done by the internal cool-
ing device of the OptiFlash®
- Off: If pre-cooling of the sample is done external, e. g. in a
refrigerator

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Parameters on the fourth page


Block pre-cooling Depends on the setting of the „Internal sample pre-cooling“ field.
temp. - If „Internal sample pre-cooling“ = Off, „Block pre-cooling
or temp.“ is displayed:
Sample pre-cooling Block cools down to a temperature below the expected flash
temp. point as set in this parameter field (e. g. 9 °C below the
expected flash point or to -35 °C, whichever is the higher).
- If „Internal sample pre-cooling“ = On, „Sample pre-cooling
temp.“ is displayed:
Sample is cooled down to a temperature below the expected
flash point as set in this parameter field (e. g. 17 °C below
the expected flash point or to -35 °C, whichever is the
higher).

5. Press the arrow Down button to access the fifth page of the Products
database.

Products database
- fifth parameter
page

The fifth parameter page of the Products database


/i

Parameters on the fifth page


X Measured flash point
A, B, C, D, E Correlation parameters
Unit Unit as requested

The correlation formula, displayed on this page, can be used to calculate


possible contamination of the sample with other substances. The degree
or percentage of the contaminating substance is calculated by entering
the correlation parameters.

6. Press the arrow Up button to return to the previous page or press the
Exit button to return to main screen of the Products database.

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7.4.2 Add new custom products


1. Select the product on the left side of the Products database main
screen that you want to use as the basis for a new product.
2. Press the Add button on the main screen of the Products database to
access the first page with parameters of the selected product.

Create a new
product

The first parameter page of the Products database with the possibility to
modify parameters and save them as a new custom product.
/i

Buttons on the parameter pages of the Products database


Cancel Cancel the action and go back to the previous page
Save Save changes made in the parameter field
Print Print parameters
Up/Down arrow Up/Down arrow buttons to scroll through the list of products

3. Press the name field to assign a new name to the product to be added.
The virtual keyboard or keypad opens.
4. Enter the name of the new product using the virtual keyboard or
keypad.
5. Confirm the entry by pressing the Enter button on the virtual keyboard
or keypad.
6. Press further parameter fields to be modified.
7. Enter the values to be modified using the virtual keyboard or keypad.
8. Confirm the entries by pressing the Enter button on the virtual
keyboard or keypad.
9. Use the arrow Down button to scroll to the next parameter page of the
Products database.
10. To modify further parameters repeat steps 6 to 9.

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CAUTION
Make sure to entry a new name for the new product. Otherwise saving
will overwrite the previous custom product (routine or QC product),
which was used as the basis for the new one.
If you try to save a factory product without renaming it, a message
appears, stating that it is not possible to overwrite a factory product.

11. When all modifications have been made, press the Save button to
store the new custom product to the Products database
or
quit without saving by pressing the Cancel button.

NOTE
The parameter pages of the products database are quite similar in the
Details and Add mode. Only the buttons at the lower center of the screen
are different:
• Exit button in Details mode
• Cancel and Save button in Add mode

For the complete overview of all parameter pages, refer to 7.4.1. View
parameter details of the products.

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7.5 The Operators database


Required access and permissions:
• Level 0 (Operator): reading of pre-set operator names
• Level 1 (Supervisor): Level 0 + adding or deleting of operator names

The Operators menu button allows access to a database, in which up to


40 pre-set operator names can be stored.
With a level 1-access authorization (Supervisor), operator names can be
displayed, added or deleted from the list.
1. Press Advanced > Environment/Operators to enter the database.
The Operators database opens.

The Operators
database

The first screen of the Operators database


/i

Buttons on the Operators database screen


Delete Delete an operator‘s name from the list
Exit Exit the operators database
Cancel Cancel modified settings
Save Exit the operators database
Up/Down Arrows Up/Down arrow button to scroll through the list

Add a new Add a new operator name to the list:


operator
1. Select any operator name from the list.
2. Press the name field to assign a new name to the operator to be
added. The virtual keyboard opens.
3. Enter the new name of the operator using the virtual keyboard or
keypad.

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The screen changes: Cancel and Save buttons appear instead of the
Exit button.
4. Confirm the entry by pressing the Enter button on the virtual keyboard
or keypad.
5. Press the Save button to store the new operator name to the
Operators database
or
quit without saving by pressing the Cancel button.

Delete an operator name from the list:


1. Select the operator‘s name to be deleted from the list.
2. Press the Delete button to remove the operator‘s name from the list.

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7.6 The Quality database


Required access and permissions:
• Level 0 (Operator): Permissions for the operator are limited to:
- reading and printing quality reports
- calibrating the touch panel screen
- adjusting the backlight of the screen
• Level 1 (Supervisor): Level 0 + calibration activities for components of
the instrument.

This section includes instructions for the calibration of measurement


circuits and component parameters of your OptiFlash®, which can be
critical to the measurement accuracy.
The Quality database is in great part dedicated to the supervisor and
service staff.
Apart from components calibration, the quality database also provides
some functionality to calibrate and adjust the screen of the instrument.
Screen adjustment is also permitted to the operator.

1. To enter the Quality database press the Advanced main menu tab and
then the Quality/More... button.
The Quality database opens.

The Quality
database

The main screen of the Quality database


/i

Buttons on the Quality database main screen


Print Send calibration data/status to a printer
Exit Exit the quality database

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Menus of the The Quality database is divided into the following menus:
Quality database
• Quality Control: deviations and statistical quality reports about test
results based on quality products
• Atmospheric pressure: calibration of the pressure measuring device
• Sample probe: calibration of the sample probe
• Extinguisher (only High End and Standard Model): periodic check of
the fire extinguisher
• Sample probe circuit (temperature circuit calibration, using calibrated
resistors)
• Arm adjustment (only High End Model)
• Touch panel calibration (screen alignment)
• Backlight (screen backlight adjustment)

7.6.1 Quality Control


The Quality Control database allows tracking of specified results of quality
control samples, for example as reference material.
Quality control products (QC products) are assigned as such by the
parameter settings in the Products database (Parameter: Product type =
QC Product).
All results of test runs based on a QC product are stored in the results
database and also in the Quality Control database.
The minimum and maximum specification limits set in the QC product,
which is selected as a test parameter to run the QC sample test, can be
displayed in the Quality Control database, allowing the laboratory
supervisor to easily see if the result is out of range. Thus, using reference
material, the laboratory supervisor can monitor the deviation of the
OptiFlash® and decide when it needs to be recalibrated.
1. To enter the Quality Control database,
- either press Advanced > Quality/Quality Control for direct access
- or press Advanced > Quality/More... > Quality Control.

The first page of the Quality Control submenu opens.

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The Quality Control submenu screen


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Buttons on the Quality Control database screen


Details Displays a list of test results based on the selected QC product
Print Send and overview of all QC products including specifications for
each product to a printer
Chart Display a graphic chart of all test results based on the selected QC
product
Up/Down Arrows Up/Down arrow button to scroll through the list
Exit Exit the quality control submenu

2. To scroll to the list of QC products press the arrow Down/Up button.


3. Select a QC product from the list:
- To print out the specifications of all QC product, press the Print
button.
- To display a list of test results based on the selected QC product,
press the Details button.
- To display the graphic chart with all results based on the selected
QC product, press the Chart button.

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The Quality Control test result list based on a selected QC product

4. To display selected results that are based on a specific QC product,


select one or more of the test results from the list. By default, all results
are selected. Use the Select button to deselect results or reselect
them again.
- To print out the specification and test results of the selected QC
product, press the Print button.
- To display the graphic chart with the selected test results, press
the Chart button.

The Quality Control graphic chart displaying selected test results which
are based on a specific QC product

5. To exit the Quality Control graphic chart, press the Exit button.

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7.6.2 Atmospheric Pressure


The Atmospheric Pressure submenu enables the calibration of the
instrument's pressure sensor.
The current air pressure may differ from the normal value by 101.3 kPa.
This has an influence on the flash point. The pressure sensor integrated
in the instrument measures the current air pressure and converts the flash
point determined to the value under normal conditions.

NOTE
For the calibration of the ambient pressure sensor, a reference barome-
ter indicating absolute pressure values (not values corrected to sea
level) is required. Only absolute values are acceptable for the pressure
sensor calibration.
The pressure gage meets the requirements for the calibration of the
instrument's ambient pressure sensor.

The atmospheric pressure sensor of the instrument can be calibrated for


different sea levels. It is possible to set several calibration points, each
corresponding to a location with a different sea level.
Once the sensor is calibrated for several locations with different sea
levels, the operator can shuttle between these locations and use the same
instrument here and there. Renewal of air pressure calibration all the time
due to a change of location is no longer necessary.
1. To enter the submenu, press the Advanced main menu tab and then
Quality/More... > Atmospheric Pressure.
The Atmospheric Pressure submenu opens.

Atmospheric
pressure
calibration

The Atmospheric Pressure submenu screen

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Buttons on the Atmospheric Pressure submenu screen


Exit Exit the atmospheric pressure submenu
Change Settings Go to another submenu to change parameter settings
Perform Calibration Perform guided calibration procedure. During the procedure, a
new calibration point can either be added (“Add new calibration
point”) or an existing one can be renewed (“Renew calibration
point”).
Up/Down arrow Up/Down arrow buttons to scroll through the list of parameters

Change Settings With the Change Settings button parameter settings can be changed or
entries be deleted.

1. To change the settings press the Change Settings button.


The next screen of the Atmospheric Pressure submenu opens.

Change settings of the Atmospheric Pressure calibration points

2. To change the parameters (Frequency:, Refuse test:), press the


respective button and fill in the parameters.
3. To delete a calibration point manually, select the respective calibration
point and press the Delete button.
4. Press the Save button to save the changes
or
quit without saving by pressing the Cancel button.

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Perform Pressing the Perform Calibration button leads to a guided atmospheric


Calibration pressure calibration procedure.

1. To perform the atmospheric pressure calibration, press the Perform


Calibration button. The next screen of the Atmospheric Pressure
submenu opens.

Add new or Renew calibration point screen

2. Select the required option:


- either press the Add new calibration point button, to add a new
calibration point.
- or press the Renew calibration point button, to renew an existing
one. If more than one calibration point is already stored in the
database you will be prompted to select the calibration point to be
renewed.
3. Highlight the calibration point to be renewed and press the Select
button.
The following parameter entry screen appears:

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Calibration points
parameter entry
screen

/i
Parameters on the Atmospheric pressure calibration points screen
Operator: Operator identification
Note: Additional notes, if required
Reference Barometer ID: Identification of the reference barometer used for pressure
calibration.
Reference Read: Current pressure as indicated by the reference barometer.
Frequency: Predefine the frequency of pressure sensor calibration.
Refuse test: Configure the OptiFlash® to refuse or allow a test start when
pressure calibration is overdue.
Yes: a test start is refused
No: a test can be started, only a warning appears

4. Fill in the calibration parameters.


5. Press the Save button to save the atmospheric pressure calibration
or
quit without saving by pressing the Cancel button.
6. Press the Exit button to return to the main screen of the Quality
database.

