Agreement
Agreement
Agreement
3 February 2015
Agreement
(Revision 2, including the amendments which entered into force on 16 October 1995)
_________
01 series of amendments to the Regulation: Date of entry into force: 22 January 2015
UNITED NATIONS
* Former title of the Agreement: Agreement Concerning the Adoption of Uniform Conditions of
Approval and Reciprocal Recognition of Approval for Motor Vehicle Equipment and Parts, done at
Geneva on 20 March 1958.
GE.15-
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Annexes
1 Information document .................................................................................................................... 28
2 Communication .............................................................................................................................. 35
3 Addendum to the communication concerning a type of retrofit emission control device (REC)
pursuant to Regulation No. 132 ..................................................................................................... 37
4 Arrangement of the REC System Type-Approval mark ................................................................ 38
5 Test of a particulate reduction REC (Class I or II REC) ................................................................ 39
6 Test of a NOx reduction REC (Class III REC) ............................................................................... 46
7 Tests of a PM and NOx reduction REC (Class IV REC) ................................................................ 49
8 Test sequences ............................................................................................................................... 50
9 Limit value equivalence tables ....................................................................................................... 53
10 Requirements of the NOx control diagnostic system of NOx reduction or NOx and particulate
reduction REC requiring a reagent ................................................................................................. 57
11 Installation and Operation instructions .......................................................................................... 66
12 Specific requirements regarding the approval of a REC with respect to the emission limits
set out in the 06 series of amendments of Regulation No. 49 ........................................................ 69
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1. Purpose
This Regulation provides a harmonized method for the classification,
evaluation and approval of Retrofit Emission Control (REC) systems for
particulate matter (PM), for oxides of nitrogen (NOx), or for both PM and
NOx, and for the determination of the levels of emissions from compression-
ignition (CI) engines used in applications within the scope indicated in
paragraph 2.
The Regulation provides a framework for approval of REC for different
applications with corresponding environmental performance levels and for
the identification in Type Approval of those levels.
2. Scope
This Regulation applies to Retrofit Emission Control devices (REC) to be
installed:
2.1. On category M2, M3 and N vehicles1 and their CI engines, excluding those
vehicles approved according to Regulation No. 83;
2.2. On CI engines having a net power higher than 18 kW but not more than
560 kW installed in non-road mobile machinery,1 operated under variable
speed;
2.3. On CI engines having a net power higher than 18 kW but not more than
560 kW installed in non-road mobile machinery,1 operated under constant
speed;
2.4. On CI engines having a net power higher than 18 kW but not more than
560 kW installed in category T vehicles. 1
3. Definitions
For the purposes of this Regulation,
3.1. "Active regeneration" means any additional measure to initiate regeneration
either on a periodic or continuously regenerating REC.
3.2. "Adjustment factors" means additive upward adjustment factor and
downward adjustment factor or multiplicative factors to be considered during
periodic regeneration.
3.3. "Application range" means the range of engines to which a Retrofit Emission
Control device (REC) approved in accordance with this Regulation can be
applied.
3.4. "Class I Retrofit Emission Control device (REC)" means a retrofit emission
control device which is intended to control particulate matter emissions only,
and which does not increase the direct NO2 emissions.
1
As defined in the Consolidated Resolution on the Construction of Vehicles (R.E.3.), document
ECE/TRANS/WP.29/78/Rev.3, para. 2. -
www.unece.org/trans/main/wp29/wp29wgs/wp29gen/wp29resolutions.html.
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3.5. "Class IIA or IIB retrofit emission control device (REC)" means a REC
device which is intended to control particulate matter emissions only, and
which does not increase the direct tailpipe NO2 emissions by more than the
percentage specified in paragraph 8.4.2 based on the engine baseline
emission NO2 level.
3.6. "Class III Retrofit Emission Control device (REC)" means a retrofit emission
control device which is intended to control NOx emissions only.
3.7. "Class IV Retrofit Emission Control device (REC)" means a retrofit emission
control device which is intended to control both particulate matter emissions
and NOx emissions.
3.8. "Continuous regeneration" means the regeneration process of an exhaust
aftertreatment system that occurs either permanently or at least once per
applicable test cycle.
3.9. "DeNOx system" means an exhaust after treatment system designed to reduce
emissions of oxides of nitrogen (NOx) (for example, passive and active lean
NOx catalysts, NOx absorbers, and selective catalytic reduction (SCR)
systems).
3.10. "Emission control monitoring system" means the system that monitors the
operation of the emission control measures implemented in the engine and/or
REC system in accordance with the requirements of paragraph 18. of this
Regulation.
3.11. "Engine baseline emission" means the emissions of a given engine or engine
system without any retrofit emission control device. For engines without after
treatment the engine baseline emissions are equal to the engine out raw
emissions. For engines with after treatment the engine baseline emissions are
equal to the tailpipe emissions downstream of the after treatment system.
3.12. "Engine family" means an engine manufacturer's grouping of engine systems
which, through their design as defined in paragraph 7. of Regulation No. 49
or paragraph 7. of Regulation No. 96 as appropriate, have similar exhaust
emission characteristics; all members of the family shall comply with the
applicable emission limit values.
3.13. "Engine system" means the engine, the emission control system and the
communication interface (hardware and messages) between the engine
system Electronic Control Unit(s) (ECU) and any other powertrain or vehicle
control unit.
3.14. "ESC" means a test cycle consisting of 13 steady state modes to be applied in
accordance with the relevant series of amendments to Regulation No. 49.
3.15. "ETC" means a test cycle consisting of 1,800 second-by-second transient
modes defined in, and to be applied in accordance with the relevant series of
amendments to Regulation No. 49.
3.16. "Gaseous pollutants" means carbon monoxide, hydrocarbons (assuming a
ratio of CH1,85 for diesel), oxides of nitrogen (NOx, expressed as NO2
equivalent) and nitrogen dioxide (NO2).
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3.17. "Load condition" means the loading of particulate matter being stored at any
moment in a particulate reduction system (such as a filter) expressed as a
proportion of the maximum loading of particulate matter that may be stored
in the system under specific driving conditions without external regeneration
measures being initiated.
3.18. "Manufacturer" means the person or body who is responsible to the Type
Approval Authority for all aspects of the type-approval and can demonstrate
that it possesses the features required and the necessary means to achieve
quality assessment and conformity of production. It is not essential that the
person or body be directly involved in all stages of the construction of the
vehicle, system, component or separate technical unit which is the subject of
the approval process.
