WS-302 Ab 11302021

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MATERIALS SPECIFICATION

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AB Tubular Steels WS-302 A. Shakhmatov 1
TITLE: DATE:
L80 Steel Tubular Products – 80 ksi Minimum Yield Strength 11/30/2021

1.0 SCOPE

1.1 This specification pertains to seamless steel tubular products that have a minimum yield strength of 80
ksi and meet the requirements of API 5CT Grade L80 Type 1 or this specification. This material is
listed in NACE MR0175 and exhibits good resistance to cracking in sour (H2S) containing
environments. When there is an apparent conflict or difference between this specification and a
referenced specification, this specification shall govern.

1.2 API 5CT covers oil country tubular goods (OCTG) such as tubing, casing and coupling stock. When
the wall thickness gets to be greater than that typically found in coupling stock, usually in the 1” (2.5
cm) range, then this specification may not be applicable. When bored bar or heavy wall mechanical
tube are used for to make L80 equivalent products for heavier wall products and API 5CT is not a
specific requirement (such as with Liner Hanger products), an acceptable alternative specification is
Weatherford WS-410. Note that there may be additional Supplemental requirements that need to be
evaluated; for example, Liner hanger products will also include at least the addition of WS-410
Supplement 2 (S2) at 14°F (-10°C) or lower but with a higher impact energy value; the minimum
average impact energy is 30 ft-lbs (41 joules) with no single test result less than 24 ft-lbs (33) joules.

1.3 When required by Purchase Order or Engineering Document, there are Supplemental Requirements that
are applicable and defined herein. A suffix attached to this specification (such as WS-302-S1S2) adds
the contents of the supplements listed to the specification requirements. Tubular products that are
required to meet cold weather impact requirements or impact tested in accordance with API 5CT shall
be tested in accordance with the relevant Supplemental Requirements. Tubular products that are
required to meet surface inspection requirements of API 5CT shall be tested in accordance with the
relevant Supplemental Requirements. Tubular product requiring compliance with API 5CT Grade L80
Type 1 in its entirety is specified when Supplement 22 is required. Supplement 26 is required for
tubular product to meet API 5CT Grades L80 Type 1 PSL-2. Supplement 60 is required for tubular
product to meet API 5CT Grades L80 Type 1 PSL-3.

1.4 Seamless casing, tubing, and coupling stock that meets the requirements of API 5CT Grade L80 Type 1
meet the requirements of this specification. The tube dimensions shall be in accordance with the
Engineering Drawing or Purchase Order. Unless specified, all ends are to be plain end.

2.0 REFERENCED SPECIFICATIONS

2.1 API 5CT: Specification for Casing and Tubing


2.2 ASTM A370: Mechanical Testing of Steel Products
2.3 ASTM A751: Test Methods, Practices and Terminology for Chemical Analysis of Steel Products
2.4 ASTM E10: Test Methods for Brinell Hardness of Metallic Materials
2.5 ASTM E18: Test Methods for Rockwell and Rockwell Superficial Hardness of Metallic Materials
2.6 ASTM E165: Standard Practice for Liquid Penetrant Inspection
2.7 ASTM E213: Ultrasonic Examination of Metal Pipe and Tubing

Uncontrolled unless stamped with a RED “Q”. © Weatherford, 2021, All rights reserved
This document is copyrighted and whether containing patentable or nonpatentable subject matter is and comprises the proprietary and confidential
information of Weatherford and by receiving this document the recipient agrees that this document is loaned in confidence with the understanding
that neither it nor the information in it will be reproduced or disclosed, in whole or in part for any purpose except the limited purpose for which it
D001103718 (AB.3) PMTD: isHowie, loaned.William 2021-12-20
This document and any facsimilies hereof shall be returned to Weatherford upon demand.
MATERIALS SPECIFICATION
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AB Tubular Steels WS-302 A. Shakhmatov 2
TITLE: DATE:
L80 Steel Tubular Products – 80 ksi Minimum Yield Strength 11/30/2021

2.8 ASTM E709: Standard Practice for Magnetic Particle Inspection


2.9 EN 10204: Metallic Products – Types of Inspection Documents
2.10 NACE MR0175: Sulfide Stress Cracking Resistant Metallic Materials for Oilfield Equipment
2.11 Weatherford Specification WS-410: 4130 – 4145 Steel - 80 ksi Min. Yield Strength
2.12 Weatherford Specification WT-401: Dimensional Requirements of API 5CT Tubulars for Single
Weight Liner Systems Products
2.13 Weatherford Specification WT-402: Dimensional Requirements of API 5CT Tubulars for Multi-
Weight Liner Systems Products

