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PERFORMANCE EVALUATION OF WATER HYACINTH
FIBER – REINFORCED CONCRETE WITH VARYING
AMOUNT OF EGG SHELL POWDER
AS CEMENT REPLACEMENT
An Undergraduate Thesis
Presented to the Faculty of College of Engineering
Polytechnic University of the Philippines
Sta. Mesa, Manila
In Partial Fulfillment of the Requirements for the Course
CIEN 3282 - Civil Engineering Project I
by
Alvarez, Andrick L.
Jota, Jolina M.
Lagadan, Daryl John V.
Magnaye, Kimberly Wealth M.
Reyes, Denise Joy
May 2020
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Chapter 1
THE PROBLEM AND ITS SETTING
Introduction
Fiber reinforcement is used in concrete to get less cracking due to plastic
shrinkage and drying shrinkage. It reduces concrete permeability to a fair
percentage which leads to better cohesion and less water bleeding. The right
percentile use results in higher flexural and shear stress.
Water hyacinth fiber is one of if not the most accessible material that can be
used as fiber reinforcement. The Pasig River that flows from Laguna de Bay
through Manila Bay contains a surplus of water hyacinth- a problem that leads to
poor navigability and water pollution. As such, the PRRC reactivated its Task
Force Water Hyacinth group to ensure that the quick proliferation of water
hyacinth will not cause inconvenience to the public especially those who board
the Pasig River Ferry Service.
The researchers would like to work with PRRC in gathering these plants and
put it to better use.
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Theoretical Framework
Conceptual Framework
The conceptual framework discusses the flow of the study to be taken. The
study used the systems approach. The system of three (3) frames is composed of
the input which went through the process or operation, and emerged as the
output.
The first frame presents the input of the study which includes the materials
and equipments needed for making the concrete sample. These are sand, gravel,
cement, water, water hyacinth fibers, and egg shell powder.
The second frame presents the processes of the study which includes the
extraction of water hyacinth fibers, the preparation, making, and curing of test
specimen, the testing of the specimen in accordance to ASTM standards.
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The third frame contains the output which includes the evaluated results of
the tests done by the researchers and the recommendations for the future
researchers.
The arrows include the workflow of information in the research process. The
feedback loop connects the output to the process involved as well as to the input.
It makes the system continue.
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Statement of the Problem
This research aimed to evaluate the performance of the water hyacinth
fiber-reinforced concrete with varying amounts of egg shell powder as cement
replacement. Moreover, this research is aimed to compare the performance of
the water hyacinth fiber-reinforced concrete with varying amounts of egg shell
powder as cement replacement to that of the normal concrete using the data and
computational works from other research materials to formulate a hypothesis.
Hypothesis
The null hypothesis tested is:
There is no significant difference between the performances of the water
hyacinth fiber-reinforced concrete with egg shell powder to that of the normal
concrete.
Scope and Limitation
This study will be limited only to the use of water hyacinth fibers as fiber-
reinforcement, and the egg shell powder to be used will be those passing the 90
microns sieve. The acquisition of the needed materials will be outside the scope
of this study, as well as the equipment needed for testing. All specifications and
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test methods in making fiber-reinforced concrete and cement replacement should
be in accordance to ASTM Standards.
The testing of the fiber-reinforced concrete specimen will be limited only to
compressive strength test, split tensile strength test, flexural strength test and
water absorption.
Significance of the Study
This study anticipates to contribute additional information to serve the
following individuals and organizations.
Department of Civil Engineering. This study will be beneficial to the
department as it gives information regarding the performance of a water hyacinth
fiber-reinforced concrete with egg shell powder as cement replacement. This can
give other students insights on how waste products can be useful in the field of
civil engineering.
Department of Environment and Natural Resources (DENR). The
utilization of waste products such as the egg shell and water hyacinth can be
beneficial to the department as it help in reducing carbon footprint and save the
aquatic biodiversity.
Construction Industry. This study can be a reference to the construction
industry as it gives information on the utilization of egg shell powder and water
hyacinth fibers in producing good quality concrete/
Other Researchers. This study will be an effective tool and reference for
other researchers who would intend to make any further relevant study regarding
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the incorporation of water hyacinth fibers in concrete and usage of egg shell
powder as cement replacement.