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7.6.3 Sample probe


The Sample probe submenu enables the calibration of the instrument's
sample temperature probe.
The sample temperature is measured with a PT100 probe, which uses the
physical property of certain metals, wherein the resistance depends on the
temperature. A PT100 probe has a resistance of 100 ohms at 0 °C/ 32 °F.
The exact resistance is different for each device and can change over
time. Therefore, it is essential to monitor the probe deviation.
The OptiFlash® corrects this deviation using the "Sample Probe
Calibration Table". The sample probe, supplied with the OptiFlash®, is
equipped with a built-in memory circuit that can store calibration points,
the probe identity and its serial number. The probe correction values are
signed (+/-) and rounded to the nearest 0.01 °C.
The OptiFlash® detects the probe at plug-in and automatically downloads
these calibration parameters into the instrument memory. This guarantees
the correct calibration values for each instrument, even if the sample
probe is replaced or exchanged between different instruments.

1. To enter the Sample probe submenu, press the Advanced main menu
tab and then Quality/More... > Sample probe.
The Sample probe submenu opens.

Sample probe
calibration

The Sample probe submenu main screen


/i

Buttons on the Sample probe submenu screen


Exit Exit the sample probe submenu
Change Settings Go to another submenu to change parameter settings
Up/Down arrow Up/Down arrow buttons to scroll through the list of parameters

2. To change the settings press the Change Settings button.


The following screen appears:

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The first page of the Sample probe settings submenu


/i

Parameters on the Sample probe settings submenu screen


Temp unit: Temperature unit: °C / °F
Reference: Reference temperature
Measured: Measured temperature

3. Fill in the parameters in the respective fields.


4. To save the settings, press the Save button.
5. To go to the next page of the Sample probe settings submenu, press
the arrow Down button.
The following screen appears:

The second page of the Sample probe settings submenu

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/i

Parameters on the second page


Frequency: Frequency of sample probe calibration in days
Refuse test: Configure the OptiFlash® to refuse or allow a test start when
pressure calibration is overdue.
Yes: a test start is refused
No: a test can be started, only a warning appears

6. To change the settings, fill in the parameters in the respective fields.


7. To save the settings, press the Save button.
8. Press the Exit button to return to the main screen of the Sample probe
submenu.

7.6.4 Extinguisher (only High End and Standard Model)


The Extinguisher periodic check submenu enables the check of the built-
in ultraviolet fire sensors.

1. To enter the Extinguisher periodic check submenu press the


Advanced main menu tab and then Quality/More... > Extinguisher.
The Extinguisher periodic check submenu opens.

Extinguisher
periodic check

The Extinguisher periodic check submenu screen


/i

Parameters on the Extinguisher periodic check submenu screen


Frequency Frequency of extinguisher checks in days
Flame detection Right sensor, Left sensor
With gas igniter, the right or left sensor (front view) can be selected
to control whether the gas flame extinguishes during a test. For
Abel instruments, gas flame detection is only possible with the
right sensor. Therefore the right sensor must always be selected
as gas flame detection sensor for this instrument.

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Parameters on the Extinguisher periodic check submenu screen


Extinguisher Yes, No
checked
UV det. UV detection: On or Off. If On, the LED lights up in green and the
sensor has detected a flame.

2. To change the settings, fill in the parameters in the respective fields or


select predefined parameters.
The buttons Save and Cancel appear at the lower center of the
screen.
3. To check the right sensor, select Right sensor in the Flame detection
field.
4. Cover the left sensor (e. g. with your hand) and turn on a lighter.
5. If the entry of the UV det field changes from Off to On and the LED
from grey to green, the right sensor has detected the flame of the
lighter and works properly.
6. To check the left sensor, repeat the steps 3 to 5 above with the left
sensor.
7. When the sensor check is completed, press the Save button to save
the changes
or press the Cancel button to cancel the action without saving.

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7.6.5 Sample probe circuit


Calibration of the sample probe temperature measurement circuit is done
through the Sample probe circuit calibration menu.

NOTE
A probe simulator is required to calibrate the sample probe circuit.
(PT100 Probe simulator, part no.: 1000-004-001, see chapter
8.5. Optional available parts and accessories).
1. To enter the Sample probe circuit submenu press the Advanced main
menu tab and then Quality/More... > Sample probe circuit.
The Sample probe circuit submenu opens.

Sample probe
circuit calibration

The Sample probe circuit calibration submenu


/i

Buttons on the Sample probe circuit submenu screen


Exit Exit the Sample probe circuit calibration submenu
Calibration History Display the list of calibration history
Change Settings Go to another submenu to change parameters
Perform Calibration Perform guided calibration procedure

2. Press the respective button to access one of the submenus below:


- Calibration History
- Change Settings
- Perform Calibration

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Calibration History

The Calibration history page


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Buttons on the Calibration history page


Exit Exit the calibration history page
Print Send calibration history reports to the printer

3. Press the Exit button to return to the main screen of the Sample probe
circuit submenu.

Change Settings

The Change Settings page of the Sample probe circuit submenu.


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Buttons on the Change settings page


Save Save changes
Cancel Cancel the action without saving

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/i

Parameters on the Change settings page


Resistance: Enter resistance value
AD points: Add resistance converter value for 80.31 ohms for - 50 °C (-58 °F)
Resistance: Enter resistance value
AD points: Add resistance converter value for 138.51 ohms for 100 °C (212 °F)
Frequency: Predefine the frequency of sample probe circuit calibration
Refuse test: Configure the OptiFlash® to refuse or allow a test start when the cali-
bration is overdue.
Yes: a test start is refused
No: a test can be started, only a warning appears

1. To change the settings, enter the parameters in the respective


fields.The virtual keyboard or keypad opens.
2. Confirm the entries by pressing the Enter button on the virtual
keyboard or keypad.
3. Press the Save button to save the changes
or press the Cancel button to cancel the action without saving.
4. Press the Exit button to return to the main screen of the Sample probe
circuit submenu.

Perform
Calibration

First page of the Sample probe circuit calibration menu


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Buttons on the Sample probe circuit calibration menu


Exit Exit the sample probe circuit calibration menu
Continue Continue with the sample probe circuit calibration

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1. Connect the probe simulator to the sample probe connector.


2. Press the Continue button to continue with the sample probe circuit
calibration procedure
or
press the Exit button to cancel the action and return to the previous
screen.

Second page of the Sample probe circuit calibration menu


/i

Parameters on the second page of the Sample probe circuit calibration menu
Resistance: Resistance value of the probe simulator at -50 °C / -58 °F)

3. Adjust the probe simulator at -50 °C / -58 °F.


4. Enter the resistance value (80.31 ohms) at -50 °C / -58 °F, using the
virtual keybord or keypad.
5. Press the Continue button to access the next page of the Sample
probe circuit calibration menu. This can take some seconds.

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Third page of the Sample probe circuit calibration menu


/i

Parameters on the third page of the Sample probe circuit calibration menu
Resistance: Resistance value of the probe simulator at 100 °C / 212 °F

6. Adjust the probe simulator at 100 °C / 212 °F.


7. Enter the resistance value (138.51 ohms) at 100 °C / 212 °F, using the
virtual keybord or keypad.
8. Press the Continue button to access the next page of the Sample
probe circuit calibration menu. This can take some seconds.

Fourth page of the Sample probe circuit calibration menu

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Parameters on the fourth page of the Sample probe circuit calibration menu
Operator: Operator identification
Simulator: Type of the probe simulator
S/N: Serial number of the probe simulator
Frequency: Predefine the frequency of sample probe circuit calibration
Refuse test: Configure the OptiFlash® to refuse or allow a test start when
the calibration is overdue.
Yes: a test start is refused
No: a test can be started, only a warning appears

9. Enter the required parameters into the respective fields.The virtual


keyboard or keypad opens.
10. Confirm the entries by pressing the Enter button on the virtual
keyboard or keypad.
11. Press the Continue button to save the calibration settings. The
following message appears.

Reminder to disconnect the probe simulator and reconnect the


temperature probe.

12. Disconnect and remove the probe simulator.


13. Connect the sample temperature probe.
14. Validate by pressing the OK button.

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7.6.6 Arm adjustment


The automatic lift arm is factory adjusted. However, it may be necessary
to re-adjust the lift arm to ensure high quality measurement results.
The calibration procedure is based on counting the steps between the
mechanical top endpoint and the bottom endpoint of the lift arm.
The arm adjustment screens of the quality menu will guide you through the
adjustment procedure.
1. To enter the Arm adjustment submenu press the Advanced main
menu tab and then Quality/More... > Arm adjustmentt.
The Arm adjustment submenu opens.

Adjusting the
automatic lift arm

The Arm adjustment submenu

2. Press the Perform Calibration button to start with the calibration


procedure
or
press the Exit button to cancel the action and return to the Quality
main menu.

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The second page of the Arm adjustment submenu

3. Press the Continue button to go on with the calibration procedure


or
press the Exit button to cancel the action and return to the previous
page.

The third page of the Arm adjustment submenu

4. Position an empty test cup into its place in the heating block.
5. Connect a test cup-cover insert to the automatic lift arm.
6. Touch the lift arm at the side and slide it to the bottom manually until
the test cup-cover insert completely covers the test cup. (The
instrument detects the number of steps.)

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7. Press the Continue button to go on with the calibration procedure


or
press the Cancel button to cancel the action and return to the Arm
adjustment submenu.

Calibration in progress message of the Arm adjustment submenu

8. Wait until the calibration in progress message disappears, then press


the Continue button.

Final screen of the Arm adjustment submenu

9. Fill in the required fields and then press the Save button to finalize the
calibration procedure
or
press the Cancel button to cancel the action and return to the Arm
adjustment submenu page.

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7.6.7 Adjustment of the touchscreen


The touchscreen is factory adjusted. However, the Quality menu offers
options to readjust the cursor sensitivity area and the brightness of the
screen to the user's own requirements.

Touch panel The cursor sensitivity area can be adjusted according to the position of
adjustment buttons on the screen.

1. Press the Advanced main menu tab and then Quality/More... > Touch
panel.
• The touch panel adjustment screen opens.
• Three yellow spots will appear successively on the screen.

The Touch panel adjustment screen

2. Follow the instructions on the screen:


• Press and hold successively each appearing yellow spot until it
changes from red to green (for a better precision, use a blunt
object to press the center of the spots).
• To cancel the adjustment and go back to the Quality menu, press
the lower text window.

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Backlight The brightness of the screen backlight can change according to the
adjustment ambient temperature and may need to be adjusted.

1. Press the Advanced main menu tab and then Quality/More... >
Backlight.
The Backlight adjustment screen opens:

The Backlight adjustment screen

2. Touch the Backlight bar and move the bar to the left or the right to
adjust the desired brightness.
3. Press the Save button to save the adjustment
or
press the Cancel button to cancel the action and return to the Quality
main menu.

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7.7 The Instrument Setup database


Required access and permissions:
• Level 0 (Operator):
Permissions for the Operator are limited to reading and printing setup
parameters
• Level 1/2 (Supervisor/Maintenance): Level 0 + changing of the
instrument setup, date/time settings, performing of backups and
restoring, updating the firmware, resetting of the instrument's internal
memory.

The Instrument The Instrument Setup database is in great part dedicated to the supervisor
Setup database and service staff.
1. Press Advanced > Instrument Setup/More... to enter the database.
The Instrument Setup database opens.