3.0 MATERIAL REQUIREMENTS

3.1 Chemical Composition: The chemical composition in weight percent shall be determined in accordance
with ATSM A751 and meet the requirements listed in the Table below:

C Mn Si P S1 Ni Cr Mo Cu
Min. --- --- --- --- --- --- --- --- ---
Max. 0.43 1.90 0.45 0.030 0.020 0.25 1.50 0.75 0.35
Note 1: When Charpy tests are successfully run in accordance with
Supplements 2 or 4, the sulfur limit is 0.025% maximum.

3.2 Mechanical Properties: The mechanical properties shall be determined at the mid radius location for
bars & heavy wall tubes and full wall (strip) sections for tube in accordance with ASTM A370 and shall
meet the requirements listed in the Table below:

Yield Strength Tensile Strength Elongation Hardness


ksi (MPa)1 ksi (MPa) Rockwell C2
Min. 80.0 (552) 95.0 (655) 17% ---
Max. 95.0 (655) 120.0 (827) --- 23.0
Note 1: Yield strength to be calculated using 0.5% by extension. When yield strength is
reported by 0.2% offset, the acceptance range is 81 ksi (558 MPa) to 94 ksi (648 MPa).
Note 2: There are applications which require a 22 HRC hardness maximum as defined in
Supplement 57.

3.3 Melt Practice: Steels made to this specification shall be electric furnace melted and fully killed. Basic
oxygen furnace melting is an acceptable route if followed by vacuum degassing and ladle refining. The
steel shall be produced using melt and refining practices proven capable of producing fine grained
steels which are free from deleterious defects. The steel may be either ingot cast or continuous cast.

3.4 Heat Treatment and Condition: The steel shall be furnished in the hot worked and quenched and
tempered condition. The minimum tempering temperature shall be 1050F (566C).

Uncontrolled unless stamped with a RED “Q”. © Weatherford, 2021, All rights reserved
This document is copyrighted and whether containing patentable or nonpatentable subject matter is and comprises the proprietary and confidential
information of Weatherford and by receiving this document the recipient agrees that this document is loaned in confidence with the understanding
that neither it nor the information in it will be reproduced or disclosed, in whole or in part for any purpose except the limited purpose for which it
D001103718 (AB.3) PMTD: isHowie, loaned.William 2021-12-20
This document and any facsimilies hereof shall be returned to Weatherford upon demand.
MATERIALS SPECIFICATION
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AB Tubular Steels WS-302 A. Shakhmatov 3
TITLE: DATE:
L80 Steel Tubular Products – 80 ksi Minimum Yield Strength 11/30/2021

3.5 Impact Toughness Test: Charpy V Notch tests shall be run in accordance with ASTM A370 at 32F
(0C) or lower. When possible by tube dimensions, the impact tests shall run in the transverse
direction. The minimum acceptable average impact value in the transverse direction shall be 15 ft-lbs
(20 joules) or in accordance with the following equation, whichever is greater:

CVN Absorbed Energy in ft-lbs = 14.4t+6.1 where t = thickness of tube at time of heat treatment.

When transverse tests cannot be conducted, longitudinal tests shall be run and the minimum acceptable
average impact value in the longitudinal direction shall be 30 ft-lbs (41 joules) or in accordance with
the following equation, whichever is greater:

CVN Absorbed Energy in ft-lbs = 28.9t+12.2 where t = thickness of tube at time of heat treatment.

3.6 Straightness and Tolerances: Tubing shall meet the dimensional tolerances of API 5CT. For
straightness, tubing shall exhibit a chord height deviation of less than 0.2%.

3.7 Repair Welding: Repair welding is not permitted.

4.0 SUPPLEMENTAL TEST REQUIREMENTS

4.1 Supplement 1- Volumetric Non-Destructive Examination (NDE): When required by Purchase Order or
Engineering Document, ultrasonic examination shall be performed in accordance with ASTM E213.
The calibration (distance amplitude curve or DAC) shall be based on notches measuring 5% of the wall
thickness in depth on the OD and ID. Indications exceeding the reference criterion must be reported
and may be a cause for rejection of the piece.