3.19. "Installer" means a person or body who is responsible for the correct and safe
installation of the approved REC.
3.20. "NOx Control Diagnostic system (NCD)" means a system of the REC which
has the capability of:
(a) Detecting a NOx Control Malfunction;
(b) Identifying the likely NOx control malfunctions by means of
information stored in computer memory and/or communicating that
information off-board.
3.21. "NOx-reduction REC" means a REC that has a NOx mass emission reduction
efficiency which qualifies it to be certified as meeting the classification class
as defined in this Regulation.
3.22. "NOx reduction REC family" means a family of NOx reduction systems that
are technically identical with respect to their functioning in accordance with
paragraph 15. of this Regulation.
3.23. "NRSC" means a test cycle consisting of steady state modes defined in, and to
be applied in accordance with, the relevant series of amendments to
Regulation No. 96.
3.24. "NRTC" means a test cycle consisting of 1,173 second-by-second transient
modes defined in, and to be applied in accordance with, the relevant series of
amendments to Regulation No. 96.
3.25. "On-board operator warning system" means a device that detects incorrect
operation or removal of the REC.
3.26. "Parent engine" means an engine selected from an engine family in such a
way that its emissions characteristics will be representative for that engine
family.
3.27. "Particulate matter (PM)" means the mass of any material collected on a
specified filter medium which is defined in the relevant series of amendments
to Regulations No. 49 or No. 96.
3.28. "Particulate reduction REC" means a REC that has a particulate mass or
particle number emission reduction efficiency which qualifies it to be
certified as meeting the classification class as defined in this Regulation. The
regeneration system and strategy are part of the particulate reduction REC.
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(b) The make and identifying part number of the REC as recorded in the
information document issued in accordance with the model set out in
Annex 1;
(c) The application range (as defined in paragraph 10. of this Regulation)
including year of manufacture, for which the REC is approved,
including, where applicable, a marking to identify if the REC is
suitable for fitting to a vehicle that is equipped with an on-board
diagnostic (OBD) system;
(d) The instruction manual for the retrofit installation;
(e) The end-user service manual including maintenance instructions.
4.3. The applicant shall provide the Information Document in accordance with
Annex 1 to this Regulation. The applicant shall also provide sample(s) of the
REC to be tested and to be retained by the Technical Service for at least five
years after the date of type approval.
2
The distinguishing numbers of the Contracting Parties to the 1958 Agreement are reproduced in
Annex 3 to the Consolidated Resolution on the Construction of Vehicles (R.E.3), document
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(b) The number of this Regulation, followed by the letter "R", a dash and
the approval number to the right of the circle as defined Annex 4 to
this Regulation. The approval number appears in the communication
form for this type (see paragraph 6.2. of this Regulation and Annex 2
to this Regulation) preceded by two figures indicating the latest series
of amendments to this Regulation;
(c) The Class of the REC.
5.4. REC samples for approval testing shall be clearly identified with at least the
applicant’s name and the reference of the application.
6. Approval
6.1. Type approval shall be granted if the REC meets the requirements of this
Regulation.
6.2. An approval number shall be assigned to each REC approved. Its first two
digits (at present 01 according to this series of amendments) shall indicate the
series of amendments incorporating the most recent major technical
amendments made to the Regulation at the time of issue of the approval. The
same type approval number shall not be assigned to another REC.
6.3. Notice of approval or of refusal or of extension of approval of a REC
pursuant to this Regulation shall be communicated to the Contracting Parties
to the Agreement applying this Regulation, by means of a Communication
form conforming to the model in Annex 2 to this Regulation.
7. General requirements
7.1. A REC approved in accordance with this Regulation shall be designed,
constructed and capable of being mounted so as to enable the application to
comply with the rules set out in this Regulation throughout the normal life of
the REC under normal conditions of use.
7.2. A REC approved in accordance with this Regulation shall be durable. That is,
it shall be designed, constructed and capable of being mounted so that
reasonable resistance is obtained to phenomena such as the corrosion,
oxidation, vibration and mechanical stress to which it will be exposed under
normal conditions of use. Specific durability requirements are in paragraph 9.
of this Regulation.
7.3. The REC manufacturer shall provide installation documents that will ensure
that the REC, when installed in the vehicle or machine, will operate, in
conjunction with the necessary machinery parts, in a manner that will comply
with the requirements of paragraphs 7., 8. and 9. of this Regulation. This
documentation shall include the detailed technical requirements and the
provisions of the REC (software, hardware, and communication) needed for
the correct installation of the REC in the machine.
7.4. Devices that by-pass or reduce the efficiency of the REC are not permitted.
7.5. A REC approved in accordance with this Regulation shall be fitted with an
on-board operator warning system that signals to the driver the presence of a
failure affecting the efficiency of the REC.
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7.5.1. A particulate reduction REC shall be equipped with a monitoring device that
detects incorrect operation or removal of the REC and that triggers an audible
and/or visual alarm to the operator. For reagent based particulate reduction
REC the monitoring device may interrupt the input of any reagent or
additive, if necessary. The warning system can be based for example on the
continuous measurement of the engine exhaust back-pressure
7.5.2. Specific requirements applicable to NOx reduction REC are provided in
paragraph 7.7. below and Annex 10 to this Regulation.
7.5.2.1. The NOx control strategy of the REC shall be operational under all
environmental conditions regularly pertaining in the territory of the
Contracting Parties, especially at low ambient temperatures.
7.5.3. Combined PM and NOx reduction REC (Class IV REC) shall meet the
provisions of paragraphs 7.5.1., 7.5.2. and 7.5.2.1. of this Regulation.
7.5.4. The filter of a particulate reduction REC or a combined PM and NO x
reduction REC shall be designed and constructed in a way that in can only be
installed in one direction. Intentionally or unintentionally reversing the filter
shall be physically impossible.
7.6. Specific requirements for REC requiring a reagent or additive.
7.6.1. Each separate storage tank installed on a vehicle or machine shall include
means for taking a sample of any fluid inside the tank. The sampling point
shall be easily accessible without the use of any specialised tool or device.
7.6.2. The driver or machine operator shall be informed of the level of reagent or
additive in the storage tank on the vehicle or machine through a specific
mechanical or electronic indication in accordance with Annex 10 to this
Regulation. The reagent level indicator and the warning indicator shall both
be placed in close proximity to the fuel level indicator.