The main screen of the Instrument Setup database


/i

Buttons on the Instrument Setup database main screen


Exit Exit the instrument setup database

Submenus of the The Instrument Setup database divides into the following submenus:
Instrument Setup
• Parameters
database
• Date & Time
• Backup/Restore
• Reset

2. Press the respective button to access the required submenu.

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7.7.1 Instrument Parameters

This section includes instructions for and information about the setting of
parameters for the specific OptiFlash® unit, such as:
• type of instrument
• conditions for a test start (physical units, preselected fields, etc.)
• access levels and permissions
• interface parameter settings
• device settings, e.g. ignition parameters
• settings for acoustic signals and safety stop conditions

7.7.1.1 General settings


1. Press Advanced > Instrument Setup/Parameters to enter the
submenu.
The Instrument parameters submenu opens.

Instrument
parameters -
General settings

The first Instrument parameters page – General settings


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Buttons on the General settings page


Exit Exit the page and return to the previous page
Print Send instrument parameter settings to a printer
Up/Down arrow Up/Down arrow buttons to scroll through the pages

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Parameters on the General settings page


Serial number: Serial number of the unique OptiFlash® device.
The parameter cannot be changed.
Device type: Type and features of the OptiFlash®.
The parameter cannot be changed.
Unit name: Unit name of the OptiFlash® device.
The parameter can be entered individually, as free text.
Language: Language setting for the MMI (Man Machine Interface)
English is always installed as the first language. A second
language can be selected, if an USB device with the lan-
guage file is connected to the USB port. Selecting of a new
language will overwrite an already installed second lan-
guage.
Beep touch: Acoustic signal at each touch on the touchscreen: Yes or No
Alphanumeric keyboard: Layout type of the virtual keyboard: QWERTY, AZERTY,
QWERTZ
Screen saver: Screen saver settings: Without image, Disable
Numeric keyboard: Layout type of the virtual numeric keyboard: phone, PC

2. To change the settings, enter the parameters into the respective


fields.The virtual keyboard or keypad opens.
3. Confirm the entries by pressing the Enter button on the virtual
keyboard or keypad.
The screen changes: Cancel and Save buttons appear instead of the
Exit button.
4. To save the settings, press the Save button.
5. To go to the next page of the Instrument parameters submenu, press
the arrow Down button.

7.7.1.2 Installing a new language


English is always installed as the first language. A second language can
be installed additionally.

NOTE
• Installing of a new second language requires an USB device with the
language file. The file must the stored on the USB device in the
FLASHPN folder, e. g. FLASHPN/Language/german.bin
• The installation of a new language will overwrite an already installed
second language.

1. Connect the USB device with the language file to one of the USB
ports.
2. Press the language field on the Instrument parameters – General
settings page. The following screen appears:

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Instrument
parameters -
Language

Language page displaying currently installed languages

The first Language page shows the languages which are currently
installed:
• Select: With this parameter field a language selection screen can be
activated when the OptiFlash® is switched on
• English: first language, cannot be changed
• Francais: e. g. as a second language, can be changed, installing of a
new language will overwrite the second language

3. To install a new language press the Install a new language button.


The following screen appears and displays the language files that are
stored on the USB device.

Install a new
language

Language page displaying language files on a USB device

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4. Select the required language file.


5. Press the Continue button to install the new language and overwrite
the current second language
or
cancel the installation process by pressing the Cancel button.

After the installation the OptiFlash® needs a restart to have the new
language available.

7.7.1.3 Test start settings

Instrument
parameters -
Test start settings

The second Instrument parameters page – Test start settings


/i

Buttons on the Test start settings page


Cancel Cancel any modified settings without saving
Save Save modified settings
Up/Down arrow Up/Down arrow buttons to scroll through the pages

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/i

Parameters on the Test start settings page


Temp unit: Setting of the temperature unit: °C / °F. Changing of the tem-
perature unit affects only the instrument settings. Tempera-
ture unit settings in the products database are not affected.
Pressure unit: Selection of the pressure measurement unit used by default:
hPa, kPa, mBar, Bar, mmHg, psi or torr
Operator at start: This parameter specifies if the operator name of the previous
run test shall appear in the operator field when a new test is
started:
- Erased, keying mandatory
- Preserve the previous name (the operator name of the
previous test appears in the operator name field)
- Use the default operator name (as specified in parame-
ter: “Default operator name“).
Default operator name: An operator's name can be defined in this field. This name
will then be displayed in the operator name field by default at
a test start.
Sample ID at start: This parameter specifies if the ID number of a sample is
incremented automatically at a test start:
- Erased, keying mandatory
- Preserve the previous ID (the sample ID of the previous
test appears in the field)
- Auto increment the ID:
The last sample number is always proposed when start-
ing a new test. If this parameter is set, the sample num-
ber is automatically incremented to avoid having the
same sample number in the result database.
Product field at start: This parameter specifies if the product of the previous run
test shall appear in the product field when a new test is
started:
- Erased, keying mandatory
- Preserve the previous product (the product of the previ-
ous test appears in the product field)
- Use the default product (as specified in parameter:
“Default product“).
Default product: A product can be defined in this field. This product will then
be displayed in the product field by default at a test start.

1. To change the settings, enter the parameters into the respective


fields.The virtual keyboard or keypad opens.
2. Confirm the entries by pressing the Enter button on the virtual
keyboard or keypad.
The screen changes: Cancel and Save buttons appear instead of the
Exit button.
3. To save the settings, press the Save button.
4. To go to the next page of the Instrument parameters submenu, press
the arrow Down button.
The following screen appears:

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7.7.1.4 Accessibility

Instrument
parameters -
Accessibility

The third Instrument parameters page – Accessibility


/i

Buttons on the Accessibility page


Cancel Cancel any modified settings without saving
Save Save modified settings
Up/Down arrow Up/Down arrow buttons to scroll through the pages

/i

Parameters on the Accessibility page


Access at power on: Access level permission when the OptiFlash® has been pow-
ered on (default access level setting):
- Operator
- Supervisor
- Maintenance
Access level reset time: The point in time when the OptiFlash® automatically returns
to the default access level, if the touchscreen does not
detect any contact up to this time. The countdown is reset at
each touchscreen contact.
Supervisor password Setup of the password for the supervisor access level
Maintenance password: Setup of the password for the maintenance access level

1. To change the settings, enter the parameters in the respective


fields.The virtual keyboard or keypad opens.
2. Confirm the entries by pressing the Enter button on the virtual
keyboard or keypad.
The screen changes: Cancel and Save buttons appear instead of the
Exit button.
3. To save the settings, press the Save button.

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4. To go to the next page of the Instrument parameters submenu, press


the arrow Down button.
The following screen appears:

7.7.1.5 Printer settings

Instrument
parameters -
Printer settings

The fourth Instrument parameters page – Printer settings


/i

Buttons on the Printer settings page


Cancel Cancel any modified settings without saving
Save Save modified settings
Up/Down arrow Up/Down arrow buttons to scroll through the pages

/i

Parameters on the Printer settings page


Company name: Company name. The parameter can be entered individually,
as free text.
Printer: Selection of the printer used:
- None (with None, the Type button is not available)
- USB
- RS232
Type: Selection of the printer type used:
• USB: Memory stick, Citizen, Seiko, Axiohm, PCL
• RS232: PC, Citizen, Seiko, Axiohm
Auto result print: Setup of automatic printing of test results after a test:
Yes/No: test results are printed/not printed automatically
The printout format (short, long, full) can only be specified in
the products database
For details about printout formats refer to chapter 10.2. Print-
out specifications for results.

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1. To change the settings, enter the parameters into the respective


fields.The virtual keyboard or keypad opens.
2. Confirm the entries by pressing the Enter button of the virtual
keyboard or keypad.
The screen changes: Cancel and Save buttons appear instead of the
Exit button.
3. To save the settings, press the Save button.
4. To go to the next page of the Instrument parameters submenu, press
the arrow Down button.
The following screen appears:

7.7.1.6 LIMS settings

Instrument
parameters -
LIMS settings

The fifth Instrument parameters page – LIMS settings


/i

Buttons on the LIMS settings page


Cancel Cancel any modified settings without saving
Save Save modified settings
Up/Down arrow Up/Down arrow buttons to scroll through the pages

/i

Parameters on the LIMS settings page


Instrument ID: Setup of the unit identification
Automatic validation: Setup of automatic validation:
Yes/No: test results are validated/not validated automatically

1. To change the settings, enter the parameters into the respective


fields.The virtual keyboard or keypad opens.
2. Confirm the entries by pressing the Enter button of the virtual
keyboard or keypad.

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The screen changes: Cancel and Save buttons appear instead of the
Exit button.
3. To save the settings, press the Save button.
4. To go to the next page of the Instrument parameters submenu, press
the arrow Down button.The following screen appears:

7.7.1.7 RS232 settings

Instrument
parameters -
RS232 settings

The sixth Instrument parameters page – RS232 settings


/i

Buttons on the RS232 settings page


Cancel Cancel any modified settings without saving
Save Save modified settings
Up/Down arrow Up/Down arrow buttons to scroll through the pages

/i

Parameters on the RS232 settings page


Interface: Setup of the interface: Off, On-line, Test, Service
- Off: no data are sent
- On-line: the data activated, e. g. for a PC, such as
LIMS or auto result print are sent
- Test: only a test string (abcdefg...) is sent
- Service: every second, a service-string with relevant
data is sent
Baud rate: Setup of the rate of transfer
Possible settings: 2400 to 115200 (default: 115200)
Data bit: 8 (cannot be changed)

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Parameters on the RS232 settings page


Parity bit: none (cannot be changed)
Stop bit: 1 (cannot be changed)
Protocol: Setup of the communication protocol used (xon-xoff, Hard-
ware or none)

1. To change the settings, enter the parameters into the respective


fields.The virtual keyboard or keypad opens.
2. Confirm the entries by pressing the Enter button of the virtual
keyboard or keypad.
The screen changes: Cancel and Save buttons appear instead of the
Exit button.
3. To save the settings, press the Save button.
4. To go to the next page of the Instrument parameters submenu, press
the arrow Down button.
The following screen appears:

7.7.1.8 Ethernet settings

Instrument
parameters -
Ethernet settings

The seventh Instrument parameters page – Ethernet settings


/i

Buttons on the Ethernet settings page


Cancel Cancel any modified settings without saving
Save Save modified settings
Up/Down arrow Up/Down arrow buttons to scroll through the pages

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/i

Parameters on the Ethernet settings page


Interface: Setup of the interface: Off, On-line
Instrument ID: Setup of the instrument ID
Instrument IP address: Setup of the instrument IP address
Subnet mask: Setup of the subnet mask

1. To change the settings, enter the parameters into the respective


fields.The virtual keyboard or keypad opens.
2. Confirm the entries by pressing the Enter button on the virtual
keyboard or keypad.
The screen changes: Cancel and Save buttons appear instead of the
Exit button.
3. To save the settings, press the Save button.
4. To go to the next page of the Instrument parameters submenu, press
the arrow Down button.
The following screen appears:

7.7.1.9 Device settings

Instrument
parameters -
Device settings
page 1

The eighth Instrument parameters page – Device settings page 1


/i

Buttons on the Device settings page 1


Cancel Cancel any modified settings without saving
Save Save modified settings
Up/Down arrow Up/Down arrow buttons to scroll through the pages

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/i

Parameters on the Device settings page


Pre ignition: Setup of the pre-ignition time. The electric igniter must have been
preheated prior to dipping into the test cup.
Ignition type: Setup of the igniter type: Electric igniter, Gas igniter
Igniter power: Setup of the electric igniter power level: levels 1 to 7
(level 4 = default)
Liquid cooling: Setup of an external liquid circulation cooling device:
• On: Liquid coolant is used to cool the Peltier element
• Off: Cooling is performed by Peltier element and fan only

1. To change the settings, enter the parameters into the respective


fields.The virtual keyboard or keypad opens.
2. Confirm the entries by pressing the Enter button of the virtual
keyboard or keypad.
The screen changes: Cancel and Save buttons appear instead of the
Exit button.
3. To save the settings, press the Save button.
4. To go to the next page of the Instrument parameters submenu, press
the arrow Down button.
The following screen appears:

Instrument
parameters -
Device settings
page 2

The ninth Instrument parameters page – Device settings page 2


/i

Additional parameters on the Device settings page 2


Postpone Exp. FP during Specifies, whether the expected flash point can be changed
a test: during a test: On, Off
Beep at Flash point: Setup of an acoustic signal when the flash point is deter-
mined: off, 1x, 3x, ...
Beep when end of test: Setup of an acoustic signal at the end of a test: off, 1x, 3x, ...