4.2 Supplement 2 - Impact Toughness Test: This Supplement has been incorporated into the main body
requirements of this specification.

4.3 Supplement 3 - Non-Destructive Examination (NDE): When required by Purchase Order or


Engineering Document, all machined tube surfaces shall be 100% inspected in accordance with the wet
fluorescent magnetic particle inspection (MPI) technique of ASTM A709 or liquid penetrant inspection
(LPI) in accordance with ASTM E165. Linear imperfections other than nonmetallic inclusions are
acceptable to lengths up to and including 1/32” (0.8 mm). Indications of nonmetallic inclusions are not
considered defects until the inclusion length exceeds 0.039” (1.0 mm).

4.4 Supplement 4 – Cold Weather Impact Toughness Test: When required by Purchase Order or
Engineering Document, the tests specified in Section 3.5 shall be performed at 14F (-10C) or lower.

4.5 Supplement 8 – Composition Restrictions: When required by Purchase Order or Engineering


Document, the composition requirements are further restricted in that chromium content shall be within
the 0.9% - 1.1% range.

Uncontrolled unless stamped with a RED “Q”. © Weatherford, 2021, All rights reserved
This document is copyrighted and whether containing patentable or nonpatentable subject matter is and comprises the proprietary and confidential
information of Weatherford and by receiving this document the recipient agrees that this document is loaned in confidence with the understanding
that neither it nor the information in it will be reproduced or disclosed, in whole or in part for any purpose except the limited purpose for which it
D001103718 (AB.3) PMTD: isHowie, loaned.William 2021-12-20
This document and any facsimilies hereof shall be returned to Weatherford upon demand.
MATERIALS SPECIFICATION
REV: SECTION: NUMBER Prepared by: PAGE APPROVAL:
AB Tubular Steels WS-302 A. Shakhmatov 4
TITLE: DATE:
L80 Steel Tubular Products – 80 ksi Minimum Yield Strength 11/30/2021

4.6 Supplement 10 – Restricted Mechanical Properties: When required by Purchase Order or Engineering
Document, the tensile strength range shall be restricted to 110.2 – 116.0 ksi (760 - 800 MPa).

4.7 Supplement 21 – Increased Mechanical Properties: When required by Purchase Order or Engineering
Document, the minimum yield strength shall be 85.0 ksi (586 MPa).

4.8 Supplement 22 – Additional Requirements to Meet API Specifications: When required by Purchase
Order or Engineering Document, casing, tubing and coupling stock shall be furnished to meet the
requirements of this specification and API 5CT for Grade L80, Type 1.

4.9 Supplement 24 – Special Customer Dictated Requirements – When required by Purchase Order or
Engineering Document:

4.9.1 Charpy V Notch tests shall be run in accordance with API 5CT (ISO 11960) SR 16 (Annex
A.10) at 14F (-10C) except as modified in this supplement with absorbed energy value
requirements giving an average (set of three) of 40 ft-lbs (54 J) with no individual specimen
less than 27 ft-lbs (37 J).

4.9.2 For tubulars with a wall thickness ≥ 0.75 inches (19 mm) the impact energy values shall the
greater of: a) an average 40 ft-lbs (54 J) with no individual specimen less than 27 ft-lbs ( 37 J)
or b) those values calculated using API 5CT (ISO 11960) equations for Grade Q125
longitudinal.

4.9.3 If reduced size specimens are required the reduction factors shall be applied as given in API
5CT, Tables C.9 and E.9 (as applicable).

4.9.4 Test specimen orientation shall be based on using a hierarchy of: 1st choice - transverse full
size; 2nd choice – longitudinal full size; 3rd choice – transverse ¾ size; 4th choice – longitudinal
¾ size; 5th choice - transverse ½ size; 6th choice – longitudinal ½ size.

4.9.5 Tubular material shall be considered acceptable at 14 °F (-10 °C) when tested at 32 °F (0 °C)
with impact energy values of at least 11 ft-lb (15 J) higher than required for 14 °F (-10 °C).

4.10 Supplement 26 – Application Driven Special Requirements: When required by Purchase Order or
Engineering Document/Drawing, casing, tubing and coupling stock shall be furnished to all
requirements of API 5CT for Grade L80 Type 1, PSL-2 material.