7.6.3. The characteristics of the reagent, including the type of reagent, information
on concentration when the reagent is in solution, operational temperature
conditions and reference to international standards for composition and
quality shall be specified by the REC manufacturer in Annex 1 to this
Regulation.
7.6.4. Detailed written information fully describing the functional operation
characteristics of the operator warning system defined in paragraph 4. of
Annex 10 to this Regulation and of the operator inducement system defined
in paragraph 5. of Annex 10 to this Regulation shall be provided to the Type
Approval Authority at the time of type approval.
7.6.5. Reagent freeze protection
7.6.5.1. It is permitted to use a heated or a non-heated reagent tank and dosing
system. A heated system shall meet the requirements of paragraph 7.6.5.2.2.
of this Regulation. A non-heated system shall meet the requirements of
paragraph 6. of Annex 10 to this Regulation. The use of a non-heated reagent
tank and dosing system shall be indicated in the written instructions to the
driver or operator of the vehicle or machine.
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7.8.2. The instructions shall indicate requirements for the proper use and
maintenance of the REC in order to maintain its emissions performance,
including the proper use of consumable reagents.
7.8.3. The instructions shall be written in a clear and non-technical manner using the
same language as is used in the operator's manual on the vehicle or machine.
7.8.4. The instructions shall specify if consumable reagents have to be refilled by the
driver or operator between normal maintenance intervals. The instructions shall
also specify the required reagent quality. They shall indicate how the driver or
operator should refill the reagent tank. The information shall also indicate a
likely rate of reagent consumption and how often it should be replenished.
7.8.5. The instructions shall specify that use of, and refilling of, a required reagent
of the correct specifications is essential in order for the vehicle or machine to
comply with the requirements for the issuing of the approval of the REC for
that vehicle or machine.
7.8.6. The instructions shall state that it may be a criminal offence to use a vehicle
or machine that does not consume any reagent if the reagent is required for
the reduction of emissions.
7.8.7. The instructions shall explain how the operator warning and inducement
systems work. In addition, the consequences, in terms of performance and
fault logging, of ignoring the warning system and not replenishing the
reagent or rectifying the problem shall be explained.
7.9. The approval shall be conditional upon the following sub-paragraphs.
7.9.1. The manufacturer providing written maintenance instructions to be given by
the installer to the driver or operator.
7.9.2. The manufacturer providing installation documents for the REC.
7.9.3. The manufacturer providing instructions for an operator warning system, an
inducement system and reagent freeze protection (where applicable) to be
given by the installer to the workshop or the driver or the operator, as
appropriate.
7.9.4. The manufacturer providing a written statement to the installer, to be given to
the driver or operator, on the normal operating conditions (temperature range,
environmental conditions, …) within which the REC will operate correctly.
8. Performance requirements
8.1. REC approved under this Regulation shall meet all of the following criteria:
(a) The emission limit values as specified in paragraph 8.2.;
(b) The reduction levels as specified in paragraph 8.3.;
(c) The NO2 emission requirements as specified in paragraph 8.4.;
(d) The secondary emissions requirements as specified in paragraph 8.6.
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PM mass NOX
Reduction level 01 90 60
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9. Durability requirements
9.1. The applicant shall declare that the REC system when used and maintained
according to the manufacturer’s instructions will comply with the applicable
provisions during normal operation over a useful life of:
(a) For category M2 and M3 and N vehicles, a mileage of 200,000 km or a
service life of 6 years, whichever occurs first;
(b) For all other applications, 4,000 operating hours or a service life of
6 years, whichever occurs first.
9.2. The applicant shall conduct a 1,000 hours durability test on an engine and
REC combination. This test shall be either a field test in a typical vehicle or
machine application agreed between the Type Approval Authority and the
applicant or a test on an engine test bed. In the case of testing on an engine
test bed, the aging cycle, load and speed shall include conditions that
approximate to 10 per cent idle, 10 per cent transient operation, 75 per cent
high speed-high load operation, and 5 per cent low speed-medium load
operation.
The engine for the durability run may be different from the test engine used
for tests to establish the reduction level of the REC, but shall be an engine
within the declared application range of the particular REC.
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An engine approved to Regulation No. 49 will be considered a variable speed engine for this purpose.
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11.4. Subject to the requirements of paragraph 11.1. of this Regulation being met,
modifications downstream of an original after treatment system are
permitted.
11.5. The performance of any On-Board Diagnostics (OBD) system and NOx
control system of the original engine system shall not be compromised by the
REC.
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17.2. The REC manufacturer may, as an alternative to using market fuel, apply to
the Type Approval Authority for permission to perform the tests on the REC
using a reference fuel. The reference fuel to be used in this case will be the
appropriate fuel specified in either Regulation No. 49 or Regulation No. 96.
17.3. The specific fuel consumption of the engine fitted with the REC during the
applicable test cycles (paragraphs 2.3. and 3.3. of Annex 5 to this Regulation,
paragraphs 2.3. and 3.3. of Annex 6 to this Regulation) shall be not more than
4 per cent greater in the retrofitted condition than the mean specific
consumption in the non-retrofitted condition.
4
Road vehicles, for this purpose, are category M2, M3 and N vehicles as defined in the Consolidated
Resolution on the Construction of Vehicles (R.E.3), (document ECE/TRANS/WP.29/78/Rev.3,
para. 2 - www.unece.org/trans/main/wp29/wp29wgs/wp29gen/wp29resolutions.html), excluding
those vehicles approved according to Regulation No. 83.
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21.2. Where the Type Approval Authority approves the modification, a reference
to the formal notification of that approval shall be included in the installation
manual for the REC.
21.3. Confirmation or refusal of approval, specifying the alteration, shall be
communicated by the procedure specified in paragraph 6. above to the
Contracting Parties to the 1958 Agreement applying this Regulation.
21.4. The Type Approval Authority issuing the extension of approval shall assign a
series number for such an extension and inform thereof the other Contracting
Parties to the 1958 Agreement applying to this Regulation of that number by
means of the Communication form specified in Annex 2 to this Regulation.
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Annex 1
Annex 1
Information document
Information document No..….. of Regulation No. 132 relating to the type approval of
Retrofit Emission Control devices (REC) for heavy duty vehicles, agricultural tractors and
non-road mobile machinery equipped with compression ignition engines.
A list of the main components has to be attached to describe the range of validity of the
type approval. Any drawings and part lists shall be supplied in appropriate scale and
sufficient detail on size A4 or on a folder of A4 format. Photographs, if any, shall show
sufficient detail.