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Additional parameters on the Device settings page 2


Alarm contact settings: Possible settings: Disabled, Fire, End of test, Cooling down,
Unit ready
The signal can be tapped from the external alarm output con-
nection at the rear of the instrument and used for customer
specific installations. For instance, to activate an exhaust
extraction system automatically at the end of a test, etc.

1. To change the settings, enter the parameters into the respective


fields.The virtual keyboard or keypad opens.
2. Confirm the entries by pressing the Enter button of the virtual
keyboard or keypad.
The screen changes: Cancel and Save buttons appear instead of the
Exit button.
3. To save the settings, press the Save button.

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7.7.2 Date & Time

1. Press Advanced > Instrument Setup/Date &Time to enter the


submenu.
The Date & time setup submenu opens.

Date & time setup

The Date & time setup page


/i

Buttons on the Date & time setup page


Exit Exit the Date & time setup page and return to the previous
screen.

/i

Parameters on the Date & time setup page


Date / Format: Setup of the date format: DDMMYYYY, DDMonthYYYY, etc.
Time / Format: Setup of the time format: 12/24
Day: Setup of the current day
Month: Setup of the current month
Year: Setup of the current year
Hour: Setup of the current hour
Minute: Setup of the current minute

2. To change the settings, enter the parameters into the respective


fields.The virtual keyboard or keypad opens.
3. Confirm the entries by pressing the Enter button on the virtual
keyboard or keypad.
The screen changes: Cancel and Save buttons appear instead of the
Exit button.
4. To save the settings, press the Save button.
5. Press the Exit button, to go back to the Instrument parameters main
screen.

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7.7.3 Firmware updates and Backup / Restore


Required access and permissions:
For all backup, restore and firmware update activities access Level 2
(Maintenance) is required.
The Backup/Restore submenu is designated to create backups of
databases and internal parameter settings, and to restore the data that
has been backed up. In addition, the Backup/Restore submenu also
supports the uploading of new firmware updates for the OptiFlash®.

Firmware updates 1. Press Advanced > Instrument Setup/More... > Backup/Restore to


and Backup / enter the submenu.
Restore The Backup/Restore submenu opens.

The Backup/Restore submenu


/i

Buttons on the Backup/Restore submenu


Exit Exit the page and return to the main screen of the Instrument setup
database.
Continue Continue with
- Update the firmware of the instrument
- Backup
- Restore

/i

Parameters on the Backup/Restore submenu


Backup This selection field enables the creation of backups, either:
- databases only,
- or databases and also some parts of the instrument‘s software.
Restore This selection field enables backed up data to be restored, either:
- databases only,
- or databases and also some parts of the instrument‘s software.

2. Press the respective Continue button to enter the next page.

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7.7.3.1 Firmware updates


The Backup/Restore submenu supports the uploading of new firmware
updates for the OptiFlash®.

NOTE
The firmware upload requires 3 files, they must be installed on the USB
device in the FLASHPN folder.
Example for firmware 1.02:
- FLASHPN/FP102.fla: OptiFlash® firmware
- FLASHPN/Flash.PN6: Hardware data
- FLASHPN/FlashPN.pac: Information file for uploading/downloading
operations
In addition, the language folder with at least one language file must be
available on the USB device: e. g. FLASHPN/Language/chinese.bin
Otherwise an error message appears at the end of the process and the
instrument will not restart automatically.

1. Connect the USB device, which contains the new firmware, to one of
the USB ports.
2. Press Advanced > Instrument Setup/More... > Backup/Restore >
Update the firmware of the instrument > Continue to enter the
firmware update page.
To make sure that firmware update is really intended, the confirmation
prompt below appears.

Firmware updates

The Firmware update confirmation prompt

NOTE
The USB device is not considered as valid if it does not contain all files
needed. In this case, an alarm message appears.

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3. Press the OK button to upload the new firmware to the internal


memory of the OptiFlash®
or
cancel the update process by pressing the Cancel button.
- If confirmed, the firmware upload will start immediately. The
process may take a few minutes.
- At the end of the upload, the instrument is reinitialized and
restarted automatically.

7.7.3.2 Backup

Backup

The Backup page


/i

Buttons on the Backup page


Cancel Cancel the action and go back to the previous page
OK Confirm and proceed with the backup
Up/Down arrow Up/Down arrow buttons to scroll through the list

1. Make sure that an USB device is connected to one of the USB ports.
2. Select the type of backup:
- All the memory: to create a backup of the internal databases and
also some parts of the instrument‘s software.
- Data only: to create a backup of databases only, such as test
results, standards, products, operators, calibration values, and
internal instrument parameters.

NOTE
The backup process stores customer data only. Factory implemented
default data is not stored during a backup.

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3. Press the OK button to start the backup process


or
cancel the action and go back to the previous page by pressing the
Cancel button.

7.7.3.3 Restore

Restore

The Restore page


/i

Buttons on the Restore page


Cancel Cancel the action and go back to the previous page.
OK Confirm and proceed with restore of the backup
Up/Down arrow Up/Down arrow buttons to scroll through the list

1. Connect the USB device with the backup to one of the USB ports.
2. Select the type of restoring:
- Parameters
- Calibrations
- Environment (standards, products, operators databases)
- All memory (factory): to restore a backup of the complete internal
memory.
NOTE
Calibration data of the sample probe are stored in the EEPROM of the
sample probe only and will not be affected by the restore function.

3. Press the OK button to start the restore process


or
cancel the action by pressing the Cancel button.

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7.7.4 Reset
The Reset submenu is designated to reset data which is stored in the
internal memory of the OptiFlash®, back to factory default settings at the
time of shipment. The reset of the internal memory can be performed
selective, e.g. only test results, event log, standards, products, operators,
calibration values, instrument parameters, etc.:
1. Press Advanced > Instrument Setup/More... > Reset to enter the
submenu.
The Reset submenu opens.

Reset

The Reset page


/i

Buttons on the Reset page


Exit Exit the page and return to the main screen of the instrument
setup database
Continue Continue with reset
Up/Down arrow Up/Down arrow buttons to scroll through the list

2. Select the type of data to be reset to factory default settings, e. g.


- Results (complete result database)
- Events log
- Environment (complete environment database: standards,
products, operators)
- Quality control (all QC data)
- Sensors calibrations (all sensor calibration date, except sample
probe)
- Instrument parameters

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NOTE
Calibration data of the sample probe are stored in the EEPROM of the
sample probe only and will not be affected by the reset function.

3. Press the Continue button to confirm the reset process


or
press the Exit button to cancel the action and return to the main
screen of the Instrument setup database.

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7.8 The Measures Diagnostic database


Required access and permissions:
• Level 2 (Maintenance)

This section includes instructions for measurement checks and testing


procedures of the instrument’s major parts, using diagnostic functions.
The Measures Diagnostic database is in great part dedicated to the main-
tenance and service staff.
1. Press Advanced > Measures Diagnostic to enter the database.
The first screen of the Measures Diagnostic database opens.

The Measures Diagnostic database screen


/i

Buttons on the Measures Diagnostic database screen


Exit Exit the measures diagnostic database
Diag mode Enter the diagnostic mode

2. To enter the dignostic mode, press the Diag. mode button.


The Measures diagnostic page opens.

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Measures page

The Measures page of the Measures Diagnostic database

The Measures page displays the current measured values of several


instrument parameters and components.
/i

Parameters on the Measures page


TSample: Current, measured temperature for the sample. In the event of a fault
caused by a short circuit or a fault in the thermometer, the display
jumps by an arbitrary value.
TBlock: Current, measured temperature for the block. In the event of a fault
caused by a short circuit or a fault in the thermometer, the display
jumps by an arbitrary value.
TBoard: Measured temperature for the mainboard. In the event of a fault
caused by a short circuit or a fault in the thermometer, the display
jumps by an arbitrary value.
Thermo 1: Measured voltage for the flash point detection sensor thermocouple
T heater: Measured temperature at the heat sink side of the Peltier element
Pressure: Measured air pressure
Igniter volt: Measured voltage for the electric igniter
Igniter curr: Measured current for the electric igniter
24vCurrent: Measured current for the internal 24 V power supply device
V1: Cooling valve
V2: Current status of valve 2 (igniter gas valve): On/Off
Ion: not used
Ign Current status of the electric ignition: On/Off
Fan: Current status of the cooling fan: On/Off
Act: not available (factory service only)
Lm1: not available (factory service only)

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Parameters on the Measures page


Lm2: not available (factory service only)
Lm3: not available (factory service only)
Lm4: not available (factory service only)
Lm5: not available (factory service only)
PWM Heating/Cooling power of heater/Peltier element [%]
Net volt: Measured voltage of the mains supply
UV: Ultraviolet sensors: On/Off
24V Ele: mainboard supply voltage for 3V3, 5V, 12V MMI
24V Dev: Supply voltage for motor, valve, fan, etc.
12V MMI: Internal voltage source for the MMI
5V: Internal voltage source for miscellaneous mainboard components
3V3: Internal voltage source for miscellaneous mainboard components
2V5: 2.5 V reference voltage
Pelt. Curr: Measured current for the Peltier element
Stirrer ADC: ADC value of the stirrer
ADC SPC: ADC value of the sample probe circuit

3. To go to the next page of the Measures Diagnostic database press the


arrow Down button.
The Valves diagnostic page opens.

Valves page

The Valves page of the Measures Diagnostic database

The Valves diagnostic page enables diagnostics to be performed by


switching the valves on and off:

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/i

Buttons on the Valves page


V1: Cooling valve: On or Off (only High End Models with built in liquid
cooling)
V2: Switching valve 2 (igniter gas valve): On or Off
Buzzer: Switching the acoustic signal: On or Off

4. To go to the next page of the Measures Diagnostic database press the


arrow Down button. The Sample Tempering diagnostic page opens.

Sample Tempering
page

The Sample Tempering page of the Measures Diagnostic database


The Sample Tempering diagnostic page enables diagnostics to be
performed by enabling/disabling or increasing/decreasing the heating
power for the heating block, recording (On/Off) of parameters on an
USB-device during diagnostics and switching the cooling fan on and off.
/i

Buttons on the Sample Tempering page


Heater: Heating/Cooling power for the heating/cooling block: On/Off
Power: Heating/Cooling power for the heating/cooling block, if Heater is set to On
- press 1x Power for heating/cooling power in %
- press 2x Power for heating/cooling block temperature in °C/°F
- press 3x Power for Off (Power button disappears)
Enter minus sign for cooling power (-100% is the maximum cooling power)
Recording: Recording of parameters during diagnostics: On/Off
(USB device is needed)
Fan: The cooling fan, to cool down the heating block at the end of a test, can be
switched on or off

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Heater and Power Button on the Sample Tempering page

Heater and Block temp Button on the Sample Tempering page

5. To go to the next page of the Measures Diagnostic database press the


arrow Down button.
The Igniter control diagnostic page opens.