4.11 Supplement 32 – Standard Dimensional Requirements: When required by Purchase Order or


Engineering Document, the dimensional requirements of single weight API 5CT Tubulars shall be in
accordance with Weatherford Specification WT-401.

Uncontrolled unless stamped with a RED “Q”. © Weatherford, 2021, All rights reserved
This document is copyrighted and whether containing patentable or nonpatentable subject matter is and comprises the proprietary and confidential
information of Weatherford and by receiving this document the recipient agrees that this document is loaned in confidence with the understanding
that neither it nor the information in it will be reproduced or disclosed, in whole or in part for any purpose except the limited purpose for which it
D001103718 (AB.3) PMTD: isHowie, loaned.William 2021-12-20
This document and any facsimilies hereof shall be returned to Weatherford upon demand.
MATERIALS SPECIFICATION
REV: SECTION: NUMBER Prepared by: PAGE APPROVAL:
AB Tubular Steels WS-302 A. Shakhmatov 5
TITLE: DATE:
L80 Steel Tubular Products – 80 ksi Minimum Yield Strength 11/30/2021

4.12 Supplement 33 – Special Dimensional Requirements: When required by Purchase Order or


Engineering Document, the dimensional requirements of multiple weight API 5CT Tubulars shall be in
accordance with Weatherford Specification WT-402.

4.13 Supplement 46 – Additional Special Low Temperature Toughness Requirements: When required by
Purchase Order or Engineering Document, Charpy V Notch tests shall be performed at -50F (-46C) or
lower in accordance with ASTM A370. The minimum average longitudinal impact energy is 20 ft-lbs
(27 joules) with no single test result less than 14 ft-lbs (19 joules). When tested in the transverse
direction, the minimum average impact energy is 15 ft-lbs (20 joules) with no single test result less than
10 ft-lbs (14 joules).

4.14 Supplement 51 – Additional Requirements to meet Statoil Standard(s): When required by Purchase
Order or Engineering Document/Drawing the following shall apply:

4.14.1 Charpy V Notch tests shall be run in accordance with API 5CT (ISO 11960) SR 16 (Annex
A.10) at 14F (-10C) except as modified in this supplement with absorbed energy acceptance
criteria per API 5CT for this grade of material.

4.14.2 Test specimen orientation shall be based on using a hierarchy of: 1st choice - transverse full
size; 2nd choice – longitudinal full size; 3rd choice – transverse ¾ size; 4th choice – longitudinal
¾ size; 5th choice - transverse ½ size; 6th choice – longitudinal ½ size. Reduction factors for
impact values for sizes other than full size shall be as given in API 5CT.

4.13.3 Volumetric examination shall be in accordance with S1 using 5% wall thickness notches with
the added condition that remaining wall shall be a minimum 90% of nominal wall thickness.
Indications exceeding the reference criterion or which reduce the net effective wall thickness
below 90% of nominal must be reported and may be a cause for rejection of the piece.

4.15 Supplement 57 – Additional Requirements: When required by Purchase Order or Engineering


Document/Drawing the following shall apply:

4.15.1 Maximum hardness shall be restricted to 22HRC maximum.

4.15.2 Volumetric examination shall be in accordance with Supplement 1 (above) and shall cover
100% of the product and be inspected for the detection of both longitudinal and transverse
imperfections. The calibration (distance amplitude curve or DAC) shall be based on notches
measuring 5% of the wall thickness in depth on the OD and ID which is in accordance with
acceptance level L2.

4.15.3 Hardness variation: Variation in hardness readings between outer wall and inner wall shall not
exceed 3 HRC for wall thickness up to 12.7 mm (1/2 inch) and 4 HRC for thickness above 12.7
mm (1/2 inch) up to 19.0 mm (3/4 inch).

Uncontrolled unless stamped with a RED “Q”. © Weatherford, 2021, All rights reserved
This document is copyrighted and whether containing patentable or nonpatentable subject matter is and comprises the proprietary and confidential
information of Weatherford and by receiving this document the recipient agrees that this document is loaned in confidence with the understanding
that neither it nor the information in it will be reproduced or disclosed, in whole or in part for any purpose except the limited purpose for which it
D001103718 (AB.3) PMTD: isHowie, loaned.William 2021-12-20
This document and any facsimilies hereof shall be returned to Weatherford upon demand.
MATERIALS SPECIFICATION
REV: SECTION: NUMBER Prepared by: PAGE APPROVAL:
AB Tubular Steels WS-302 A. Shakhmatov 6
TITLE: DATE:
L80 Steel Tubular Products – 80 ksi Minimum Yield Strength 11/30/2021

4.16 Supplement 60 - Additional Requirements to meet API 5CT PSL-3: When required by Purchase
Order or Engineering Document/Drawing, casing, tubing and coupling stock shall be furnished to all
requirements of API 5CT for Grade L80 Type 1, PSL-3 material.