Upon request of the Type Approval Authority, further information may be needed for REC
family members to demonstrate compliance with paragraphs 14., 15. or 16. of this
Regulation, as appropriate.
If the system, components or separate technical units have electronic controls, information
concerning their performance shall be supplied.
1. General
1.1. Make (trade name of manufacturer): .................................................................
1.2. Name and address of manufacturer: ..................................................................
...........................................................................................................................
1.3. Type of REC: ....................................................................................................
1.4. Location and method of affixing of the approval mark: ...................................
...........................................................................................................................
1.5. Address(es) of assembly plant(s): ......................................................................
...........................................................................................................................
2. Description of the device
2.1. Class of REC: ....................................................................................................
2.2. Make(s) (Commercial name), and manufacturer's type identification of the
REC: ..................................................................................................................
...........................................................................................................................
2.2.1. Identifying part number(s) of the REC: ............................................................
...........................................................................................................................
2.3. Engine type or types for which the REC is intended (application range): .........
...........................................................................................................................
2.4. Number(s) and/or character(s) characterising the engine baseline emission(s)
performance: 1....................................................................................................
1
As defined in paragraph 8.2. of this Regulation.
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2
Strike out what does not apply.
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4.5.4. Control strategy (for example delay periods, reagent dosing rates, positioning
and characteristics of sensors, flow characteristics and reagent introduction
location): ............................................................................................................
4.6. Heated system: Yes/No2
4.6.1. Temperature control method (catalytic, thermal or electrothermal): .................
4.7. Description of NOx control diagnostic system (in accordance with Annex 10):
...........................................................................................................................
4.8. Description of any modifications to the original engine or emissions control
system as defined in paragraph 11. of this Regulation: ....................................
...........................................................................................................................
4.9. Normal operating temperature: ........... (K) and pressure range: ............. (kPa)
4.10. Use of insulation: Yes/No2
4.10.1. Design and characteristics of the insulation:......................................................
5. Characteristics of the NOx and PM reduction REC and the NOx and PM
reduction REC family
5.1. Dimensions, shape(s) and active volume(s) of the NOx and PM reduction
system: ..............................................................................................................
5.2. Maximum distance to the REC inlet from the outlet of the turbocharger
(turbine) or the outlet plane of the exhaust manifold where no turbocharger is
fitted): ...............................................................................................................
5.3. Description, drawings and part lists of the NO x and Particulate Matter (PM)
reduction REC
The description shall include a list of the main components (stating the part
numbers) that are assembled to a REC for each application. Furthermore the
description shall provide all information necessary to permit decisions
relating to the REC family to be made in accordance with paragraph 16 of
this Regulation.
5.3.1. Type of retention of the active element(s) (for example, adhesive or
mechanical fixing): ...........................................................................................
5.3.2. Working principles of the NOx reduction active element (for example
Selective Catalytic Reduction, NOx Storage and Reduction) and of the PM
reduction active element (for example metallic or ceramic material and
material type, barrier filtration or aerodynamic separation): ............................
...........................................................................................................................
5.3.3. Design and characteristics of the substrate(s) and active material(s) as defined
in paragraph 14.1. (c) and 15.1. (d) and (e) of this Regulation: ........................
...........................................................................................................................
5.3.3.1. Type(s) of catalytically active material(s): ........................................................
5.3.3.2. Physical design of the substrate(s): ...................................................................
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5.3.3.3. Working principle of the PM reduction active element (for example metallic
or ceramic material including material type, barrier filtration or aerodynamic
separation) .........................................................................................................
5.3.3.4. Cell density, porosity, mean pore size and pore size distribution of the PM
reduction active element: ..................................................................................
...........................................................................................................................
5.3.4. Location (upstream/downstream), function and working principle (e.g.
oxidation) of any supplementary catalyst(s): .....................................................
5.3.4.1. Type(s) of catalytically active material(s): ........................................................
5.3.4.2. Physical design of the substrate: ........................................................................
5.3.4.3. Cell density: .......................................................................................................
5.3.5. Minimum volumetric concentration of catalytically active materials of each
element of the NOx and PM reduction system including supplementary
catalysts (if fitted) (grams/m³): .........................................................................
...........................................................................................................................
5.3.6. Maximum volumetric concentration of catalytically active materials of each
element of the NOx and PM reduction system including supplementary
catalysts (if fitted) (grams/m³): ..........................................................................
...........................................................................................................................
5.3.7. The design characteristics of the canning or packaging: ..................................
5.3.8. Volume of each active component: ...................................................................
5.4. Method(s) or system(s) of regeneration (if applicable) (comprehensive
description and/or drawing): .............................................................................
5.4.1. Type of PM reduction system regeneration (for example periodic or
continuous): ......................................................................................................
5.4.2. PM reduction system regeneration principle and regeneration strategy: ..........
...........................................................................................................................
5.5. Method and control strategy for introducing additives or reagents (if used):
...........................................................................................................................
5.5.1. Type and concentration of reagent(s) or additive(s) (if used): ..........................
...........................................................................................................................
5.5.2. Frequency of reagent(s) or additive(s) refill: ....................................................
5.5.3. Normal operational temperature range of NOx reduction reagent(s): ......... (K)
5.5.4. Control strategy (for example delay periods, reagent dosing rates, positioning
and characteristics of sensors, flow characteristics and reagent introduction
location): ...........................................................................................................
5.6. Heated system: Yes/No2
5.6.1. Temperature control method (catalytic, thermal or electrothermal): .................
5.7. Description of PM reduction system monitoring (in accordance with
paragraph 7.5.1. of this Regulation): .................................................................
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5.8. Description of NOx control diagnostic system (in accordance with Annex 10):
...........................................................................................................................
5.9. Description of any modifications to the original engine or emissions control
system as defined in paragraph 11. of this Regulation: ....................................
...........................................................................................................................
5.10. Normal operating temperature: ........... (K) and pressure range: ............. (kPa)
5.11. Use of insulation: Yes/No2
5.11.1. Design and characteristics of the insulation:......................................................
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Annex 2
Annex 2
Communication
(Maximum format: A4 (210 x 297 mm))
1
1
Distinguishing number of the country which has granted/extended/refused/withdrawn approval (see
approval provisions in the Regulation).
2
Strike out what does not apply.
