Class 11 Experiment 2 Chemistry

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AIM OF THE EXPERIMENT

M
To prepare 250 mL of standard solution of oxalic acid.
20
MATERIALS REQUIRED
Beaker. glass rod, volumetric flask (250 mL), pipette, weight box, chemical balance, solid oxalic acid, distilled
water

THEORY
acidsawhitecrysaline soid. t is
Ori
dissociates oralate and H ions
into

coOH
COOH
24,0 , coo
CoO
poisonoun

(o4)
in nature. tiaa weak acid and dibasic. When it is disokved in water, t

2H(0g) 24,0)

Weight of oxalic acid required for the preparation ofstandard solution


20
Molarity
20
W, =?
M, = 126 g Mol
V 250 mL
I000
M= %
Mb
T_W 1000
20 126 250
26 g
W -=I.575

PROCEDURE
1. Take a watch glass, wash it with distilled water and then dry it.
2. Weigh the clean and dried watch glass accurately and record its weight in the note
book.
Weigh 9 lk oud
3. erearbonate on the watch glass accurately and record this weight
in the note-book.
4. Transfer gently and carefully sodium carbonate from the watch glass into a clean
250 ml beaker. Wash the watch glass with distilled water with the help of a wash
bottle to transfer the particles sticking to it into beaker (PgFSA The volume of
distilled wat for this purpose should not be more than 50 ml.
5. Dissolve socn.arbonate crystals in the beaker by gentle stirring with a clean glass
rod.
6.
6. When the icagd
the sediumorbonate in the beaker is completely dissolved, transfer carefully
the entire solution from the beaker into a 250 ml measuring flask with the help of a
funnel g 8
7. Wash the beaker with distilled water. Transfer the washings into the measuring
flask )
8. Finally wash the funnel thoroughly with distilled water with the help of a wash
bottle to transfer the solution sticking to the funnel into the measuring flask
9. Add enough distilled water to the measuring flask carefully
upto just below the etched
mark on it, with the help of wash bottle.
10. Add the last few drops of distilled water with a pipette until the lower level of the
meniscus just touches the mark on the measuring flask Eg BH].
11. Stopper the measuring flask and shake gently to make the solution uniform through-
M Oxplue
out. Label it as
aad
sodium-earbonate solution.
10

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