Chapter 2
REVIEW OF RELATED LITERATURE AND STUDIES
To be able to develop a complete understanding and profound institution
into previous works and trends which were pertinent to the subject, as well as to
obtain specific goals of the study, the researchers pondered on various
references, both foreign and local literature and studies. These references were
gathered through journals, other reading materials, and electronic sources. It also
included related foreign and local studies acquired through the Internet, and past
thesis of the same field and discipline. These provided an adequate background
for the discussion to analysis of the findings regarding water hyacinth fiber–
reinforced concrete with varying amounts of egg shell powder as cement
replacement.
Foreign Literature
Fiber–reinforced concrete, according to Mishra, is a composite material
consisting of mixture of cement, mortar or concrete, and discontinuous, discrete,
uniformly dispersed suitable fibers. These fibers increase the structural integrity
of the concrete. Though mainly used on shotcrete, fiber-reinforcement can also
be used on normal concrete. Fibers are usually used in concrete to control plastic
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cracking and drying shrinkage cracking. It also lowers the permeability of
concrete and thus reduces bleeding of water.
One type of fiber used as fiber-reinforcement is the natural fiber. This kind of
fiber is produced by plants, animals, or geological processes. A good example of
natural fiber is water hyacinth fiber.
Water hyacinth (Eichhornia crassipes) is a free-floating perennial aquatic
plant. Harvesting water hyacinth for industrial use serves as a means of
environmental control since it is prolific. It is a good source of fibers and is
commonly used in some countries in Asia. The fibers from water hyacinth are
dried, woven, and interlinked together to form a braid or cord used for making
bags, footwear, wreaths, hats, vases, Christmas lanterns, and other decorative
materials. (https://en.wikipedia.org/wiki/Natural_fiber)
According to an article published by Stop Aquatic Hitchhikers, water
hyacinth is considered invasive throughout the world because it grows rapidly and
can form thick layers over the water. Though considered as a good source of
fibers, water hyacinth mats shade out the other aquatic plants, causing oxygen
depletion in the water resulting in fishes unable to survive. This plant mats also
interfere with boat navigation and prevent fishing, swimming, and other
recreational activities.
Since water hyacinth can grow rapidly over a short period of time, it can be
a sustainable source of fiber which can be used as fiber-reinforcement on
concrete. Using it as fiber-reinforcement can help save the environment and
resolve some environmental issues.
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The global production of cement, on the other hand, grows also from 1.39
billion tons back in 1995 to 4.2 billion tons in 2019, according to an article
published by Garside. Cement manufacturing releases carbon dioxide in the
atmosphere both directly when calcium carbonate (one of its composition) is
heated, and indirectly through the use of energy when its production involves the
emission of carbon dioxide. The development of the construction industry gives
way to the increase of production of cement, thus also leading to carbon emission
harmful to the environment.
According to Rodgers, cement is the source of about 8% of the world’s
carbon dioxide emission. China produces most cement and therefore most
cement-related carbon dioxide emissions, with 1800 million tons in 2010. Next to
China is India and USA, with 220 and 63.5 million tons respectively.
Local Literature
Water hyacinth has severely infested Philippine water with its rapid rate of
proliferation. According to Teves, Laguna de Bay, the country’s largest inland
body of water, is at risk of proliferation of free-floating water hyacinth. A science
research specialist from the Department of Environment and Natural Resources
said that the worsening water pollution from continuous discharge of waste and
untreated wastewater into Laguna de Bay promotes the proliferation of water
hyacinth. These invasive plants multiply fast as well as threaten native aquatic
biodiversity, ecosystems, and composition of Laguna de Bay.
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In 2012, Department of Science and Technology’s Metals Industry
Research and Development Center (DOST-MIRDC) developed a machine that
addresses the increasing number of water hyacinth clogging the metro waterways
and elsewhere. This machine is called Water Hyacinth Harvester, which scoops
up the plants and puts them into good use. It can collect and hold up to 25
kilograms of water hyacinth per load. The collected plants are then discharged by
the harvester into a dumping site or an assisting barge.
On the other side of its otherwise notorious reputation, the water hyacinth
can actually be a very good raw material for novel products that can churn in
income for individuals and communities. Among these products are handicrafts,
pieces of furniture, and tablewares.