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7.1. Has the REC demonstrated compatibility with OBD requirements: Yes/No 2
8. Location and method of affixing of the approval mark: ...................................
9. Submitted for type-approval on: ........................................................................
10. Technical Service responsible for approval tests: .............................................
10.1. Date of test report: ............................................................................................
10.2. Number of test report: .......................................................................................
11. Type-approval granted / extended / refused / withdrawn 2
12. Reason(s) of extension (if applicable): .............................................................
13. Engine type or types for which the REC is intended (application range) based
on test results: ...................................................................................................
14. REC Class I / II / III / IV 2 and reduction efficiency: .......................................
14.1. Designed for fitment to an engine meeting the emissions requirements of
(Regulation and Stage): ....................................................................................
14.2. The engine + REC system meets the requirements of (Regulation and Stage)
........................................................................... for NOx / PM / NOx and PM 2
14.3. The engine + REC system continues to meet the requirements of the above
Regulation and Stage for other pollutants regulated by that Regulation and
Stage: Yes/No 2
15. Annexed to this communication is a list of documents in the type approval
file deposited at the Type Approval Authority having delivered the type
approval and which can be obtained upon request.
16. The following documents, bearing the approval number shown above, are
annexed to this communication: .......................................................................
16.1. Verification of the engine baseline emissions: ..................................................
16.2. Determination of emissions with the REC fitted: .............................................
16.3. Results of the reduction efficiency: ..................................................................
16.4. Performance of an endurance run: ....................................................................
16.5. Determination of the NO2 emissions and of emissions of the other regulated
pollutants: .........................................................................................................
16.6. Declaration on noise emissions: .......................................................................
...........................................................................................................................
17. Place: ................................................................................................................
18. Date: .................................................................................................................
19. Signature: ..........................................................................................................
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Annex 3
1. Engines on which the retrofit emission control device has been tested:
Engine No. 1 2 n
Make
Type
Engine
Power
Category
2. Test results:
...........................................................................................................................
...........................................................................................................................
...........................................................................................................................
...........................................................................................................................
...........................................................................................................................
...........................................................................................................................
...........................................................................................................................
3. Engine type(s) for which the REC device is qualified (application range):
Number
Vehicle or engine manufacturer
Model year from/to
Engine type
Capacity / cylinder (cm³)
Capacity VH (cm³)
engine net power (kW with min-1)
Engine baseline emissions
Silencer replaced
Type identification of the REC
REC Type and Reduction Level
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Annex 4
Class II A
a = 8 mm min
The above example type-approval mark affixed to a REC shows that the type
concerned has been approved in the Netherlands (E 4), pursuant to Regulation No. 132
under type-approval No. 011234. The first two digits of the type-approval number indicate
that the approval was granted in accordance with the requirements of Regulation No. 132
in the form amended by this series. The approval mark shall also show the Class of REC (I,
IIA, IIB, III or IV).
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Annex 5
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The gaseous emissions and the particulate mass, and the particle number
when appropriate, shall be measured during at least each fifth test cycle. A
separate test of the particulate reduction system is carried out for each family
or application range defined in the type approval procedure for the engine
with which the REC system is intended to be used. That is, one system test
takes place for each application area.
4.3. A particulate reduction REC is considered to have been proved to have a
continuously operating regeneration process if a suitable assessment variable
can be regarded as constant over at least 25 applicable test cycles. The
average particulate emission and the average exhaust gas backpressure are
regarded as suitable assessment variables for this purpose.
If an applicant wishes to use one or more different assessment variables, he
shall present a robust technical case to the Type Approval Authority in
support of his request to do so.
Where a continuously regenerating system as defined above also contains
provision for active regeneration, then the assessment criteria defined in
paragraph 4.6. of this annex shall be applied.
The PM mass emission and the exhaust gas backpressure are considered
constant within the meaning of this Regulation where there is a coefficient of
variance of less than 25 per cent over 25 test cycles. The exhaust gas
backpressure is measured continuously for the purposes of this assessment and
the particulate emissions are measured during at least every fifth test cycle.
The coefficient of variance (CoV) is calculated as follows:
n x 2 x
2
Standard deviation
n n 1
and:
Average value ( x1 x2 ... xn ) / n
Where:
n= number of measured values
x= respective single measured value
4.4. Test of the regeneration characteristic of a particulate reduction REC
This testing is carried out by loading the system with particulate matter until a
constant exhaust gas backpressure is reached or over a time period of a
maximum of 100 hours if no constant value for the backpressure has been
achieved before that time. The exhaust gas backpressure is considered constant
if, when measured after a period of at least 50 hours, the exhaust gas
backpressure does not vary by more than plus or minus 4 mbar within a period
of 30 min. The test points of the cycle used for loading the system are to be
selected so that a maximum exhaust gas temperature of 180 °C at the inlet of
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the particulate reduction system is not exceeded. The loading of the system
with particulate matter is preferably carried out by running the test engine at a
constant speed of between 50 per cent and 75 per cent of its rated speed.
After the REC has been loaded with particulate matter until the backpressure
is constant, or after a maximum of 100 hours of running to load the system as
defined above, regeneration is activated. This can, for example, be activated
by running the engine at a higher load mode step so as to increase the exhaust
temperature. After completion of the regeneration, exhaust gas measurements
are to be taken during at least three iterations of the appropriate test cycle
(That is, three ESC cycles, ETC cycles, WHSC cycles, WHTC cycles, NRSC
cycles, or NRTC cycles.) The measured exhaust gas pollutant values shall not
deviate from the measured exhaust gas pollutant values before the REC
loading procedure by more than 15 per cent for the gaseous emissions or
more than 20 per cent for the particulate mass or particle number.
The manufacturer shall confirm in writing that the maximum temperatures
occurring during the regeneration process will not damage or significantly
shorten the effective life of the REC.
As an alternative to using the loading procedure described above, the
manufacturer may provide a particulate reduction REC already loaded to the
limit for the regeneration test.
4.5. Assessment criteria for continuously regenerating particulate reduction REC
The REC system test of the particulate reduction REC is considered
satisfactory if the particulate emissions measured as defined in paragraph 8.
of this Regulation are met.
4.5.1. Regulated pollutants
The emissions of the regulated pollutants are determined by measurements
taken immediately after the tests to establish the regeneration characteristics.
The emissions of the regulated pollutants (CO, HC, PM and NO x) in the
initial condition and in the retrofitted condition shall be within the limit
values for the emissions stage or standard for which the engine was originally
type-approved. The NO2 to NOx ratio for the initial condition and the
retrofitted condition is to be recorded and shown in the test report.