4.17 SUPPLEMENT 65 - Additional Requirements to meet BHP standard(s): When required by Purchase
Order or Engineering Document/Drawing the following shall apply:

4.17.1 Material shall be supplied to the requirements of API 5CT PSL2.

4.17.2 Quadrant Hardness testing. The maximum acceptable hardness variation between any position
in any quadrant shall be as defined in the following Table:

Wall Thickness Range Maximum Allowable Hardness Variation


0.500” (12.7 mm) or less 3.0 Rockwell C
0.501 (12.8 mm) – 0.749” (19.0 mm) 4.0 Rockwell C
0.750” (19.1 mm) or greater 5.0 Rockwell C

4.17.3 Prior austenite grain size shall be ASTM 5 or finer.

4.17.4 All mechanical testing (tensile, Charpy impact and hardness) shall be performed twice on each
lot of material.

5.0 QUALITY REQUIREMENTS

5.1 Traceability: The heat identification shall be maintained through all stages of processing. The heat
treat batch identities shall be maintained with the heat lot traceability.

5.2 Surface Quality – Visual Inspection: The tube shall be free cracks, laps, seams or other defects.
Removal of surface defects to the limits of API 5CT Grade L80 is acceptable.

Uncontrolled unless stamped with a RED “Q”. © Weatherford, 2021, All rights reserved
This document is copyrighted and whether containing patentable or nonpatentable subject matter is and comprises the proprietary and confidential
information of Weatherford and by receiving this document the recipient agrees that this document is loaned in confidence with the understanding
that neither it nor the information in it will be reproduced or disclosed, in whole or in part for any purpose except the limited purpose for which it
D001103718 (AB.3) PMTD: isHowie, loaned.William 2021-12-20
This document and any facsimilies hereof shall be returned to Weatherford upon demand.
MATERIALS SPECIFICATION
REV: SECTION: NUMBER Prepared by: PAGE APPROVAL:
AB Tubular Steels WS-302 A. Shakhmatov 7
TITLE: DATE:
L80 Steel Tubular Products – 80 ksi Minimum Yield Strength 11/30/2021

5.3 Test Requirements: The tests required with frequency are defined in the following Table:

Test Required Test Frequency Method & Acceptance Reference


Chemical Composition Once per heat Para. 3.1 & as required by S8
Tensile Properties twice per heat & heat treat batch Paragraph 3.2 & as required by S10, S21
Surface Hardness Once, each length or piece Paragraph 3.2 or S57
Hardenability One per heat S65
Volumetric Inspection 100% volume As required by S1, 22, 26, 51 or S57
Impact Toughness One set per heat & heat treat batch Para 3.5 and as required by S2, 4, 24, 46
or 51
Surface NDE Inspected 100% machined surfaces As required by S3
Surface Inspection 100% visual Paragraph 5.2
Quadrant Hardness Once per lot S57 or S65
All Mechanical Testing Twice per lot S65

5.4 Reports: A material test report (MTR) shall be prepared for each heat of material. The test report shall
contain the following minimum information: results of tests listed in Section 5.3, heat lot identification,
heat treat batch/lot identification, statement of compliance to this specification, and Purchase Order
Number. Personnel and laboratories performing testing shall be independent of the manufacturing
department in accordance with EN 10204 type 3.1 inspection certificate.

Uncontrolled unless stamped with a RED “Q”. © Weatherford, 2021, All rights reserved
This document is copyrighted and whether containing patentable or nonpatentable subject matter is and comprises the proprietary and confidential
information of Weatherford and by receiving this document the recipient agrees that this document is loaned in confidence with the understanding
that neither it nor the information in it will be reproduced or disclosed, in whole or in part for any purpose except the limited purpose for which it
D001103718 (AB.3) PMTD: isHowie, loaned.William 2021-12-20
This document and any facsimilies hereof shall be returned to Weatherford upon demand.

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