Researchers from the Philippines and across the globe also find ways for
this water hyacinth to be useful. Many of which are the integration of water
hyacinth fibers into concrete, the production of paper out of the fibers, and
incorporating fibers into polymers to make a good sound-proofing material.
Big oil and cement companies have the most carbon footprint that play a
clear role in climate change resulting in adverse impact, says CHR Commissioner
Roberto Cadiz in an article released by Rappler Philippines. These big
companies may be held legally and morally liable for their hand in climate change
and its effects.
In 2018, carbon dioxide emissions per capita for the Philippines is 1.39
metric tons. It increased from 0.99 metric tons in 1999 to 1.39 metric tons in 2018
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growing at an average annual rate of 1.92%, according to an article released by
Kneoma.com.
With the growing construction industry and the infrastructure projects of the
government, there is a greater demand on cement. With that, the carbon footprint
also increases. Researchers find ways or alternatives to lessen the cement
demand in the country. Studies show that there are possible cement
replacements.
Foreign Studies
There are numerous studies in the country and across the globe on how
incorporating waste products can strengthen a concrete. Two of which is by using
water hyacinth fibers and egg shell powder.
In a study conducted by Boban, results show that the concrete incorporated
by water hyacinth fibers has greater compressive and tensile strength than that of
normal concrete. The water absorbing property of water hyacinth incorporated
concrete is less than the normal concrete so it can be used on exposed surfaces.
Results also suggest that this water hyacinth concrete can be used where weight
of the structure is to be reduced because it is lighter than the normal concrete.
The orientation of water hyacinth fibers in a concrete sample affects also the
resulting compressive and tensile strength. According to the study conducted by
Kiptum, the tensile strength and compressive strength of a concrete with vertical
and horizontal orientation of water hyacinth fibers decreased as the amount of
water hyacinth fiber increase. Authors of this study suggested to further
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investigate properties on water hyacinth fiber-reinforced concrete with random or
inclined orientation of fibers.
While there are studies suggesting the use of water hyacinth fibers to
increase the performance of a concrete, there are also investigations on the use
of egg shell powder as cement replacement.
According to Ansari, eggs shell powder is a good replacement material for
cement, after conducting tests. The result of this study shows that the
replacement of about 10%-15% of egg shell powder is effective in increasing the
performance of a concrete. Increasing the amount of egg shell powder beyond
15% will decrease the compressive strength.
In a comparative study between egg shell powder and fly ash conducted by
Dhanalakshmi, egg shell concrete gives greater split tensile and flexural strength
compared to a normal concrete. Combination of egg shell powder and fly ash
gives greater flexural strength for all percentage variation of fly ash with optimum
content of egg shell powder. This combination, on the other hand, reduces the
compressive strength of the concrete compared to egg shell concrete mixes
beyond 5% replacement of fly ash to optimum egg shell content concrete.
Same result is concluded in the experimental study made by Praveen.
Findings show that the compressive and flexural strength of the concrete with egg
shell powder replacement increases. The split tensile strength, on the other hand,
decreases with the addition of egg shell powder.
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Local Studies
As the Philippines go for sustainability and taking into consideration the
effects on the environment of climate change, many researchers find ways to look
for sustainable and eco-friendly materials needed in various aspects of daily
living.
In the study conducted by Abion, the use of water hyacinth fibers with
varying amounts of rice hull ash in concrete resulted in higher compressive and
flexural strength compared to a normal concrete. The same study tested also the
flowability, the passing ability, and filling ability of the concrete with water hyacinth
fibers and rice hull ash.
Synthesis
Accordingly, the related literature and studies just reviewed provided guides
and directions necessary for the researchers to meet the desired objectives. The
above-mentioned studies covered various areas in cement replacement and the
incorporation of fibers in concrete. Though some of the materials cited above are
not included in the scope of the study, it enables the researchers to have firm
background knowledge of the problem study.
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This study focuses on the performance evaluation of water hyacinth fiber-
reinforced concrete with varying amounts of egg shell powder as cement
replacement for which the researchers were able to find similar studies.
The present study is similar to the study conducted by Boban, et al (2017),
where they incorporated water hyacinth fibers in concrete, and evaluated the
performance of that concrete. The present study, however, aims to evaluate the
performance of a concrete with water hyacinth fibers and egg shell powder as
cement replacement.