The determination of the NO 2 and NOx mass emissions is to be determined
by simultaneous measurement in accordance with paragraph 13.2. of this
Regulation.
4.6. Assessment criteria for periodically regenerating particulate reduction REC
This provision only applies to REC which utilise active regeneration.
The emissions shall be measured during at least three appropriate hot-start test
cycles (That is, three hot-start ESC cycles, ETC cycles, WHSC cycles, WHTC
cycles, NRSC cycles, or NRTC cycles.) One of the cycles from which
measurements are taken should include a regeneration event on a stabilized
REC system. The other two cycles from which measurements are taken should
be cycles in which regeneration does not occur. If regeneration takes longer
than one test cycle, consecutive test cycles shall be run until regeneration is
complete.
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The REC manufacturer shall declare the conditions under which the
regeneration process normally occurs (the particulate loading, temperature,
exhaust back-pressure, or other relevant parameters). The manufacturer shall
also provide the frequency of the regeneration event in terms of the fraction
of tests during which the regeneration occurs. The exact procedure used to
determine this fraction shall be agreed with the manufacturer by the Type
Approval Authority on the basis of good engineering judgement. (This
frequency fraction is the factor F in the procedure for calculation of nominal
particulate emissions set out below.)
For a regeneration test, the manufacturer shall provide a particulate reduction
REC system that has been loaded with particulate matter. As an option, the
manufacturer may run consecutive test cycles as set out in paragraph 4.4. of
this annex until the particulate reduction REC is loaded. Emissions
measurement is not required on cycles run for the purposes of loading the
REC with particulate matter.
Average emissions between regeneration phases shall be determined from the
arithmetic mean of several tests approximately equidistant in terms of the
number of unmeasured test cycles between them. As a minimum, at least one
test cycle as close as possible prior to a regeneration test and one test cycle
immediately after a regeneration test shall be included in the calculation of
the arithmetic mean.
During the regeneration test, all the data needed to detect regeneration shall
be recorded (CO or NOx emissions, temperature before and after the REC,
exhaust back pressure, and any other relevant parameters). It is permissible
for the applicable emission limits to be exceeded during the regeneration
process. The test procedure is shown schematically in Figure 1.
Figure 1
Scheme of periodic regeneration
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Where:
F = frequency of the regeneration event in terms of the fraction of tests
during which the regeneration occurs
Mgaswor = average specific emission from a test in which the regeneration
does not occur [g/kWh]
Mgasr = average specific emission from a test in which the regeneration
occurs [g/kWh]
The manufacturer may choose, on the basis of good engineering analysis, to
calculate either a multiplicative or an additive the regeneration adjustment
factor kr, expressing the average emission rate, as follows:
k r = Mgas / Mgaswor (multiplicative adjustment factor)
or
k Ur = Mgas - Mgaswor (upward adjustment factor)
or
k Dr = Mgas - Mgas r (downward adjustment factor)
4.7. Determination of NO2 emissions
The testing shall be performed on the test engine selected by the criteria
described in paragraph 12. of this Regulation.
4.7.1. Selection of the particulate reduction REC for NO2 determination.
The REC used for testing may be different from the REC used in
paragraph 4.5. of this annex. The particulate reduction REC to be tested shall
be:
(a) A particulate reduction REC with the largest active volume and, if a
diesel oxidation catalyst (DOC) is used upstream, the catalytic
converter with the largest active surface area and
(b) The particulate reduction REC containing the maximum charge of
platinum with the maximum total charge of catalytically active
material within the defined REC family.
The chosen particulate reduction REC shall be fitted in such a way that the
shortest distance between the engine and the particulate reduction REC, as
specified in the application range for the particulate reduction REC, is
achieved.
The particulate reduction REC shall be unloaded and shall not have been run
in for longer than 125 hours.
4.7.2. Determination of NO2 emissions
Three successive WHTC or NRTC test cycles, as appropriate to the
application, shall be conducted. The emissions shall be determined over all
three cycles and averaged. If the range of these results is greater than
±15 per cent of the mean, then an additional test cycle should be run.
The calculation of the NOx and NO2 emissions shall be determined for CI
engines used in vehicles of category M and N over the complete WHTC
cycle.
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Annex 6
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4.2. The NO2 to NOx ratio for the initial condition and the retrofitted condition is
to be recorded and shown in the test report.
The determination of the NO2 and NOx mass emissions is to be determined
by simultaneous measurement in accordance with paragraph 13.2. of this
Regulation.
4.3. Determination of NO2 emissions
The testing shall be performed on the test engine selected by the criteria
described in paragraph 12. of this Regulation.
Three successive WHTC or NRTC test cycles, as appropriate to the
application, shall be conducted. The emissions shall be determined over all
three cycles and averaged. If the range of these results is greater than
±15 per cent of the mean, then an additional test cycle shall be run.
The calculation of the NOx and NO2 emissions shall be determined for CI
engines used in vehicles of category M and N over the complete WHTC
cycle.
For CI engines used in non-road mobile machinery or Category T vehicles
having an installed net power higher than 18 kW, but not more than 560 kW
the calculation of the NOx and NO2 emissions shall be determined over the
complete NRTC cycle.
5. Test cycles
5.1. In cases where the approval of the engine with which the REC is to be used is
an on-road approval (performed in accordance with Regulation No. 49) the
test cycle to be used for approval of the REC shall be the test cycle associated
with the emissions stage in Regulation No. 49 for which approval of the REC
is being sought.
5.2. Where the engine is being used in an on-road application and has an approval
issued in accordance with the requirements of Regulation No. 49, the test
cycle to be used for the establishment of the base emissions of the engine
shall be the test cycle associated with the emissions stage in Regulation
No. 49 for which the engine has an approval.
5.3. Where the engine is being used in an on-road application but does not have
an approval issued in accordance with the requirements of Regulation No. 49,
the test cycle to be used for the establishment of the base emissions of the
engine shall be the test cycle associated with the emissions stage in
Regulation No. 49 for which approval of the REC is being sought.
5.4. In cases where the approval of the engine with which the REC is to be used is
a non-road approval (performed in accordance with Regulation No. 96) the
test cycle to be used for approval of the REC shall be the test cycle associated
with the emissions stage in Regulation No. 96 for which approval of the REC
is being sought.