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Igniter control
page

The Igniter control page of the Measures Diagnostic database

The Igniter control diagnostic page enables diagnostics to be performed


for the igniter.
/i

Buttons on the Igniter control page


Igniter Power: The electric igniter power level can be set from 1 to 7; default level = 4
Igniter: The electric igniter can be enabled or disabled: On/Off
V2: The valve V2 (gas igniter supply valve) can be enabled or disabled:
On/Off
Cycle: Simulates that the igniter dips into the test cup
Calibrate: Searches for the zero-point of the shutter device

/i

Additional parameter on the Igniter control page


Str steps: Number of steps for the shutter device from zero-point to end position

6. To go to the next page of the Measures Diagnostic database press the


arrow Down button.
The Motors control diagnostic page opens.

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Motors control
page

The Motors control page of the Measures Diagnostic database

The Motors control diagnostic page enables diagnostics to be performed


for the different motors used in the instrument.
/i

Buttons on the Motors control page


Igniter: The motor of the shutter drive, which brings the electric igniter to dip-
in, can be enabled or disabled: On/Off
Arrow Up Dipping the igniter into the test cup
Arrow Down Taking the igniter out of the test cup
Stirrer: Switching the stirrer off
Arrow Up Switching the stirrer on
Spin RPM: Stirrer spin speed settings can be set from 0 to 300 rpm
Arm: The automatic lift arm drive can be enabled or disabled: On/Off
Arrow Up Moving the lift arm up
Arrow Down Moving the lift arm down

7. To exit the Measures Diagnostic database and go back to the


Advanced main menu, press the Exit button.

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7.9 The Information database


Required access and permissions:
• Level 0 (Operator)

The information database is divided into four submenus:


• Event log (logged warnings and alarms)
• About (specifications of the instrument and its components)
• Counters (operating hours, number of tests, warnings, alarms)
• Contact (information to contact PAC)

1. To enter the information database press the Advanced menu tab and
then:
- either press Information/Event log for direct access to the Event
log submenu;
- or press Information/About for direct access to the About
submenu;
- or press Information/More... for access to the complete
information database.

The Information database opens.

Information
database

The main screen of the Information database

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7.9.1 Event log


The Event log menu contains warning and alarm messages that have
occurred and logged during operation and test runs. These events can be
displayed in the Event log menu.
1. To enter the Event log menu,
- either press Advanced > Information/Event log for direct access
- or press Advanced > Information/More... > Event log.

The Event log menu opens.

Event log menu

The Event log menu of the Information database


/i

Buttons on the Event log menu screen


Show in the list The categories of events displayed in the list can be selected by
pressing the button Show in the list:, such as:
- all the events
- only the alarms and warnings
- only the information
- the active alarms and warnings
Exit Exit the event log menu and return to the previous page
Print Send details of the highlighted logged event to a printer
Up/Down arrow Up/Down arrow buttons to scroll through the list of logged events

2. To change the category of logged events, press the Show in the list
button and select a category.

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The Event log menu of the Information database – categories of logged


events
/i

Details on the Event log menu screen


Code: Code number of the occurred event.
Severity: Severity of the occurred event: Warning, Alarm
Session: Session status of the instrument when the event has occurred.
> ... Dialogue message that was displayed when the event occurred.

The left side of the Event log menu page displays the list of logged events
including date, time and kind of the occurred event.
The right side of the page displays details about the event, which is
currently highlighted in the list.

3. Use the Up/Down arrow buttons to scroll through the list of logged of
events.
4. To select an event, press the event to highlight it.
5. To print out details of the highlighted event, press the Print button.
6. To exit the Event log menu and go back to the previous page, press
the Exit button.

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7.9.2 About
The About menu contains information about the OptiFlash® and its com-
ponents, such as
• specifications, serial number and firmware revision of the instrument
• specifications of internal boards, sample probe and igniter

NOTE
The information displayed in the About menu pages is in great part dedi-
cated to service and maintenance staff.
Any modifications of information displayed in the About menu pages can
only be carried out by factory service staff.

1. To enter the About menu,


- either press Advanced > Information/About for direct access
- or press Advanced > Information/More... > About.

The first page of the About menu opens.

About - Instrument

The Instrument information page of the About menu


/i

Buttons on the About menu pages


Exit Exit the about menu and return to the previous page
Print Send details of the screen to a printer
Up/Down arrow Up/Down arrow buttons to scroll through the pages

The first page of the About menu displays information about the
instrument, such as serial number, the type of the instrument, firmware
release and further hard- and software information.

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2. The steps below can be carried out on any of the eight About pages:
- To scroll to the next/previous page, press the arrow Down/Up
button.
- To print out details about the actual page, press the Print button.
- To exit the About menu, press the Exit button.

About - CPU board

The CPU board information page of the About menu

The second page of the About menu displays information about the CPU
board, such as part number, manufacturer, revision level and other
characteristics to identify the specific CPU board used in the instrument.

About - MMI board

The MMI board information page of the About menu

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OptiFlash® Database Management

The third page of the About menu displays information about the MMI
board, such as part number, manufacturer, revision level and other
characteristics to identify the specific MMI board used in the instrument.

About -
Control board

The Control board information page of the About menu

The fourth page of the About menu displays information about the control
board, such as part number, manufacturer, revision level and other
characteristics to identify the specific Control board used in the
instrument.

About -
Peltier board

The Peltier board information page of the About menu

The fifth page of the About menu displays information about the Peltier
board, such as part number, manufacturer, revision level and other
characteristics to identify the specific Peltier board used in the instrument.

164 UM Abel_V1.0B_EN
Database Management OptiFlash®

About -
Extinguisher
board (only High
End and Standard
Model)

The Extinguisher board information page of the About menu

For the High End and Standard Model, the sixth page of the About menu
displays information about the extinguisher board, such as part number,
manufacturer, revision level and other characteristics to identify the
specific extinguisher board used in the instrument.

About -
Sample probe

The Sample probe information page of the About menu

The seventh page of the About menu displays information about the
sample probe, such as part number, manufacturer, revision level and other
characteristics of the specific sample probe used with the instrument.

UM Abel_V1.0B_EN 165
OptiFlash® Database Management

About - Igniter

The Igniter information page of the About menu

The eighth page of the About menu displays information about the electric
igniter such as part number, manufacturer, revision level and other
characteristics of the specific igniter used with the instrument.

166 UM Abel_V1.0B_EN
Database Management OptiFlash®

7.9.3 Counters
The Counters menu contains information about installation date and
added values of the specific instrument, such as:
• installation date
• power on hours
• total number of test runs
• total number of warnings that have occurred
• total number of alarms that have occurred

1. To enter the Counters menu, press Advanced > Information/More... >


Counters.
The Counters menu opens.

Counters menu

The Counters information page


/i

Buttons on the Counters page


Exit Exit the counters menu and return to the previous page
Print Send details of the screen to a printer

2. To print out details of the actual page, press the Print button.
3. To exit the Counters menu, press the Exit button.

UM Abel_V1.0B_EN 167
OptiFlash® Database Management

7.9.4 Contacts
The Contacts menu provides contact information of PAC.
1. To enter the Contacts menu, press Advanced > Information/More... >
Contacts.
The Contacts menu opens.

Contacts menu

The Contacts information page

2. To exit the Contacts menu, press the Exit button.

168 UM Abel_V1.0B_EN
Maintenance OptiFlash®

8 Maintenance

UM Abel_V1.0B_EN 169
OptiFlash® Maintenance

8.1 Routine maintenance


Before starting the first test run or periodically thereafter, check the
pressure and temperature measurements. Measurement checks are part
of routine maintenance. The minimum checks to perform are, in particular,
the atmospheric pressure and sample temperature measurement.

8.2 Maintenance intervals


The interval for the frequency of maintenance checks is to be determined
by the user according to the OptiFlash® environment, its frequency of use
and the customer’s quality assurance program. However, the table below
contains general recommendations for maintenance actions for the
different components.
/i

Maintenance interval Action


After every test run • Clean the test cup, test cup-cover insert and test
equipment, see chapter:
- 8.3. Cleaning the test equipment
Every Year • Calibrate the atmospheric pressure and sample tem-
perature measurement system, see chapters:
- 7.6.2. Atmospheric Pressure
- 7.6.3. Sample probe
- 7.6.5. Sample probe circuit

• Check the ultraviolet fire sensors of the extinguisher


system, see chapter:
- 7.6.4. Extinguisher (only High End and Standard
Model)

• Perform complete diagnostics for the instrument‘s


components, see chapter:
- 7.8. The Measures Diagnostic database
After each igniter replace- • Perform igniter calibration, see chapter:
ment - 8.4. Calibration of the igniter

8.3 Cleaning the test equipment


The test equipment must be cleaned after the end of a test or, at the latest,
before running a new test.

WARNING
The parts of the test equipment may be hot. Risk of burns!
Take care when removing the hot test equipment.

170 UM Abel_V1.0B_EN
Maintenance OptiFlash®

NOTE
Remaining sample residues on test equipment from previous tests will
cause incorrect flash point measurement results.
Clean the test equipment thoroughly after a test has been finished or, at
the latest, before running a new test.

1. When using a gas igniter, close the gas supply valve and disconnect
the gas igniter from the gas connector.
2. Remove the test cup-cover insert and accessories from the
instrument.
3. Remove the electric igniter, flash point detection sensor and sample
temperature probe from the supports at the test cup-cover insert.
4. Clean the flash point detection sensor and the sample temperature
probe thoroughly, using a soft cleaning cloth.

NOTE
Cleaning of the electric igniter and gas igniter (if used) is not necessary.

5. Clean the test cup, the shutter plate and the test cup-cover insert:
a. first use a soft cleaning cloth for coarse cleaning
b. then use a burner flame to burn off residues - ensure that the
flame comes into contact with the parts for a short time only.

6. Cleaning of the shutter plate might be easier when removing it.


To remove the shutter plate from the test cup-cover insert, first remove
the knurled head screw (A), then pull out the shutter plate (B).

Removing the shutter plate

UM Abel_V1.0B_EN 171
OptiFlash® Maintenance

8.4 Calibration of the igniter


To obtain precise measurement results, it is vital that the immersion depth
of the igniter is accurately adjusted. During normal operation, calibration
of the igniter is not necessary. However, igniter calibration should be
performed after each igniter replacement.

WARNING
The parts of the test equipment may be hot. Risk of burns!
Let the test equipment cool down before doing any calibration work.

NOTE
To calibrate the igniter the following available adjustment tools are
required:
- Igniter dummy (for electric igniter calibration only): P/N 326-070
- Igniter adjustment gauge with recesses labelled with an E for electric
and with a G for gas ignition: P/N 402-119
For more adjustment tools and accessories refer to chapter 8.5. Optional
available parts and accessories.

A B

A Igniter dummy (for electric igniter calibration only)


B Igniter adjustment gauge with recesses labelled E (for Electric igniters) and G (for Gas
igniters)

172 UM Abel_V1.0B_EN
Maintenance OptiFlash®

8.4.1 Calibration of an electric igniter

CAUTION
Never use the electric igniter itself for the calibration. It will be damaged.
Always use the available igniter dummy.