The study conducted by Kiptum, et al. (2019) is similar to the present study
in the sense that it also evaluated the properties of water hyacinth fibers in
concrete. However, the present study does not focus on the orientation of the
fibers in the concrete and how it will affect the performance of the concrete.
The present study is similar to the study conducted by Abion, Dabu, and
Hernaez (2017) in the sense that they also used water hyacinth fibers as fiber-
reinforcement and uses rice hull ash as admixture. The present study, however,
does not include the addition of rice hull ash as admixture. Furthermore, it does
not also include the testing of flowability, the passing ability, and the filling ability
of the concrete incorporated by water hyacinth fibers.
The present study is also similar to the findings by Ansari, et al. (2016) and
Praveen, Vijaya and Jose (2015), wherein they used egg shell powder as cement
replacement and evaluated its effect on concrete, resulting in a better
performance of concrete.
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The present study is also similar to the study conducted by Dhanalakshmi,
et al. (2015), where they assessed the effect of egg shell powder and fly ash in
concrete. The present study, however, does not include the usage of fly ash on
its scope.
The present study confirms the facts stated in the literature and studies,
both foreign and local regarding the incorporation of water hyacinth fibers and the
usage of egg shell powder as cement replacement. The information given by the
reference assists the researchers in conducting a study that would contribute to
the existing body of knowledge about the topic.
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Chapter 3
METHODOLOGY
Materials and Methods
Water Hyacinth plants
Water hyacinth fibers were manually harvested from the Pasig River which
flows north-northwest through the market town of Pasig and bisects Manila, then
enters the bay between the North and South harbors. Collected water hyacinth
was submerged in 10% NaOH solution for 24 hours to remove impurities such as
mud and other contaminants. The plant was cleansed with distilled water and
placed in an absorbing piece of cloth under a shade and then dried for 2 days.
After that, the roots and leaves were removed, then the remaining fiber was cut
into 40 millimeter fibers.
Egg shell powder
Egg shell remains were collected from local sources. The collected shells
were cleaned thoroughly with distilled water and air dried in an absorbing piece of
cloth under a shade for 5 days. The dried shells then hand crushed, grinded then
sieved using a 90µm sieve. Only the 90µm sieved egg shells were used for the
cement replacement.
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Coarse and Fine Aggregates (ASTM) – Class C
Standard Method for Sieve Analysis of Fine and Coarse Aggregates (ASTM C136)
It is used to determine the grading of materials and to determine the particle
size distribution where specifications are being followed to achieve a quality control
of production of various aggregate products and mixtures containing aggregates.
1. Grading (Fine Aggregates) – The fineness modulus of the fine aggregate
shall not be lower than 2.3 and higher than 3.1. The fineness does not vary
more than 0.20. The fine aggregates shall not pass 45% from a single sieve
and retained on the next sieve size as shown in table-1.
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2. Grading (Coarse Aggregates) – Proportioning and sizing is one of the ways
to achieve a well graded aggregate, it maximizes the volume of aggregate in
the concrete while preserving its performing strength. Balancing the
proportion enabling us to fill each void to achieve a good quality product of
aggregates.
Fresh concrete
Mix Cement Sand Gravel Water WHF ESP
(kg) (L) (L) (L) (kg) (kg)
SCC w/ 10 20 40 7 0.44 0
0% ESP
SCC w/ 9.5 20 40 7 0.44 0.5
5% ESP
SCC w/ 9.0 20 40 7 0.44 1.0
10% ESP
SCC w/ 8.5 20 40 7 0.44 1.5
15% ESP
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Curing of Concrete
A batch of 4 samples, all 0.4% volume of WHF and with 0%, 5%,10%,15% by
volume ESP were cured for 14 days. Another batch of 4 samples, with the same
components were cured for 21 days. Another batch of 4 samples, with the same
components were cured for 28 days. Curing was done by submerging the samples
in a container filled with water.
Water Absorption of Concrete
In calculating the water of absorption of the concrete, we use:
B− A
Water Absorption = ( ) x 100
A
A = Dry weight of test specimen (Concrete Cylinder)
B = Wet weight of test specimen after immersion in water for 48 hrs.