5.5. Where the engine is being used in a non-road application and has an approval
issued in accordance with the requirements of Regulation No. 96, the test
cycle to be used for the establishment of the base emissions of the engine
shall be the test cycle associated with the emissions stage in Regulation
No. 96 for which the engine has an approval.
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5.6. Where the engine is being used in a non-road application but does not have
an approval issued in accordance with the requirements of Regulation No. 96,
the test cycle to be used for the establishment of the base emissions of the
engine shall be the test cycle associated with the emissions stage in
Regulation No. 96 for which approval of the REC is being sought
5.7. For the purposes of establishing the REC efficiency and the emissions of NO 2
the appropriate test cycle is that defined in paragraph 8.3. of this Regulation.
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Annex 7
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Annex 8
Test sequences
1. Test sequence for particulate reduction REC
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Start
1000h Durability
testing
Paragraph 9
YES
NO
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Start
1000h Durability
testing
Paragraph 9
YES
Specific requirements for
REC requiring a REC requiring a
reagent or additive? reagent or additive
Paragraph 7.6
Paragraphs 7.6 and
and 7.7
7.7
NO
Active
regeneration
provisions ? YES
NO
Requirements of the NOx control diagnostic system of NOx or NOx and PM reduction REC requiring a
reagent; Annex 10
Particulate and NOx reduction REC in accordance with Paragraph 8 and Annex 7
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Annex 9
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Table A9/2
Equivalence Matrix for Regulation No. 96 / REC Class I / II
Baseline* Net Power Component Class I / II, to the standard of
[kW] [g/kWh] H I J K L M N P Q R
E 130 ≤ P ≤ 560 PM - - - - 0.025 - - - 0.025 -
F 75 ≤ P < 130 PM - - - - - 0.025 - - - 0.025
G 37 ≤ P < 75 PM - - - - - - 0.025 (1)
0.025 -(2)
- 0.025 (1)
D 18 ≤ P < 37 PM - - - 0.6 (3) - - - - - -
L 130 ≤ P ≤ 560 PM - - - - - - - - - -
M 75 ≤ P < 130 PM - - - - - - - - - -
N 56 ≤ P < 75 PM - - - - - - - - - -
P 37 ≤ P < 56 PM - - - - - - - - - -
(1)
Only for engines 56 ≤ P < 75
(2)
Only for engines 37 ≤ P < 56
(3)
Only for engines 19 ≤ P < 37. Engines 18 ≤ P <19 are to be treated as having no further stage
*
Where the baseline corresponds to that in Regulation No. 96, Revision 2.
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Table A9/3
Equivalence Matrix for Regulation No. 96 / REC Class III
Baseline* Net Power Component Class III, to the standard of
[kW] [g/kWh] H I J K L M N P Q R
E 130 ≤ P ≤ 560 NOx 4.0 (4) - - - 2.0 - - - 0.4 -
F 75 ≤ P < 130 NOx - 4.0 (4)
- - - 3.3 - - - 0,4
G 37 ≤ P < 75 NOx - - 4.7 (4)
- - - 3.3 (1)
4.7 (2,4)
- - 0.4 (1)-
D 18 ≤ P < 37 NOx - - - 7.5 (3,4) - - - - - -
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Table A9/4
Equivalence Matrix for Regulation No. 96 / REC Class IV
Baseline* Net Power Component Class IV, to the standard of
[kW] [g/kWh] H I J K L M N P Q R
PM - - - - 0.025 - - - 0.025 -
E 130 ≤ P ≤ 560
(4)
NOx 4.0 - - - 2.0 - - - 0.4 -
PM - - - - - 0.025 - - - 0.025
F 75 ≤ P < 130
(4)
NOx - 4.0 - - - 3.3 - - - 0.4
(1) (2)
PM - - - - - - 0.025 0.025 - - 0.025 (1)
G 37 ≤ P < 75
NOx - - 4.7 (4) - - - 3.3 (1) 4.7(2,4)- - 0.4 (1)
PM - - - 0.6 (3) - - - - - -
D 18 ≤ P < 37
(3,4)
NOx - - - 7.5 - - - - - -
PM - - - - 0.025 - - - 0.025 -
H 130 ≤ P ≤ 560
(3)
NOx - - - - 2.0 - - - 0.4 -
PM - - - - - 0.025 - - - 0.025
I 75 ≤ P < 130
NOx (3) - - - - - 3.3 - - - 0.4
(1) (2)
PM - - - - - - 0.025 0.025 - - 0.025 (1)
J 37 ≤ P < 75
NOx (3) - - - - - - 3.3 (1) 4.7 (2,4) - 0.4 (1)
PM - - - - - - - - - -
K 19 ≤ P < 37
NOx (3) - - - - - - - - - -
PM - - - - - - - - - -
L 130 ≤ P ≤ 560
NOx - - - - - - - - 0.4 -
PM - - - - - - - - - -
M 75 ≤ P < 130
NOx - - - - - - - - - 0.4
PM - - - - - - - - - -
N 56 ≤ P < 75
NOx - - - - - - - - - 0.4
PM - - - - - - - - - -
P 37 ≤ P < 56
NOx - - - - - - - - - -
(1)
Only for engines 56 ≤ P < 75
(2)
Only for engines 37 ≤ P < 56
(3)
Only for engines only for engines 19 ≤ P < 37. Engines 18 ≤ P <19 are to be treated as having no further
(4)
Sum of hydrocarbons and oxides of nitrogen
*
Where the baseline corresponds to that in Regulation No. 96, Revision 2.
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Annex 10
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6.1.4. Non-erasable failure messages identifying the reason of failures of the REC
system shall be stored by the NCD system for at least 400 days.
6.1.4.1. The failures messages shall be accessible via a generic scan-tool, as defined
in paragraph 3.36.1. of this Regulation.
6.1.5. If the failure has been remedied after the engine shut-off, the NCD system
may enable an engine re-start prior to the 48 hours period upon request of a
proprietary scan-tool, as defined in paragraph 3.36.2. of this Regulation,
using a pass code provided by the REC manufacturer or an authorized dealer
upon request.
6.1.5.1. The REC manufacturer shall ensure that adequate tools are available on
market for service or dealers.
6.1.5.2. The provision in paragraph 6.1.5. of this annex shall not be used more than
one time.
6.1.5.3. The provisions of paragraph 6.1.4. of this annex apply.
6.2. Non-heated REC system
6.2.1. The operator warning system described in paragraph 4.3. of this annex shall
be activated if no reagent dosing occurs at an ambient temperature ≤ 266 K
(-7 °C) in accordance with paragraph 2.3.2. of this annex.