1. Remove the electric igniter, flash point detection sensor and sample
temperature probe from the supports at the test cup-cover insert.
2. Install the igniter dummy to the electric igniter support.
3. Hold the test cup cover vertically, so that it is in the same position as
during a test and the igniter dummy is in a fully immersed position.
4. Use the igniter adjustment
gauge with the recess labelled
E (electric igniter) and hold it
perpendicular to the bottom of
the test cup-cover, so that the
igniter dummy fits into the
recess.
a If the igniter dummy fits
into the recess exactly, the
calibration is correct.
b If the igniter dummy does
not fit into the recess
exactly, continue with the
steps below.
5. To adjust the immersion
depth, loosen the counter nut
and adjust the igniter using the
adjustment screw (A).
6. Fasten the counter nut and
check again if the igniter
dummy fits exactly into the
recess of the adjustment A
gauge.
7. Repeat the above steps until
the igniter dummy fits exactly
into the recess of the
adjustment gauge.

UM Abel_V1.0B_EN 173
OptiFlash® Maintenance

8.4.2 Calibration of a gas igniter


The calibration of the immersion depth for a gas igniter is very similar to
the procedure for an electric igniter, except:
• the calibration of a gas igniter is performed with the gas igniter itself,
an igniter dummy is not necessary
• the igniter adjustment gauge with the recess labelled G (for gas
igniters) is used

With the exception of the above points perform the calibration of a gas
igniter according to section 8.4.1. Calibration of an electric igniter.

174 UM Abel_V1.0B_EN
Maintenance OptiFlash®

8.5 Optional available parts and accessories

/i

Quantity P/N Description


1 1700-000-004 Barcode Reader with cable
1 102165 USB Thermal Ticket Printer 100-230V

1 1200-004-002 External printer

1 1700-000-001 Printer cable

1 1700-000-007 Ethernet cable


1 1700-000-006 RS232 cable
1 1000-004-001 Calibrator for the temperature measuring system
1 402-119 Depth Gauge Alignment Tool Abel (re-immersion)
1 326-070 Alignment Tool (igniter dummy)
1 5201-000-001 Allen key set, wrench size 1.5/2/2.5/3/4/5
1 103734 Sample temperature sensor, metal,
calibrated at 40°C and 200°C
1 102644 Set of 2 screen protection Foil 7
1 103733 Electric igniter
1 105457 Upgrade Kit Gas Ignition for Abel
1 102159 External Cooler for Flash Points down to -10°C with 80W
at -20°C, 230V
1 102373 External Cooler for Flash Points down to -10°C with 80W
at -20°C, 115V
1 08299-000-00 External Cooler for Flash Points below -10°C with 110W
at -40°C, 230V
1 103148 External Cooler for Flash Points below -10°C with 110W
at -40°C, 115V
1 301-047 Hose for External Cooler connection (2 required)

UM Abel_V1.0B_EN 175
OptiFlash® Maintenance

176 UM Abel_V1.0B_EN
Troubleshooting OptiFlash®

9 Troubleshooting

UM Abel_V1.0B_EN 177
OptiFlash® Troubleshooting

9.1 Dealing with alarm and warning messages


This chapter is a guide provided to aid in isolating and correcting problems
that may arise while operating the OptiFlash®.
Alarms and warnings, that have occurred and logged during operation and
test runs are automatically stored in the Event log menu and can be
displayed again at any time, see section 7.9.1 Event log.)

Example of an alarm message

WARNING
The OptiFlash® contains live voltage components. Risk of electric shock!
• Switch off the instrument and disconnect it from the mains before
opening the housing or removing any cover panel.
• Make sure that the instrument cannot be switched on unintentionally.

If an alarm or warning message appears proceed as follows:


1. Press the OK button to acquit the alarm/warning and stop the buzzer.
2. Refer to section 9.2 List of alarm messages or 9.3 List of warning
messages and locate the alarm or warning code in the left column of
the table.
3. Then follow the description and suggestion for possible solutions/
actions.
4. If the operator or supervisor can not handle the proposed action,
a. switch off the instrument and disconnect it from the mains
b. contact a service engineer for advice or service.

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Troubleshooting OptiFlash®

9.2 List of alarm messages


/i

Code Alarm/Message Description Possible Solutions/Actions


69 xx °C/°F Cabinet Tempera- The cabinet temperature measure is Please contact service!
ture out of limits for 60 seconds.
Temperature is out of limits: -10 °C / +14 °F < Temperature must
-10 °C to +80 °C be < +80 °C / +176 °F
+14 °F / +176 °F The temperature is measured by the
BMP180 component on the control
board.
Possible causes:
1) Unit operates outside the allowed
temperature range
2) Temperature sensor on main board
is broken
73 xx °C/°F Sample Tempera- The Sample temperature measure is Check, if the sample probe is con-
ture out of limits for 5 seconds. nected correctly.
Temperature is out of limits: -60 °C / -76 °F < Temperature must Change the sample probe.
-60 °C to +700 °C be < +700 °C / +1292°F If the alarm appears again, please
-76 °F to +1292 °F Possible causes: contact service.
1) Sample probe not connected
2) Sample probe broken
3) Sample temperature is out of limits
74 Atmospheric Pressure The pressure is out of limits for 60 Check atmospheric pressure at the
The pressure is out of limits: seconds. 66.0 kPa < Pressure must unit with a reference barometer.
66kPa to 110kPa be < 110.0 kPa Restart unit.
The pressure is measured by the If the alarm appears again, contact
BMP180 component on the control service, please.
board.
Possible causes:
1) Unit operates outside the allowed
pressure range
2) Pressure sensor on main board is
broken
75 Stirrer motor The start up test found that the cur- Please contact service!
Please check the stirrer rent for the stirrer motor is either
motor connection lower than 50mA or higher than
and restart the device. 1500mA.
Possible causes:
1) Stirrer motor is not connected to
the main board
2) Stirrer motor is broken
3) Stirrer motor cable is broken

UM Abel_V1.0B_EN 179
OptiFlash® Troubleshooting

Code Alarm/Message Description Possible Solutions/Actions


76 Lift arm error A failure of the lift arm movement was Check if the lift arm is possibly
Error might be caused by: detected or the start up test found that blocked by any objects in its range of
1) Lift arm blocked the current for the lift arm motor is motion.
2) No movement detected either lower than 50mA or higher than Go to Advanced->Diagnostics menu
1500mA. and try to move the arm via a button
Possible causes: up or down:
1) Lift arm is blocked 1) Motor does not make any noise:
2) Lift arm movement took too long - Please contact service!
3) Number of steps done does not 2) Motor makes strange noise, but
correspond to the expected value does not move:
4) Lift arm motor is not connected to - Please contact service!
the main board 3) Motor turns but the arm does not
5) Lift arm motor is broken move:
6) Lift arm cable is broken - Please contact service!
7) Limit switch problem 4) An error is shown during arm going
down (arm moves normally but during
cup closing an error is shown):
- Check whether the cup is placed
correctly
- Perform arm motor calibration
5) Arm moves but after some time an
error is shown:
- Please contact service!
6) Motor arm does not stop in the top/
bottom position and continues to
move:
- Please contact service!
77 Shutter motor 77-0 - Shutter Motor: Check if the shutter is possibly
Shutter error might be A failure of the shutter drive move- blocked by any objects in its range of
caused by: ment was detected or the start up test motion.
1) Cabling problem found that the current for the shutter If the shutter is not blocked by any
2) Shutter is blocked motor is either lower than 50mA or objects or due to other mechanical
higher than 1500mA. issues, please contact service!
Possible causes:
1) Shutter drive is blocked
2) Shutter drive movement took too
long
3) Number of steps done does not
correspond to the expected value
4) Shutter motor is not connected to
the main board
5) Shutter motor is broken
6) Shutter cable is broken
7) Limit switch problem

81 Fan 1 The start-up test found that the cur- Please contact service!
Please check the Fan 1 con- rent for Fan 1 is either lower than
nection and restart the 50mA or higher than 1500mA.
device. Possible causes:
1) Fan is not connected to the main
board
2) Fan is broken
3) Fan cable is broken

180 UM Abel_V1.0B_EN
Troubleshooting OptiFlash®

Code Alarm/Message Description Possible Solutions/Actions


82 Calibration to do Refuse the test flag is set (Refuse Perform "Atmospheric Pressure" cali-
The date of pressure calibra- test: "Yes") in calibration menu bration in Advanced->Quality->More-
tion has elapsed. The test "Atmospheric Pressure" and the cali- >Atmospheric Pressure or set the
cannot be started. Please bration period has expired or not been "Refuse test" question to "No" in the
perform the calibration. done yet. mentioned menu to get only a warn-
ing.
83 Calibration to do Refuse the test flag is set (Refuse Perform "Sample probe" calibration in
The date of sample probe test: "Yes") in calibration menu "Sam- Advanced->Quality->More->Sample
calibration has elapsed. The ple probe" and the calibration period probe or set the "Refuse test" question
test cannot be started. has expired or has not been done yet. to "No" in the mentioned menu to get
Please perform the calibra- only a warning.
tion.
84 Calibration to do Refuse the test flag is set (Refuse Perform "Sample probe circuit" cali-
The date of sample circuit test: "Yes") in calibration menu "Sam- bration in Advanced->Quality->More-
calibration has elapsed. The ple probe circuit" and the calibration >Sample probe circuit or set the
test cannot be started. period has expired or has not been "Refuse test" question to "No" in the
Please perform the calibra- done yet. mentioned menu to get only a warn-
tion. ing.
85 Electric igniter failed The igniter current is lower than 3A or Check in diagnostic menu on page 4 if
Igniter broken higher than 20A. igniter works correctly.
Possible causes: -> if not: Exchange igniter
1) Igniter broken
2) Igniter was assembled incorrectly
86 Electric ign. test failed The ADC value from the flash point Check correct placement of flash point
Please check the igniter and sensor signal has increased insuffi- sensor and igniter.
make sure that the thermo- ciently during igniter test at the begin- Check connection of flash point sen-
couple is connected prop- ning of the test. sor.
erly. Possible causes: Check in the diagnostic menu (reading
1) Igniter or flash point sensor is not "Thermo 1") if sensor reacts on tem-
installed correctly perature changes (e.g. touch the sen-
2) Flash point sensor not connected sor with the fingers or apply it to a
3) Flash point sensor malfunction different temperature).
4) Igniter malfunction -> if not: Exchange flash point sensor.
Check in diagnostic menu on page 4 if
igniter works correctly.
-> if not: Exchange igniter.