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Sorptivity Test on Concrete
It is defined as a measure of the capacity of the medium to absorb or desorb liquid
by capillarity. The cumulative water absorption (per unit area of the inflow surface)
increases as the square root of elapsed time (t) I=S.t 1/ 2
I Δw
S= 1 I=
t 2 Ad
Where:
S = sorptivity in mm Δw = Change in weight (W2 – W1)
t = elapsed time in min. W1 = Oven Dry weight of cylinder
in grams
W2 = Weight of cylinder after 30 mins
capillary suction of water in grams
A = Surface area of specimen through
which water penetrated
d = Density of water
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3.6 Hardened Concrete
Strength of concrete is considered as one of most valuable properties, it usually
gives an overall picture of the quality of the concrete.
A .Compressive Strength
B. Flexural Strength
C. Split- Tensile Strength
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Chapter 4
SWOT ANALYSIS
STRENGHTS
In the research study of Incorporation of Water hyacinth in Concrete, it’s
possible to utilize it in maritime structures.
Water absorption of concrete = 1.24%
Water absorption of Water-hyacinth incorporated concrete = 1.15%
Water hyacinth reinforced integrated concrete has a higher water absorption
capacity than regular concrete, implying that it has a higher water absorption
capacity. It’s water absorbing properties are less than the normal concrete,
allowing it to be utilized on exposed surfaces
In the research study of Incorporation of Water hyacinth in Concrete the
weight of the normal concrete is 8.508 kg while the weight of water-hyacinth
reinforced incorporated concrete weighs 8.382 kg. It has a permeability capacity
that is lower than the typical concrete. Water hyacinth integrated concrete can be
utilized in places where structural weight must be decreased since it is lighter than
regular concrete.
They also have good heat resistance capacity and increases its overall strength.
Compressive Strength of Normal Concrete Cube after 24 hours of heating :
SI NO. BREAKING LOAD (kN) COMPRESSIVE
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STRENGTH (N/mm2)
1. 500 22.22
2. 500 22.22
3. 500 22.22
Avg value = 22.22 N/mm2
For 0.5% Water Hyacinth incorporated concrete
Compressive Strength of Water hyacinth Incorporated Concrete Cube after
24 hours of heating :
SI NO. BREAKING LOAD (kN) COMPRESSIVE
STRENGTH (N/mm2)
1. 750 33.33
2. 750 33.33
3. 750 31.11
Avg value = 32.59 N/mm2
According to Viwatsakpol et al. (2011), the compressive strength of mortar
varies depending on the size of fiber used, such as "milled dry fiber" (M-DF),
"crushed dry fiber" (Cr-DF), and "long dry fiber" L-DF. It was discovered that the
mortar containing 9% L-DF had the maximum compressive strength.
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However, this finding was unsatisfactory because the material did not break
when examined. The 1 percent M-DF mortar produced the best results. In
comparison to the lower size, it was discovered that the 1% #20DF mortar
produced the best results.
The water hyacinth is resilient, it contains a tensile strength of 100-150
N/mm2. The abrasiveness of water hyacinth is significantly lower, resulting in
benefits in terms of composite material technical processes in general. When
compared to glass, carbon, and aramid fibers, dried water hyacinths are light.
It is scientifically proven that the eggshell is mostly made up of calcium
compounds that are quite like cement because of the additional calcium oxide
added by eggshell ash, it has been shown to be an excellent accelerator for
cement bound materials. Increasing the eggshell ash content will enhance the
cement stabilized matrix's strength characteristics by around 35 percent on
average. This shows that using eggshell ash as a concrete addition increases the
concrete's strength. In addition to this, adding an eggshell ash to the Ordinary
Portland Cement decrease the setting time of the cement
Test Ash Volume of
Water Initial Decrease Final Decrease in
# Content water( ml)
Conten setting in final setting final setting
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time(mins setting time
t time (%)
) time(%) (mins)
1 0 37 148 143 - 247 -
2 0.1 37 148 141 1.40 240 2.83
3 0.5 37 148 129 9.79 221 10.53
4 1 37 148 118 17.48 203 17.82
5 1.5 37 148 109 23.78 182 26.32
6 2 37 148 105 26.57 175 29.15
7 2.5 37 148 97 32.17 163 34.01
According to Olarewaju et al., (2011), eggshells combined with lateritic soil
can create low binding characteristics and significantly enhance soil strength,
making it suitable for use as a subgrade. The stabilizing capacities did not meet
the requirements for the foundation or subbase for road building.