6.2.2. The operator inducement system described in paragraphs 5.3. to 5.6. of this
annex shall be activated if no reagent dosing occurs within a maximum of
70 minutes after engine start at an ambient temperature ≤ 266 K (-7 °C).
7. Reagent availability
7.1. Reagent level indicator
The minimum acceptable performance level for the reagent indicator is that it
shall continuously indicate the reagent level whilst the operator warning
system referred to in paragraph 4. of this annex is activated. The reagent
indicator may be in the form of an analogue or digital display, and may show
the level as a proportion of the full tank capacity, the amount of remaining
reagent, or the estimated operating hours remaining.
7.2. Activation of the operator warning system
7.2.1. The operator warning system shall be activated in accordance with
paragraph 4.3. of this annex when the level of reagent goes below
(a) 10 per cent of the capacity of the reagent tank or a higher percentage
at the choice of the REC manufacturer; or
(b) A level corresponding to 12 hours of usage of the vehicle or machine
under average conditions of operation.
7.2.2. The warning provided shall be sufficiently clear, in conjunction with the
reagent indicator, for the driver or operator to understand that the reagent
level is low. When the warning system includes a message display system,
the visual warning shall display a message indicating a low level of reagent.
(For example "urea level low", "AdBlue level low", or "reagent low").
7.2.3. Paragraphs 4.4. to 4.6. of this annex do not apply.
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7.2.4. The operator warning system shall escalate in intensity when the level of
reagent goes below:
(a) 2.5 per cent of the capacity of the reagent tank or a higher percentage
at the choice of the REC manufacturer; or
(b) A level corresponding to 3 hours of usage of the vehicle or machine
under average conditions of operation.
This warning shall be clearly displayed by:
(a) Activating a second lamp, whose meaning is described in the REC
manual; or
(b) Display a message, for example "fill up urea", "fill up AdBlue", or
"fill up reagent".
7.2.5. It shall not be possible to turn off the operator warning system until the
reagent has been replenished to a level not requiring its activation.
7.3. Activation of the operator inducement system
7.3.1. The operator inducement system described in paragraphs 5.3. to 5.6. of this
annex shall be activated if the reagent tank is empty, or at any level below
2.5 per cent of its nominally full capacity at the discretion of the REC
manufacturer.
7.3.2. It shall not be possible to turn off the operator inducement system until the
reagent has been replenished to a level not requiring their respective
activation.
8. Reagent quality monitoring
8.1. The REC shall include a means of determining the presence of an incorrect
reagent in the tank, for example NOx sensor, reagent quality sensor, or
equivalent.
8.2. The manufacturer shall specify a minimum acceptable reagent concentration
CDmin, which results in tailpipe NOx emissions not exceeding
(a) 0.9 g/kWh for retrofitted engine systems complying with the NO x
emission limit for stage Q and R of Regulation No. 96; or
(b) The NOx emission limit + 1.5 g/kWh for all other systems.
8.2.1. The correct value of CDmin shall be demonstrated during type approval as
follows and recorded in the documentation package as specified in Annex 1.
8.2.1.1. The test shall be conducted by performing the hot part of the WHTC or
NRTC cycle, whichever applies, using a reagent with the concentration
CDmin.
8.2.1.2. A WHTC or NRTC preconditioning cycle or REC manufacturer defined pre-
conditioning cycle may be conducted, permitting a closed loop NO x control
system to perform adaptation to the quality of the reagent with the
concentration CDmin.
8.2.1.3. The NOx emission resulting from this test shall be lower than the NO x
threshold specified in paragraph 8.2. of this annex.
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8.2.2. Any reagent concentration lower than CDmin shall be detected and be
regarded, for the purpose of paragraph 8.1. of this annex, as being incorrect
reagent.
8.3. A specific counter ("the reagent quality counter") shall be attributed to the
reagent quality. The reagent quality counter shall count the number of
operating hours with an incorrect reagent.
8.3.1. Optionally, the manufacturer may group the reagent quality failure together
with the failures listed in paragraphs 9. and 10. of this annex into a single
counter.
8.4. Activation of the operator warning system
8.4.1. The operator warning system shall be activated in accordance with
paragraph 4. of this annex.
8.4.2. When the operator warning system includes a message display system, it
shall display a message indicating the reason of the warning if technically
feasible (for example "incorrect urea detected", "incorrect AdBlue detected",
or "incorrect reagent detected").
8.5. Activation of the operator inducement system
8.5.1. The operator inducement system shall be activated in accordance with
paragraph 5. of this annex.
9. Reagent dosing activity
9.1. The engine shall include a means of determining interruption of dosing.
9.2. A specific counter shall be attributed to the dosing activity (the "dosing
activity counter"). The counter shall count the number of operating hours
which occur with an interruption of the reagent dosing activity. This is not
required where such interruption is demanded because vehicle or machine
operating conditions are such that their emission performance does not
require reagent dosing.
9.2.1. Optionally, the REC manufacturer may group the reagent dosing failure
together with the failures listed in paragraphs 8. and 10. of this annex into a
single counter.
9.3. Activation of the operator warning system
9.3.1. The operator warning system shall be activated in accordance with
paragraph 4. of this annex.
9.3.2. When the warning system includes a message display system, it shall display
a message indicating the reason of the warning (e.g. "urea dosing
malfunction", "AdBlue dosing malfunction", or "reagent dosing
malfunction").
9.4. Activation of the operator inducement system
9.4.1. The operator inducement system shall be activated in accordance with
paragraph 5. of this annex.
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4.2. The instructions shall indicate any requirements or limitations on the use of
the vehicle or machine that are necessary in order to ensure correct
functioning of the REC.
4.3. The instructions shall specify whether any reagents or additives need to be
refilled by the vehicle or machine operator between normal maintenance
intervals, and to indicate a likely rate of reagent consumption.
4.4. The instructions shall specify the type and quality of any consumable
reagents or additives used.
4.5. The instructions shall remind the owner and operator of the vehicle or
machine that, where the fitting of the REC is a condition for its operation in a
particular country or area, or where fitting of the REC entitles the vehicle or
machine owner to incentives or privileges, the failure to maintain the REC in
proper working order (including the failure to ensure a proper supply of any
reagent or additive), may constitute a breach of contract or be a criminal
offence.
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Annex 12
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