UM Abel_V1.0B_EN 181
OptiFlash® Troubleshooting

Code Alarm/Message Description Possible Solutions/Actions


87 Gas ignition test failed The UV detection (with fire extin- In case of no flame:
Error might be caused by: guisher) or the resistance measure- 1) Check gas bottle connection
1) No gas flow ment at the igniter (without fire 2) Check gas tube connections
2) No gas flame detected extinguisher) could not detect a 3) Verify that needle valve at the front
flame. or at the gas igniter are open
Possible causes: 4) Check igniter connection & function
1) No flame 5) Check igniter position to gas outlet
2) Flame not detected Go to diagnostic menu and check
solenoid valve in unit (button "V2“). If
no "click" is audible:
Please contact service!
If flame is visible but not detected (for
UV detection):
1) Check in calibration menu "Extin-
guisher" if correct sensor has been
selected
2) Check the proper function of the UV
detection in calibration menu "Extin-
guisher"
If the alarm appears again, please
contact service!
89 Product not found The chosen product for the current Choose another product.
Please check the product test does not exist anymore.
name
91 Fire Both UV sensors have detected a If fire was not the cause:
After extinguishing, please, flame for 5s. - Make sure that no other flame is
restart the device. range of vision of UV detection
- For gas ignition: make sure that the
gas flame is not too big
- Check UV detection
92 Flash outside dipping A flashpoint was detected outside the Make sure you have selected the cor-
Flash appeared outside the dipping cycle. A significant increase in rect sample, product and expected
dipping cycle. the flash point sensor signal was flash point.
detected outside the dipping cycle, Make sure that the flash point sensor
which is in the range of a flash point is placed right. Check the connection
signal. & functionality of the flash point sen-
sor.
93 Igniter not installed Unit cannot read EEPROM of igniter Check igniter connection.
Please connect the igniter Possible causes: If the alarm appears again, please
1) No igniter connected contact service!
2) EEPROM of igniter damaged or not
programmed correctly
3) Connector or internal cabling prob-
lem
94 Sample probe not installed Unit cannot read EEPROM of sample Check sample probe connection.
Please connect the sample probe If the alarm appears again, please
probe. Possible causes: contact service!
1) No sample probe connected
2) EEPROM of sample probe dam-
aged or not programmed right
3) Plug not connected to main board

182 UM Abel_V1.0B_EN
Troubleshooting OptiFlash®

Code Alarm/Message Description Possible Solutions/Actions


95 Stirrer problem Limit switch LM1 detects whether the Check if the stirrer is possibly blocked
Please check the stirrer motor turns. This error is shown in by any objects in its range of motion.
mechanism case that the unit does not get If the stirrer is not blocked by any
impulses from this limit switch when it objects, please contact service!
turns.
96 Heater problem 96-0 - Heater problem Switch off the unit for at least 10 s and
Please check the heater Heater/Block temperature does not try it again (safety protection on main-
connection and restart the increase/decrease as expected. The board).
unit. heater needs to increase/decrease After this, restart the unit.
temperature by at least 3 °C in 5 min- If the alarm appears again, please
utes, if required. contact service!

96-1 - Heater problem


Heater thermocouple temperature is
not or too less increasing.
97 Flame outside the cup A flame was detected outside the cup Make sure you have selected the cor-
Sample with abnormal flash with the UV detection. This can hap- rect sample, product and expected
point pen with a sample, with an abnormal flash point.
flash point or when the sample tem- Make sure that no other flame is range
perature is already higher than the of vision of UV detection.
real flash point. Check UV detection.
98 xx °C/°F Block temperature The cell temperature measure is out Cool down the block in case it is too
Block temperature is outside of limits: hot.
of allowed temperature -60 °C to +160 °C Please contact service!
range. (-76 °F to +320 °F)
99 Connected sensors During a test, the unit checks whether Check whether the sample probe and
Please check whether the the sample temperature is increasing flash thermocouple are connected and
sample probe and thermo- and also whether the flash thermo- placed correctly.
couple are installed properly. couple value is increasing. In case
that no increase / very small increase
is detected this error is shown.
Sample temperature needs to
increase by at least 3 °C every 10
minutes (heating rate higher than
5 °C/min) or 15 minutes (heating rate
lower than 5 °C/min). Thermocouple
voltage needs to increase every 15 °C
by 0,045mV.
100 Sample probe max. temp. Sample temperature is higher than: Cool down the sample.
Sample temperature has 140 °C (284 °F) Make sure that the sample probe is
exceeded its maximum connected and placed properly.
allowed value. Check reading of sample probe
(Tsample in diagnostics menu) and
exchange sample probe, if necessary.
101 Cooling does not work The sample needs to cool down by at Make sure that:
least 3°C every 10 minutes during 1) Fan is working (air cooling selected)
internal pre-cooling (Abel and Tag). 2) Valve 1 is working, the liquid cool-
ing is on and the liquid has appropri-
ate temperature (liquid cooling
selected)
3) Peltier is working

UM Abel_V1.0B_EN 183
OptiFlash® Troubleshooting

Code Alarm/Message Description Possible Solutions/Actions


102 High temperature alarm Firmware gets HIGH_T_ALM from Cool down the sample, block & heater.
Make sure the block temper- electronics either if the block temper- Check reading of PT100 (Tblock in
ature probe is connected ature is over 650°C or the heater tem- diagnostic menu) and heater thermo-
properly and restart the perature over 1200°C couple (Theater). Please contact ser-
device. Possible causes: vice!
1) Temperatures are really above the
limits
2) Block PT100 or heater thermocou-
ple is not installed
3) Wrong reading from block PT100
or heater thermocouple
103 Shutter blocked FW counted less shutter movement Make sure that the shutter is not
Shutter is blocked by some steps than expected (Abel < 515). blocked by any objects or due to other
mechanical parts. The shutter moves to a calibration mechanical issues.
point first (limit switch LM2 changes Go to diagnostics mode and try to ini-
value). Then the motor moves tialize number of steps (Button "Cali-
towards the cup till the cover is fully brate" on page 4). Cup and cup-cover
open, then it goes backwards. There must be installed, arm closed - bottom
should be a constant amount of steps position:
between the calibration point and If number of calibration steps is out-
front position (Abel: 590 ± 75 steps). side of 590 ± 75 (Abel) - please con-
tact service!
104 Cup cover not installed FW counted more shutter movement Make sure that the cup and cup-cover
Please make sure, that the steps than expected (Abel > 665). are installed properly.
cup cover and the cup are The shutter moves to a calibration Go to diagnostics mode and try to ini-
installed properly. point first (limit switch LM2 changes tialize number of steps (Button "Cali-
value). Then the motor moves brate" on page 4). Cup and cup-cover
towards the cup till the cover is fully must be installed, arm closed - bottom
open, then it goes backwards. There position:
should be a constant amount of steps If number of calibration steps is out-
between the calibration point and side of 590 ± 75 (Abel) - please con-
front position (Abel: 590 ± 75 steps). tact service!
115 Fail writing to the FS The system is not able to write the First switch off the instrument and
The system fails to record data in the Flash memory. unplug the USB flash drive and then
the data In some cases the USB flash drive switch it on. The instrument is able to
might be the reason. If the USB flash work without them. If the alarm
drive is corrupted, the system might appears again, the reason could be
try to open a lot of files or directories the CPU board. If the alarm does not
which will block the operation with the reappear, check on a computer the
Flash memory. USB flash drive and format it in FAT if
there are corrupted files.
116 Parameters File Parameters file is defective. Internal The Internal parameters are initialized
Parameters file is defective. parameters are initialized. with some default values. Navigate to
Internal parameters are ini- Advanced > Instrument Setup >
tialized. Parameters and verify the settings.
117 Operators File The Operators file is defective. The operators names are initialized.
The Operators file is defec- The operators names are initialized. Navigate to Advanced > Environment
tive. The operators names > Operators and verify the settings.
are initialized.

184 UM Abel_V1.0B_EN
Troubleshooting OptiFlash®

Code Alarm/Message Description Possible Solutions/Actions


119 Calibration file is defective. The calibration file does not exist or The calibrations are initialized. Please
The Calibrations are initial- cannot be read. perform the calibration.
ized. Each calibration is saved in the File
The calibration file does not system in Flash memory. The alarm
exist or cannot be read. appears once at power on.
Each calibration is saved in
the File system in Flash
memory. The alarm appears
once at power on.
121 Internal voltage Some of the voltage is out of range: Please contact service!
Voltage out of range! alarm 121-1 - 24V devices (+/-1V)
Please check the voltage alarm 121-2 - 24V electronics (+/-1V)
measurement in menu diag- alarm 121-3 - 12V MMI (+/-0.4V)
nostics and restart the alarm 121-4 - 5V on the main board
device. (+/-0.3V)
alarm 121-5 - 3.3V on main board
(+/-0.15V)
alarm 121-6 - 2.5V on main board
(+/-0.1V)
122 Net voltage The net voltage measured in the unit Make sure that your net voltage is
Net voltage is outside of is outside of the allowed range. Possi- between the allowed range.
range 60V to 300V. Please ble cause could be the net voltage or For a check of connections and fuses
check the fuse on a power a broken connection or fuse at the on the power board, please contact
board. power board. service!

UM Abel_V1.0B_EN 185
OptiFlash® Troubleshooting

9.3 List of warning messages


/i

Code Warning/Message Description Possible Solutions/Actions


131 End of test Set at the end of a test - for informa- -
tion only
132 Standard not found The standard (the product is using) Select a different standard.
Selected standard does not was not found/was erased.
exist. Please select a differ-
ent standard.
134 Pretest Information for the user, that the test -
Flash point was detected was performed with pretest enabled.
with Pretest. The detected flash point should be
considered approximate and can be
used as expected flash point for the
next test with new specimen.
135 Flash Point too low Flash point should be detected around Run a new test with a fresh sample
Error caused by: expected Flash point temperature. In and select lower expected flash point
1) Flash Point during Safety case that it is detected on the first dip/ or use pretest.
Test Interval safety test interval, result should be
2) Flash Point on first dip in discarded.
137 Sample temperature Product settings allows to remove User is allowed to remove the sample
Sample temperature is over sample with a higher temperature with a higher temperature, but he/she
55 °C/130 °F than 55 °C/130 °F - and sample tem- must be careful to avoid burnings.
perature is higher than 55 °C/130 °F. In case you want to disable this
option, set the cooling temperature
to 55 °C/130 °F or lower.
138 Extinguisher A warning message that the fire extin- Check the extinguisher functionality
Extinguisher board removed guisher was removed/disconnected and go to menu Advanced> Quality>
(only High End and Standard (before the last switch off - it was More> Extinguisher and check that
Model) installed). the extinguisher was tested.
139 Extinguisher Extinguisher needs to be Verify whether the extinguisher works
Please, check the extin- checked regularly to verify that it is and go to Advanced > Calibration >
guisher functionality working properly. Extinguisher and store that you have
(only High End and Standard performed a test.
Model)
140 Max. sample temperature Sample temperature reached maxi- Make sure that you selected the cor-
Sample reached the safety mum allowed temperature for this rect sample, product and expected
stop temperature of xx °C/°F product. The maximum sample tem- flash point.
perature is specified in the product Modify the product settings to allow a
settings ("Safety stop at sample higher sample temperature ("Safety
temp."). stop at sample temp.").
141 No Flash Point found Flash point was not detected. Test is Make sure you have selected the cor-
Test stopped at xx °C/°F stopped at expected flash point + end rect sample, product and expected
of test temperature (specified in pro- flash point.
duct settings). Run a new test with a fresh sample
and a higher expected flash point.
142 Sample not cold enough According to the standard the sample Cool down the sample
Sample temperature was too should be at least 17°C (Abel)
high. below expected flash point.