Egg Shell ash may be utilized as a cement substitute, resulting in better
compressive strength on lateritic soil. Constant Cement of 6 and 8% mixed with
egg ash powder of 0-10% at 2% intervals increased compressive strength by 35%
but fell short of the durability requirements.
They discovered that a soil-cement eggshell combination may be utilized to
pave roads.
WEAKNESS
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Due to the corrosion problem of steel, there is an increasing need for
concrete reinforcing materials which can replace steel rebars. Concrete has been
reinforced with various natural fibers such as bamboo, coconut, sisal, etc. for
developing cost-effective and sustainable building constructions. Addition of these
natural fibers to concrete was found helpful to improve various mechanical
performances including flexural properties, impact resistance, fracture toughness,
etc. and in some cases, even found better than glass and carbon fibers.
Natural fibers possess some disadvantages when considered as building
materials such as variability in properties, less durability due to high moisture and
chemical absorption, generation of concrete cracks due to swelling and volume
changes, weakening due to alkaline environment of cement and poor interface
between natural fibers and polymeric or cementitious matrices.
*Water Absorption - Water absorption is a significant aspect in the water hyacinth
fiber composite's durability. Water hyacinth fiber has the potential to absorb a lot of
water, which could make the composite unstable.
However, methods including drying, heating, beating, and dehydration can be used
to reduce the high moisture content of water hyacinth. The most popular and
affordable technique is drying.
*Unevenness - When fibers are added to the concrete mixture, it is impossible to
tell where in the mix the fibers will end up. Some portions of the concrete will end
up having more fibers than other parts. This will cause the concrete to have
different properties in higher fiber areas versus lower fiber areas.
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*Biodegradability - Water hyacinth is a biodegradable plant material. It could be a
problem since the concrete structural material is expected to be used for a long
period of time. However, according to Intermediate Technology Development
Group, water hyacinth can be treated with sodium metabisulphite also known as
organic salt to prevent it from rotting.
OPPORTUNITIES
Reduce of carbon footprint in a construction The demand for sustainable
materials came about as too much waste and pollutions came from fast
urbanization and industrialization. Biomaterials tend to have lower carbon footprint
than the carbon emitted before and after construction.
Reduce threats brought by water hyacinth plants to aquatic ecosystem
locally. The utilization of waste products such as the eggshell and water hyacinth
can be beneficial to the department as it helps in reducing carbon footprint and
save the aquatic biodiversity. Water hyacinth has severely infested Philippine
water with its rapid rate of proliferation. According to Teves, Laguna de Bay, the
country’s largest inland body of water, is at risk of proliferation of free-floating water
hyacinth. A science research specialist from the Department of Environment and
Natural Resources said that the worsening water pollution from continuous
discharge of waste and untreated wastewater into Laguna de Bay promotes the
proliferation of water hyacinth. These invasive plants multiply fast as well as
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threaten native aquatic biodiversity, ecosystems, and composition of Laguna de
Bay.
Local Sourcing In response to reducing threats of Water Hyacinth to aquatic
nature, adaptation by utilization of locally available materials is good for the local
community. Local sourcing uses less transportation, therefore reduction in
emissions and energy. Also, it creates local job opportunities by acquiring local
workers to harvest Water Hyacinth plants and eggshells.
THREATS
On the largest inland body of water, Laguna de Bay, resides the water
hyacinth clusters - the main resource location of this research. The lake is at risk
with the proliferation of free-floating water hyacinth, an invasive water species
known to cause major obstruction to the flow of waterways. With this reason, the
Anti-Pollution Task Force (APTF), under the Department of Environment and
Natural Resources (DENR), has been tasked to prioritize the removal of water
hyacinth in Pasig River and Laguna de Bay. Water hyacinth is an expendable
resource and the full removal of this water species will be an immense drawback
for this research.
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Furthermore, the collection and actual testing of this project was halted due
to pandemic restraints. Dependency on past studies and information must not be
overlooked.
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fbclid=IwAR2XvlSLz65ENJMgYJp-RM20V3sSD1trXAh9sXBDt0ofZNbv_W5eE7fJzMg
https://theconstructor.org/building/aggregates-concrete-american-standards-astm/39552/?
fbclid=IwAR2XvlSLz65ENJMgYJp-RM20V3sSD1trXAh9sXBDt0ofZNbv_W5eE7fJzMg