186 UM Abel_V1.0B_EN
Troubleshooting OptiFlash®

Code Warning/Message Description Possible Solutions/Actions


146 Calibration to do Refuse the test flag is not set (Refuse Perform "Atmospheric Pressure" cali-
The date of a pressure cali- test: "No") in calibration menu "Atmos- bration in Advanced > Quality > More
bration has elapsed. The test pheric Pressure" and the calibration > Atmospheric Pressure.
can be started, but please, period has expired or not been done
renew the calibration. yet.
147 Calibration to do Refuse the test flag is not set (Refuse Perform "Sample probe" calibration in
The date of a sample probe test: "No") in calibration menu "Sam- Advanced > Quality > More > Sample
calibration has elapsed. The ple probe" and the calibration period probe.
test can be started, but has expired or not been done yet.
please, renew the calibration.
148 Calibration to do Refuse the test flag is not set (Refuse Perform "Sample probe circuit" cali-
The date of a sample circuit test: "No") in calibration menu "Sam- bration in Advanced > Quality > More
calibration has elapsed. The ple probe circuit" and the calibration >Sample probe circuit.
test can be started, but period has expired or not been done
please, renew the calibration. yet.
149 USB Unit cannot detect a connected USB Connect an USB flash drive. If the
USB stick not connected. flash drive. USB flash drive is connected, but an
icon is not shown in the status bar,
restart the unit or try to use a different
USB flash drive (file system on USB
flash drive should be FAT(32)!).
150 PDS Ethernet interface is enabled and no Make sure the Ethernet cable is con-
PDS connection failed. TCP IP connection is established for nected.
60s. The connection is established by Make sure the PDS server is running.
a PDS server. In case you do not want to use the
PDS connection, disable it in the
instrument parameters.
151 LIMS No LIMS connection is detected. This Make sure the cable is connected
LIMS connection failed. is detected by signal CTS (on the con- properly.
nector) which needs to be in logic "1". Make sure that the LIMS server is run-
ning.
In case you do not want to use LIMS,
disable the it in the instrument param-
eters.
152 Printer Unit prints results/calibrations/... but Verify whether the printer/USB flash
Printer connection failed. no printer found. drive is connected and switched on.
USB - no USB flash drive/printer is UART printer:
connected. make sure that the CTS signal is set
UART - the CTS bit (signal on the to logic "1".
UART connector) needs to be in logic In case you do not want to use a
"1". printer, disable it in the instrument
parameters.
153 Low expected FP For expected Flashpoints below 10°C/ For High End Model: Connect exter-
For expected FP below 50°F the air cooling might not be suffi- nal chiller to unit according to the
10°C/50°F it is recom- cient. Risk that desired block/sample instruction.
mended to use liquid cooling. temperature cannot be reached.
Therefore liquid cooling is recom-
mended.

UM Abel_V1.0B_EN 187
OptiFlash® Troubleshooting

188 UM Abel_V1.0B_EN
Appendix OptiFlash®

10 Appendix

UM Abel_V1.0B_EN 189
OptiFlash® Appendix

10.1 LIMS specification for results


LIMS offers two options: Short, Full

Short LIMS
/i

Field Signification Format Comment


communication
format ( Start of the message
1 Unit number 99 Instrument ID - LIMS set-
tings of the Instrument
parameters
2 Type of message “R” Stands for a result message
3 Date at the end of “YYYY-MM-DD”
test
3 Time at the end of “HH:MM” Mode 24h
test
4 Unit name “01234567890123456789” 20 char
5 Sample ID “01234567890123456789” 20 char
6 Product name “01234567890123456789” 20 char
7 Pretest “Off” “Off” or “On”, depends on
what was selected
8 Temperature unit UNIT UNIT:“°C” or “°F”
9 Expected flash point X.Y UNIT UNIT:“°C” or “°F”
10 Measured flash point X.Y UNIT Uncorrected flash point,
UNIT:“°C” or “°F”
11 Ambient pressure X.Y UNIT UNIT:“kPA”, “hPA”, ...
12 Corrected flash point X.Y UNIT UNIT:“°C” or “°F”
13 Sample end X.Y UNIT UNIT:“°C” or “°F”
temperature
14 Warning during test 0x00000000 32 Bits coded
15 End of test 0x00000000 32 Bits coded
16 Alarm which stopped Shown only if some alarm
test stopped a test
17 Result status
) End of the message
Checksum 2 characters

Example of a short LIMS communication format:

( 1,"R ","2015-03-26 ","11:06 ","104011 "," ethanol-1 ","EN-


ISO 13736-ic ","Off","°C", 12.0°C ,11.5°C ,98.4kPa , 12.0°C ,11.6°C ,
,"Stop on flashpoint "," "," Result ok ")B5

190 UM Abel_V1.0B_EN
Appendix OptiFlash®

Full LIMS
/i

Field Signification Format Comment


communication
format ( Start of the message
1 Unit number 99 Instrument ID - LIMS set-
tings of the Instrument
parameters
2 Type of message “R” Stands for a result message
3 Date at the end of “YYYY-MM-DD”
test
3 Time at the end of “HH:MM” Mode 24h
test
4 Unit name “01234567890123456789” 20 char
5 Company name “01234567890123456789” 20 char
6 Device type Abel
7 Serial number “01234567890123456789” 20 char
8 Sample probe serial “01234567890123456789” 20 char
number
9 FW version 1.00
10 Operator name “01234567890123456789” 20 char
11 Sample ID “01234567890123456789” 20 char
12 Sample description “01234567890123456789” 20 char
13 Sample note “01234567890123456789 40 char
01234567890123456789”
14 Standard name “01234567890123456789” 20 char
15 Product name “01234567890123456789” 20 char
16 Pretest “Off” “Off” or “On”, depends on
what was selected
17 Temperature unit UNIT UNIT:“°C” or “°F”
18 Expected flash point X.Y UNIT UNIT:“°C” or “°F”
19 Measured flash point X.Y UNIT Uncorrected flash point,
UNIT:“°C” or “°F”
20 Ambient pressure X.Y UNIT UNIT:“kPA”, “hPA”, ...
21 Corrected flash point X.Y UNIT UNIT:“°C” or “°F”
22 Sample end X.Y UNIT UNIT:“°C” or “°F”
temperature
23 Warning during test 0x00000000 32 Bits coded
24 End of test “Stop on flashpoint”
25 Alarm which stopped “Alarm description“ Shown only if some alarm
test stopped a test
26 Result status “Result status“
) End of the message
Checksum 2 char

UM Abel_V1.0B_EN 191
OptiFlash® Appendix

Example of a full LIMS communication line format:

(1 ,"R ","2015-03-26 ","11:06 ","104011 ","Lab name


","OptiFlash Abel ","000072 ","14090052 ","9.11 ","PAC
User ","ethanol-1 ","des123 ","note note ",
"EN-ISO 13736 ","EN-ISO 13736-ic ","Off","°C",12.0°C ,11.5°C
,98.4kPa ,12.0°C ,11.6°C , ,"Stop on flash point ","
","Result ok ")34

10.2 Printout specifications for results


Result printout offers three options: Short, Long, Full

Short result ====================================


printout example OptiFlash S/N: 000072
V 9.11 Print date: 31 Mar 2015
============= Result =============

Date: 26 Mar 2015 11:06 v9.11


Operator: PAC User
Sample ID: ethanol-1
Sample des.: description
Note: note note
note note
Standard: EN-ISO 13736
Product: EN-ISO 13736-ic

Expected flash point: 12.0°C


Uncorrected flash point: 11.5°C
Ambient pressure: 98.4kPa
Corrected flash point: 12.0°C
Ending: Stop on flash point
Alarm: – only shown when an alarm
Alarm – only shown when an alarm
Status: Result ok

------------------------------------

192 UM Abel_V1.0B_EN
Appendix OptiFlash®

Long result ====================================


printout example OptiFlash S/N: 000072
V 9.11 Print date: 31 Mar 2015
============= Result =============

Date: 26 Mar 2015 11:06 v9.11


Operator: PAC User
Sample ID: ethanol-1
Sample des.: description
Note: note note
note note
Standard: EN-ISO 13736
Product: EN-ISO 13736-ic

Expected flash point: 12.0°C


Uncorrected flash point: 11.5°C
Ambient pressure: 98.4kPa
Corrected flash point: 12.0°C
Ending: Stop on flash point
Alarm: - only shown when an alarm
Alarm - only shown when an alarm
Status: Result ok
Min.: °C Max.: °C
Instrument name: 104011
Ignition type: Electric
Pretest: Off
Internal pre-cooling: On
Warnings:
Max sample temp: 11.6°C
Sample probe SN: 14090052
Correlation:

------------------------------------

Full result ====================================


printout example OptiFlash S/N: 000072
V 9.11 Print date: 31 Mar 2015
============= Result =============

Date: 26 Mar 2015 11:06 v9.11


Operator: PAC User
Sample ID: ethanol-1
Sample des.: description
Note: note note
note note
Standard: EN-ISO 13736
Product: EN-ISO 13736-ic

Expected flash point: 12.0°C


Uncorrected flash point: 11.5°C

UM Abel_V1.0B_EN 193
OptiFlash® Appendix

Ambient pressure: 98.4kPa


Corrected flash point: 12.0°C
Ending: Stop on flash point
Alarm: – only shown when an alarm
Alarm – only shown when an alarm
Status: Result ok
Min.: °C Max.: °C
Instrument name: 104011
Ignition type: Electric
Pretest: Off
Internal pre-cooling: On
Warnings:
Max sample temp: 11.6°C
Sample probe SN: 14090052
Correlation:

============= Product ============

Name: EN-ISO 13736-ic


Standard: EN-ISO 13736
Type: Routine product
Temp. unit: °C
Expected flash point: °C
Min.: °C Max.: °C
Start test: 9.0°C
End of test: 8.0°C
Stirrer speed: 30rpm
Pretest question: On
Safety test int start: °C
Safety test interval: °C
Safety stop at sample temp: 130.0°C
Switch heat rate temp: °C
Heating rate 1: 1.0°C/min
Heating rate 2: 1.0°C/min
Switch test interval temp: °C
Test interval 1: 0.5°C
Test interval 2: 0.5°C
Cooling temp.: 55.0°C
Result Offset: 0.0°C
Lims report: Full
Print report: Full
Correlation formula A: 0.000
B: 0.000 C: 0.000
D: 0.000 E: 0.000
Unit:
Internal pre-cooling: On
Pre-cooling temp.: 17.0°C

------------------------------------

194 UM Abel_V1.0B_EN
OptiFlash®

/i

NOTES

UM Abel_V1.0B_EN 195
OptiFlash®

Web site: http://www.paclp.com


/i

PAC Companies
Address: PAC L.P.
PAC Corporate Headquarters
8824 Fallbrook Drive
Houston, Texas 77064
USA
Phone: +1 (0) 281 580 0339
Fax: +1 (0) 281 580 0719
Sales: [email protected]
Service: [email protected]
Address: PAC ISL
BP 70285 - Verson
Parc d’Activités de la Mesnillière
14653 Carpiquet Cedex
France
Phone: +33 (0) 231 264 300
Fax: +33 (0) 231 266 293
Sales: [email protected]
Service: [email protected]
Address: PAC Herzog
Badstrasse 3 - 5
P.O. Box 1241
DE-97912 Lauda-Königshofen
Germany
Phone: +49 (0) 9343 640 0
Fax: +49 (0) 9343 640 101
Sales: [email protected]
Service: [email protected]
Address: PAC Rotterdam
Innsbruckweg 35
3047 AG Rotterdam
The Netherlands
Phone: +31 (0) 10 462 4811
Fax: +31 (0) 10 462 6330
Sales: [email protected]
Service: [email protected]

196 UM Abel_V1.0B_EN

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